Contenido

Introducción ................................................................................................................. 2
Equipo utilizado para el análisis del muestreo ................................................................ 3
El Cerro de Oro ............................................................................................................. 4
Fisiografía y Geomorfología: ....................................................................................... 4
Geología Regional:..................................................................................................... 4
Mineralización y Alteración: ........................................................................................ 5
Magmatismo Orogénico: ............................................................................................ 5
Orogenia Laramide: ................................................................................................... 5
Fisiografía y Geomorfología: ....................................................................................... 5
Microfacies y Geoquímica: ......................................................................................... 5

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1
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Introducción

El Cerro de Oro, ubicado en el municipio de Rayón en el estado de Sonora, México, se erige

como un testigo geológico de la compleja historia tectónica y volcánica de la región. Esta
área se sitúa dentro de la provincia fisiográfica de Sierras Sepultadas, caracterizada por
sierras alineadas en dirección NW-SE y valles rellenos de conglomerados y material
aluvial, legado de la tectónica distensiva del Terciario Medio que moldeó el noroeste de
México1.

En el presente estudio, se ha llevado a cabo un muestreo exhaustivo en la zona del Cerro

de Oro, empleando la tecnología de fluorescencia de rayos X (XRF) portátil, una
herramienta indispensable en la exploración geoquímica moderna. Los analizadores XRF
portátiles permiten la caracterización in situ de elementos químicos en suelos, rocas y
minerales, proporcionando datos geoquímicos en tiempo real que son cruciales para la
toma de decisiones rápidas y precisas en el campo2.

El muestreo y análisis XRF realizado en el Cerro de Oro busca no solo entender la

composición mineralógica y la distribución de elementos traza y mayoritarios en la región,
sino también identificar zonas de interés económico y geológico que podrían indicar la
presencia de recursos minerales valiosos.

[Fecha]

2
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Equipo utilizado para el análisis del muestreo
Los equipos XRF Spectro Scout son espectrómetros de fluorescencia de rayos X por
energía dispersiva (ED-XRF) que ofrecen una solución portátil para el análisis elemental.
Su importancia radica en su capacidad para realizar análisis de calidad de laboratorio en
lugares remotos, lo que los hace ideales para aplicaciones en campo o en plantas de
producción donde el acceso a un laboratorio convencional no es posible o es impráctico.

En términos de eficiencia, los equipos XRF Spectro Scout eliminan la necesidad de

transportar muestras desde el sitio de recolección hasta un laboratorio, lo que ahorra
tiempo significativo y reduce los costos asociados con el análisis de muestras. Además,
estos equipos pueden ser operados con un mínimo de entrenamiento, lo que los hace
accesibles para un rango más amplio de usuarios.

Comparándolos con un laboratorio tradicional, los equipos XRF Spectro Scout ofrecen
varias ventajas:

Portabilidad: Son fáciles de transportar y pueden utilizarse en cualquier lugar, lo que es

especialmente útil para análisis en sitios de difícil acceso.

Rapidez: Permiten obtener resultados de análisis en tiempo real, sin la demora que implica
el envío de muestras a un laboratorio.

Costo-Efectividad: Representan una alternativa económica a los instrumentos de

laboratorio más grandes y costosos.

Precisión: A pesar de su tamaño compacto, ofrecen una precisión y sensibilidad

comparables a los analizadores de laboratorio para una amplia gama de niveles de
detección.

Sin embargo, es importante mencionar que los espectrómetros de fluorescencia de rayos

X dispersiva de longitud de onda (WDXRF) utilizados en laboratorios pueden ofrecer una
sensibilidad mayor, lo que los hace más adecuados para ciertas aplicaciones que
requieren una detección de elementos a niveles de traza más bajos.
[Fecha]

3
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El Cerro de Oro
Ubicado en Rayón, Sonora, es un área geológicamente interesante con una rica historia.
Permíteme explorar algunos aspectos clave relacionados con su geología estructural y las
alteraciones presentes:

Fisiografía y Geomorfología:
El estado de Sonora se divide en varias provincias fisiográficas, y el área de estudio se
encuentra dentro de la provincia de Sierras Sepultadas. Esta provincia se caracteriza por
sierras con orientación NW-SE, valles rellenos por conglomerados mal consolidados y
material aluvial. Estos depósitos son producto de la tectónica distensiva del Terciario
Medio que afectó al noroeste de México.

En la región de estudio, encontramos:

Sierras con morfologías cársticas en el margen sureste, representadas por unidades del
basamento de edad Precámbrico y Cretácico inferior.

Derrames alargados con orientación NW-SE correspondientes a las unidades volcánicas

del Oligoceno-Mioceno.

El Cerro Picacho, con la morfología más escarpada de la región.

Morfologías abruptas menos escarpadas como el Cerro Las Agujas y los Cerros La
Nopalera-Los Columpios.

En la parte norte, prevalece una morfología con fuerte relieve compuesta por unidades
volcánicas que contrastan con el bajo relieve de los abanicos aluviales que rellenan los
valles.

Geología Regional:
Trabajos previos han enfocado en la geología de las rocas del basamento Precámbrico,
Cretácico, y zonas de importancia económica. Se han realizado diversos trabajos de tesis y
cartas geológicas en la región, proporcionando información detallada sobre la geología
local.
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4
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Mineralización y Alteración:
Magmatismo Orogénico:
La región ha experimentado magmatismo orogénico asociado a la subducción de la placa
Farallón durante el Neógeno. Este magmatismo se distribuye en una faja con orientación
NW-SE y presenta tendencias calcoalcalinas, calcoalcalinas altas en potasio y
shoshoníticas.

Se han identificado dos unidades principales:

Miembro volcánico Cerro Prieto: Compuesto por lavas andesíticas vítreas con dos
piroxenos y olivino.

Complejo volcánico Las Agujas: Constituido por intrusivos hipabisales, domos y lavas de
composición dacítica con dos piroxenos y anfíbol.

Estas unidades son geoquímicamente calcoalcalinas y muestran un enriquecimiento en

elementos de las Tierras Raras ligeras, un fraccionamiento pronunciado de los elementos
de las Tierras Raras pesadas, una baja concentración de Y e Yb y un alto contenido de Sr.

Orogenia Laramide:
Durante el Cretácico superior, la región fue afectada por la Orogenia Laramide,
caracterizada por plegamientos y cabalgamiento de rocas sedimentarias del Precámbrico
sobre rocas del Cretácico inferior y el desarrollo de magmatismo calcoalcalino.

Fisiografía y Geomorfología:
El área de estudio se ubica dentro de la provincia de Sierras Sepultadas, caracterizada por
sierras con orientación NW-SE, valles rellenos por conglomerados mal consolidados y
material aluvial, producto de la tectónica distensiva del Terciario Medio.

Microfacies y Geoquímica:
Estudios de microfacies y geoquímica en la Caliza Mural en la sección Cerro de Oro han
permitido determinar ambientes de depósito y proporcionar más detalles sobre la historia
geológica de la región.
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5
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 [Fecha]

6
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 4/17/2024

Sample Name 796102 A Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 12:12 PM
Operator Converter Evaluation Date 4/15/2024 10:57 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0905 % 0.0067
14 SiO₂ Siliconoxide 0.2170 % 0.0040
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3453 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.224 % 0.010
20 CaO Calciumoxide 0.4752 % 0.0048
22 TiO₂ Titanoxid 0.0265 % 0.0016
23 V Vanadium 175.1 µg/g 4.0
24 Cr Chromium < 3.5 µg/g -
25 MnO Manganeseoxide < 2.6 µg/g -
26 Fe₂O₃ Ironoxide 21.61 % 0.02
27 Co Cobalt < 13 µg/g -
28 Ni Nickel 7.2 µg/g 0.3
29 Cu Copper 0.00983 % 0.00015
30 Zn Zinc 0.01368 % 0.00014
31 Ga Gallium 13.4 µg/g 2.1
33 As Arsenic ≈ 5058 µg/g 13
34 Se Selenium 8.0 µg/g 0.7
35 Br Bromine 0.203 µg/g 0.200
37 Rb Rubidium 64.0 µg/g 0.8
38 Sr Strontium 763.8 µg/g 2.4
39 Y Yttrium 11.2 µg/g 0.4
40 Zr Zirconium 41.0 µg/g 1.2
41 Nb Niobium 2.7 µg/g 0.4
42 Mo Molybdenum < 1.8 µg/g -
47 Ag Silver < 19 µg/g -
48 Cd Cadmium 101.6 µg/g 7.3
50 Sn Tin < 2.9 µg/g -
51 Sb Antimony < 4.3 µg/g -
55 Cs Cesium < 17 µg/g -
56 Ba Barium 642 µg/g 14
57 La Lanthanium 85 µg/g 19
58 Ce Cerium 106 µg/g 21
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.4 µg/g -
73 Ta Tantalum < 2.1 µg/g -
74 W Tungsten 10.6 µg/g 0.8
79 Au Gold 14.9 µg/g 3.1
80 Hg Mercury 17.2 µg/g 2.5
1 / 148
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81 Tl Thallium 3.9 µg/g 2.0

82 Pb Lead 0.00061 % 0.00007
83 Bi Bismuth 3.2 µg/g 0.9
90 Th Thorium < 1.4 µg/g -
92 U Uranium 1.5 µg/g 0.8
Sum of concentration 24.73 %

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Sample Name 796102 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 12:17 PM
Operator Converter Evaluation Date 4/15/2024 11:02 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1286 % 0.0097
14 SiO₂ Siliconoxide 0.1155 % 0.0045
15 P₂O₅ Phosphorusoxide 0.00425 % 0.00064
16 S Sulfur 0.5984 % 0.0022
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.060 % 0.011
20 CaO Calciumoxide 0.5241 % 0.0059
22 TiO₂ Titanoxid < 0.0013 % -
23 V Vanadium 210.6 µg/g 4.8
24 Cr Chromium 20.6 µg/g 0.7
25 MnO Manganeseoxide < 2.6 µg/g -
26 Fe₂O₃ Ironoxide 35.32 % 0.04
27 Co Cobalt < 17 µg/g -
28 Ni Nickel 6.9 µg/g 0.3
29 Cu Copper 0.01642 % 0.00023
30 Zn Zinc 0.01006 % 0.00015
31 Ga Gallium < 4.3 µg/g -
33 As Arsenic ≈ 6601 µg/g 18
34 Se Selenium 9.0 µg/g 1.0
35 Br Bromine 3.5 µg/g 2.6
37 Rb Rubidium 27.5 µg/g 0.8
38 Sr Strontium 761.2 µg/g 2.9
39 Y Yttrium 4.8 µg/g 0.3
40 Zr Zirconium 20.4 µg/g 1.4
41 Nb Niobium < 1.1 µg/g -
42 Mo Molybdenum < 2.6 µg/g -
47 Ag Silver < 16 µg/g -
48 Cd Cadmium 147 µg/g 12
50 Sn Tin < 4.1 µg/g -
51 Sb Antimony < 5.6 µg/g -
55 Cs Cesium < 23 µg/g -
56 Ba Barium 955 µg/g 17
57 La Lanthanium 92 µg/g 24
58 Ce Cerium 109 µg/g 26
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.9 µg/g -
73 Ta Tantalum < 2.9 µg/g -
74 W Tungsten 8.4 µg/g 0.9
79 Au Gold 20.7 µg/g 4.2
80 Hg Mercury 21.2 µg/g 3.6

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81 Tl Thallium 4.9 µg/g 2.8

82 Pb Lead < 0.00022 % -
83 Bi Bismuth < 2.8 µg/g -
90 Th Thorium < 2.3 µg/g -
92 U Uranium 3.4 µg/g 1.1
Sum of concentration 38.68 %

4 / 148
 4/17/2024

Sample Name 796102 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 12:23 PM
Operator Converter Evaluation Date 4/15/2024 11:07 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0464 % 0.0040
14 SiO₂ Siliconoxide 0.0776 % 0.0024
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2363 % 0.0010
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.6291 % 0.0067
20 CaO Calciumoxide 1.277 % 0.007
22 TiO₂ Titanoxid 0.0982 % 0.0022
23 V Vanadium 84.1 µg/g 3.0
24 Cr Chromium 3.6 µg/g 0.2
25 MnO Manganeseoxide 171.1 µg/g 5.1
26 Fe₂O₃ Ironoxide 15.13 % 0.02
27 Co Cobalt < 11 µg/g -
28 Ni Nickel 15.5 µg/g 0.5
29 Cu Copper 0.01149 % 0.00014
30 Zn Zinc 0.01998 % 0.00014
31 Ga Gallium < 2.6 µg/g -
33 As Arsenic ≈ 4001 µg/g 10
34 Se Selenium 4.4 µg/g 0.5
35 Br Bromine 2.7 µg/g 1.4
37 Rb Rubidium 62.4 µg/g 0.7
38 Sr Strontium 459.1 µg/g 1.6
39 Y Yttrium 15.5 µg/g 0.4
40 Zr Zirconium 53.2 µg/g 0.9
41 Nb Niobium 9.4 µg/g 0.5
42 Mo Molybdenum 5.9 µg/g 0.7
47 Ag Silver < 25 µg/g -
48 Cd Cadmium < 25 µg/g -
50 Sn Tin < 2.4 µg/g -
51 Sb Antimony 16.8 µg/g 2.0
55 Cs Cesium 22.0 µg/g 8.2
56 Ba Barium 1028 µg/g 13
57 La Lanthanium 80 µg/g 17
58 Ce Cerium 80 µg/g 18
60 Nd Neodymium < 12 µg/g -
72 Hf Hafnium < 1.1 µg/g -
73 Ta Tantalum 3.7 µg/g 0.4
74 W Tungsten 5.6 µg/g 0.5
79 Au Gold 10.4 µg/g 2.4
80 Hg Mercury 15.2 µg/g 2.0

5 / 148
 4/17/2024

81 Tl Thallium 3.5 µg/g 1.4

82 Pb Lead 0.00359 % 0.00013
83 Bi Bismuth 63.4 µg/g 2.5
90 Th Thorium 9.9 µg/g 1.1
92 U Uranium 5.4 µg/g 1.0
Sum of concentration 18.15 %

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 4/17/2024

Sample Name 796103 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 12:29 PM
Operator Converter Evaluation Date 4/15/2024 11:13 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0787 % 0.0043
14 SiO₂ Siliconoxide 0.3173 % 0.0034
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.1984 % 0.0009
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.713 % 0.010
20 CaO Calciumoxide 0.7522 % 0.0055
22 TiO₂ Titanoxid 0.0217 % 0.0011
23 V Vanadium 74.8 µg/g 2.7
24 Cr Chromium 10.9 µg/g 0.5
25 MnO Manganeseoxide 28.6 µg/g 3.1
26 Fe₂O₃ Ironoxide 7.445 % 0.009
27 Co Cobalt < 7.2 µg/g -
28 Ni Nickel 7.2 µg/g 0.2
29 Cu Copper 0.00653 % 0.00008
30 Zn Zinc 0.00339 % 0.00005
31 Ga Gallium 21.2 µg/g 1.5
33 As Arsenic 139.5 µg/g 1.4
34 Se Selenium < 0.6 µg/g -
35 Br Bromine < 0.5 µg/g -
37 Rb Rubidium 116.1 µg/g 0.7
38 Sr Strontium 101.3 µg/g 0.6
39 Y Yttrium 2.1 µg/g 0.4
40 Zr Zirconium 56.0 µg/g 0.5
41 Nb Niobium 3.8 µg/g 0.4
42 Mo Molybdenum < 1.0 µg/g -
47 Ag Silver < 30 µg/g -
48 Cd Cadmium < 18 µg/g -
50 Sn Tin < 2.0 µg/g -
51 Sb Antimony 5.3 µg/g 1.5
55 Cs Cesium < 12 µg/g -
56 Ba Barium 862 µg/g 13
57 La Lanthanium < 29 µg/g -
58 Ce Cerium 57 µg/g 16
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 5.8 µg/g 0.6
74 W Tungsten < 1.0 µg/g -
79 Au Gold < 1.0 µg/g -
80 Hg Mercury < 2.0 µg/g -

7 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00079 % 0.00006
83 Bi Bismuth < 1.0 µg/g -
90 Th Thorium 7.0 µg/g 0.4
92 U Uranium 1.7 µg/g 0.7
Sum of concentration 10.69 %

8 / 148
 4/17/2024

Sample Name 796103 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 12:34 PM
Operator Converter Evaluation Date 4/15/2024 11:18 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0444 % 0.0038
14 SiO₂ Siliconoxide 0.1186 % 0.0023
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2235 % 0.0009
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.8510 % 0.0062
20 CaO Calciumoxide 0.2265 % 0.0027
22 TiO₂ Titanoxid 0.1265 % 0.0019
23 V Vanadium 89.4 µg/g 2.7
24 Cr Chromium 25.0 µg/g 0.7
25 MnO Manganeseoxide < 2.6 µg/g -
26 Fe₂O₃ Ironoxide 10.13 % 0.01
27 Co Cobalt < 8.3 µg/g -
28 Ni Nickel 1.8 µg/g 0.1
29 Cu Copper 0.00530 % 0.00008
30 Zn Zinc 0.00119 % 0.00004
31 Ga Gallium 17.7 µg/g 1.4
33 As Arsenic 809.0 µg/g 3.4
34 Se Selenium < 0.6 µg/g -
35 Br Bromine < 0.9 µg/g -
37 Rb Rubidium 74.9 µg/g 0.6
38 Sr Strontium 121.7 µg/g 0.7
39 Y Yttrium 1.9 µg/g 0.3
40 Zr Zirconium 93.1 µg/g 0.6
41 Nb Niobium 8.3 µg/g 0.4
42 Mo Molybdenum < 1.1 µg/g -
47 Ag Silver < 29 µg/g -
48 Cd Cadmium < 18 µg/g -
50 Sn Tin < 1.9 µg/g -
51 Sb Antimony 7.4 µg/g 1.6
55 Cs Cesium < 12 µg/g -
56 Ba Barium 933 µg/g 14
57 La Lanthanium 52 µg/g 17
58 Ce Cerium 62 µg/g 17
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum < 1.4 µg/g -
74 W Tungsten < 1.1 µg/g -
79 Au Gold 4.2 µg/g 1.0
80 Hg Mercury < 2.2 µg/g -

9 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00070 % 0.00005
83 Bi Bismuth < 1.4 µg/g -
90 Th Thorium 3.8 µg/g 0.3
92 U Uranium 1.8 µg/g 0.7
Sum of concentration 11.96 %

10 / 148
 4/17/2024

Sample Name 796103 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 12:38 PM
Operator Converter Evaluation Date 4/15/2024 11:22 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.01112 % 0.00067
14 SiO₂ Siliconoxide 0.0816 % 0.0019
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2597 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.212 % 0.009
20 CaO Calciumoxide 9.505 % 0.022
22 TiO₂ Titanoxid 0.1417 % 0.0026
23 V Vanadium 46.7 µg/g 2.9
24 Cr Chromium 8.2 µg/g 0.4
25 MnO Manganeseoxide 179.9 µg/g 5.2
26 Fe₂O₃ Ironoxide 11.02 % 0.01
27 Co Cobalt < 9.5 µg/g -
28 Ni Nickel 11.7 µg/g 0.4
29 Cu Copper 0.00467 % 0.00009
30 Zn Zinc 0.00567 % 0.00008
31 Ga Gallium 16.1 µg/g 1.9
33 As Arsenic 408.0 µg/g 3.0
34 Se Selenium < 0.8 µg/g -
35 Br Bromine 1.4 µg/g 0.5
37 Rb Rubidium 88.0 µg/g 0.8
38 Sr Strontium 255.7 µg/g 1.2
39 Y Yttrium 7.8 µg/g 0.4
40 Zr Zirconium 58.3 µg/g 0.8
41 Nb Niobium 10.0 µg/g 0.5
42 Mo Molybdenum 7.1 µg/g 0.7
47 Ag Silver < 25 µg/g -
48 Cd Cadmium < 24 µg/g -
50 Sn Tin < 2.4 µg/g -
51 Sb Antimony < 3.2 µg/g -
55 Cs Cesium < 14 µg/g -
56 Ba Barium 1115 µg/g 12
57 La Lanthanium 51 µg/g 14
58 Ce Cerium 56 µg/g 14
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.0 µg/g -
73 Ta Tantalum 6.3 µg/g 0.6
74 W Tungsten < 1.4 µg/g -
79 Au Gold 9.1 µg/g 1.1
80 Hg Mercury < 2.5 µg/g -

11 / 148
 4/17/2024

81 Tl Thallium 1.5 µg/g 0.4

82 Pb Lead 0.00377 % 0.00012
83 Bi Bismuth < 1.5 µg/g -
90 Th Thorium 13.2 µg/g 0.6
92 U Uranium < 1.8 µg/g -
Sum of concentration 22.48 %

12 / 148
 4/17/2024

Sample Name 796104 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 12:44 PM
Operator Converter Evaluation Date 4/15/2024 11:28 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0754 % 0.0044
14 SiO₂ Siliconoxide 0.3280 % 0.0037
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.1986 % 0.0009
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5720 % 0.0063
20 CaO Calciumoxide 0.7369 % 0.0054
22 TiO₂ Titanoxid 0.0418 % 0.0016
23 V Vanadium 27.7 µg/g 1.8
24 Cr Chromium 16.8 µg/g 0.6
25 MnO Manganeseoxide 1181 µg/g 7
26 Fe₂O₃ Ironoxide 9.143 % 0.011
27 Co Cobalt < 7.8 µg/g -
28 Ni Nickel 39.4 µg/g 0.7
29 Cu Copper 0.01101 % 0.00011
30 Zn Zinc 0.01258 % 0.00009
31 Ga Gallium 12.1 µg/g 1.5
33 As Arsenic 90.0 µg/g 1.6
34 Se Selenium < 0.6 µg/g -
35 Br Bromine < 0.5 µg/g -
37 Rb Rubidium 84.6 µg/g 0.6
38 Sr Strontium 70.6 µg/g 0.5
39 Y Yttrium 9.9 µg/g 0.4
40 Zr Zirconium 65.3 µg/g 0.6
41 Nb Niobium 7.2 µg/g 0.4
42 Mo Molybdenum < 1.1 µg/g -
47 Ag Silver < 26 µg/g -
48 Cd Cadmium < 18 µg/g -
50 Sn Tin < 2.0 µg/g -
51 Sb Antimony < 2.8 µg/g -
55 Cs Cesium < 12 µg/g -
56 Ba Barium 1200 µg/g 14
57 La Lanthanium 27 µg/g 15
58 Ce Cerium 71 µg/g 16
60 Nd Neodymium 42.1 µg/g 1.8
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 2.1 µg/g 0.3
74 W Tungsten < 1.1 µg/g -
79 Au Gold < 1.1 µg/g -
80 Hg Mercury < 2.1 µg/g -

13 / 148
 4/17/2024

81 Tl Thallium < 0.6 µg/g -

82 Pb Lead 0.00748 % 0.00013
83 Bi Bismuth < 1.1 µg/g -
90 Th Thorium 5.1 µg/g 0.4
92 U Uranium 3.5 µg/g 0.8
Sum of concentration 11.42 %

14 / 148
 4/17/2024

Sample Name 796104 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 12:48 PM
Operator Converter Evaluation Date 4/15/2024 11:34 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0905 % 0.0045
14 SiO₂ Siliconoxide 0.4304 % 0.0042
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2535 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.928 % 0.012
20 CaO Calciumoxide 2.006 % 0.011
22 TiO₂ Titanoxid 0.1113 % 0.0023
23 V Vanadium 73.9 µg/g 4.7
24 Cr Chromium 19.9 µg/g 1.3
25 MnO Manganeseoxide 1078 µg/g 8
26 Fe₂O₃ Ironoxide 3.981 % 0.005
27 Co Cobalt < 5.8 µg/g -
28 Ni Nickel 11.5 µg/g 0.4
29 Cu Copper 0.00699 % 0.00008
30 Zn Zinc 0.00616 % 0.00006
31 Ga Gallium 13.3 µg/g 1.6
33 As Arsenic 59.2 µg/g 1.3
34 Se Selenium < 0.6 µg/g -
35 Br Bromine 0.3 µg/g 0.1
37 Rb Rubidium 108.1 µg/g 0.7
38 Sr Strontium 83.6 µg/g 0.6
39 Y Yttrium 8.1 µg/g 0.4
40 Zr Zirconium 82.9 µg/g 0.6
41 Nb Niobium 7.4 µg/g 0.4
42 Mo Molybdenum < 1.0 µg/g -
47 Ag Silver < 29 µg/g -
48 Cd Cadmium < 19 µg/g -
50 Sn Tin < 2.0 µg/g -
51 Sb Antimony 4.9 µg/g 1.5
55 Cs Cesium < 12 µg/g -
56 Ba Barium 1433 µg/g 14
57 La Lanthanium < 27 µg/g -
58 Ce Cerium < 36 µg/g -
60 Nd Neodymium 65.0 µg/g 3.2
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 8.7 µg/g 1.0
74 W Tungsten < 1.1 µg/g -
79 Au Gold < 0.9 µg/g -
80 Hg Mercury < 2.0 µg/g -

15 / 148
 4/17/2024

81 Tl Thallium < 0.6 µg/g -

82 Pb Lead 0.00562 % 0.00011
83 Bi Bismuth < 1.0 µg/g -
90 Th Thorium 6.7 µg/g 0.4
92 U Uranium 2.8 µg/g 0.9
Sum of concentration 9.13 %

16 / 148
 4/17/2024

Sample Name 796104 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 12:54 PM
Operator Converter Evaluation Date 4/15/2024 11:38 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0701 % 0.0038
14 SiO₂ Siliconoxide 0.1723 % 0.0028
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2440 % 0.0010
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.216 % 0.010
20 CaO Calciumoxide 1.968 % 0.010
22 TiO₂ Titanoxid 0.2541 % 0.0028
23 V Vanadium 75.3 µg/g 5.0
24 Cr Chromium 28.0 µg/g 1.6
25 MnO Manganeseoxide 957.1 µg/g 7.0
26 Fe₂O₃ Ironoxide 3.348 % 0.005
27 Co Cobalt 6.7 µg/g 0.7
28 Ni Nickel 13.6 µg/g 0.4
29 Cu Copper 0.00317 % 0.00006
30 Zn Zinc 0.00626 % 0.00006
31 Ga Gallium 15.7 µg/g 1.4
33 As Arsenic 77.5 µg/g 1.4
34 Se Selenium < 0.5 µg/g -
35 Br Bromine 5.3 µg/g 0.3
37 Rb Rubidium 90.4 µg/g 0.6
38 Sr Strontium 85.1 µg/g 0.6
39 Y Yttrium 19.0 µg/g 0.4
40 Zr Zirconium 81.7 µg/g 0.6
41 Nb Niobium 11.8 µg/g 0.4
42 Mo Molybdenum < 0.9 µg/g -
47 Ag Silver < 29 µg/g -
48 Cd Cadmium < 17 µg/g -
50 Sn Tin < 1.8 µg/g -
51 Sb Antimony 3.2 µg/g 1.4
55 Cs Cesium < 11 µg/g -
56 Ba Barium 1376 µg/g 13
57 La Lanthanium 77 µg/g 14
58 Ce Cerium 154 µg/g 17
60 Nd Neodymium 35.1 µg/g 1.9
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 10.5 µg/g 0.8
74 W Tungsten < 1.0 µg/g -
79 Au Gold < 0.8 µg/g -
80 Hg Mercury < 2.0 µg/g -

17 / 148
 4/17/2024

81 Tl Thallium < 0.6 µg/g -

82 Pb Lead 0.00713 % 0.00012
83 Bi Bismuth < 1.0 µg/g -
90 Th Thorium 11.9 µg/g 0.5
92 U Uranium 2.9 µg/g 0.8
Sum of concentration 7.60 %

18 / 148
 4/17/2024

Sample Name 796105 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:00 PM
Operator Converter Evaluation Date 4/15/2024 11:44 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1006 % 0.0048
14 SiO₂ Siliconoxide 0.6942 % 0.0054
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2653 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.111 % 0.010
20 CaO Calciumoxide 0.2667 % 0.0048
22 TiO₂ Titanoxid 0.2382 % 0.0027
23 V Vanadium 54.4 µg/g 4.7
24 Cr Chromium 31.5 µg/g 1.7
25 MnO Manganeseoxide 99.9 µg/g 3.6
26 Fe₂O₃ Ironoxide 3.930 % 0.005
27 Co Cobalt < 5.6 µg/g -
28 Ni Nickel 7.7 µg/g 0.3
29 Cu Copper 0.00086 % 0.00004
30 Zn Zinc 0.00193 % 0.00004
31 Ga Gallium 6.6 µg/g 1.3
33 As Arsenic 19.7 µg/g 0.7
34 Se Selenium < 0.5 µg/g -
35 Br Bromine < 0.3 µg/g -
37 Rb Rubidium 44.9 µg/g 0.4
38 Sr Strontium 13.7 µg/g 0.3
39 Y Yttrium 9.4 µg/g 0.4
40 Zr Zirconium 165.3 µg/g 0.7
41 Nb Niobium 2.1 µg/g 0.4
42 Mo Molybdenum < 1.0 µg/g -
47 Ag Silver < 29 µg/g -
48 Cd Cadmium < 18 µg/g -
50 Sn Tin < 1.8 µg/g -
51 Sb Antimony 3.7 µg/g 1.5
55 Cs Cesium < 11 µg/g -
56 Ba Barium 367 µg/g 12
57 La Lanthanium < 26 µg/g -
58 Ce Cerium 78 µg/g 16
60 Nd Neodymium 20.6 µg/g 2.5
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 8.9 µg/g 0.6
74 W Tungsten < 1.1 µg/g -
79 Au Gold < 0.8 µg/g -
80 Hg Mercury < 2.0 µg/g -

19 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00087 % 0.00006
83 Bi Bismuth < 0.9 µg/g -
90 Th Thorium 2.9 µg/g 0.3
92 U Uranium < 1.2 µg/g -
Sum of concentration 6.70 %

20 / 148
 4/17/2024

Sample Name 796105 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:04 PM
Operator Converter Evaluation Date 4/15/2024 11:48 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1204 % 0.0055
14 SiO₂ Siliconoxide 0.4496 % 0.0045
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2816 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.106 % 0.014
20 CaO Calciumoxide 0.3349 % 0.0058
22 TiO₂ Titanoxid 0.3252 % 0.0030
23 V Vanadium 120.6 µg/g 6.2
24 Cr Chromium 111.6 µg/g 3.4
25 MnO Manganeseoxide 89.2 µg/g 4.0
26 Fe₂O₃ Ironoxide 5.150 % 0.007
27 Co Cobalt < 6.5 µg/g -
28 Ni Nickel 19.4 µg/g 0.5
29 Cu Copper 0.00165 % 0.00005
30 Zn Zinc 0.00266 % 0.00005
31 Ga Gallium 14.0 µg/g 1.6
33 As Arsenic 25.0 µg/g 0.9
34 Se Selenium < 0.6 µg/g -
35 Br Bromine 2.0 µg/g 0.2
37 Rb Rubidium 65.6 µg/g 0.6
38 Sr Strontium 17.5 µg/g 0.3
39 Y Yttrium 19.8 µg/g 0.5
40 Zr Zirconium 107.6 µg/g 0.7
41 Nb Niobium 3.8 µg/g 0.5
42 Mo Molybdenum < 1.1 µg/g -
47 Ag Silver < 27 µg/g -
48 Cd Cadmium < 19 µg/g -
50 Sn Tin < 2.1 µg/g -
51 Sb Antimony 7.5 µg/g 1.6
55 Cs Cesium 16.2 µg/g 7.5
56 Ba Barium 370 µg/g 13
57 La Lanthanium 36 µg/g 16
58 Ce Cerium 38 µg/g 14
60 Nd Neodymium 36.8 µg/g 3.7
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 8.6 µg/g 0.7
74 W Tungsten < 1.1 µg/g -
79 Au Gold < 1.1 µg/g -
80 Hg Mercury < 2.2 µg/g -

21 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00161 % 0.00008
83 Bi Bismuth < 1.0 µg/g -
90 Th Thorium 10.5 µg/g 0.5
92 U Uranium 1.4 µg/g 0.7
Sum of concentration 8.89 %

22 / 148
 4/17/2024

Sample Name 796105 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:09 PM
Operator Converter Evaluation Date 4/15/2024 11:53 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0975 % 0.0052
14 SiO₂ Siliconoxide 0.1983 % 0.0034
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3335 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.063 % 0.015
20 CaO Calciumoxide 0.2335 % 0.0057
22 TiO₂ Titanoxid 0.3974 % 0.0029
23 V Vanadium 107.9 µg/g 8.1
24 Cr Chromium 69.4 µg/g 3.3
25 MnO Manganeseoxide 162.0 µg/g 4.6
26 Fe₂O₃ Ironoxide 3.779 % 0.005
27 Co Cobalt < 6.0 µg/g -
28 Ni Nickel 13.6 µg/g 0.4
29 Cu Copper 0.00136 % 0.00006
30 Zn Zinc 0.00278 % 0.00005
31 Ga Gallium 8.6 µg/g 1.6
33 As Arsenic 15.8 µg/g 0.8
34 Se Selenium < 0.6 µg/g -
35 Br Bromine 0.8 µg/g 0.2
37 Rb Rubidium 96.6 µg/g 0.7
38 Sr Strontium 25.9 µg/g 0.4
39 Y Yttrium 32.0 µg/g 0.6
40 Zr Zirconium 297.7 µg/g 1.1
41 Nb Niobium 10.7 µg/g 0.5
42 Mo Molybdenum < 1.1 µg/g -
47 Ag Silver < 26 µg/g -
48 Cd Cadmium < 20 µg/g -
50 Sn Tin < 2.1 µg/g -
51 Sb Antimony 2.8 µg/g 1.7
55 Cs Cesium 26.4 µg/g 7.5
56 Ba Barium 737 µg/g 13
57 La Lanthanium 77 µg/g 16
58 Ce Cerium 124 µg/g 18
60 Nd Neodymium 40.2 µg/g 4.1
72 Hf Hafnium < 0.9 µg/g -
73 Ta Tantalum 12.2 µg/g 0.8
74 W Tungsten 1.2 µg/g 0.1
79 Au Gold < 1.0 µg/g -
80 Hg Mercury < 2.4 µg/g -

23 / 148
 4/17/2024

81 Tl Thallium < 0.8 µg/g -

82 Pb Lead 0.00140 % 0.00008
83 Bi Bismuth < 1.0 µg/g -
90 Th Thorium 9.5 µg/g 0.5
92 U Uranium 2.4 µg/g 0.9
Sum of concentration 7.29 %

24 / 148
 4/17/2024

Sample Name 796106 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:14 PM
Operator Converter Evaluation Date 4/15/2024 11:58 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0928 % 0.0080
14 SiO₂ Siliconoxide 0.2411 % 0.0046
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2654 % 0.0013
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.067 % 0.009
20 CaO Calciumoxide 0.0835 % 0.0027
22 TiO₂ Titanoxid 0.3774 % 0.0035
23 V Vanadium 80.8 µg/g 3.1
24 Cr Chromium 70.1 µg/g 1.4
25 MnO Manganeseoxide < 2.6 µg/g -
26 Fe₂O₃ Ironoxide 31.98 % 0.04
27 Co Cobalt < 16 µg/g -
28 Ni Nickel 5.7 µg/g 0.2
29 Cu Copper < 0.00011 % -
30 Zn Zinc 0.00109 % 0.00004
31 Ga Gallium 36.5 µg/g 2.7
33 As Arsenic 352.9 µg/g 3.7
34 Se Selenium 5.9 µg/g 0.7
35 Br Bromine < 1.2 µg/g -
37 Rb Rubidium 126.0 µg/g 1.2
38 Sr Strontium 324.4 µg/g 1.7
39 Y Yttrium 23.5 µg/g 0.8
40 Zr Zirconium 201.1 µg/g 1.4
41 Nb Niobium 16.2 µg/g 0.6
42 Mo Molybdenum 25.7 µg/g 1.3
47 Ag Silver < 19 µg/g -
48 Cd Cadmium 96.7 µg/g 8.7
50 Sn Tin < 3.5 µg/g -
51 Sb Antimony < 4.6 µg/g -
55 Cs Cesium < 17 µg/g -
56 Ba Barium 375 µg/g 13
57 La Lanthanium 108 µg/g 19
58 Ce Cerium 128 µg/g 21
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.8 µg/g -
73 Ta Tantalum < 2.6 µg/g -
74 W Tungsten 15.1 µg/g 1.1
79 Au Gold 10.6 µg/g 1.5
80 Hg Mercury 7.8 µg/g 1.6

25 / 148
 4/17/2024

81 Tl Thallium 2.8 µg/g 0.8

82 Pb Lead 0.00276 % 0.00013
83 Bi Bismuth < 2.4 µg/g -
90 Th Thorium 21.0 µg/g 1.1
92 U Uranium 6.2 µg/g 1.3
Sum of concentration 34.32 %

26 / 148
 4/17/2024

Sample Name 796106 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:18 PM
Operator Converter Evaluation Date 4/15/2024 12:02 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0727 % 0.0047
14 SiO₂ Siliconoxide 0.3271 % 0.0037
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2069 % 0.0009
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.7278 % 0.0068
20 CaO Calciumoxide 0.0720 % 0.0023
22 TiO₂ Titanoxid 0.0984 % 0.0017
23 V Vanadium 16.1 µg/g 1.1
24 Cr Chromium 35.8 µg/g 1.0
25 MnO Manganeseoxide < 2.6 µg/g -
26 Fe₂O₃ Ironoxide 10.43 % 0.01
27 Co Cobalt < 8.4 µg/g -
28 Ni Nickel 2.5 µg/g 0.1
29 Cu Copper 0.00059 % 0.00003
30 Zn Zinc 0.00053 % 0.00003
31 Ga Gallium 6.6 µg/g 1.4
33 As Arsenic 29.4 µg/g 0.8
34 Se Selenium 5.2 µg/g 0.5
35 Br Bromine < 0.3 µg/g -
37 Rb Rubidium 41.1 µg/g 0.5
38 Sr Strontium 126.0 µg/g 0.7
39 Y Yttrium 3.7 µg/g 0.3
40 Zr Zirconium 42.2 µg/g 0.6
41 Nb Niobium 1.4 µg/g 0.4
42 Mo Molybdenum < 1.2 µg/g -
47 Ag Silver < 26 µg/g -
48 Cd Cadmium < 18 µg/g -
50 Sn Tin < 2.0 µg/g -
51 Sb Antimony < 2.8 µg/g -
55 Cs Cesium < 12 µg/g -
56 Ba Barium 119 µg/g 12
57 La Lanthanium 58 µg/g 17
58 Ce Cerium 52 µg/g 16
60 Nd Neodymium < 9.4 µg/g -
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 1.3 µg/g 0.1
74 W Tungsten < 1.0 µg/g -
79 Au Gold < 0.9 µg/g -
80 Hg Mercury < 2.1 µg/g -

27 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00054 % 0.00006
83 Bi Bismuth < 1.0 µg/g -
90 Th Thorium 2.2 µg/g 0.3
92 U Uranium < 1.2 µg/g -
Sum of concentration 11.99 %

28 / 148
 4/17/2024

Sample Name 796106 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:23 PM
Operator Converter Evaluation Date 4/15/2024 12:07 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0997 % 0.0053
14 SiO₂ Siliconoxide 0.1750 % 0.0031
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2775 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.319 % 0.014
20 CaO Calciumoxide 0.1726 % 0.0048
22 TiO₂ Titanoxid 0.9336 % 0.0048
23 V Vanadium 138.5 µg/g 8.8
24 Cr Chromium 88.1 µg/g 3.2
25 MnO Manganeseoxide 46.3 µg/g 3.6
26 Fe₂O₃ Ironoxide 4.695 % 0.006
27 Co Cobalt 15.9 µg/g 1.3
28 Ni Nickel 8.9 µg/g 0.3
29 Cu Copper 0.00123 % 0.00005
30 Zn Zinc 0.00143 % 0.00004
31 Ga Gallium 28.1 µg/g 1.6
33 As Arsenic 33.9 µg/g 1.0
34 Se Selenium < 0.7 µg/g -
35 Br Bromine 6.5 µg/g 0.3
37 Rb Rubidium 138.5 µg/g 0.8
38 Sr Strontium 445.7 µg/g 1.3
39 Y Yttrium 37.2 µg/g 0.6
40 Zr Zirconium 278.5 µg/g 1.1
41 Nb Niobium 32.4 µg/g 0.5
42 Mo Molybdenum 5.3 µg/g 0.6
47 Ag Silver < 27 µg/g -
48 Cd Cadmium < 19 µg/g -
50 Sn Tin 5.6 µg/g 0.6
51 Sb Antimony 4.2 µg/g 1.5
55 Cs Cesium < 11 µg/g -
56 Ba Barium 544 µg/g 11
57 La Lanthanium 130 µg/g 14
58 Ce Cerium 229 µg/g 17
60 Nd Neodymium 32.0 µg/g 4.1
72 Hf Hafnium < 0.9 µg/g -
73 Ta Tantalum 14.3 µg/g 0.8
74 W Tungsten 2.2 µg/g 0.2
79 Au Gold 1.0 µg/g 0.7
80 Hg Mercury < 2.3 µg/g -

29 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00210 % 0.00009
83 Bi Bismuth < 1.0 µg/g -
90 Th Thorium 25.3 µg/g 0.6
92 U Uranium 9.5 µg/g 1.2
Sum of concentration 8.91 %

30 / 148
 4/17/2024

Sample Name 796107 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:27 PM
Operator Converter Evaluation Date 4/15/2024 12:11 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0795 % 0.0046
14 SiO₂ Siliconoxide 0.8916 % 0.0060
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2728 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.546 % 0.015
20 CaO Calciumoxide 0.3720 % 0.0062
22 TiO₂ Titanoxid 0.0727 % 0.0017
23 V Vanadium 68.6 µg/g 4.7
24 Cr Chromium 10.9 µg/g 1.4
25 MnO Manganeseoxide 3288 µg/g 13
26 Fe₂O₃ Ironoxide 1.436 % 0.003
27 Co Cobalt < 3.6 µg/g -
28 Ni Nickel 4.8 µg/g 0.2
29 Cu Copper 0.00343 % 0.00006
30 Zn Zinc 0.00294 % 0.00005
31 Ga Gallium 14.1 µg/g 1.4
33 As Arsenic 13.8 µg/g 0.6
34 Se Selenium < 0.5 µg/g -
35 Br Bromine 0.3 µg/g 0.1
37 Rb Rubidium 133.5 µg/g 0.7
38 Sr Strontium 10.4 µg/g 0.2
39 Y Yttrium 6.5 µg/g 0.5
40 Zr Zirconium 82.1 µg/g 0.6
41 Nb Niobium 7.3 µg/g 0.4
42 Mo Molybdenum < 0.9 µg/g -
47 Ag Silver < 29 µg/g -
48 Cd Cadmium < 17 µg/g -
50 Sn Tin < 1.8 µg/g -
51 Sb Antimony < 2.4 µg/g -
55 Cs Cesium < 11 µg/g -
56 Ba Barium 719 µg/g 12
57 La Lanthanium 24 µg/g 13
58 Ce Cerium < 33 µg/g -
60 Nd Neodymium < 8.1 µg/g -
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 11.4 µg/g 0.9
74 W Tungsten < 1.0 µg/g -
79 Au Gold < 0.9 µg/g -
80 Hg Mercury < 2.0 µg/g -

31 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00062 % 0.00006
83 Bi Bismuth < 0.8 µg/g -
90 Th Thorium 7.2 µg/g 0.4
92 U Uranium < 1.9 µg/g -
Sum of concentration 6.12 %

32 / 148
 4/17/2024

Sample Name 796107 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:32 PM
Operator Converter Evaluation Date 4/15/2024 12:16 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1002 % 0.0049
14 SiO₂ Siliconoxide 0.8458 % 0.0059
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2708 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 3.153 % 0.017
20 CaO Calciumoxide 1.109 % 0.009
22 TiO₂ Titanoxid 0.0653 % 0.0018
23 V Vanadium 61.8 µg/g 5.5
24 Cr Chromium < 3.6 µg/g -
25 MnO Manganeseoxide 1836 µg/g 10
26 Fe₂O₃ Ironoxide 0.8804 % 0.0020
27 Co Cobalt < 2.9 µg/g -
28 Ni Nickel 1.4 µg/g 0.1
29 Cu Copper 0.02784 % 0.00015
30 Zn Zinc 0.00763 % 0.00007
31 Ga Gallium 11.8 µg/g 1.4
33 As Arsenic 4.3 µg/g 0.6
34 Se Selenium < 0.5 µg/g -
35 Br Bromine < 0.3 µg/g -
37 Rb Rubidium 117.2 µg/g 0.7
38 Sr Strontium 56.8 µg/g 0.5
39 Y Yttrium 6.5 µg/g 0.5
40 Zr Zirconium 67.9 µg/g 0.5
41 Nb Niobium 8.5 µg/g 0.4
42 Mo Molybdenum < 0.9 µg/g -
47 Ag Silver < 28 µg/g -
48 Cd Cadmium < 16 µg/g -
50 Sn Tin < 1.8 µg/g -
51 Sb Antimony < 2.6 µg/g -
55 Cs Cesium < 11 µg/g -
56 Ba Barium 2134 µg/g 14
57 La Lanthanium < 24 µg/g -
58 Ce Cerium < 32 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 9.4 µg/g 1.8
74 W Tungsten < 1.0 µg/g -
79 Au Gold < 0.9 µg/g -
80 Hg Mercury < 2.0 µg/g -

33 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00135 % 0.00007
83 Bi Bismuth < 0.8 µg/g -
90 Th Thorium 7.6 µg/g 0.4
92 U Uranium 3.1 µg/g 0.9
Sum of concentration 6.89 %

34 / 148
 4/17/2024

Sample Name 796107 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:36 PM
Operator Converter Evaluation Date 4/15/2024 12:20 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0808 % 0.0041
14 SiO₂ Siliconoxide 0.1999 % 0.0030
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2637 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.996 % 0.013
20 CaO Calciumoxide 2.332 % 0.012
22 TiO₂ Titanoxid 0.1185 % 0.0023
23 V Vanadium 77.7 µg/g 4.9
24 Cr Chromium 13.9 µg/g 1.1
25 MnO Manganeseoxide 1851 µg/g 10
26 Fe₂O₃ Ironoxide 3.041 % 0.004
27 Co Cobalt < 5.1 µg/g -
28 Ni Nickel 8.5 µg/g 0.3
29 Cu Copper 0.01332 % 0.00011
30 Zn Zinc 0.00647 % 0.00006
31 Ga Gallium 14.6 µg/g 1.3
33 As Arsenic 48.8 µg/g 1.1
34 Se Selenium < 0.5 µg/g -
35 Br Bromine 10.3 µg/g 0.4
37 Rb Rubidium 121.1 µg/g 0.7
38 Sr Strontium 55.4 µg/g 0.5
39 Y Yttrium 10.6 µg/g 0.5
40 Zr Zirconium 87.4 µg/g 0.6
41 Nb Niobium 9.7 µg/g 0.4
42 Mo Molybdenum 4.3 µg/g 0.6
47 Ag Silver < 28 µg/g -
48 Cd Cadmium < 17 µg/g -
50 Sn Tin < 1.8 µg/g -
51 Sb Antimony 6.2 µg/g 1.4
55 Cs Cesium < 11 µg/g -
56 Ba Barium 1637 µg/g 14
57 La Lanthanium 33 µg/g 14
58 Ce Cerium < 34 µg/g -
60 Nd Neodymium 27.0 µg/g 1.1
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 8.9 µg/g 1.3
74 W Tungsten < 1.1 µg/g -
79 Au Gold < 0.9 µg/g -
80 Hg Mercury < 2.0 µg/g -

35 / 148
 4/17/2024

81 Tl Thallium < 0.6 µg/g -

82 Pb Lead 0.00406 % 0.00010
83 Bi Bismuth < 1.0 µg/g -
90 Th Thorium 10.2 µg/g 0.5
92 U Uranium 3.4 µg/g 0.9
Sum of concentration 8.46 %

36 / 148
 4/17/2024

Sample Name 796108 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:43 PM
Operator Converter Evaluation Date 4/15/2024 12:27 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0462 % 0.0050
14 SiO₂ Siliconoxide 0.1075 % 0.0038
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.7484 % 0.0024
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5061 % 0.0076
20 CaO Calciumoxide 2.320 % 0.011
22 TiO₂ Titanoxid 0.2397 % 0.0037
23 V Vanadium 227.4 µg/g 5.7
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 368 µg/g 10
26 Fe₂O₃ Ironoxide 44.30 % 0.05
27 Co Cobalt < 21 µg/g -
28 Ni Nickel < 1.8 µg/g -
29 Cu Copper 0.01060 % 0.00023
30 Zn Zinc 0.06574 % 0.00044
31 Ga Gallium < 9.9 µg/g -
33 As Arsenic ≈ 10730 µg/g 30
34 Se Selenium 23.6 µg/g 1.6
35 Br Bromine 12.1 µg/g 4.2
37 Rb Rubidium 14.0 µg/g 1.0
38 Sr Strontium 899.9 µg/g 3.4
39 Y Yttrium 217.1 µg/g 1.4
40 Zr Zirconium 93.0 µg/g 1.8
41 Nb Niobium 6.1 µg/g 0.6
42 Mo Molybdenum 49.6 µg/g 1.8
47 Ag Silver 36.8 µg/g 3.8
48 Cd Cadmium 227 µg/g 18
50 Sn Tin < 4.9 µg/g -
51 Sb Antimony 339.3 µg/g 5.2
55 Cs Cesium < 21 µg/g -
56 Ba Barium 1228 µg/g 16
57 La Lanthanium 188 µg/g 21
58 Ce Cerium 621 µg/g 26
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 3.6 µg/g -
73 Ta Tantalum < 5.8 µg/g -
74 W Tungsten 15.6 µg/g 2.3
79 Au Gold 107.4 µg/g 6.4
80 Hg Mercury 37.1 µg/g 6.0

37 / 148
 4/17/2024

81 Tl Thallium 4.4 µg/g 0.4

82 Pb Lead 0.3127 % 0.0012
83 Bi Bismuth 79.0 µg/g 5.7
90 Th Thorium < 2.4 µg/g -
92 U Uranium 1.9 µg/g 1.1
Sum of concentration 50.21 %

38 / 148
 4/17/2024

Sample Name 796108 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:50 PM
Operator Converter Evaluation Date 4/15/2024 12:34 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1323 % 0.0089
14 SiO₂ Siliconoxide 0.3660 % 0.0060
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.6358 % 0.0022
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.6395 % 0.0099
20 CaO Calciumoxide 0.2333 % 0.0046
22 TiO₂ Titanoxid 0.0409 % 0.0024
23 V Vanadium 231.0 µg/g 6.3
24 Cr Chromium 13.4 µg/g 0.6
25 MnO Manganeseoxide < 0.8 µg/g -
26 Fe₂O₃ Ironoxide 17.91 % 0.02
27 Co Cobalt < 13 µg/g -
28 Ni Nickel 1.1 µg/g 0.1
29 Cu Copper 0.00530 % 0.00012
30 Zn Zinc 0.03211 % 0.00022
31 Ga Gallium < 6.4 µg/g -
33 As Arsenic ≈ 9760 µg/g 22
34 Se Selenium 17.8 µg/g 1.1
35 Br Bromine < 5.2 µg/g -
37 Rb Rubidium 1.5 µg/g 0.6
38 Sr Strontium 354.3 µg/g 1.7
39 Y Yttrium < 0.6 µg/g -
40 Zr Zirconium 15.5 µg/g 0.9
41 Nb Niobium < 1.0 µg/g -
42 Mo Molybdenum 7.7 µg/g 0.9
47 Ag Silver 74.4 µg/g 6.0
48 Cd Cadmium < 31 µg/g -
50 Sn Tin < 3.6 µg/g -
51 Sb Antimony 230.2 µg/g 3.4
55 Cs Cesium < 17 µg/g -
56 Ba Barium 736 µg/g 15
57 La Lanthanium 50 µg/g 18
58 Ce Cerium 79 µg/g 19
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.6 µg/g -
73 Ta Tantalum 10.6 µg/g 0.9
74 W Tungsten < 2.1 µg/g -
79 Au Gold 85.7 µg/g 4.7
80 Hg Mercury 42.0 µg/g 4.3

39 / 148
 4/17/2024

81 Tl Thallium 4.8 µg/g 0.4

82 Pb Lead 0.2368 % 0.0009
83 Bi Bismuth 106.0 µg/g 5.0
90 Th Thorium < 4.7 µg/g -
92 U Uranium < 1.4 µg/g -
Sum of concentration 21.41 %

40 / 148
 4/17/2024

Sample Name 796108 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 1:55 PM
Operator Converter Evaluation Date 4/15/2024 12:39 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0814 % 0.0062
14 SiO₂ Siliconoxide 0.1613 % 0.0036
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3836 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.032 % 0.009
20 CaO Calciumoxide 0.7055 % 0.0058
22 TiO₂ Titanoxid 0.5605 % 0.0045
23 V Vanadium 121.2 µg/g 5.3
24 Cr Chromium 14.4 µg/g 0.6
25 MnO Manganeseoxide 3057 µg/g 13
26 Fe₂O₃ Ironoxide 15.87 % 0.02
27 Co Cobalt 39.1 µg/g 2.0
28 Ni Nickel 8.5 µg/g 0.4
29 Cu Copper 0.02049 % 0.00020
30 Zn Zinc 0.08592 % 0.00033
31 Ga Gallium < 6.6 µg/g -
33 As Arsenic ≈ 7595 µg/g 19
34 Se Selenium 12.3 µg/g 0.9
35 Br Bromine 9.2 µg/g 2.6
37 Rb Rubidium 69.8 µg/g 0.9
38 Sr Strontium 292.6 µg/g 1.4
39 Y Yttrium 85.6 µg/g 0.6
40 Zr Zirconium 180.2 µg/g 1.2
41 Nb Niobium 15.2 µg/g 0.6
42 Mo Molybdenum 23.5 µg/g 0.9
47 Ag Silver 158 µg/g 10
48 Cd Cadmium < 31 µg/g -
50 Sn Tin < 3.8 µg/g -
51 Sb Antimony ≈ 867.8 µg/g 4.6
55 Cs Cesium < 16 µg/g -
56 Ba Barium 916 µg/g 13
57 La Lanthanium 90 µg/g 16
58 Ce Cerium 245 µg/g 19
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.7 µg/g -
73 Ta Tantalum 21.8 µg/g 2.2
74 W Tungsten 11.7 µg/g 1.2
79 Au Gold 80.7 µg/g 4.1
80 Hg Mercury 33.1 µg/g 3.7

41 / 148
 4/17/2024

81 Tl Thallium 3.5 µg/g 0.3

82 Pb Lead 0.3053 % 0.0009
83 Bi Bismuth 83.5 µg/g 4.3
90 Th Thorium 15.0 µg/g 2.7
92 U Uranium 5.4 µg/g 1.1
Sum of concentration 20.61 %

42 / 148
 4/17/2024

Sample Name 8 hnos ore Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 2:00 PM
Operator Converter Evaluation Date 4/15/2024 12:45 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0622 % 0.0035
14 SiO₂ Siliconoxide 1.026 % 0.007
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.5458 % 0.0020
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.1458 % 0.0074
20 CaO Calciumoxide 0.1467 % 0.0046
22 TiO₂ Titanoxid 0.01023 % 0.00020
23 V Vanadium 20.6 µg/g 4.7
24 Cr Chromium 11.7 µg/g 1.3
25 MnO Manganeseoxide 31.1 µg/g 3.4
26 Fe₂O₃ Ironoxide 1.394 % 0.003
27 Co Cobalt < 4.2 µg/g -
28 Ni Nickel < 0.6 µg/g -
29 Cu Copper 0.00200 % 0.00007
30 Zn Zinc 0.00279 % 0.00006
31 Ga Gallium < 2.3 µg/g -
33 As Arsenic 263.4 µg/g 2.6
34 Se Selenium < 0.7 µg/g -
35 Br Bromine 0.7 µg/g 0.4
37 Rb Rubidium 3.8 µg/g 0.3
38 Sr Strontium 11.1 µg/g 0.3
39 Y Yttrium 16.4 µg/g 0.4
40 Zr Zirconium 40.2 µg/g 0.6
41 Nb Niobium 9.0 µg/g 0.6
42 Mo Molybdenum < 1.2 µg/g -
47 Ag Silver < 21 µg/g -
48 Cd Cadmium < 19 µg/g -
50 Sn Tin < 2.3 µg/g -
51 Sb Antimony 139.4 µg/g 2.3
55 Cs Cesium < 13 µg/g -
56 Ba Barium 71 µg/g 11
57 La Lanthanium 73 µg/g 14
58 Ce Cerium 76 µg/g 15
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.9 µg/g -
73 Ta Tantalum 14.7 µg/g 1.1
74 W Tungsten < 1.3 µg/g -
79 Au Gold 3.6 µg/g 0.9
80 Hg Mercury < 2.3 µg/g -

43 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00905 % 0.00017
83 Bi Bismuth < 1.4 µg/g -
90 Th Thorium 4.8 µg/g 0.5
92 U Uranium < 0.9 µg/g -
Sum of concentration 3.42 %

44 / 148
 4/17/2024

Sample Name 796109 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 2:06 PM
Operator Converter Evaluation Date 4/15/2024 12:51 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0678 % 0.0040
14 SiO₂ Siliconoxide 0.6075 % 0.0051
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.6808 % 0.0019
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.3847 % 0.0070
20 CaO Calciumoxide 0.6161 % 0.0064
22 TiO₂ Titanoxid 0.3933 % 0.0032
23 V Vanadium 24.1 µg/g 3.7
24 Cr Chromium 7.7 µg/g 0.6
25 MnO Manganeseoxide 71.5 µg/g 3.6
26 Fe₂O₃ Ironoxide 4.927 % 0.006
27 Co Cobalt < 6.6 µg/g -
28 Ni Nickel 2.3 µg/g 0.1
29 Cu Copper 0.00209 % 0.00006
30 Zn Zinc 0.00374 % 0.00006
31 Ga Gallium < 2.6 µg/g -
33 As Arsenic 3221 µg/g 8
34 Se Selenium 3.3 µg/g 0.4
35 Br Bromine 0.5971 µg/g 0.6000
37 Rb Rubidium 16.7 µg/g 0.4
38 Sr Strontium 38.9 µg/g 0.4
39 Y Yttrium 33.0 µg/g 0.4
40 Zr Zirconium 136.6 µg/g 0.7
41 Nb Niobium 10.2 µg/g 0.5
42 Mo Molybdenum 4.7 µg/g 0.6
47 Ag Silver < 28 µg/g -
48 Cd Cadmium < 20 µg/g -
50 Sn Tin < 2.1 µg/g -
51 Sb Antimony 111.0 µg/g 2.0
55 Cs Cesium < 12 µg/g -
56 Ba Barium 84 µg/g 12
57 La Lanthanium 54 µg/g 16
58 Ce Cerium 158 µg/g 19
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.9 µg/g -
73 Ta Tantalum 14.4 µg/g 1.0
74 W Tungsten < 1.2 µg/g -
79 Au Gold 30.1 µg/g 1.8
80 Hg Mercury 10.7 µg/g 1.5

45 / 148
 4/17/2024

81 Tl Thallium 4.1 µg/g 0.6

82 Pb Lead 0.04635 % 0.00030
83 Bi Bismuth 15.6 µg/g 1.9
90 Th Thorium 4.6 µg/g 0.8
92 U Uranium < 0.7 µg/g -
Sum of concentration 8.14 %

46 / 148
 4/17/2024

Sample Name 796109 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 2:11 PM
Operator Converter Evaluation Date 4/15/2024 12:55 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1215 % 0.0100
14 SiO₂ Siliconoxide 0.5344 % 0.0081
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 3.237 % 0.006
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5375 % 0.0095
20 CaO Calciumoxide 0.1338 % 0.0040
22 TiO₂ Titanoxid 0.4989 % 0.0052
23 V Vanadium < 5.1 µg/g -
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide < 2.6 µg/g -
26 Fe₂O₃ Ironoxide 31.93 % 0.04
27 Co Cobalt 77.4 µg/g 3.3
28 Ni Nickel 13.0 µg/g 0.5
29 Cu Copper 0.00142 % 0.00008
30 Zn Zinc 0.00918 % 0.00013
31 Ga Gallium 25.7 µg/g 3.9
33 As Arsenic ≈ 4745 µg/g 16
34 Se Selenium 10.5 µg/g 1.0
35 Br Bromine 3.0 µg/g 2.4
37 Rb Rubidium 10.3 µg/g 0.6
38 Sr Strontium 194.5 µg/g 1.5
39 Y Yttrium 26.3 µg/g 0.5
40 Zr Zirconium 72.7 µg/g 1.1
41 Nb Niobium 13.7 µg/g 0.7
42 Mo Molybdenum 14.7 µg/g 1.2
47 Ag Silver 43.3 µg/g 4.4
48 Cd Cadmium < 45 µg/g -
50 Sn Tin < 4.2 µg/g -
51 Sb Antimony 19.5 µg/g 3.2
55 Cs Cesium 29 µg/g 13
56 Ba Barium 47 µg/g 12
57 La Lanthanium < 35 µg/g -
58 Ce Cerium 149 µg/g 23
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.7 µg/g -
73 Ta Tantalum 4.8 µg/g 0.3
74 W Tungsten 33.0 µg/g 1.6
79 Au Gold 21.2 µg/g 4.0
80 Hg Mercury 30.9 µg/g 4.1

47 / 148
 4/17/2024

81 Tl Thallium 6.3 µg/g 1.2

82 Pb Lead 0.05416 % 0.00055
83 Bi Bismuth 9.6 µg/g 1.9
90 Th Thorium 4.4 µg/g 1.2
92 U Uranium 3.9 µg/g 0.9
Sum of concentration 37.62 %

48 / 148
 4/17/2024

Sample Name 796109 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 2:16 PM
Operator Converter Evaluation Date 4/15/2024 1:00 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1072 % 0.0077
14 SiO₂ Siliconoxide 0.2424 % 0.0048
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 1.082 % 0.003
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.3901 % 0.0075
20 CaO Calciumoxide 0.2275 % 0.0041
22 TiO₂ Titanoxid 0.5314 % 0.0048
23 V Vanadium 27.5 µg/g 2.8
24 Cr Chromium 4.3 µg/g 0.2
25 MnO Manganeseoxide 28.4 µg/g 5.3
26 Fe₂O₃ Ironoxide 14.09 % 0.02
27 Co Cobalt 46.2 µg/g 2.4
28 Ni Nickel 8.3 µg/g 0.4
29 Cu Copper 0.00223 % 0.00009
30 Zn Zinc 0.00551 % 0.00009
31 Ga Gallium 3.5 µg/g 3.0
33 As Arsenic ≈ 5937 µg/g 15
34 Se Selenium 14.4 µg/g 0.8
35 Br Bromine 1.14 µg/g 1.10
37 Rb Rubidium 15.2 µg/g 0.5
38 Sr Strontium 73.4 µg/g 0.7
39 Y Yttrium 69.0 µg/g 0.6
40 Zr Zirconium 150.8 µg/g 1.0
41 Nb Niobium 18.7 µg/g 0.6
42 Mo Molybdenum 9.0 µg/g 0.8
47 Ag Silver 26.3 µg/g 3.8
48 Cd Cadmium < 30 µg/g -
50 Sn Tin < 2.9 µg/g -
51 Sb Antimony 119.0 µg/g 2.6
55 Cs Cesium 20.7 µg/g 9.0
56 Ba Barium 210 µg/g 11
57 La Lanthanium 72 µg/g 16
58 Ce Cerium 105 µg/g 17
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.3 µg/g -
73 Ta Tantalum 25.8 µg/g 1.3
74 W Tungsten 20.9 µg/g 1.0
79 Au Gold 19.9 µg/g 3.4
80 Hg Mercury 32.2 µg/g 3.0

49 / 148
 4/17/2024

81 Tl Thallium 5.0 µg/g 0.6

82 Pb Lead 0.09771 % 0.00055
83 Bi Bismuth 41.3 µg/g 3.2
90 Th Thorium 1.8 µg/g 1.1
92 U Uranium 3.4 µg/g 0.8
Sum of concentration 17.49 %

50 / 148
 4/17/2024

Sample Name 796110 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 2:22 PM
Operator Converter Evaluation Date 4/15/2024 1:06 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1105 % 0.0060
14 SiO₂ Siliconoxide 0.5675 % 0.0063
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3856 % 0.0016
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.445 % 0.012
20 CaO Calciumoxide 5.007 % 0.017
22 TiO₂ Titanoxid 0.9438 % 0.0060
23 V Vanadium 136.9 µg/g 7.2
24 Cr Chromium 28.2 µg/g 1.2
25 MnO Manganeseoxide 1899 µg/g 12
26 Fe₂O₃ Ironoxide 12.97 % 0.02
27 Co Cobalt < 10 µg/g -
28 Ni Nickel 17.7 µg/g 0.6
29 Cu Copper 0.3406 % 0.0008
30 Zn Zinc 0.9198 % 0.0014
31 Ga Gallium 21.4 µg/g 4.1
33 As Arsenic 43.2 µg/g 7.7
34 Se Selenium < 1.1 µg/g -
35 Br Bromine 1.0 µg/g 0.3
37 Rb Rubidium 161.1 µg/g 1.2
38 Sr Strontium 416.7 µg/g 1.8
39 Y Yttrium 42.7 µg/g 0.6
40 Zr Zirconium 254.0 µg/g 1.5
41 Nb Niobium 15.3 µg/g 0.7
42 Mo Molybdenum < 1.7 µg/g -
47 Ag Silver < 19 µg/g -
48 Cd Cadmium 179 µg/g 10
50 Sn Tin 3.7 µg/g 0.5
51 Sb Antimony 8.9 µg/g 2.6
55 Cs Cesium 154 µg/g 10
56 Ba Barium < 17 µg/g -
57 La Lanthanium 68 µg/g 15
58 Ce Cerium < 32 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 15.2 µg/g 4.4
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 32.4 µg/g 2.1
79 Au Gold < 1.6 µg/g -
80 Hg Mercury < 5.0 µg/g -

51 / 148
 4/17/2024

81 Tl Thallium 1.1 µg/g 0.1

82 Pb Lead 0.1568 % 0.0007
83 Bi Bismuth < 3.4 µg/g -
90 Th Thorium 25.1 µg/g 1.8
92 U Uranium 4.9 µg/g 1.4
Sum of concentration 23.20 %

52 / 148
 4/17/2024

Sample Name 796110 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 2:27 PM
Operator Converter Evaluation Date 4/15/2024 1:11 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0523 % 0.0044
14 SiO₂ Siliconoxide 0.2157 % 0.0038
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.4436 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.1295 % 0.0061
20 CaO Calciumoxide 1.537 % 0.010
22 TiO₂ Titanoxid 0.0851 % 0.0023
23 V Vanadium < 5.1 µg/g -
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 30350 µg/g 60
26 Fe₂O₃ Ironoxide 7.375 % 0.011
27 Co Cobalt 93.3 µg/g 1.8
28 Ni Nickel < 0.7 µg/g -
29 Cu Copper 11.33 % 0.01
30 Zn Zinc 0.9372 % 0.0016
31 Ga Gallium < 22 µg/g -
33 As Arsenic < 0.4 µg/g -
34 Se Selenium < 3.7 µg/g -
35 Br Bromine 15.7 µg/g 1.8
37 Rb Rubidium 23.1 µg/g 1.4
38 Sr Strontium 238.4 µg/g 1.7
39 Y Yttrium ≈ 343.8 µg/g 2.5
40 Zr Zirconium 100.4 µg/g 1.2
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 20.7 µg/g 1.0
47 Ag Silver 69.2 µg/g 8.1
48 Cd Cadmium 61 µg/g 11
50 Sn Tin < 7.0 µg/g -
51 Sb Antimony < 5.7 µg/g -
55 Cs Cesium < 21 µg/g -
56 Ba Barium 50 µg/g 13
57 La Lanthanium < 10 µg/g -
58 Ce Cerium 46 µg/g 13
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 2142 µg/g 100
73 Ta Tantalum 981 µg/g 38
74 W Tungsten < 2.0 µg/g -
79 Au Gold 21.2 µg/g 6.0
80 Hg Mercury < 15 µg/g -

53 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 2.837 % 0.005
83 Bi Bismuth < 7.2 µg/g -
90 Th Thorium 209 µg/g 10
92 U Uranium 19.5 µg/g 1.8
Sum of concentration 28.42 %

54 / 148
 4/17/2024

Sample Name 796110 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 2:33 PM
Operator Converter Evaluation Date 4/15/2024 1:17 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0617 % 0.0047
14 SiO₂ Siliconoxide 0.1100 % 0.0031
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3559 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.4153 % 0.0070
20 CaO Calciumoxide 2.446 % 0.011
22 TiO₂ Titanoxid 0.2248 % 0.0031
23 V Vanadium 8.3 µg/g 0.8
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 5807 µg/g 19
26 Fe₂O₃ Ironoxide 17.17 % 0.02
27 Co Cobalt 63.9 µg/g 2.3
28 Ni Nickel 5.5 µg/g 0.3
29 Cu Copper 2.232 % 0.003
30 Zn Zinc 1.183 % 0.002
31 Ga Gallium < 10 µg/g -
33 As Arsenic 110 µg/g 17
34 Se Selenium < 1.7 µg/g -
35 Br Bromine 6.0 µg/g 0.9
37 Rb Rubidium 86.5 µg/g 1.2
38 Sr Strontium 64.0 µg/g 0.8
39 Y Yttrium ≈ 126.8 µg/g 1.2
40 Zr Zirconium 89.5 µg/g 0.9
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 10.8 µg/g 0.9
47 Ag Silver 58.8 µg/g 7.2
48 Cd Cadmium 143 µg/g 14
50 Sn Tin < 3.6 µg/g -
51 Sb Antimony 46.6 µg/g 2.8
55 Cs Cesium 50.3 µg/g 9.9
56 Ba Barium 234 µg/g 13
57 La Lanthanium 33 µg/g 16
58 Ce Cerium 58 µg/g 14
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 249 µg/g 26
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten < 3.3 µg/g -
79 Au Gold 4.0 µg/g 1.2
80 Hg Mercury < 7.6 µg/g -

55 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.7200 % 0.0017
83 Bi Bismuth 42.1 µg/g 4.1
90 Th Thorium 58.6 µg/g 4.2
92 U Uranium 7.5 µg/g 1.3
Sum of concentration 25.65 %

56 / 148
 4/17/2024

Sample Name 796111 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 6:10 PM
Operator Converter Evaluation Date 4/15/2024 4:55 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0677 % 0.0070
14 SiO₂ Siliconoxide 0.1979 % 0.0043
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3129 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.0572 % 0.0052
20 CaO Calciumoxide 0.1276 % 0.0036
22 TiO₂ Titanoxid 0.0193 % 0.0015
23 V Vanadium < 5.1 µg/g -
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 1076 µg/g 11
26 Fe₂O₃ Ironoxide 33.72 % 0.04
27 Co Cobalt 39.4 µg/g 1.8
28 Ni Nickel < 0.7 µg/g -
29 Cu Copper 2.997 % 0.005
30 Zn Zinc ≈ 6.472 % 0.009
31 Ga Gallium ≈ 22 µg/g 0.0
33 As Arsenic 128 µg/g 33
34 Se Selenium < 3.7 µg/g -
35 Br Bromine 91.0 µg/g 3.8
37 Rb Rubidium 10.9 µg/g 1.3
38 Sr Strontium 25.0 µg/g 0.8
39 Y Yttrium ≈ 192.3 µg/g 2.1
40 Zr Zirconium 27.5 µg/g 0.8
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 2.6 µg/g 0.7
47 Ag Silver 112 µg/g 10
48 Cd Cadmium 679 µg/g 19
50 Sn Tin < 6.2 µg/g -
51 Sb Antimony 64.5 µg/g 5.3
55 Cs Cesium 35 µg/g 13
56 Ba Barium 36 µg/g 14
57 La Lanthanium 55 µg/g 19
58 Ce Cerium < 12 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 254 µg/g 47
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten ≈ 479 µg/g 11
79 Au Gold < 5.8 µg/g -
80 Hg Mercury ≈ 912 µg/g 19

57 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 1.385 % 0.003
83 Bi Bismuth 45.9 µg/g 5.9
90 Th Thorium 71.1 µg/g 8.0
92 U Uranium 17.9 µg/g 1.7
Sum of concentration 45.79 %

58 / 148
 4/17/2024

Sample Name 796111 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 6:16 PM
Operator Converter Evaluation Date 4/15/2024 5:00 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0712 % 0.0054
14 SiO₂ Siliconoxide 0.2647 % 0.0039
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2252 % 0.0009
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.6266 % 0.0078
20 CaO Calciumoxide 0.4603 % 0.0049
22 TiO₂ Titanoxid 0.1333 % 0.0024
23 V Vanadium 33.9 µg/g 2.9
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 21650 µg/g 40
26 Fe₂O₃ Ironoxide 7.900 % 0.010
27 Co Cobalt 157.8 µg/g 2.3
28 Ni Nickel < 0.7 µg/g -
29 Cu Copper 3.534 % 0.004
30 Zn Zinc 0.7402 % 0.0011
31 Ga Gallium < 12 µg/g -
33 As Arsenic 60 µg/g 22
34 Se Selenium < 3.3 µg/g -
35 Br Bromine 3.4 µg/g 0.9
37 Rb Rubidium 229.2 µg/g 1.5
38 Sr Strontium 100.4 µg/g 0.9
39 Y Yttrium ≈ 158.2 µg/g 1.4
40 Zr Zirconium 113.6 µg/g 0.9
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 5.0 µg/g 0.8
47 Ag Silver 55.6 µg/g 7.4
48 Cd Cadmium < 5.1 µg/g -
50 Sn Tin < 4.2 µg/g -
51 Sb Antimony < 4.6 µg/g -
55 Cs Cesium < 20 µg/g -
56 Ba Barium 4807 µg/g 23
57 La Lanthanium < 28 µg/g -
58 Ce Cerium 64 µg/g 18
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 467 µg/g 34
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten < 2.0 µg/g -
79 Au Gold < 3.3 µg/g -
80 Hg Mercury < 8.3 µg/g -

59 / 148
 4/17/2024

81 Tl Thallium < 0.1 µg/g -

82 Pb Lead 1.215 % 0.002
83 Bi Bismuth < 8.5 µg/g -
90 Th Thorium 81.5 µg/g 4.9
92 U Uranium 6.0 µg/g 1.6
Sum of concentration 17.97 %

60 / 148
 4/17/2024

Sample Name 796111 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 6:21 PM
Operator Converter Evaluation Date 4/15/2024 5:05 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0744 % 0.0062
14 SiO₂ Siliconoxide 0.1556 % 0.0039
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3108 % 0.0013
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.3118 % 0.0064
20 CaO Calciumoxide 1.190 % 0.008
22 TiO₂ Titanoxid 0.2379 % 0.0032
23 V Vanadium 10.7 µg/g 0.8
24 Cr Chromium < 4.4 µg/g -
25 MnO Manganeseoxide 4549 µg/g 17
26 Fe₂O₃ Ironoxide 22.11 % 0.03
27 Co Cobalt 83.4 µg/g 2.8
28 Ni Nickel 2.7 µg/g 0.1
29 Cu Copper 1.544 % 0.002
30 Zn Zinc 1.058 % 0.002
31 Ga Gallium < 11 µg/g -
33 As Arsenic 161 µg/g 18
34 Se Selenium < 1.8 µg/g -
35 Br Bromine 4.7 µg/g 1.0
37 Rb Rubidium 70.6 µg/g 1.2
38 Sr Strontium 54.8 µg/g 0.8
39 Y Yttrium ≈ 129.9 µg/g 1.3
40 Zr Zirconium 74.1 µg/g 0.8
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 10.4 µg/g 0.9
47 Ag Silver 76.5 µg/g 8.1
48 Cd Cadmium 348 µg/g 18
50 Sn Tin < 3.8 µg/g -
51 Sb Antimony 66.4 µg/g 3.2
55 Cs Cesium < 17 µg/g -
56 Ba Barium 154 µg/g 13
57 La Lanthanium < 10 µg/g -
58 Ce Cerium < 12 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 132 µg/g 20
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 78.8 µg/g 1.9
79 Au Gold 17.1 µg/g 2.9
80 Hg Mercury 19.6 µg/g 3.4

61 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.7319 % 0.0018
83 Bi Bismuth 63.8 µg/g 4.4
90 Th Thorium 54.5 µg/g 4.6
92 U Uranium 8.8 µg/g 1.3
Sum of concentration 28.34 %

62 / 148
 4/17/2024

Sample Name 796112 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 6:28 PM
Operator Converter Evaluation Date 4/15/2024 5:12 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0948 % 0.0059
14 SiO₂ Siliconoxide 0.4493 % 0.0049
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2620 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5938 % 0.0072
20 CaO Calciumoxide 0.4787 % 0.0047
22 TiO₂ Titanoxid 0.2155 % 0.0027
23 V Vanadium 10.7 µg/g 0.9
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 7743 µg/g 20
26 Fe₂O₃ Ironoxide 15.58 % 0.02
27 Co Cobalt 70.1 µg/g 2.5
28 Ni Nickel < 1.3 µg/g -
29 Cu Copper 0.9321 % 0.0015
30 Zn Zinc 0.4976 % 0.0009
31 Ga Gallium < 7.6 µg/g -
33 As Arsenic < 20 µg/g -
34 Se Selenium < 1.3 µg/g -
35 Br Bromine 17.2 µg/g 0.8
37 Rb Rubidium 42.9 µg/g 0.8
38 Sr Strontium 21.8 µg/g 0.4
39 Y Yttrium 13.0 µg/g 0.1
40 Zr Zirconium 80.2 µg/g 0.8
41 Nb Niobium < 1.0 µg/g -
42 Mo Molybdenum 3.1 µg/g 0.7
47 Ag Silver 111.5 µg/g 8.3
48 Cd Cadmium 182.2 µg/g 9.4
50 Sn Tin < 3.1 µg/g -
51 Sb Antimony 41.2 µg/g 2.5
55 Cs Cesium < 13 µg/g -
56 Ba Barium 46.5 µg/g 9.3
57 La Lanthanium 37 µg/g 14
58 Ce Cerium < 30 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 78 µg/g 12
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten < 2.0 µg/g -
79 Au Gold 12.9 µg/g 2.5
80 Hg Mercury 18.4 µg/g 2.6

63 / 148
 4/17/2024

81 Tl Thallium < 0.1 µg/g -

82 Pb Lead 0.4356 % 0.0010
83 Bi Bismuth 28.9 µg/g 3.1
90 Th Thorium 48.3 µg/g 3.4
92 U Uranium 9.2 µg/g 1.0
Sum of concentration 20.40 %

64 / 148
 4/17/2024

Sample Name 796112 c (1) Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 6:33 PM
Operator Converter Evaluation Date 4/15/2024 5:17 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0391 % 0.0038
14 SiO₂ Siliconoxide 0.1212 % 0.0033
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3612 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.4000 % 0.0069
20 CaO Calciumoxide 2.854 % 0.012
22 TiO₂ Titanoxid 0.2096 % 0.0030
23 V Vanadium 10.0 µg/g 0.9
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 5098 µg/g 18
26 Fe₂O₃ Ironoxide 18.64 % 0.02
27 Co Cobalt 63.7 µg/g 2.4
28 Ni Nickel 5.5 µg/g 0.3
29 Cu Copper 1.956 % 0.003
30 Zn Zinc 1.144 % 0.002
31 Ga Gallium < 11 µg/g -
33 As Arsenic 136 µg/g 19
34 Se Selenium < 1.8 µg/g -
35 Br Bromine 6.4 µg/g 1.0
37 Rb Rubidium 81.8 µg/g 1.2
38 Sr Strontium 66.5 µg/g 0.8
39 Y Yttrium ≈ 143.7 µg/g 1.3
40 Zr Zirconium 99.2 µg/g 0.9
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 11.7 µg/g 0.9
47 Ag Silver 99.8 µg/g 9.0
48 Cd Cadmium 250 µg/g 17
50 Sn Tin < 4.0 µg/g -
51 Sb Antimony 39.1 µg/g 3.0
55 Cs Cesium 67 µg/g 10
56 Ba Barium 189 µg/g 13
57 La Lanthanium 49 µg/g 17
58 Ce Cerium < 36 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 215 µg/g 24
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 21.9 µg/g 0.6
79 Au Gold 12.6 µg/g 2.6
80 Hg Mercury 8.2 µg/g 2.0

65 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.8411 % 0.0019
83 Bi Bismuth 68.6 µg/g 4.8
90 Th Thorium 51.0 µg/g 4.7
92 U Uranium 9.2 µg/g 1.3
Sum of concentration 27.25 %

66 / 148
 4/17/2024

Sample Name 796113 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 6:40 PM
Operator Converter Evaluation Date 4/15/2024 5:24 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0415 % 0.0029
14 SiO₂ Siliconoxide 0.1778 % 0.0041
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 1.426 % 0.004
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.9376 % 0.0100
20 CaO Calciumoxide 8.454 % 0.023
22 TiO₂ Titanoxid 0.1500 % 0.0030
23 V Vanadium 12.1 µg/g 0.9
24 Cr Chromium 12.5 µg/g 0.5
25 MnO Manganeseoxide 89.8 µg/g 7.0
26 Fe₂O₃ Ironoxide 20.48 % 0.02
27 Co Cobalt < 13 µg/g -
28 Ni Nickel 1.3 µg/g 0.1
29 Cu Copper 0.09229 % 0.00044
30 Zn Zinc 0.00721 % 0.00011
31 Ga Gallium 28.8 µg/g 2.5
33 As Arsenic 31.0 µg/g 2.2
34 Se Selenium < 1.1 µg/g -
35 Br Bromine < 0.8 µg/g -
37 Rb Rubidium 61.9 µg/g 0.8
38 Sr Strontium 69.9 µg/g 0.8
39 Y Yttrium 1.8 µg/g 0.3
40 Zr Zirconium 12.5 µg/g 0.7
41 Nb Niobium < 1.0 µg/g -
42 Mo Molybdenum 3.8 µg/g 0.8
47 Ag Silver < 18 µg/g -
48 Cd Cadmium 257 µg/g 12
50 Sn Tin 16.9 µg/g 1.1
51 Sb Antimony < 4.7 µg/g -
55 Cs Cesium < 17 µg/g -
56 Ba Barium 29 µg/g 10
57 La Lanthanium < 27 µg/g -
58 Ce Cerium 46 µg/g 15
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.4 µg/g -
73 Ta Tantalum < 1.2 µg/g -
74 W Tungsten 65.0 µg/g 1.6
79 Au Gold 2.5 µg/g 1.3
80 Hg Mercury < 5.3 µg/g -

67 / 148
 4/17/2024

81 Tl Thallium < 0.9 µg/g -

82 Pb Lead 0.00809 % 0.00021
83 Bi Bismuth 196.7 µg/g 3.3
90 Th Thorium < 4.1 µg/g -
92 U Uranium 2.3 µg/g 1.0
Sum of concentration 31.87 %

68 / 148
 4/17/2024

Sample Name 796113 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 6:45 PM
Operator Converter Evaluation Date 4/15/2024 5:29 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0111 % 0.0012
14 SiO₂ Siliconoxide 0.1778 % 0.0037
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.9155 % 0.0024
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.6669 % 0.0070
20 CaO Calciumoxide 3.775 % 0.012
22 TiO₂ Titanoxid 0.1309 % 0.0023
23 V Vanadium 12.4 µg/g 0.7
24 Cr Chromium 4.8 µg/g 0.2
25 MnO Manganeseoxide 1280 µg/g 10
26 Fe₂O₃ Ironoxide 30.78 % 0.04
27 Co Cobalt < 15 µg/g -
28 Ni Nickel < 1.1 µg/g -
29 Cu Copper 0.2329 % 0.0008
30 Zn Zinc 0.00789 % 0.00012
31 Ga Gallium 55.2 µg/g 3.3
33 As Arsenic 63.2 µg/g 2.6
34 Se Selenium < 1.4 µg/g -
35 Br Bromine < 0.9 µg/g -
37 Rb Rubidium 57.5 µg/g 0.8
38 Sr Strontium 88.5 µg/g 0.9
39 Y Yttrium 3.0 µg/g 0.4
40 Zr Zirconium 15.8 µg/g 0.7
41 Nb Niobium 2.8 µg/g 0.4
42 Mo Molybdenum 4.2 µg/g 0.7
47 Ag Silver 24.8 µg/g 3.1
48 Cd Cadmium 314 µg/g 15
50 Sn Tin < 3.6 µg/g -
51 Sb Antimony < 5.1 µg/g -
55 Cs Cesium < 17 µg/g -
56 Ba Barium 49 µg/g 10
57 La Lanthanium < 28 µg/g -
58 Ce Cerium 33 µg/g 14
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.9 µg/g -
73 Ta Tantalum 0.10 µg/g 0.04
74 W Tungsten 161.9 µg/g 2.7
79 Au Gold 6.9 µg/g 1.6
80 Hg Mercury < 6.6 µg/g -

69 / 148
 4/17/2024

81 Tl Thallium 1.9 µg/g 0.5

82 Pb Lead 0.00973 % 0.00025
83 Bi Bismuth ≈ 208.8 µg/g 3.9
90 Th Thorium < 4.6 µg/g -
92 U Uranium 3.6 µg/g 1.0
Sum of concentration 36.95 %

70 / 148
 4/17/2024

Sample Name 796113 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/15/2024 6:50 PM
Operator Converter Evaluation Date 4/15/2024 5:34 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0223 % 0.0020
14 SiO₂ Siliconoxide 0.0491 % 0.0020
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.6273 % 0.0018
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.6445 % 0.0068
20 CaO Calciumoxide 3.868 % 0.012
22 TiO₂ Titanoxid 0.1246 % 0.0024
23 V Vanadium 8.8 µg/g 0.6
24 Cr Chromium 3.2 µg/g 0.1
25 MnO Manganeseoxide 113.0 µg/g 5.3
26 Fe₂O₃ Ironoxide 17.89 % 0.02
27 Co Cobalt < 11 µg/g -
28 Ni Nickel < 0.8 µg/g -
29 Cu Copper 0.09087 % 0.00038
30 Zn Zinc 0.00757 % 0.00010
31 Ga Gallium 27.9 µg/g 2.3
33 As Arsenic 38.4 µg/g 2.1
34 Se Selenium < 1.0 µg/g -
35 Br Bromine < 0.4 µg/g -
37 Rb Rubidium 82.6 µg/g 0.8
38 Sr Strontium 106.9 µg/g 0.8
39 Y Yttrium 5.5 µg/g 0.4
40 Zr Zirconium 55.7 µg/g 0.7
41 Nb Niobium 5.2 µg/g 0.4
42 Mo Molybdenum 11.0 µg/g 0.8
47 Ag Silver 27.0 µg/g 4.0
48 Cd Cadmium < 28 µg/g -
50 Sn Tin 21.4 µg/g 1.0
51 Sb Antimony < 3.6 µg/g -
55 Cs Cesium 47.5 µg/g 8.5
56 Ba Barium 423 µg/g 11
57 La Lanthanium < 26 µg/g -
58 Ce Cerium < 33 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.3 µg/g -
73 Ta Tantalum < 1.0 µg/g -
74 W Tungsten 93.4 µg/g 1.7
79 Au Gold 2.3 µg/g 1.1
80 Hg Mercury < 4.5 µg/g -

71 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.01245 % 0.00022
83 Bi Bismuth ≈ 225.8 µg/g 3.0
90 Th Thorium < 3.7 µg/g -
92 U Uranium 2.6 µg/g 0.9
Sum of concentration 23.47 %

72 / 148
 4/17/2024

Sample Name 796114 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 12:13 PM
Operator Converter Evaluation Date 4/16/2024 10:58 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0766 % 0.0051
14 SiO₂ Siliconoxide 0.3860 % 0.0041
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.4340 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.021 % 0.012
20 CaO Calciumoxide 0.0434 % 0.0030
22 TiO₂ Titanoxid 0.2570 % 0.0030
23 V Vanadium 69.9 µg/g 4.4
24 Cr Chromium 21.4 µg/g 1.0
25 MnO Manganeseoxide 36.6 µg/g 3.5
26 Fe₂O₃ Ironoxide 6.389 % 0.008
27 Co Cobalt < 6.9 µg/g -
28 Ni Nickel 4.7 µg/g 0.2
29 Cu Copper 0.00736 % 0.00009
30 Zn Zinc 0.00255 % 0.00005
31 Ga Gallium 17.7 µg/g 1.5
33 As Arsenic 13.3 µg/g 0.9
34 Se Selenium < 0.6 µg/g -
35 Br Bromine < 0.3 µg/g -
37 Rb Rubidium 185.0 µg/g 0.9
38 Sr Strontium 7.9 µg/g 0.2
39 Y Yttrium 48.6 µg/g 0.7
40 Zr Zirconium 264.5 µg/g 0.9
41 Nb Niobium 16.4 µg/g 0.5
42 Mo Molybdenum 134.7 µg/g 0.8
47 Ag Silver < 29 µg/g -
48 Cd Cadmium < 19 µg/g -
50 Sn Tin 7.3 µg/g 0.6
51 Sb Antimony < 2.6 µg/g -
55 Cs Cesium < 12 µg/g -
56 Ba Barium 687 µg/g 12
57 La Lanthanium 40 µg/g 15
58 Ce Cerium 57 µg/g 15
60 Nd Neodymium 38.3 µg/g 3.7
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 6.3 µg/g 0.8
74 W Tungsten 10.6 µg/g 0.5
79 Au Gold < 1.0 µg/g -
80 Hg Mercury < 2.7 µg/g -

73 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00317 % 0.00009
83 Bi Bismuth < 1.1 µg/g -
90 Th Thorium 9.2 µg/g 0.5
92 U Uranium 3.7 µg/g 1.0
Sum of concentration 9.79 %

74 / 148
 4/17/2024

Sample Name 796114 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 12:19 PM
Operator Converter Evaluation Date 4/16/2024 11:03 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0915 % 0.0057
14 SiO₂ Siliconoxide 0.3217 % 0.0041
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.6296 % 0.0018
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.470 % 0.014
20 CaO Calciumoxide 0.0740 % 0.0038
22 TiO₂ Titanoxid 0.1152 % 0.0024
23 V Vanadium 25.9 µg/g 2.6
24 Cr Chromium 14.8 µg/g 0.8
25 MnO Manganeseoxide 47.0 µg/g 4.2
26 Fe₂O₃ Ironoxide 9.102 % 0.011
27 Co Cobalt < 8.3 µg/g -
28 Ni Nickel 4.0 µg/g 0.2
29 Cu Copper 0.00738 % 0.00010
30 Zn Zinc 0.00330 % 0.00006
31 Ga Gallium 16.4 µg/g 1.7
33 As Arsenic 10.8 µg/g 1.0
34 Se Selenium < 0.7 µg/g -
35 Br Bromine < 0.4 µg/g -
37 Rb Rubidium 267.6 µg/g 1.2
38 Sr Strontium 13.3 µg/g 0.3
39 Y Yttrium 49.2 µg/g 0.9
40 Zr Zirconium 65.2 µg/g 0.6
41 Nb Niobium 33.6 µg/g 0.6
42 Mo Molybdenum 45.9 µg/g 0.8
47 Ag Silver < 24 µg/g -
48 Cd Cadmium < 21 µg/g -
50 Sn Tin < 2.2 µg/g -
51 Sb Antimony 12.7 µg/g 1.8
55 Cs Cesium < 14 µg/g -
56 Ba Barium 1452 µg/g 15
57 La Lanthanium 29 µg/g 16
58 Ce Cerium 39 µg/g 14
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.9 µg/g -
73 Ta Tantalum 5.9 µg/g 0.7
74 W Tungsten 5.6 µg/g 0.4
79 Au Gold < 1.2 µg/g -
80 Hg Mercury < 2.5 µg/g -

75 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00365 % 0.00010
83 Bi Bismuth 9.5 µg/g 0.8
90 Th Thorium 7.8 µg/g 0.7
92 U Uranium 5.6 µg/g 1.4
Sum of concentration 13.03 %

76 / 148
 4/17/2024

Sample Name 796114 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 12:24 PM
Operator Converter Evaluation Date 4/16/2024 11:08 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0817 % 0.0052
14 SiO₂ Siliconoxide 0.1477 % 0.0030
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3595 % 0.0013
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.821 % 0.012
20 CaO Calciumoxide 0.1327 % 0.0040
22 TiO₂ Titanoxid 0.3080 % 0.0032
23 V Vanadium 60.5 µg/g 4.3
24 Cr Chromium 5.5 µg/g 0.3
25 MnO Manganeseoxide 31.9 µg/g 3.9
26 Fe₂O₃ Ironoxide 8.613 % 0.010
27 Co Cobalt < 8.1 µg/g -
28 Ni Nickel 4.1 µg/g 0.2
29 Cu Copper 0.00910 % 0.00010
30 Zn Zinc 0.00252 % 0.00005
31 Ga Gallium 17.6 µg/g 1.7
33 As Arsenic 27.0 µg/g 1.5
34 Se Selenium < 0.7 µg/g -
35 Br Bromine < 0.4 µg/g -
37 Rb Rubidium 164.2 µg/g 0.9
38 Sr Strontium 25.3 µg/g 0.4
39 Y Yttrium 54.2 µg/g 0.7
40 Zr Zirconium 224.6 µg/g 0.9
41 Nb Niobium 19.1 µg/g 0.5
42 Mo Molybdenum 381.5 µg/g 1.3
47 Ag Silver < 27 µg/g -
48 Cd Cadmium < 21 µg/g -
50 Sn Tin 5.4 µg/g 0.4
51 Sb Antimony 7.5 µg/g 1.7
55 Cs Cesium < 13 µg/g -
56 Ba Barium 1669 µg/g 14
57 La Lanthanium 74 µg/g 15
58 Ce Cerium 149 µg/g 18
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.9 µg/g -
73 Ta Tantalum 8.8 µg/g 1.0
74 W Tungsten 20.4 µg/g 0.7
79 Au Gold < 1.1 µg/g -
80 Hg Mercury < 2.8 µg/g -

77 / 148
 4/17/2024

81 Tl Thallium < 0.7 µg/g -

82 Pb Lead 0.00996 % 0.00016
83 Bi Bismuth 11.9 µg/g 0.9
90 Th Thorium 14.4 µg/g 0.7
92 U Uranium 5.3 µg/g 1.2
Sum of concentration 11.78 %

78 / 148
 4/17/2024

Sample Name 796115 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 12:30 PM
Operator Converter Evaluation Date 4/16/2024 11:14 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0541 % 0.0068
14 SiO₂ Siliconoxide 0.1953 % 0.0044
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3926 % 0.0016
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.3180 % 0.0058
20 CaO Calciumoxide 0.4488 % 0.0045
22 TiO₂ Titanoxid 0.1481 % 0.0025
23 V Vanadium < 4.9 µg/g -
24 Cr Chromium < 4.4 µg/g -
25 MnO Manganeseoxide 776.2 µg/g 9.6
26 Fe₂O₃ Ironoxide 40.36 % 0.05
27 Co Cobalt 18.9 µg/g 0.8
28 Ni Nickel < 1.7 µg/g -
29 Cu Copper 0.5178 % 0.0014
30 Zn Zinc 0.3376 % 0.0010
31 Ga Gallium 8.0 µg/g 3.5
33 As Arsenic 15.6 µg/g 2.7
34 Se Selenium < 1.6 µg/g -
35 Br Bromine < 0.9 µg/g -
37 Rb Rubidium 23.5 µg/g 0.8
38 Sr Strontium 32.4 µg/g 0.7
39 Y Yttrium 11.7 µg/g 0.5
40 Zr Zirconium 84.0 µg/g 1.0
41 Nb Niobium 5.5 µg/g 0.4
42 Mo Molybdenum 9.1 µg/g 0.9
47 Ag Silver 21.0 µg/g 2.7
48 Cd Cadmium 135 µg/g 13
50 Sn Tin < 4.0 µg/g -
51 Sb Antimony < 5.5 µg/g -
55 Cs Cesium < 18 µg/g -
56 Ba Barium 44 µg/g 11
57 La Lanthanium < 33 µg/g -
58 Ce Cerium 64 µg/g 20
60 Nd Neodymium < 18 µg/g -
72 Hf Hafnium < 3.2 µg/g -
73 Ta Tantalum 0.10 µg/g 0.03
74 W Tungsten 63.3 µg/g 2.5
79 Au Gold < 2.3 µg/g -
80 Hg Mercury < 6.2 µg/g -

79 / 148
 4/17/2024

81 Tl Thallium 2.3 µg/g 0.5

82 Pb Lead 0.01077 % 0.00027
83 Bi Bismuth 51.7 µg/g 2.3
90 Th Thorium 2.8 µg/g 0.9
92 U Uranium 5.3 µg/g 1.1
Sum of concentration 42.92 %

80 / 148
 4/17/2024

Sample Name 796115 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 12:34 PM
Operator Converter Evaluation Date 4/16/2024 11:18 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0485 % 0.0049
14 SiO₂ Siliconoxide 0.2893 % 0.0039
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2812 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5560 % 0.0059
20 CaO Calciumoxide 0.4912 % 0.0042
22 TiO₂ Titanoxid 0.1641 % 0.0021
23 V Vanadium 19.9 µg/g 1.0
24 Cr Chromium < 3.8 µg/g -
25 MnO Manganeseoxide 961.1 µg/g 8.7
26 Fe₂O₃ Ironoxide 33.49 % 0.04
27 Co Cobalt 51.9 µg/g 1.9
28 Ni Nickel < 0.7 µg/g -
29 Cu Copper 1.168 % 0.002
30 Zn Zinc 0.3304 % 0.0008
31 Ga Gallium < 5.6 µg/g -
33 As Arsenic 116.0 µg/g 3.9
34 Se Selenium 7.9 µg/g 0.6
35 Br Bromine 6.6 µg/g 0.8
37 Rb Rubidium 85.5 µg/g 1.2
38 Sr Strontium 54.0 µg/g 0.8
39 Y Yttrium 17.0 µg/g 0.7
40 Zr Zirconium 75.0 µg/g 0.9
41 Nb Niobium 8.6 µg/g 0.6
42 Mo Molybdenum 8.7 µg/g 0.9
47 Ag Silver 25.8 µg/g 4.3
48 Cd Cadmium 295 µg/g 13
50 Sn Tin < 3.7 µg/g -
51 Sb Antimony < 5.6 µg/g -
55 Cs Cesium 56 µg/g 10
56 Ba Barium 94 µg/g 12
57 La Lanthanium < 10 µg/g -
58 Ce Cerium < 12 µg/g -
60 Nd Neodymium 23.8 µg/g 1.4
72 Hf Hafnium 83 µg/g 15
73 Ta Tantalum 225 µg/g 31
74 W Tungsten 134.3 µg/g 2.6
79 Au Gold 9.4 µg/g 1.9
80 Hg Mercury < 8.1 µg/g -

81 / 148
 4/17/2024

81 Tl Thallium 5.0 µg/g 0.6

82 Pb Lead 0.01746 % 0.00040
83 Bi Bismuth ≈ 2386 µg/g 12
90 Th Thorium < 15 µg/g -
92 U Uranium 9.4 µg/g 1.4
Sum of concentration 37.31 %

82 / 148
 4/17/2024

Sample Name 796115 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 12:39 PM
Operator Converter Evaluation Date 4/16/2024 11:24 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0598 % 0.0058
14 SiO₂ Siliconoxide 0.1411 % 0.0036
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3477 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.8238 % 0.0081
20 CaO Calciumoxide 0.9710 % 0.0063
22 TiO₂ Titanoxid 0.2822 % 0.0033
23 V Vanadium 51.8 µg/g 2.7
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 1226 µg/g 9
26 Fe₂O₃ Ironoxide 19.41 % 0.02
27 Co Cobalt 55.3 µg/g 2.2
28 Ni Nickel 8.6 µg/g 0.4
29 Cu Copper 0.5766 % 0.0011
30 Zn Zinc 0.2299 % 0.0006
31 Ga Gallium 16.5 µg/g 2.8
33 As Arsenic 66.5 µg/g 3.1
34 Se Selenium < 1.2 µg/g -
35 Br Bromine 4.6 µg/g 0.5
37 Rb Rubidium 86.3 µg/g 0.9
38 Sr Strontium 99.1 µg/g 0.8
39 Y Yttrium 16.4 µg/g 0.5
40 Zr Zirconium 101.3 µg/g 0.9
41 Nb Niobium 9.6 µg/g 0.5
42 Mo Molybdenum 13.5 µg/g 0.9
47 Ag Silver < 22 µg/g -
48 Cd Cadmium < 30 µg/g -
50 Sn Tin 39.8 µg/g 1.2
51 Sb Antimony < 3.8 µg/g -
55 Cs Cesium < 14 µg/g -
56 Ba Barium 280 µg/g 10
57 La Lanthanium 68 µg/g 15
58 Ce Cerium 66 µg/g 15
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 41.6 µg/g 7.6
73 Ta Tantalum 11.0 µg/g 2.4
74 W Tungsten 127.9 µg/g 2.3
79 Au Gold 3.1 µg/g 1.0
80 Hg Mercury < 5.7 µg/g -

83 / 148
 4/17/2024

81 Tl Thallium 1.4 µg/g 0.3

82 Pb Lead 0.02643 % 0.00033
83 Bi Bismuth ≈ 267.8 µg/g 3.4
90 Th Thorium < 4.3 µg/g -
92 U Uranium 6.8 µg/g 1.1
Sum of concentration 23.14 %

84 / 148
 4/17/2024

Sample Name 796116 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 12:44 PM
Operator Converter Evaluation Date 4/16/2024 11:28 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0213 % 0.0021
14 SiO₂ Siliconoxide 0.2407 % 0.0045
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.9404 % 0.0026
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.3370 % 0.0064
20 CaO Calciumoxide 4.506 % 0.014
22 TiO₂ Titanoxid 0.1166 % 0.0026
23 V Vanadium 26.6 µg/g 1.3
24 Cr Chromium < 4.8 µg/g -
25 MnO Manganeseoxide < 1.1 µg/g -
26 Fe₂O₃ Ironoxide 32.10 % 0.04
27 Co Cobalt < 16 µg/g -
28 Ni Nickel < 1.1 µg/g -
29 Cu Copper 0.1740 % 0.0007
30 Zn Zinc 0.04751 % 0.00030
31 Ga Gallium 37.8 µg/g 3.1
33 As Arsenic 601.4 µg/g 5.2
34 Se Selenium < 1.4 µg/g -
35 Br Bromine < 0.5 µg/g -
37 Rb Rubidium 19.2 µg/g 0.7
38 Sr Strontium 43.1 µg/g 0.7
39 Y Yttrium 9.3 µg/g 0.4
40 Zr Zirconium 29.8 µg/g 0.7
41 Nb Niobium 5.0 µg/g 0.5
42 Mo Molybdenum 14.0 µg/g 1.1
47 Ag Silver < 18 µg/g -
48 Cd Cadmium 78.6 µg/g 8.6
50 Sn Tin 31.9 µg/g 1.1
51 Sb Antimony < 4.7 µg/g -
55 Cs Cesium < 17 µg/g -
56 Ba Barium 45 µg/g 10
57 La Lanthanium < 28 µg/g -
58 Ce Cerium < 35 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.8 µg/g -
73 Ta Tantalum 0.10 µg/g 0.04
74 W Tungsten 182.1 µg/g 3.1
79 Au Gold 11.5 µg/g 1.9
80 Hg Mercury < 7.0 µg/g -

85 / 148
 4/17/2024

81 Tl Thallium 3.3 µg/g 0.8

82 Pb Lead 0.00839 % 0.00027
83 Bi Bismuth ≈ 383.7 µg/g 5.2
90 Th Thorium < 1.2 µg/g -
92 U Uranium 4.5 µg/g 0.9
Sum of concentration 38.64 %

86 / 148
 4/17/2024

Sample Name 796116 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 12:49 PM
Operator Converter Evaluation Date 4/16/2024 11:33 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0470 % 0.0051
14 SiO₂ Siliconoxide 0.1966 % 0.0037
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.4536 % 0.0016
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5443 % 0.0062
20 CaO Calciumoxide 0.6815 % 0.0049
22 TiO₂ Titanoxid 0.1278 % 0.0021
23 V Vanadium 20.0 µg/g 1.0
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 92.7 µg/g 5.3
26 Fe₂O₃ Ironoxide 22.06 % 0.03
27 Co Cobalt < 12 µg/g -
28 Ni Nickel 2.5 µg/g 0.1
29 Cu Copper 0.1642 % 0.0006
30 Zn Zinc 0.02835 % 0.00019
31 Ga Gallium 28.7 µg/g 2.5
33 As Arsenic 44.8 µg/g 2.3
34 Se Selenium < 1.1 µg/g -
35 Br Bromine 1.5 µg/g 0.4
37 Rb Rubidium 47.1 µg/g 0.7
38 Sr Strontium 37.7 µg/g 0.5
39 Y Yttrium 1.3 µg/g 0.2
40 Zr Zirconium 43.6 µg/g 0.6
41 Nb Niobium 4.1 µg/g 0.4
42 Mo Molybdenum 6.1 µg/g 0.7
47 Ag Silver 29.2 µg/g 4.2
48 Cd Cadmium < 30 µg/g -
50 Sn Tin < 2.9 µg/g -
51 Sb Antimony < 4.0 µg/g -
55 Cs Cesium 21.2 µg/g 9.1
56 Ba Barium 64 µg/g 11
57 La Lanthanium < 29 µg/g -
58 Ce Cerium < 38 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 1.5 µg/g 0.4
73 Ta Tantalum 0.10 µg/g 0.03
74 W Tungsten 94.8 µg/g 1.8
79 Au Gold 4.1 µg/g 1.4
80 Hg Mercury < 4.8 µg/g -

87 / 148
 4/17/2024

81 Tl Thallium 1.6 µg/g 0.3

82 Pb Lead 0.01341 % 0.00028
83 Bi Bismuth ≈ 747.4 µg/g 5.4
90 Th Thorium < 0.4 µg/g -
92 U Uranium 2.4 µg/g 0.9
Sum of concentration 24.45 %

88 / 148
 4/17/2024

Sample Name 796116 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 12:56 PM
Operator Converter Evaluation Date 4/16/2024 11:40 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0606 % 0.0053
14 SiO₂ Siliconoxide 0.1215 % 0.0034
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.4854 % 0.0017
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5035 % 0.0066
20 CaO Calciumoxide 1.645 % 0.008
22 TiO₂ Titanoxid 0.1825 % 0.0028
23 V Vanadium 23.4 µg/g 1.4
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 133.0 µg/g 5.8
26 Fe₂O₃ Ironoxide 20.93 % 0.02
27 Co Cobalt 27.2 µg/g 1.3
28 Ni Nickel 1.4 µg/g 0.1
29 Cu Copper 0.1458 % 0.0005
30 Zn Zinc 0.05836 % 0.00027
31 Ga Gallium 25.3 µg/g 2.6
33 As Arsenic 112.6 µg/g 2.7
34 Se Selenium < 1.3 µg/g -
35 Br Bromine < 0.4 µg/g -
37 Rb Rubidium 59.6 µg/g 0.7
38 Sr Strontium 69.8 µg/g 0.7
39 Y Yttrium 8.5 µg/g 0.4
40 Zr Zirconium 79.3 µg/g 0.8
41 Nb Niobium 7.8 µg/g 0.5
42 Mo Molybdenum 10.7 µg/g 0.8
47 Ag Silver < 22 µg/g -
48 Cd Cadmium < 31 µg/g -
50 Sn Tin 131.6 µg/g 2.0
51 Sb Antimony < 3.9 µg/g -
55 Cs Cesium < 15 µg/g -
56 Ba Barium 491 µg/g 11
57 La Lanthanium 39 µg/g 15
58 Ce Cerium < 34 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.3 µg/g -
73 Ta Tantalum 0.10 µg/g 0.02
74 W Tungsten 258.6 µg/g 3.0
79 Au Gold 7.4 µg/g 1.5
80 Hg Mercury < 6.6 µg/g -

89 / 148
 4/17/2024

81 Tl Thallium 2.2 µg/g 0.4

82 Pb Lead 0.01468 % 0.00028
83 Bi Bismuth ≈ 522.4 µg/g 4.7
90 Th Thorium < 5.9 µg/g -
92 U Uranium 5.9 µg/g 1.0
Sum of concentration 24.35 %

90 / 148
 4/17/2024

Sample Name 796117 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:02 PM
Operator Converter Evaluation Date 4/16/2024 11:46 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0834 % 0.0083
14 SiO₂ Siliconoxide 0.1604 % 0.0048
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3850 % 0.0017
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.2749 % 0.0078
20 CaO Calciumoxide 0.5774 % 0.0067
22 TiO₂ Titanoxid 0.0246 % 0.0020
23 V Vanadium < 8.2 µg/g -
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 70350 µg/g 110
26 Fe₂O₃ Ironoxide 17.82 % 0.02
27 Co Cobalt 45.9 µg/g 1.5
28 Ni Nickel < 0.7 µg/g -
29 Cu Copper 17.97 % 0.02
30 Zn Zinc 1.266 % 0.002
31 Ga Gallium < 14 µg/g -
33 As Arsenic 235 µg/g 20
34 Se Selenium < 3.9 µg/g -
35 Br Bromine 9.7 µg/g 1.3
37 Rb Rubidium 12.5 µg/g 0.9
38 Sr Strontium 35.7 µg/g 0.9
39 Y Yttrium ≈ 69.9 µg/g 1.3
40 Zr Zirconium 7.3 µg/g 0.4
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 15.4 µg/g 1.1
47 Ag Silver 93.0 µg/g 9.3
48 Cd Cadmium 213 µg/g 16
50 Sn Tin < 5.9 µg/g -
51 Sb Antimony < 8.2 µg/g -
55 Cs Cesium < 28 µg/g -
56 Ba Barium 402 µg/g 18
57 La Lanthanium < 25 µg/g -
58 Ce Cerium 63 µg/g 17
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 2966 µg/g 150
73 Ta Tantalum 3926 µg/g 130
74 W Tungsten < 2.0 µg/g -
79 Au Gold < 7.4 µg/g -
80 Hg Mercury < 11 µg/g -

91 / 148
 4/17/2024

81 Tl Thallium < 0.4 µg/g -

82 Pb Lead 0.4108 % 0.0017
83 Bi Bismuth < 10 µg/g -
90 Th Thorium 146.6 µg/g 5.1
92 U Uranium 9.6 µg/g 1.4
Sum of concentration 46.83 %

92 / 148
 4/17/2024

Sample Name 796117 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:06 PM
Operator Converter Evaluation Date 4/16/2024 11:50 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0576 % 0.0052
14 SiO₂ Siliconoxide 0.3111 % 0.0040
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2271 % 0.0010
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.6781 % 0.0066
20 CaO Calciumoxide 0.2713 % 0.0035
22 TiO₂ Titanoxid 0.1835 % 0.0022
23 V Vanadium 53.5 µg/g 2.5
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 68840 µg/g 100
26 Fe₂O₃ Ironoxide 16.79 % 0.02
27 Co Cobalt 243.8 µg/g 4.0
28 Ni Nickel 15.2 µg/g 0.6
29 Cu Copper 1.959 % 0.003
30 Zn Zinc 1.842 % 0.003
31 Ga Gallium < 9.1 µg/g -
33 As Arsenic 362 µg/g 14
34 Se Selenium < 1.6 µg/g -
35 Br Bromine 4.2 µg/g 0.9
37 Rb Rubidium 47.1 µg/g 0.9
38 Sr Strontium 75.7 µg/g 0.8
39 Y Yttrium ≈ 87.9 µg/g 1.0
40 Zr Zirconium 36.7 µg/g 0.7
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 13.6 µg/g 1.0
47 Ag Silver 132.0 µg/g 9.2
48 Cd Cadmium 300 µg/g 13
50 Sn Tin < 3.9 µg/g -
51 Sb Antimony 273.1 µg/g 4.1
55 Cs Cesium 20.3 µg/g 9.7
56 Ba Barium 205 µg/g 12
57 La Lanthanium < 10 µg/g -
58 Ce Cerium < 5.6 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 147 µg/g 24
73 Ta Tantalum 162 µg/g 13
74 W Tungsten 55.2 µg/g 1.6
79 Au Gold < 2.4 µg/g -
80 Hg Mercury < 7.3 µg/g -

93 / 148
 4/17/2024

81 Tl Thallium 0.26 µg/g 0.02

82 Pb Lead 0.4310 % 0.0013
83 Bi Bismuth 127.2 µg/g 4.2
90 Th Thorium 9.5 µg/g 3.0
92 U Uranium 13.3 µg/g 1.2
Sum of concentration 29.87 %

94 / 148
 4/17/2024

Sample Name 796117 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:11 PM
Operator Converter Evaluation Date 4/16/2024 11:55 AM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0709 % 0.0068
14 SiO₂ Siliconoxide 0.1420 % 0.0038
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2826 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.8972 % 0.0088
20 CaO Calciumoxide 0.3829 % 0.0046
22 TiO₂ Titanoxid 0.2333 % 0.0032
23 V Vanadium 31.1 µg/g 2.1
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 19040 µg/g 40
26 Fe₂O₃ Ironoxide 19.49 % 0.02
27 Co Cobalt 146.6 µg/g 3.8
28 Ni Nickel 4.4 µg/g 0.2
29 Cu Copper 1.156 % 0.002
30 Zn Zinc 1.808 % 0.003
31 Ga Gallium < 9.4 µg/g -
33 As Arsenic 428 µg/g 15
34 Se Selenium 2.2 µg/g 0.2
35 Br Bromine < 0.8 µg/g -
37 Rb Rubidium 112.0 µg/g 1.1
38 Sr Strontium 114.0 µg/g 1.0
39 Y Yttrium ≈ 89.3 µg/g 1.1
40 Zr Zirconium 89.0 µg/g 0.9
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 22.8 µg/g 1.0
47 Ag Silver 54.0 µg/g 6.8
48 Cd Cadmium 232 µg/g 16
50 Sn Tin < 3.7 µg/g -
51 Sb Antimony 125.1 µg/g 3.4
55 Cs Cesium < 17 µg/g -
56 Ba Barium 579 µg/g 14
57 La Lanthanium 43 µg/g 16
58 Ce Cerium 50 µg/g 14
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 89 µg/g 16
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 97.8 µg/g 3.1
79 Au Gold 3.2 µg/g 0.7
80 Hg Mercury < 7.2 µg/g -

95 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.4716 % 0.0014
83 Bi Bismuth ≈ 211.2 µg/g 4.8
90 Th Thorium 25.9 µg/g 4.0
92 U Uranium 8.3 µg/g 1.4
Sum of concentration 27.09 %

96 / 148
 4/17/2024

Sample Name 796118 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:17 PM
Operator Converter Evaluation Date 4/16/2024 12:01 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0945 % 0.0058
14 SiO₂ Siliconoxide 0.5032 % 0.0055
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3054 % 0.0013
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.8019 % 0.0088
20 CaO Calciumoxide 1.731 % 0.009
22 TiO₂ Titanoxid 0.3962 % 0.0039
23 V Vanadium 85.9 µg/g 4.8
24 Cr Chromium 19.6 µg/g 1.0
25 MnO Manganeseoxide 16740 µg/g 30
26 Fe₂O₃ Ironoxide 8.985 % 0.011
27 Co Cobalt 102.3 µg/g 3.5
28 Ni Nickel 22.5 µg/g 0.7
29 Cu Copper 0.1141 % 0.0004
30 Zn Zinc 0.9203 % 0.0013
31 Ga Gallium 4.4 µg/g 3.3
33 As Arsenic 125.8 µg/g 6.8
34 Se Selenium < 0.9 µg/g -
35 Br Bromine < 0.5 µg/g -
37 Rb Rubidium 16.0 µg/g 0.4
38 Sr Strontium 27.3 µg/g 0.4
39 Y Yttrium 32.6 µg/g 0.4
40 Zr Zirconium 154.2 µg/g 0.9
41 Nb Niobium 7.0 µg/g 0.5
42 Mo Molybdenum 9.5 µg/g 0.8
47 Ag Silver < 24 µg/g -
48 Cd Cadmium 164.9 µg/g 8.8
50 Sn Tin < 2.5 µg/g -
51 Sb Antimony 24.1 µg/g 2.1
55 Cs Cesium < 14 µg/g -
56 Ba Barium 268 µg/g 10
57 La Lanthanium 72 µg/g 14
58 Ce Cerium 149 µg/g 17
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.9 µg/g -
73 Ta Tantalum 18.0 µg/g 3.9
74 W Tungsten 60.5 µg/g 3.3
79 Au Gold < 1.4 µg/g -
80 Hg Mercury 4.8 µg/g 1.1

97 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.1547 % 0.0006
83 Bi Bismuth 12.2 µg/g 1.6
90 Th Thorium 21.7 µg/g 1.6
92 U Uranium 11.8 µg/g 0.8
Sum of concentration 15.82 %

98 / 148
 4/17/2024

Sample Name 796118 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:22 PM
Operator Converter Evaluation Date 4/16/2024 12:06 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0940 % 0.0060
14 SiO₂ Siliconoxide 0.4655 % 0.0053
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3408 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.504 % 0.012
20 CaO Calciumoxide 1.837 % 0.010
22 TiO₂ Titanoxid 0.3852 % 0.0040
23 V Vanadium 63.0 µg/g 4.3
24 Cr Chromium < 4.3 µg/g -
25 MnO Manganeseoxide 20780 µg/g 40
26 Fe₂O₃ Ironoxide 12.27 % 0.01
27 Co Cobalt 131.2 µg/g 4.1
28 Ni Nickel 14.9 µg/g 0.6
29 Cu Copper 0.4225 % 0.0009
30 Zn Zinc ≈ 2.694 % 0.003
31 Ga Gallium 40.5 µg/g 4.7
33 As Arsenic 241.0 µg/g 8.0
34 Se Selenium < 1.3 µg/g -
35 Br Bromine 3.2 µg/g 0.6
37 Rb Rubidium 151.3 µg/g 1.3
38 Sr Strontium 197.5 µg/g 1.3
39 Y Yttrium ≈ 46.6 µg/g 0.8
40 Zr Zirconium 96.4 µg/g 1.0
41 Nb Niobium 5.1 µg/g 0.6
42 Mo Molybdenum 11.5 µg/g 0.9
47 Ag Silver 17.3 µg/g 3.2
48 Cd Cadmium 584 µg/g 18
50 Sn Tin < 3.4 µg/g -
51 Sb Antimony 75.7 µg/g 3.1
55 Cs Cesium 32 µg/g 10
56 Ba Barium 1248 µg/g 16
57 La Lanthanium 37 µg/g 18
58 Ce Cerium < 12 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 3.8 µg/g -
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 179.8 µg/g 5.8
79 Au Gold < 1.9 µg/g -
80 Hg Mercury < 5.7 µg/g -

99 / 148
 4/17/2024

81 Tl Thallium < 0.3 µg/g -

82 Pb Lead 0.1578 % 0.0007
83 Bi Bismuth 29.2 µg/g 2.3
90 Th Thorium 19.6 µg/g 2.0
92 U Uranium 8.7 µg/g 1.4
Sum of concentration 22.57 %

100 / 148
 4/17/2024

Sample Name 796118 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:26 PM
Operator Converter Evaluation Date 4/16/2024 12:10 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0754 % 0.0056
14 SiO₂ Siliconoxide 0.1519 % 0.0034
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2875 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.201 % 0.010
20 CaO Calciumoxide 1.015 % 0.007
22 TiO₂ Titanoxid 0.2855 % 0.0033
23 V Vanadium 54.3 µg/g 3.5
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 20220 µg/g 40
26 Fe₂O₃ Ironoxide 11.65 % 0.01
27 Co Cobalt 154.5 µg/g 4.2
28 Ni Nickel 21.7 µg/g 0.7
29 Cu Copper 0.4047 % 0.0009
30 Zn Zinc ≈ 2.877 % 0.004
31 Ga Gallium 39.2 µg/g 4.6
33 As Arsenic 229.7 µg/g 7.9
34 Se Selenium < 1.5 µg/g -
35 Br Bromine < 0.5 µg/g -
37 Rb Rubidium 163.0 µg/g 1.2
38 Sr Strontium 166.9 µg/g 1.2
39 Y Yttrium ≈ 47.9 µg/g 0.8
40 Zr Zirconium 89.3 µg/g 0.9
41 Nb Niobium 6.1 µg/g 0.5
42 Mo Molybdenum 17.0 µg/g 0.8
47 Ag Silver 18.5 µg/g 3.5
48 Cd Cadmium 293 µg/g 16
50 Sn Tin < 3.0 µg/g -
51 Sb Antimony 178.7 µg/g 3.1
55 Cs Cesium < 15 µg/g -
56 Ba Barium 729 µg/g 13
57 La Lanthanium 43 µg/g 14
58 Ce Cerium 38 µg/g 11
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 3.8 µg/g -
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 204.7 µg/g 6.1
79 Au Gold < 1.8 µg/g -
80 Hg Mercury < 5.8 µg/g -

101 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.1680 % 0.0007
83 Bi Bismuth 30.3 µg/g 2.2
90 Th Thorium 18.0 µg/g 1.9
92 U Uranium 8.8 µg/g 1.4
Sum of concentration 20.39 %

102 / 148
 4/17/2024

Sample Name 796119 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:31 PM
Operator Converter Evaluation Date 4/16/2024 12:15 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide < 0.0038 % -
14 SiO₂ Siliconoxide 0.1775 % 0.0025
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2090 % 0.0010
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.6227 % 0.0063
20 CaO Calciumoxide 12.96 % 0.02
22 TiO₂ Titanoxid 0.1973 % 0.0027
23 V Vanadium 12.7 µg/g 1.1
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 12720 µg/g 30
26 Fe₂O₃ Ironoxide 15.82 % 0.02
27 Co Cobalt < 9.4 µg/g -
28 Ni Nickel 11.9 µg/g 0.6
29 Cu Copper 1.400 % 0.002
30 Zn Zinc ≈ 3.395 % 0.004
31 Ga Gallium 26.8 µg/g 6.2
33 As Arsenic 175 µg/g 12
34 Se Selenium < 1.6 µg/g -
35 Br Bromine 3.4 µg/g 0.7
37 Rb Rubidium 26.1 µg/g 0.7
38 Sr Strontium 67.5 µg/g 0.8
39 Y Yttrium ≈ 58.7 µg/g 0.9
40 Zr Zirconium 23.7 µg/g 0.6
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 29.1 µg/g 1.0
47 Ag Silver 28.7 µg/g 4.5
48 Cd Cadmium 213 µg/g 12
50 Sn Tin < 3.3 µg/g -
51 Sb Antimony < 4.7 µg/g -
55 Cs Cesium 20.0 µg/g 9.7
56 Ba Barium 39 µg/g 11
57 La Lanthanium 44 µg/g 14
58 Ce Cerium < 12 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 105 µg/g 19
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 150.9 µg/g 4.6
79 Au Gold < 2.3 µg/g -
80 Hg Mercury < 7.1 µg/g -

103 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.3365 % 0.0011
83 Bi Bismuth 49.3 µg/g 3.2
90 Th Thorium 9.8 µg/g 2.5
92 U Uranium 13.2 µg/g 1.0
Sum of concentration 36.50 %

104 / 148
 4/17/2024

Sample Name 796119 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:36 PM
Operator Converter Evaluation Date 4/16/2024 12:21 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0635 % 0.0054
14 SiO₂ Siliconoxide 0.2085 % 0.0036
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3117 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5211 % 0.0063
20 CaO Calciumoxide 0.3794 % 0.0040
22 TiO₂ Titanoxid 0.0965 % 0.0020
23 V Vanadium < 4.3 µg/g -
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 3526 µg/g 13
26 Fe₂O₃ Ironoxide 22.66 % 0.03
27 Co Cobalt 46.9 µg/g 1.9
28 Ni Nickel < 0.7 µg/g -
29 Cu Copper 0.5745 % 0.0012
30 Zn Zinc 1.684 % 0.002
31 Ga Gallium 6.6 µg/g 6.3
33 As Arsenic 168 µg/g 14
34 Se Selenium < 1.4 µg/g -
35 Br Bromine 2.7 µg/g 0.8
37 Rb Rubidium 316.9 µg/g 1.8
38 Sr Strontium 30.1 µg/g 0.6
39 Y Yttrium ≈ 82.1 µg/g 1.2
40 Zr Zirconium 21.1 µg/g 0.5
41 Nb Niobium < 0.3 µg/g -
42 Mo Molybdenum 15.7 µg/g 0.9
47 Ag Silver 42.4 µg/g 5.8
48 Cd Cadmium 66.2 µg/g 9.2
50 Sn Tin < 3.6 µg/g -
51 Sb Antimony 23.9 µg/g 2.8
55 Cs Cesium < 16 µg/g -
56 Ba Barium 43 µg/g 12
57 La Lanthanium 51 µg/g 16
58 Ce Cerium < 12 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 23.9 µg/g 6.9
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 87.8 µg/g 3.8
79 Au Gold < 2.4 µg/g -
80 Hg Mercury < 6.3 µg/g -

105 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.4954 % 0.0014
83 Bi Bismuth 38.0 µg/g 3.1
90 Th Thorium 24.2 µg/g 3.2
92 U Uranium 8.8 µg/g 1.8
Sum of concentration 27.46 %

106 / 148
 4/17/2024

Sample Name 796119 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:41 PM
Operator Converter Evaluation Date 4/16/2024 12:25 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0749 % 0.0064
14 SiO₂ Siliconoxide 0.0712 % 0.0031
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2793 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.8983 % 0.0090
20 CaO Calciumoxide 0.8881 % 0.0065
22 TiO₂ Titanoxid 0.2696 % 0.0033
23 V Vanadium 44.4 µg/g 2.8
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 12300 µg/g 30
26 Fe₂O₃ Ironoxide 17.12 % 0.02
27 Co Cobalt 121.4 µg/g 3.7
28 Ni Nickel 7.2 µg/g 0.3
29 Cu Copper 0.6376 % 0.0012
30 Zn Zinc 1.724 % 0.002
31 Ga Gallium < 8.4 µg/g -
33 As Arsenic 358 µg/g 13
34 Se Selenium < 1.4 µg/g -
35 Br Bromine < 0.8 µg/g -
37 Rb Rubidium 125.2 µg/g 1.2
38 Sr Strontium 107.8 µg/g 1.0
39 Y Yttrium ≈ 79.5 µg/g 1.0
40 Zr Zirconium 105.9 µg/g 0.9
41 Nb Niobium 5.5 µg/g 0.6
42 Mo Molybdenum 21.5 µg/g 0.9
47 Ag Silver 36.0 µg/g 5.5
48 Cd Cadmium 298 µg/g 17
50 Sn Tin < 3.4 µg/g -
51 Sb Antimony 92.7 µg/g 3.0
55 Cs Cesium < 16 µg/g -
56 Ba Barium 459 µg/g 13
57 La Lanthanium 52 µg/g 16
58 Ce Cerium 84 µg/g 16
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 45.7 µg/g 9.9
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 119.5 µg/g 4.0
79 Au Gold 6.9 µg/g 1.1
80 Hg Mercury 11.7 µg/g 2.0

107 / 148
 4/17/2024

81 Tl Thallium 0.23 µg/g 0.02

82 Pb Lead 0.4074 % 0.0012
83 Bi Bismuth 180.2 µg/g 4.2
90 Th Thorium 29.7 µg/g 3.6
92 U Uranium 7.9 µg/g 1.3
Sum of concentration 23.84 %

108 / 148
 4/17/2024

Sample Name 796120 a Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:46 PM
Operator Converter Evaluation Date 4/16/2024 12:30 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0938 % 0.0065
14 SiO₂ Siliconoxide 0.4581 % 0.0056
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3070 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5425 % 0.0073
20 CaO Calciumoxide 1.238 % 0.007
22 TiO₂ Titanoxid 0.3341 % 0.0034
23 V Vanadium 34.3 µg/g 2.1
24 Cr Chromium 5.8 µg/g 0.2
25 MnO Manganeseoxide 4482 µg/g 16
26 Fe₂O₃ Ironoxide 21.53 % 0.02
27 Co Cobalt 86.0 µg/g 3.1
28 Ni Nickel 17.4 µg/g 0.6
29 Cu Copper 0.4022 % 0.0010
30 Zn Zinc 0.9481 % 0.0015
31 Ga Gallium 16.1 µg/g 3.6
33 As Arsenic 90.8 µg/g 6.4
34 Se Selenium < 1.2 µg/g -
35 Br Bromine < 0.9 µg/g -
37 Rb Rubidium 63.5 µg/g 0.8
38 Sr Strontium 23.8 µg/g 0.5
39 Y Yttrium 20.2 µg/g 0.4
40 Zr Zirconium 70.1 µg/g 0.8
41 Nb Niobium 5.8 µg/g 0.5
42 Mo Molybdenum 8.6 µg/g 0.9
47 Ag Silver < 20 µg/g -
48 Cd Cadmium 214 µg/g 12
50 Sn Tin < 3.1 µg/g -
51 Sb Antimony 89.0 µg/g 3.0
55 Cs Cesium < 16 µg/g -
56 Ba Barium 46 µg/g 10
57 La Lanthanium < 27 µg/g -
58 Ce Cerium 46 µg/g 15
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 13.9 µg/g 4.0
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 94.9 µg/g 3.7
79 Au Gold < 1.7 µg/g -
80 Hg Mercury < 5.0 µg/g -

109 / 148
 4/17/2024

81 Tl Thallium 0.7 µg/g 0.1

82 Pb Lead 0.1032 % 0.0006
83 Bi Bismuth 12.8 µg/g 1.4
90 Th Thorium 13.1 µg/g 1.6
92 U Uranium 8.0 µg/g 1.1
Sum of concentration 26.50 %

110 / 148
 4/17/2024

Sample Name 796120 b Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:52 PM
Operator Converter Evaluation Date 4/16/2024 12:36 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0806 % 0.0065
14 SiO₂ Siliconoxide 0.4854 % 0.0057
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3263 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.7083 % 0.0078
20 CaO Calciumoxide 0.9077 % 0.0063
22 TiO₂ Titanoxid 0.2631 % 0.0031
23 V Vanadium 34.7 µg/g 1.9
24 Cr Chromium 8.5 µg/g 0.3
25 MnO Manganeseoxide 5156 µg/g 17
26 Fe₂O₃ Ironoxide 23.85 % 0.03
27 Co Cobalt 79.7 µg/g 3.0
28 Ni Nickel 17.0 µg/g 0.5
29 Cu Copper 0.2224 % 0.0007
30 Zn Zinc 0.9686 % 0.0015
31 Ga Gallium 23.3 µg/g 3.4
33 As Arsenic 131.5 µg/g 5.3
34 Se Selenium < 1.2 µg/g -
35 Br Bromine < 0.5 µg/g -
37 Rb Rubidium 82.1 µg/g 0.9
38 Sr Strontium 20.7 µg/g 0.5
39 Y Yttrium 19.3 µg/g 0.5
40 Zr Zirconium 51.5 µg/g 0.8
41 Nb Niobium 4.3 µg/g 0.5
42 Mo Molybdenum 8.0 µg/g 0.9
47 Ag Silver < 19 µg/g -
48 Cd Cadmium 201 µg/g 12
50 Sn Tin < 3.3 µg/g -
51 Sb Antimony 81.9 µg/g 3.0
55 Cs Cesium < 16 µg/g -
56 Ba Barium 47 µg/g 10
57 La Lanthanium 48 µg/g 16
58 Ce Cerium < 35 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 2.6 µg/g -
73 Ta Tantalum 5.5 µg/g 1.3
74 W Tungsten 91.9 µg/g 4.0
79 Au Gold < 1.7 µg/g -
80 Hg Mercury < 5.0 µg/g -

111 / 148
 4/17/2024

81 Tl Thallium 0.6 µg/g 0.1

82 Pb Lead 0.06532 % 0.00050
83 Bi Bismuth 2.7 µg/g 0.5
90 Th Thorium 14.4 µg/g 1.4
92 U Uranium 8.0 µg/g 1.2
Sum of concentration 28.49 %

112 / 148
 4/17/2024

Sample Name 796120 c Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 1:57 PM
Operator Converter Evaluation Date 4/16/2024 12:41 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0724 % 0.0056
14 SiO₂ Siliconoxide 0.1363 % 0.0035
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3116 % 0.0013
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.5980 % 0.0074
20 CaO Calciumoxide 1.433 % 0.008
22 TiO₂ Titanoxid 0.3313 % 0.0035
23 V Vanadium 41.9 µg/g 2.6
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 7572 µg/g 20
26 Fe₂O₃ Ironoxide 18.44 % 0.02
27 Co Cobalt 98.7 µg/g 3.4
28 Ni Nickel 17.1 µg/g 0.5
29 Cu Copper 0.2114 % 0.0006
30 Zn Zinc 0.9824 % 0.0015
31 Ga Gallium 20.4 µg/g 3.7
33 As Arsenic 92.9 µg/g 7.0
34 Se Selenium < 1.1 µg/g -
35 Br Bromine < 0.9 µg/g -
37 Rb Rubidium 103.6 µg/g 0.9
38 Sr Strontium 47.0 µg/g 0.6
39 Y Yttrium 28.1 µg/g 0.5
40 Zr Zirconium 107.7 µg/g 0.9
41 Nb Niobium 8.4 µg/g 0.5
42 Mo Molybdenum 14.6 µg/g 0.9
47 Ag Silver < 22 µg/g -
48 Cd Cadmium 100.3 µg/g 8.2
50 Sn Tin < 2.8 µg/g -
51 Sb Antimony 111.6 µg/g 2.7
55 Cs Cesium 68.2 µg/g 9.2
56 Ba Barium 228 µg/g 11
57 La Lanthanium 57 µg/g 15
58 Ce Cerium < 33 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 3.9 µg/g 1.3
73 Ta Tantalum < 2.0 µg/g -
74 W Tungsten 111.3 µg/g 3.9
79 Au Gold < 1.7 µg/g -
80 Hg Mercury 10.3 µg/g 2.1

113 / 148
 4/17/2024

81 Tl Thallium 0.7 µg/g 0.1

82 Pb Lead 0.1343 % 0.0007
83 Bi Bismuth 22.6 µg/g 1.8
90 Th Thorium 15.3 µg/g 1.8
92 U Uranium 11.1 µg/g 1.3
Sum of concentration 23.54 %

114 / 148
 4/17/2024

Sample Name 796120 A R Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:01 PM
Operator Converter Evaluation Date 4/16/2024 12:45 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0539 % 0.0035
14 SiO₂ Siliconoxide 1.250 % 0.007
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2816 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.0552 % 0.0045
20 CaO Calciumoxide 0.0499 % 0.0024
22 TiO₂ Titanoxid 0.00537 % 0.00034
23 V Vanadium < 5.1 µg/g -
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 56.8 µg/g 3.4
26 Fe₂O₃ Ironoxide 5.071 % 0.006
27 Co Cobalt < 6.1 µg/g -
28 Ni Nickel < 0.5 µg/g -
29 Cu Copper 0.03707 % 0.00018
30 Zn Zinc 0.01773 % 0.00010
31 Ga Gallium < 2.2 µg/g -
33 As Arsenic 52.4 µg/g 2.3
34 Se Selenium < 0.6 µg/g -
35 Br Bromine < 0.4 µg/g -
37 Rb Rubidium 0.7 µg/g 0.2
38 Sr Strontium 3.5 µg/g 0.2
39 Y Yttrium 2.2 µg/g 0.1
40 Zr Zirconium 5.5 µg/g 0.4
41 Nb Niobium < 0.7 µg/g -
42 Mo Molybdenum 3.8 µg/g 0.6
47 Ag Silver 201 µg/g 13
48 Cd Cadmium < 19 µg/g -
50 Sn Tin 5.6 µg/g 0.7
51 Sb Antimony 11.6 µg/g 1.5
55 Cs Cesium 16.1 µg/g 6.8
56 Ba Barium 253 µg/g 12
57 La Lanthanium 82 µg/g 16
58 Ce Cerium 68 µg/g 16
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.8 µg/g -
73 Ta Tantalum 2.5 µg/g 0.7
74 W Tungsten < 1.1 µg/g -
79 Au Gold 2.6 µg/g 0.8
80 Hg Mercury < 2.1 µg/g -

115 / 148
 4/17/2024

81 Tl Thallium < 0.4 µg/g -

82 Pb Lead 0.03002 % 0.00023
83 Bi Bismuth < 1.4 µg/g -
90 Th Thorium 6.0 µg/g 0.6
92 U Uranium 0.9 µg/g 0.4
Sum of concentration 6.93 %

116 / 148
 4/17/2024

Sample Name 796120 B R Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:05 PM
Operator Converter Evaluation Date 4/16/2024 12:49 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0646 % 0.0054
14 SiO₂ Siliconoxide 1.100 % 0.008
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2702 % 0.0013
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.0452 % 0.0039
20 CaO Calciumoxide 0.0981 % 0.0024
22 TiO₂ Titanoxid 0.01441 % 0.00095
23 V Vanadium < 5.1 µg/g -
24 Cr Chromium 10.7 µg/g 0.4
25 MnO Manganeseoxide < 2.6 µg/g -
26 Fe₂O₃ Ironoxide 19.02 % 0.02
27 Co Cobalt 11.8 µg/g 0.7
28 Ni Nickel < 0.9 µg/g -
29 Cu Copper 0.1897 % 0.0006
30 Zn Zinc 0.3126 % 0.0007
31 Ga Gallium < 4.0 µg/g -
33 As Arsenic 654.8 µg/g 6.4
34 Se Selenium < 0.9 µg/g -
35 Br Bromine < 1.3 µg/g -
37 Rb Rubidium 2.9 µg/g 0.4
38 Sr Strontium 6.1 µg/g 0.3
39 Y Yttrium 5.9 µg/g 0.2
40 Zr Zirconium 12.0 µg/g 0.5
41 Nb Niobium 1.8 µg/g 0.4
42 Mo Molybdenum 14.9 µg/g 0.9
47 Ag Silver < 21 µg/g -
48 Cd Cadmium < 26 µg/g -
50 Sn Tin 6.0 µg/g 0.4
51 Sb Antimony < 3.6 µg/g -
55 Cs Cesium < 14 µg/g -
56 Ba Barium 68 µg/g 11
57 La Lanthanium 46 µg/g 16
58 Ce Cerium 51 µg/g 16
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.5 µg/g -
73 Ta Tantalum 26.0 µg/g 4.7
74 W Tungsten < 1.9 µg/g -
79 Au Gold 7.0 µg/g 1.3
80 Hg Mercury 11.5 µg/g 1.8

117 / 148
 4/17/2024

81 Tl Thallium 1.0 µg/g 0.2

82 Pb Lead 0.08295 % 0.00051
83 Bi Bismuth 68.9 µg/g 2.4
90 Th Thorium 11.9 µg/g 1.7
92 U Uranium 4.6 µg/g 0.7
Sum of concentration 21.30 %

118 / 148
 4/17/2024

Sample Name 796121 A Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:13 PM
Operator Converter Evaluation Date 4/16/2024 12:57 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0993 % 0.0058
14 SiO₂ Siliconoxide 0.4725 % 0.0046
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2348 % 0.0010
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.570 % 0.013
20 CaO Calciumoxide 0.0637 % 0.0035
22 TiO₂ Titanoxid 0.2709 % 0.0033
23 V Vanadium 66.7 µg/g 4.0
24 Cr Chromium 42.0 µg/g 1.4
25 MnO Manganeseoxide 912.3 µg/g 7.7
26 Fe₂O₃ Ironoxide 11.69 % 0.01
27 Co Cobalt < 9.5 µg/g -
28 Ni Nickel 8.7 µg/g 0.3
29 Cu Copper 0.06197 % 0.00029
30 Zn Zinc 0.1266 % 0.0004
31 Ga Gallium 7.2 µg/g 3.9
33 As Arsenic 276.6 µg/g 9.6
34 Se Selenium 10.5 µg/g 0.6
35 Br Bromine < 0.6 µg/g -
37 Rb Rubidium 266.5 µg/g 1.3
38 Sr Strontium 73.6 µg/g 0.6
39 Y Yttrium 14.4 µg/g 0.2
40 Zr Zirconium 118.4 µg/g 0.8
41 Nb Niobium 4.8 µg/g 0.5
42 Mo Molybdenum 3.9 µg/g 0.7
47 Ag Silver < 25 µg/g -
48 Cd Cadmium < 24 µg/g -
50 Sn Tin < 2.5 µg/g -
51 Sb Antimony 31.2 µg/g 2.1
55 Cs Cesium < 15 µg/g -
56 Ba Barium 2479 µg/g 16
57 La Lanthanium 32 µg/g 15
58 Ce Cerium 66 µg/g 16
60 Nd Neodymium 20.1 µg/g 1.4
72 Hf Hafnium 2.1 µg/g 0.4
73 Ta Tantalum 20.5 µg/g 3.2
74 W Tungsten 22.5 µg/g 1.2
79 Au Gold < 1.5 µg/g -
80 Hg Mercury < 3.9 µg/g -

119 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.2788 % 0.0007
83 Bi Bismuth 45.5 µg/g 2.6
90 Th Thorium 13.9 µg/g 2.1
92 U Uranium 8.6 µg/g 1.5
Sum of concentration 16.32 %

120 / 148
 4/17/2024

Sample Name 796121 B Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:18 PM
Operator Converter Evaluation Date 4/16/2024 1:02 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1215 % 0.0058
14 SiO₂ Siliconoxide 0.5975 % 0.0050
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2772 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 3.112 % 0.015
20 CaO Calciumoxide 0.0602 % 0.0039
22 TiO₂ Titanoxid 0.5794 % 0.0041
23 V Vanadium 105.9 µg/g 6.2
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 1290 µg/g 8
26 Fe₂O₃ Ironoxide 7.142 % 0.009
27 Co Cobalt < 7.4 µg/g -
28 Ni Nickel 1.8 µg/g 0.1
29 Cu Copper 0.02963 % 0.00017
30 Zn Zinc 0.06128 % 0.00021
31 Ga Gallium 15.6 µg/g 1.9
33 As Arsenic 94.9 µg/g 2.6
34 Se Selenium 7.8 µg/g 0.5
35 Br Bromine < 0.6 µg/g -
37 Rb Rubidium 283.3 µg/g 1.2
38 Sr Strontium 18.8 µg/g 0.3
39 Y Yttrium 8.1 µg/g 0.5
40 Zr Zirconium 76.7 µg/g 0.6
41 Nb Niobium 11.8 µg/g 0.5
42 Mo Molybdenum 2.2 µg/g 0.6
47 Ag Silver < 27 µg/g -
48 Cd Cadmium < 21 µg/g -
50 Sn Tin 19.6 µg/g 1.0
51 Sb Antimony 68.6 µg/g 1.9
55 Cs Cesium < 13 µg/g -
56 Ba Barium 583 µg/g 12
57 La Lanthanium 35 µg/g 15
58 Ce Cerium 43 µg/g 14
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.0 µg/g -
73 Ta Tantalum 10.2 µg/g 1.7
74 W Tungsten 24.1 µg/g 1.0
79 Au Gold < 1.0 µg/g -
80 Hg Mercury < 2.2 µg/g -

121 / 148
 4/17/2024

81 Tl Thallium 1.3 µg/g 0.2

82 Pb Lead 0.02877 % 0.00024
83 Bi Bismuth 14.6 µg/g 1.1
90 Th Thorium 12.5 µg/g 0.8
92 U Uranium 5.1 µg/g 1.3
Sum of concentration 12.28 %

122 / 148
 4/17/2024

Sample Name 796121 C Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:24 PM
Operator Converter Evaluation Date 4/16/2024 1:08 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0917 % 0.0054
14 SiO₂ Siliconoxide 0.2688 % 0.0036
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2779 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 3.030 % 0.016
20 CaO Calciumoxide 0.0818 % 0.0043
22 TiO₂ Titanoxid 0.1946 % 0.0029
23 V Vanadium 71.6 µg/g 5.5
24 Cr Chromium 6.3 µg/g 0.6
25 MnO Manganeseoxide 3239 µg/g 13
26 Fe₂O₃ Ironoxide 3.718 % 0.005
27 Co Cobalt 9.4 µg/g 0.9
28 Ni Nickel 2.7 µg/g 0.2
29 Cu Copper 0.04743 % 0.00021
30 Zn Zinc 0.06545 % 0.00021
31 Ga Gallium 3.5 µg/g 2.1
33 As Arsenic 180.2 µg/g 4.2
34 Se Selenium < 0.7 µg/g -
35 Br Bromine 1.9 µg/g 0.4
37 Rb Rubidium 264.9 µg/g 1.1
38 Sr Strontium 133.5 µg/g 0.7
39 Y Yttrium 22.3 µg/g 0.4
40 Zr Zirconium 117.2 µg/g 0.7
41 Nb Niobium 10.1 µg/g 0.5
42 Mo Molybdenum 7.8 µg/g 0.6
47 Ag Silver < 29 µg/g -
48 Cd Cadmium < 20 µg/g -
50 Sn Tin < 2.0 µg/g -
51 Sb Antimony 47.4 µg/g 1.7
55 Cs Cesium 18.0 µg/g 7.1
56 Ba Barium 2196 µg/g 14
57 La Lanthanium 39 µg/g 13
58 Ce Cerium 38 µg/g 12
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.9 µg/g -
73 Ta Tantalum 10.3 µg/g 2.2
74 W Tungsten 3.4 µg/g 0.3
79 Au Gold 1.5 µg/g 0.9
80 Hg Mercury < 2.5 µg/g -

123 / 148
 4/17/2024

81 Tl Thallium 1.4 µg/g 0.1

82 Pb Lead 0.08703 % 0.00040
83 Bi Bismuth 59.7 µg/g 1.7
90 Th Thorium 21.2 µg/g 1.3
92 U Uranium 9.2 µg/g 1.4
Sum of concentration 8.51 %

124 / 148
 4/17/2024

Sample Name 796122 A Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:28 PM
Operator Converter Evaluation Date 4/16/2024 1:12 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0964 % 0.0051
14 SiO₂ Siliconoxide 0.5046 % 0.0047
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2875 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.761 % 0.013
20 CaO Calciumoxide 0.1745 % 0.0048
22 TiO₂ Titanoxid 0.1087 % 0.0020
23 V Vanadium 39.9 µg/g 4.2
24 Cr Chromium 25.3 µg/g 1.7
25 MnO Manganeseoxide 484.4 µg/g 5.9
26 Fe₂O₃ Ironoxide 3.610 % 0.005
27 Co Cobalt < 4.3 µg/g -
28 Ni Nickel < 0.9 µg/g -
29 Cu Copper 0.5231 % 0.0009
30 Zn Zinc 0.07319 % 0.00023
31 Ga Gallium 6.6 µg/g 3.9
33 As Arsenic 314.3 µg/g 9.7
34 Se Selenium < 0.9 µg/g -
35 Br Bromine < 0.6 µg/g -
37 Rb Rubidium 128.3 µg/g 0.8
38 Sr Strontium 60.2 µg/g 0.5
39 Y Yttrium ≈ 0.8 µg/g 0.0
40 Zr Zirconium 42.4 µg/g 0.5
41 Nb Niobium < 0.8 µg/g -
42 Mo Molybdenum 2.2 µg/g 0.6
47 Ag Silver < 28 µg/g -
48 Cd Cadmium < 21 µg/g -
50 Sn Tin 7.4 µg/g 0.7
51 Sb Antimony 50.2 µg/g 1.8
55 Cs Cesium < 13 µg/g -
56 Ba Barium 1029 µg/g 13
57 La Lanthanium 40 µg/g 15
58 Ce Cerium 99 µg/g 17
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 36.4 µg/g 6.1
73 Ta Tantalum 1.4 µg/g 0.3
74 W Tungsten < 1.4 µg/g -
79 Au Gold < 3.3 µg/g -
80 Hg Mercury < 3.6 µg/g -

125 / 148
 4/17/2024

81 Tl Thallium < 0.1 µg/g -

82 Pb Lead 0.3228 % 0.0007
83 Bi Bismuth 65.1 µg/g 2.7
90 Th Thorium 9.3 µg/g 2.1
92 U Uranium 5.5 µg/g 1.1
Sum of concentration 7.71 %

126 / 148
 4/17/2024

Sample Name 796122 B Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:33 PM
Operator Converter Evaluation Date 4/16/2024 1:17 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.1075 % 0.0052
14 SiO₂ Siliconoxide 0.6787 % 0.0053
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3362 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.997 % 0.016
20 CaO Calciumoxide 1.138 % 0.009
22 TiO₂ Titanoxid 0.2493 % 0.0031
23 V Vanadium 88.4 µg/g 5.8
24 Cr Chromium 9.5 µg/g 0.8
25 MnO Manganeseoxide 1649 µg/g 10
26 Fe₂O₃ Ironoxide 4.744 % 0.006
27 Co Cobalt < 6.1 µg/g -
28 Ni Nickel 3.8 µg/g 0.2
29 Cu Copper 0.1263 % 0.0004
30 Zn Zinc 0.07228 % 0.00023
31 Ga Gallium 19.1 µg/g 3.0
33 As Arsenic 271.3 µg/g 7.2
34 Se Selenium < 0.7 µg/g -
35 Br Bromine < 0.8 µg/g -
37 Rb Rubidium 210.3 µg/g 1.0
38 Sr Strontium 85.2 µg/g 0.6
39 Y Yttrium 6.6 µg/g 0.1
40 Zr Zirconium 79.5 µg/g 0.7
41 Nb Niobium 5.6 µg/g 0.5
42 Mo Molybdenum 2.1 µg/g 0.6
47 Ag Silver < 26 µg/g -
48 Cd Cadmium < 19 µg/g -
50 Sn Tin 2.6 µg/g 0.3
51 Sb Antimony 37.0 µg/g 1.8
55 Cs Cesium < 13 µg/g -
56 Ba Barium 1169 µg/g 13
57 La Lanthanium 25 µg/g 13
58 Ce Cerium 62 µg/g 14
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 1.8 µg/g 0.6
73 Ta Tantalum 0.10 µg/g 0.03
74 W Tungsten < 1.4 µg/g -
79 Au Gold 1.5 µg/g 1.4
80 Hg Mercury < 2.9 µg/g -

127 / 148
 4/17/2024

81 Tl Thallium < 0.2 µg/g -

82 Pb Lead 0.2018 % 0.0006
83 Bi Bismuth 82.3 µg/g 2.3
90 Th Thorium 1.5 µg/g 1.2
92 U Uranium 6.5 µg/g 1.3
Sum of concentration 11.03 %

128 / 148
 4/17/2024

Sample Name 796122 C Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:38 PM
Operator Converter Evaluation Date 4/16/2024 1:22 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0948 % 0.0054
14 SiO₂ Siliconoxide 0.2740 % 0.0037
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2738 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.682 % 0.016
20 CaO Calciumoxide 0.1179 % 0.0049
22 TiO₂ Titanoxid 0.2774 % 0.0031
23 V Vanadium 95.3 µg/g 6.3
24 Cr Chromium < 5.2 µg/g -
25 MnO Manganeseoxide 1415 µg/g 10
26 Fe₂O₃ Ironoxide 5.443 % 0.007
27 Co Cobalt 18.8 µg/g 1.4
28 Ni Nickel 3.5 µg/g 0.2
29 Cu Copper 0.1970 % 0.0005
30 Zn Zinc 0.08178 % 0.00026
31 Ga Gallium < 6.3 µg/g -
33 As Arsenic 413 µg/g 12
34 Se Selenium < 1.0 µg/g -
35 Br Bromine 1.5 µg/g 0.7
37 Rb Rubidium 255.1 µg/g 1.2
38 Sr Strontium 138.8 µg/g 0.8
39 Y Yttrium 10.5 µg/g 0.1
40 Zr Zirconium 108.9 µg/g 0.8
41 Nb Niobium 6.1 µg/g 0.5
42 Mo Molybdenum 13.7 µg/g 0.7
47 Ag Silver < 27 µg/g -
48 Cd Cadmium < 23 µg/g -
50 Sn Tin < 2.5 µg/g -
51 Sb Antimony 214.9 µg/g 2.4
55 Cs Cesium < 13 µg/g -
56 Ba Barium 1133 µg/g 12
57 La Lanthanium 55 µg/g 13
58 Ce Cerium 90 µg/g 14
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium 13.4 µg/g 2.9
73 Ta Tantalum 17.4 µg/g 4.0
74 W Tungsten < 1.6 µg/g -
79 Au Gold 19.5 µg/g 2.6
80 Hg Mercury 25.2 µg/g 2.5

129 / 148
 4/17/2024

81 Tl Thallium 0.49 µg/g 0.03

82 Pb Lead 0.4110 % 0.0009
83 Bi Bismuth ≈ 262.3 µg/g 3.9
90 Th Thorium 42.7 µg/g 3.2
92 U Uranium 14.2 µg/g 1.7
Sum of concentration 10.29 %

130 / 148
 4/17/2024

Sample Name 796123 A Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:43 PM
Operator Converter Evaluation Date 4/16/2024 1:27 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0528 % 0.0026
14 SiO₂ Siliconoxide 0.4751 % 0.0045
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2855 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.234 % 0.013
20 CaO Calciumoxide 9.806 % 0.025
22 TiO₂ Titanoxid 0.4194 % 0.0039
23 V Vanadium 123.7 µg/g 7.6
24 Cr Chromium 14.9 µg/g 1.2
25 MnO Manganeseoxide 2001 µg/g 11
26 Fe₂O₃ Ironoxide 4.356 % 0.006
27 Co Cobalt < 6.9 µg/g -
28 Ni Nickel 12.7 µg/g 0.5
29 Cu Copper 0.01891 % 0.00015
30 Zn Zinc 0.04680 % 0.00019
31 Ga Gallium 9.8 µg/g 1.9
33 As Arsenic 43.0 µg/g 2.0
34 Se Selenium < 0.8 µg/g -
35 Br Bromine < 0.4 µg/g -
37 Rb Rubidium 97.7 µg/g 0.8
38 Sr Strontium 1933 µg/g 3
39 Y Yttrium 27.7 µg/g 0.5
40 Zr Zirconium 85.7 µg/g 1.4
41 Nb Niobium 8.7 µg/g 0.5
42 Mo Molybdenum 4.9 µg/g 0.7
47 Ag Silver < 24 µg/g -
48 Cd Cadmium < 22 µg/g -
50 Sn Tin < 2.1 µg/g -
51 Sb Antimony < 2.8 µg/g -
55 Cs Cesium < 13 µg/g -
56 Ba Barium 661 µg/g 11
57 La Lanthanium 35 µg/g 13
58 Ce Cerium 48 µg/g 13
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.0 µg/g -
73 Ta Tantalum 15.1 µg/g 2.2
74 W Tungsten < 1.4 µg/g -
79 Au Gold < 1.1 µg/g -
80 Hg Mercury < 2.6 µg/g -

131 / 148
 4/17/2024

81 Tl Thallium 0.8 µg/g 0.2

82 Pb Lead 0.01389 % 0.00019
83 Bi Bismuth < 1.5 µg/g -
90 Th Thorium 10.5 µg/g 0.6
92 U Uranium < 2.3 µg/g -
Sum of concentration 18.22 %

132 / 148
 4/17/2024

Sample Name 796123 B Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:47 PM
Operator Converter Evaluation Date 4/16/2024 1:31 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0765 % 0.0035
14 SiO₂ Siliconoxide 0.3925 % 0.0040
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2565 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 2.021 % 0.012
20 CaO Calciumoxide 5.897 % 0.018
22 TiO₂ Titanoxid 0.3855 % 0.0036
23 V Vanadium 85.9 µg/g 6.0
24 Cr Chromium 13.3 µg/g 1.0
25 MnO Manganeseoxide 2990 µg/g 13
26 Fe₂O₃ Ironoxide 4.521 % 0.006
27 Co Cobalt 10.9 µg/g 1.0
28 Ni Nickel 12.0 µg/g 0.4
29 Cu Copper 0.03236 % 0.00018
30 Zn Zinc 0.06865 % 0.00022
31 Ga Gallium 14.9 µg/g 1.8
33 As Arsenic 131.0 µg/g 2.6
34 Se Selenium < 0.7 µg/g -
35 Br Bromine 2.1 µg/g 0.3
37 Rb Rubidium 130.8 µg/g 0.8
38 Sr Strontium 81.5 µg/g 0.6
39 Y Yttrium 19.7 µg/g 0.5
40 Zr Zirconium 122.3 µg/g 0.7
41 Nb Niobium 7.2 µg/g 0.5
42 Mo Molybdenum 2.3 µg/g 0.6
47 Ag Silver < 27 µg/g -
48 Cd Cadmium < 20 µg/g -
50 Sn Tin < 2.2 µg/g -
51 Sb Antimony 20.3 µg/g 1.7
55 Cs Cesium 13.4 µg/g 7.5
56 Ba Barium 383 µg/g 12
57 La Lanthanium 51 µg/g 15
58 Ce Cerium 68 µg/g 15
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 0.9 µg/g -
73 Ta Tantalum 3.5 µg/g 0.9
74 W Tungsten < 1.2 µg/g -
79 Au Gold < 1.0 µg/g -
80 Hg Mercury < 2.5 µg/g -

133 / 148
 4/17/2024

81 Tl Thallium 0.9 µg/g 0.2

82 Pb Lead 0.02655 % 0.00024
83 Bi Bismuth 18.0 µg/g 1.1
90 Th Thorium 10.4 µg/g 0.8
92 U Uranium 3.5 µg/g 1.0
Sum of concentration 14.10 %

134 / 148
 4/17/2024

Sample Name 796123 C Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:52 PM
Operator Converter Evaluation Date 4/16/2024 1:36 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0599 % 0.0033
14 SiO₂ Siliconoxide 0.1692 % 0.0028
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2618 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 1.915 % 0.012
20 CaO Calciumoxide 4.819 % 0.016
22 TiO₂ Titanoxid 0.3030 % 0.0034
23 V Vanadium 94.1 µg/g 6.1
24 Cr Chromium 14.2 µg/g 1.1
25 MnO Manganeseoxide 3914 µg/g 14
26 Fe₂O₃ Ironoxide 3.958 % 0.005
27 Co Cobalt 10.6 µg/g 1.0
28 Ni Nickel 9.7 µg/g 0.4
29 Cu Copper 0.05214 % 0.00022
30 Zn Zinc 0.09250 % 0.00025
31 Ga Gallium 6.1 µg/g 1.9
33 As Arsenic 111.8 µg/g 3.4
34 Se Selenium < 0.8 µg/g -
35 Br Bromine 4.5 µg/g 0.4
37 Rb Rubidium 168.5 µg/g 0.9
38 Sr Strontium 160.7 µg/g 0.8
39 Y Yttrium 20.7 µg/g 0.4
40 Zr Zirconium 101.9 µg/g 0.7
41 Nb Niobium 9.4 µg/g 0.5
42 Mo Molybdenum 4.2 µg/g 0.6
47 Ag Silver < 28 µg/g -
48 Cd Cadmium < 20 µg/g -
50 Sn Tin < 2.1 µg/g -
51 Sb Antimony 54.0 µg/g 1.8
55 Cs Cesium 20.0 µg/g 7.2
56 Ba Barium 1514 µg/g 13
57 La Lanthanium 43 µg/g 13
58 Ce Cerium 67 µg/g 14
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.0 µg/g -
73 Ta Tantalum 5.2 µg/g 1.4
74 W Tungsten < 1.3 µg/g -
79 Au Gold < 1.0 µg/g -
80 Hg Mercury < 2.5 µg/g -

135 / 148
 4/17/2024

81 Tl Thallium 0.7 µg/g 0.1

82 Pb Lead 0.05747 % 0.00033
83 Bi Bismuth 19.3 µg/g 1.3
90 Th Thorium 12.2 µg/g 0.9
92 U Uranium 5.3 µg/g 1.1
Sum of concentration 12.33 %

136 / 148
 4/17/2024

Sample Name 796124 A Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 2:57 PM
Operator Converter Evaluation Date 4/16/2024 1:41 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0794 % 0.0059
14 SiO₂ Siliconoxide 0.5670 % 0.0060
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.3066 % 0.0014
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.2794 % 0.0060
20 CaO Calciumoxide 1.129 % 0.007
22 TiO₂ Titanoxid 0.3110 % 0.0034
23 V Vanadium 42.9 µg/g 2.4
24 Cr Chromium 3.3 µg/g 0.1
25 MnO Manganeseoxide 654.3 µg/g 7.8
26 Fe₂O₃ Ironoxide 19.58 % 0.02
27 Co Cobalt 28.9 µg/g 1.5
28 Ni Nickel 1.6 µg/g 0.1
29 Cu Copper 0.01889 % 0.00020
30 Zn Zinc 0.02521 % 0.00018
31 Ga Gallium < 4.1 µg/g -
33 As Arsenic 524.4 µg/g 5.5
34 Se Selenium 46.5 µg/g 1.2
35 Br Bromine 4.5 µg/g 0.9
37 Rb Rubidium 23.0 µg/g 1.1
38 Sr Strontium 15.5 µg/g 0.4
39 Y Yttrium 14.3 µg/g 0.4
40 Zr Zirconium 141.7 µg/g 1.0
41 Nb Niobium 7.7 µg/g 0.5
42 Mo Molybdenum 81.1 µg/g 1.2
47 Ag Silver < 21 µg/g -
48 Cd Cadmium < 32 µg/g -
50 Sn Tin 157.2 µg/g 2.3
51 Sb Antimony 54.2 µg/g 2.6
55 Cs Cesium 81.4 µg/g 9.0
56 Ba Barium 27.9 µg/g 9.6
57 La Lanthanium < 25 µg/g -
58 Ce Cerium < 31 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.4 µg/g -
73 Ta Tantalum 13.2 µg/g 1.4
74 W Tungsten 351.3 µg/g 3.4
79 Au Gold 25.0 µg/g 2.2
80 Hg Mercury < 7.6 µg/g -

137 / 148
 4/17/2024

81 Tl Thallium 3.5 µg/g 0.4

82 Pb Lead 0.04515 % 0.00052
83 Bi Bismuth ≈ 2704 µg/g 11
90 Th Thorium < 13 µg/g -
92 U Uranium 12.3 µg/g 1.2
Sum of concentration 22.84 %

138 / 148
 4/17/2024

Sample Name 796124 B Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 3:01 PM
Operator Converter Evaluation Date 4/16/2024 1:45 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0168 % 0.0016
14 SiO₂ Siliconoxide 0.1814 % 0.0034
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2167 % 0.0011
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.2307 % 0.0046
20 CaO Calciumoxide 3.777 % 0.011
22 TiO₂ Titanoxid 0.1441 % 0.0022
23 V Vanadium < 4.5 µg/g -
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 10530 µg/g 30
26 Fe₂O₃ Ironoxide 37.78 % 0.05
27 Co Cobalt < 18 µg/g -
28 Ni Nickel < 1.6 µg/g -
29 Cu Copper 0.09547 % 0.00056
30 Zn Zinc 0.1146 % 0.0005
31 Ga Gallium < 4.0 µg/g -
33 As Arsenic 41.4 µg/g 3.8
34 Se Selenium < 1.6 µg/g -
35 Br Bromine < 1.0 µg/g -
37 Rb Rubidium 14.0 µg/g 0.7
38 Sr Strontium 53.7 µg/g 0.8
39 Y Yttrium 14.9 µg/g 0.5
40 Zr Zirconium 30.6 µg/g 0.8
41 Nb Niobium 2.7 µg/g 0.3
42 Mo Molybdenum 22.3 µg/g 1.3
47 Ag Silver < 19 µg/g -
48 Cd Cadmium 207 µg/g 15
50 Sn Tin < 3.8 µg/g -
51 Sb Antimony < 5.3 µg/g -
55 Cs Cesium 19 µg/g 11
56 Ba Barium 58 µg/g 11
57 La Lanthanium < 34 µg/g -
58 Ce Cerium < 42 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 3.0 µg/g -
73 Ta Tantalum < 4.0 µg/g -
74 W Tungsten 233.5 µg/g 4.5
79 Au Gold 3.8 µg/g 1.7
80 Hg Mercury < 8.1 µg/g -

139 / 148
 4/17/2024

81 Tl Thallium 2.1 µg/g 0.4

82 Pb Lead 0.02545 % 0.00039
83 Bi Bismuth 178.6 µg/g 3.7
90 Th Thorium < 2.2 µg/g -
92 U Uranium 6.4 µg/g 1.0
Sum of concentration 43.72 %

140 / 148
 4/17/2024

Sample Name 796124 C Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 3:06 PM
Operator Converter Evaluation Date 4/16/2024 1:50 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0238 % 0.0019
14 SiO₂ Siliconoxide 0.1366 % 0.0032
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2840 % 0.0013
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.3393 % 0.0060
20 CaO Calciumoxide 5.153 % 0.014
22 TiO₂ Titanoxid 0.1827 % 0.0027
23 V Vanadium 25.9 µg/g 1.3
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 5051 µg/g 18
26 Fe₂O₃ Ironoxide 29.65 % 0.03
27 Co Cobalt < 15 µg/g -
28 Ni Nickel 7.4 µg/g 0.3
29 Cu Copper 0.09078 % 0.00048
30 Zn Zinc 0.1171 % 0.0005
31 Ga Gallium 19.8 µg/g 2.8
33 As Arsenic 67.3 µg/g 3.7
34 Se Selenium 2.3 µg/g 0.3
35 Br Bromine 1.6 µg/g 0.5
37 Rb Rubidium 23.8 µg/g 0.6
38 Sr Strontium 60.9 µg/g 0.8
39 Y Yttrium 11.6 µg/g 0.4
40 Zr Zirconium 36.8 µg/g 0.8
41 Nb Niobium 3.7 µg/g 0.4
42 Mo Molybdenum 18.0 µg/g 1.1
47 Ag Silver < 19 µg/g -
48 Cd Cadmium 159 µg/g 12
50 Sn Tin < 3.4 µg/g -
51 Sb Antimony < 4.8 µg/g -
55 Cs Cesium < 16 µg/g -
56 Ba Barium 78 µg/g 11
57 La Lanthanium 36 µg/g 16
58 Ce Cerium < 36 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.9 µg/g -
73 Ta Tantalum < 2.1 µg/g -
74 W Tungsten 125.2 µg/g 3.1
79 Au Gold 5.4 µg/g 1.5
80 Hg Mercury < 6.0 µg/g -

141 / 148
 4/17/2024

81 Tl Thallium 0.7 µg/g 0.2

82 Pb Lead 0.02980 % 0.00039
83 Bi Bismuth 149.6 µg/g 3.0
90 Th Thorium 2.2 µg/g 1.1
92 U Uranium 5.5 µg/g 0.9
Sum of concentration 36.60 %

142 / 148
 4/17/2024

Sample Name 796125 A Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 3:12 PM
Operator Converter Evaluation Date 4/16/2024 1:56 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0380 % 0.0038
14 SiO₂ Siliconoxide 0.1031 % 0.0031
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2601 % 0.0012
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.1790 % 0.0046
20 CaO Calciumoxide 2.308 % 0.009
22 TiO₂ Titanoxid 0.1546 % 0.0024
23 V Vanadium 31.3 µg/g 1.3
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 4242 µg/g 16
26 Fe₂O₃ Ironoxide 34.64 % 0.04
27 Co Cobalt 25.7 µg/g 1.1
28 Ni Nickel < 1.3 µg/g -
29 Cu Copper 0.1142 % 0.0006
30 Zn Zinc 0.1422 % 0.0005
31 Ga Gallium < 3.8 µg/g -
33 As Arsenic 59.4 µg/g 4.3
34 Se Selenium < 1.4 µg/g -
35 Br Bromine 2.3 µg/g 0.5
37 Rb Rubidium 10.1 µg/g 0.6
38 Sr Strontium 37.1 µg/g 0.7
39 Y Yttrium 10.3 µg/g 0.3
40 Zr Zirconium 63.6 µg/g 0.9
41 Nb Niobium 4.3 µg/g 0.4
42 Mo Molybdenum 20.3 µg/g 1.1
47 Ag Silver < 19 µg/g -
48 Cd Cadmium 92.1 µg/g 8.9
50 Sn Tin 60.1 µg/g 1.4
51 Sb Antimony < 4.7 µg/g -
55 Cs Cesium 21.4 µg/g 9.5
56 Ba Barium 56 µg/g 12
57 La Lanthanium < 34 µg/g -
58 Ce Cerium < 44 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 2.4 µg/g -
73 Ta Tantalum < 2.4 µg/g -
74 W Tungsten 165.9 µg/g 3.7
79 Au Gold 3.6 µg/g 1.5
80 Hg Mercury < 6.5 µg/g -

143 / 148
 4/17/2024

81 Tl Thallium 1.3 µg/g 0.3

82 Pb Lead 0.03763 % 0.00043
83 Bi Bismuth 92.0 µg/g 2.8
90 Th Thorium 3.9 µg/g 1.2
92 U Uranium 6.3 µg/g 0.9
Sum of concentration 38.48 %

144 / 148
 4/17/2024

Sample Name 796125 B Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 3:16 PM
Operator Converter Evaluation Date 4/16/2024 2:00 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0497 % 0.0040
14 SiO₂ Siliconoxide 0.0923 % 0.0029
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2871 % 0.0013
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.1861 % 0.0050
20 CaO Calciumoxide 2.957 % 0.011
22 TiO₂ Titanoxid 0.1360 % 0.0025
23 V Vanadium 27.8 µg/g 1.3
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 12740 µg/g 30
26 Fe₂O₃ Ironoxide 28.92 % 0.03
27 Co Cobalt 180.2 µg/g 4.8
28 Ni Nickel 3.4 µg/g 0.2
29 Cu Copper 0.07199 % 0.00042
30 Zn Zinc 0.1807 % 0.0006
31 Ga Gallium 12.9 µg/g 2.9
33 As Arsenic 46.4 µg/g 2.8
34 Se Selenium < 1.3 µg/g -
35 Br Bromine < 0.9 µg/g -
37 Rb Rubidium 7.8 µg/g 0.5
38 Sr Strontium 57.8 µg/g 0.8
39 Y Yttrium 7.8 µg/g 0.4
40 Zr Zirconium 24.5 µg/g 0.7
41 Nb Niobium 4.4 µg/g 0.4
42 Mo Molybdenum 18.7 µg/g 1.1
47 Ag Silver < 20 µg/g -
48 Cd Cadmium < 36 µg/g -
50 Sn Tin < 3.4 µg/g -
51 Sb Antimony < 4.7 µg/g -
55 Cs Cesium 26 µg/g 10
56 Ba Barium 96 µg/g 12
57 La Lanthanium 70 µg/g 18
58 Ce Cerium < 40 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 1.8 µg/g -
73 Ta Tantalum < 2.1 µg/g -
74 W Tungsten 135.2 µg/g 3.4
79 Au Gold 4.6 µg/g 1.3
80 Hg Mercury < 6.1 µg/g -

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81 Tl Thallium 2.1 µg/g 0.4

82 Pb Lead 0.01428 % 0.00027
83 Bi Bismuth 109.3 µg/g 2.9
90 Th Thorium 14.1 µg/g 2.0
92 U Uranium 5.5 µg/g 0.8
Sum of concentration 34.25 %

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Sample Name 796125 C Dilution Material -

Method Geo Ag Sample Mass 5.0000
Sample Folder Week 16 2024 Dilution Mass -
Sample Type Powder Dilution Factor -
Sample Status AAA Measurement Date 3/16/2024 3:20 PM
Operator Converter Evaluation Date 4/16/2024 2:05 PM

Results
The error is the statistical error with 1 sigma confidence interval

Element Concentration Abs. Error

11 Na₂O Sodiumoxide < 0.14 % -
12 MgO Magnesiumoxide < 0.017 % -
13 Al₂O₃ Aluminumoxide 0.0299 % 0.0034
14 SiO₂ Siliconoxide 0.0929 % 0.0031
15 P₂O₅ Phosphorusoxide < 0.00069 % -
16 S Sulfur 0.2751 % 0.0013
17 Cl Chlorine < 0.0030 % -
19 K₂O Potassiumoxide 0.1686 % 0.0048
20 CaO Calciumoxide 2.435 % 0.009
22 TiO₂ Titanoxid 0.1333 % 0.0024
23 V Vanadium 37.5 µg/g 1.5
24 Cr Chromium < 3.0 µg/g -
25 MnO Manganeseoxide 4777 µg/g 17
26 Fe₂O₃ Ironoxide 34.72 % 0.04
27 Co Cobalt 54.7 µg/g 2.2
28 Ni Nickel < 1.3 µg/g -
29 Cu Copper 0.1268 % 0.0006
30 Zn Zinc 0.1549 % 0.0006
31 Ga Gallium < 4.2 µg/g -
33 As Arsenic 60.8 µg/g 4.7
34 Se Selenium < 1.5 µg/g -
35 Br Bromine < 0.5 µg/g -
37 Rb Rubidium 17.4 µg/g 0.7
38 Sr Strontium 87.7 µg/g 1.0
39 Y Yttrium 16.8 µg/g 0.4
40 Zr Zirconium 41.0 µg/g 0.8
41 Nb Niobium 5.2 µg/g 0.4
42 Mo Molybdenum 23.9 µg/g 1.2
47 Ag Silver 19.3 µg/g 2.6
48 Cd Cadmium 122 µg/g 11
50 Sn Tin 33.2 µg/g 1.0
51 Sb Antimony 13.2 µg/g 2.9
55 Cs Cesium < 17 µg/g -
56 Ba Barium 152 µg/g 11
57 La Lanthanium 68 µg/g 17
58 Ce Cerium < 38 µg/g -
60 Nd Neodymium < 20 µg/g -
72 Hf Hafnium < 2.4 µg/g -
73 Ta Tantalum < 2.1 µg/g -
74 W Tungsten 205.7 µg/g 4.0
79 Au Gold 4.5 µg/g 1.6
80 Hg Mercury < 7.1 µg/g -

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81 Tl Thallium 2.3 µg/g 0.3

82 Pb Lead 0.04430 % 0.00048
83 Bi Bismuth 149.8 µg/g 3.3
90 Th Thorium 7.9 µg/g 2.0
92 U Uranium 8.1 µg/g 1.0
Sum of concentration 38.77 %

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