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Polysorbate 80

This document contains results from an analysis of ethylene glycol standards at different concentrations. It reports the peak areas, corrected areas, sample weights, measured concentrations in parts per million, theoretical concentrations, and percent recoveries for unspiked samples and samples spiked at 80%, 100%, and 120% of the theoretical concentration. The results show good accuracy with average percent recoveries ranging from 118% to 92%.

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32 views3 pages

Polysorbate 80

This document contains results from an analysis of ethylene glycol standards at different concentrations. It reports the peak areas, corrected areas, sample weights, measured concentrations in parts per million, theoretical concentrations, and percent recoveries for unspiked samples and samples spiked at 80%, 100%, and 120% of the theoretical concentration. The results show good accuracy with average percent recoveries ranging from 118% to 92%.

Uploaded by

truckgal80
Copyright
© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as XLS, PDF, TXT or read online on Scribd
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Peak Areas

STD Set 1
Vial

Ethylene Glycol

1911472.68684

1982054.79179

Solution Weight

Ethylene Glycol

Set 1
Set 2
Set 3

311.27000
311.27000
311.27000

Accuracy
Area
271066.6423
291075.9634
287201.6148
283114.7402

Corrected Area

Unspike 1
Unspike 2
Unspike 3
Average
80% Spiked 1
80% Spiked 2
80% Spiked 3

2149756.033
2135240.09566
2143875.052

1866641.29262
1852125.356
1860760.31167

100% Spiked 1
100% Spiked 2
100% Spiked 3

2609196.24139
2648553.08675
2616413.08123

2326081.50124
2365438.34660
2333298.34108

120% Spiked 1
120% Spiked 2
120% Spiked 3

2989586.296
2965306.175
3025818.761

2706471.556
2682191.435
2742704.021

1971600.26958

2006773.89596

1968982.03524

Sample Wt(mg)

ppm Recovery

Theoretical ppm

5009.380
5009.380
5009.380

590.97233
586.37664
589.11044

498.03200
498.03200
498.03200
Mean
Std Dev
%RSD

5011.500
5011.500
5011.500

734.73965
747.17131
737.01924

622.54000
622.54000
622.54000
Mean
Std Dev
%RSD

5007.170
5007.170
5007.170

855.63279
847.95679
867.08744

933.81000
933.81000
933.81000
Mean
Std Dev
%RSD

Average

1957220.57922

1966350.70977

% Recovery

119
118
118
118
0.5
0.4
118
120
118
119
1.1
0.9
92
91
93
92
1.0
1.1

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