Scribd
Upload
34 views1 page

Ethylene Oxide and Dioxane

This document provides instructions for preparing solutions used in a method to analyze ethylene oxide and dioxane. It lists the necessary reagents and their storage conditions. It then details how to prepare stock solutions of acetaldehyde, ethylene oxide, and dioxane, as well as several standard and sample solutions involving varying amounts of the reagents and solvents. Health and safety precautions for ethylene oxide are also mentioned.

Uploaded by

truckgal80
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOC, PDF, TXT or read online on Scribd
34 views1 page

Ethylene Oxide and Dioxane

This document provides instructions for preparing solutions used in a method to analyze ethylene oxide and dioxane. It lists the necessary reagents and their storage conditions. It then details how to prepare stock solutions of acetaldehyde, ethylene oxide, and dioxane, as well as several standard and sample solutions involving varying amounts of the reagents and solvents. Health and safety precautions for ethylene oxide are also mentioned.

Uploaded by

truckgal80
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOC, PDF, TXT or read online on Scribd
You are on page 1/ 1

Ethylene oxide and Dioxane Last updated 06NOV2013

USP Ethylene oxide and Dioxane Geneal !hapte 22"


Method I
Reagents:
#$etaldehyde %&ept in 'ee(e) on$e opened) only *ood 'o one yea+
Ethylene oxide %&ept in a headspa$e ,ial in 'ee(e) $onsult senio analyst i' -oe is needed+
1)./Dioxane %&ept in 'la--a0les $a0inet #/D+
1n house D1 2
2
O
Polyethylene Gly$ol 200 %&ept on P ea*ent shel') should ha,e ,ei'i$ation in'o on 0ottle+
Di-ethyla$eta-ide %D3#+ %&ept in 'la--a0les $a0inet #/D+
Solution Prep
#$etaldehyde Solution4 10 5*6-L solution
Ethylene oxide Sto$& Solution4 WE DO NOT USE TE PREP IN TE !ENER"#
$"PTER%%%% 7e -odi'y the pep to use the ethylene oxide ea*ent that is pe/pu$hased 'o-
Si*-a #ldi$h %to $ut do8n on analyst eo and EO is a health ha(ad+9 7e -a&e a :0 pp-
solution) then dilute do8n to 10 5*6-L solution9 %Please $onsult an old 8ite up to ensue the
pope pep o' solution9+ 3a&e a note in you note0oo& $on$enin* the di''een$e in peps o' the
Sto$& Solution9 Please sho8 to ;e$&y and ha,e he si*n o'' on it ON TE D"& O' PREP%
See an old 8ite up to *et 8odin* 'o the note9
Dioxane Solution4 :00 5*6-L solution
Standad Solution #4 091 -L o' Ethylene oxide Solution) 091 -L o' Dioxane Solution and 091
-L o' #$etaldehyde in a headspa$e ,ial9 Sealed9 %<his is you syste- suit solution9+
Standad Solution ;4 7ei*h 190* o' sa-ple into headspa$e ,ial) then add 091 -L o' Ethylene
oxide solution and 091 -L o' Dioxane Solution) and 190 -L o' D3#9 Sealed9
Sa-ple Solution4 7ei*h 190* o' sa-ple into a headspa$e ,ial) and added 190 -L o' D3# and
092 -L o' 8ate9 Sealed9

You might also like