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Sample 1 PH VM D1 VD D2

The document contains data from three titration experiments measuring pH, volume of titrant added, and the first and second derivatives of the titration curves. For each experiment, the pH, volume of titrant added, and first and second derivatives are recorded at regular intervals. The experiments measure the titration of an unknown substance with hydrochloric acid.

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31 views

Sample 1 PH VM D1 VD D2

The document contains data from three titration experiments measuring pH, volume of titrant added, and the first and second derivatives of the titration curves. For each experiment, the pH, volume of titrant added, and first and second derivatives are recorded at regular intervals. The experiments measure the titration of an unknown substance with hydrochloric acid.

Uploaded by

AmandaLe
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as XLSX, PDF, TXT or read online on Scribd
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Sample 1

Volume
0
1
2
3
4
5
6
6.2
6.4
6.6
6.8
7
7.2
7.4
7.6
7.8
8
8.2
8.4
8.6
8.8
9
9.2
9.4
9.6
9.8
10
11
12
13
14
15
16
16.2
16.4
16.6
16.8
17
17.2
17.4
17.6

pH

Vm
11.08
10.65
10.37
10.17
9.97
9.78
9.56
9.51
9.46
9.41
9.35
9.28
9.21
9.11
9.02
8.92
8.79
8.61
8.29
7.92
7.65
7.43
7.31
7.25
7.14
7.09
6.97
6.67
6.46
6.26
6.06
5.82
5.53
5.46
5.39
5.27
5.13
4.86
5.27
3.28
2.98

D1
0.5
1.5
2.5
3.5
4.5
5.5
6.1
6.3
6.5
6.7
6.9
7.1
7.3
7.5
7.7
7.9
8.1
8.3
8.5
8.7
8.9
9.1
9.3
9.5
9.7
9.9
10.5
11.5
12.5
13.5
14.5
15.5
16.1
16.3
16.5
16.7
16.9
17.1
17.3
17.5
17.7

Vd
-0.43
-0.28
-0.2
-0.2
-0.19
-0.22
-0.25
-0.25
-0.25
-0.3
-0.35
-0.35
-0.5
-0.45
-0.5
-0.65
-0.9
-1.6
-1.85
-1.35
-1.1
-0.6
-0.3
-0.55
-0.25
-0.6
-0.3
-0.21
-0.2
-0.2
-0.24
-0.29
-0.35
-0.35
-0.6
-0.7
-1.35
2.05
-9.95
-1.5
-0.95

D2
1
0.15
2
0.08
3
0
4
0.01
5
-0.03
5.8
-0.05
6.2 4.4409E-014
6.4 -4.996E-014
6.6
-0.25
6.8
-0.25
7 4.4409E-014
7.2
-0.75
7.4
0.25
7.6
-0.25
7.8
-0.75
8
-1.25
8.2
-3.5
8.4
-1.25
8.6
2.5
8.8
1.25
9
2.5
9.2
1.5
9.4
-1.25
9.6
1.5
9.8
-1.75
10.2
0.5
11
0.09
12
0.01
13
0
14
-0.04
15
-0.05
15.8
-0.1
16.2
0
16.4
-1.25
16.6
-0.5
16.8
-3.25
17
17
17.2
-60
17.4
42.25
17.6
2.75
17.8
2.25

17.8
18
18.2
18.4
18.6
18.8
19
19.2
19.4
19.6
19.8
20
21
22
23
24
25
26

Sample 2
Volume (mL)pH
0
1
2
3
4
5
6
7
7.2
7.4
7.6
7.8
8
8.2
8.4
8.6
8.8
9
9.2
9.4
9.6

2.79
2.69
2.56
2.49
2.41
2.35
2.3
2.26
2.22
2.18
2.15
2.12
2
1.92
1.85
1.8
1.75
1.7

17.9
-0.5
18.1
-0.65
18.3
-0.35
18.5
-0.4
18.7
-0.3
18.9
-0.25
19.1
-0.2
19.3
-0.2
19.5
-0.2
19.7
-0.15
19.9
-0.15
20.5
-0.12
21.5
-0.08
22.5
-0.07
23.5
-0.05
24.5
-0.05
25.5
-0.05
13 0.06538462

Vm
11.13
10.74
10.48
10.26
10.07
9.89
9.7
9.47
9.43
9.37
9.3
9.24
9.16
9.08
8.98
8.86
8.73
8.53
8.29
7.94
7.65

D1
0.5
1.5
2.5
3.5
4.5
5.5
6.5
7.1
7.3
7.5
7.7
7.9
8.1
8.3
8.5
8.7
8.9
9.1
9.3
9.5
9.7

18
18.2
18.4
18.6
18.8
19
19.2
19.4
19.6
19.8
20.2
21
22
23
24
25
19.25
6.5

Vd
-0.39
-0.26
-0.22
-0.19
-0.18
-0.19
-0.23
-0.2
-0.3
-0.35
-0.3
-0.4
-0.4
-0.5
-0.6
-0.65
-1
-1.2
-1.75
-1.45
-0.85

-0.75
1.5
-0.25
0.5
0.25
0.25
1.1102E-014
6.6613E-015
0.25
1.1102E-014
0.05
0.04
0.01
0.02
0
2.2204E-016
-0.00923077
0.00502959

D2
1
0.13
2
0.04
3
0.03
4
0.01
5
-0.01
6
-0.04
6.8
0.05
7.2
-0.5
7.4
-0.25
7.6
0.25
7.8
-0.5
8 -8.882E-015
8.2
-0.5
8.4
-0.5
8.6
-0.25
8.8
-1.75
9
-1
9.2
-2.75
9.4
1.5
9.6
3
9.8
1.25

9.8
10
10.2
10.4
10.6
10.8
11
12
13
14
15
16
17
18
18.2
18.4
18.6
18.8
19
19.2
19.4
19.6
19.8
20
20.2
20.4
20.6
20.8
21
21.2
21.4
21.6
21.8
22
23
24
25
26
27
28

Sample 3

7.48
7.36
7.27
7.18
7.09
7.03
6.98
6.71
6.5
6.45
6.14
5.93
5.68
5.29
5.17
4.95
4.6
3.65
3.09
2.86
2.69
2.62
2.53
2.43
2.4
2.35
2.3
2.27
2.22
2.2
2.16
2.13
2.1
2.08
1.99
1.91
1.85
1.79
1.74
1.72

9.9
-0.6
10.1
-0.45
10.3
-0.45
10.5
-0.45
10.7
-0.3
10.9
-0.25
11.5
-0.27
12.5
-0.21
13.5
-0.05
14.5
-0.31
15.5
-0.21
16.5
-0.25
17.5
-0.39
18.1
-0.6
18.3
-1.1
18.5
-1.75
18.7
-4.75
18.9
-2.8
19.1
-1.15
19.3
-0.85
19.5
-0.35
19.7
-0.45
19.9
-0.5
20.1
-0.15
20.3
-0.25
20.5
-0.25
20.7
-0.15
20.9
-0.25
21.1
-0.1
21.3
-0.2
21.5
-0.15
21.7
-0.15
21.9
-0.1
22.5
-0.09
23.5
-0.08
24.5
-0.06
25.5
-0.06
26.5
-0.05
27.5
-0.02
14 0.06142857

10
10.2
10.4
10.6
10.8
11.2
12
13
14
15
16
17
17.8
18.2
18.4
18.6
18.8
19
19.2
19.4
19.6
19.8
20
20.2
20.4
20.6
20.8
21
21.2
21.4
21.6
21.8
22.2
23
24
25
26
27
20.75
7

0.75
4.2188E-014
-1.998E-014
0.75
0.25
-0.03333333
0.06
0.16
-0.26
0.1
-0.04
-0.14
-0.35
-2.5
-3.25
-15
9.75
8.25
1.5
2.5
-0.5
-0.25
1.75
-0.5
1.1102E-014
0.5
-0.5
0.75
-0.5
0.25
0
0.25
0.01666667
0.01
0.02
0
0.01
0.03
-0.00603175
0.00438776

Volume (mL)pH
0
1
2
3
4
5
5.2
5.4
5.6
5.8
6
6.2
6.4
6.6
6.8
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21

Vm
10.95
10.55
10.26
10
9.71
9.37
9.3
9.18
9.03
8.87
8.64
8.2
7.86
7.55
7.35
7.24
6.82
6.51
6.27
5.99
5.78
5.57
3.39
2.44
2.2
2.05
1.95
1.88
1.81
1.76

D1
0.5
-0.4
1.5
-0.29
2.5
-0.26
3.5
-0.29
4.5
-0.34
5.1
-0.35
5.3
-0.6
5.5
-0.75
5.7
-0.8
5.9
-1.15
6.1
-2.2
6.3
-1.7
6.5
-1.55
6.7
-1
6.9
-0.55
7.5
-0.42
8.5
-0.31
9.5
-0.24
10.5
-0.28
11.5
-0.21
12.5
-0.21
13.5
-2.18
14.5
-0.95
15.5
-0.24
16.5
-0.15
17.5
-0.1
18.5
-0.07
19.5
-0.07
20.5
-0.05
10.5 0.08380952

Vd

D2
1
2
3
4
4.8
5.2
5.4
5.6
5.8
6
6.2
6.4
6.6
6.8
7.2
8
9
10
11
12
13
14
15
16
17
18
19
20
15.5
5.25

0.11
0.03
-0.03
-0.05
-0.01666667
-1.25
-0.75
-0.25
-1.75
-5.25
2.5
0.75
2.75
2.25
0.21666667
0.11
0.07
-0.04
0.07
0
-1.97
1.23
0.71
0.09
0.05
0.03
4.4409E-016
0.02
-0.01338095
0.00798186

Trial 1
12
10
8
pH

Column B

4
2
0
0

10

15

20

25

30

Volume HCl Added (mL)

1st Derivative
4
2
0
-2
Vm

10

15

20

25

Column D

-4
-6
-8
-10
-12
D1

2nd Derivative
60
40

30

2nd Derivative
60
40
20
0
Vd

10

15

20

25

30

Column F

-20
-40
-60
-80
D2

Trial 2
12
10
8
pH

Column B

4
2
0
0

10

15

20

25

Volume HCl Added (mL)

1st Derivative
0
-0.5

10

15

20

25

30

30

1st Derivative
0
-0.5

10

15

20

25

30

-1
-1.5
-2
Column D

Vm -2.5
-3
-3.5
-4
-4.5
-5
D1

2nd Derivative
15
10
5
0
0

Vd

10

15

-5
-10
-15
-20
D2

20

25

30

Column F

Trial 3
12
10
8
6

pH

Column B

4
2
0
0

10

15

20

25

VOlume HCl Added (mL)

1st Derivative
0
0

10

15

20

25

-0.5
-1

Column D

Vm
-1.5
-2
-2.5
D1

2nd Derivative
4
3

2nd Derivative
4
3
2
1
0
Vd

-1

10

15

-2
-3
-4
-5
-6
D2

20

25

Column F

Column B

30

Column D

Column F

Column B

30

Column D

Column F

Column B

25

Column D

Column F

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