Metering Standards
Metering Standards
12/5/2004
18/3/2012
Date
Final document
Final document
1
2
Revision number
Distribution
Open
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Revision history
Revision 1: First edition, 2004
Revision 2: Second edition, 2012
Drafts issued for comments from the NORSOK measurement standards editing committee.
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Petroleum liquids and liquefied petroleum gases - Measurement Standard reference conditions
Abstract of standards
ISO 5024:1999 Petroleum liquids and liquefied petroleum gases - Measurement - Standard reference
conditions defines different standard reference conditions, important for calculation of standard
volume, heating value
ISO 13443:1996 Natural gas - Standard reference conditions specifies the standard reference conditions
of temperature, pressure and humidity to be used for measurements and calculations carried out
on natural gases and similar fluids.
ISO 80000-1:2009 Quantities and Units Part 1 : General gives general information and definitions
concerning quantities, systems of quantities, units, quantity and unit symbols, and coherent unit
systems, especially the International System of Quantities, ISQ, and the International System of
Units, SI.
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API-MPMS Chapter 15: 2007 Guidelines for Use of the International System of Units (SI) in the
Petroleum and Allied Industries specifies the API preferred units for quantities involved in
petroleum industry measurements and indicates factors for conversion of quantities expressed in
customary units to the API-preferred metric units. The quantities that comprise the tables are
grouped into convenient categories related to their use. They were chosen to meet the needs of the
many and varied aspects of the petroleum industry but also should be useful in similar process
industries.
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Abstract of standards
ISO 9000:2005 Quality management systems - Fundamentals and vocabulary describes fundamentals
of quality management systems, which form the subject of the ISO 9000 family, and defines
related terms.
It is applicable to the following:
a) organizations seeking advantage through the implementation of a quality management
system;
b) organizations seeking confidence from their suppliers that their product requirements will be
satisfied;
c) users of the products;
d) those concerned with a mutual understanding of the terminology used in quality management
(e.g. suppliers, customers, regulators);
e) those internal or external to the organization who assess the quality management system or
audit it for conformity with the requirements of ISO 9001 (e.g. auditors, regulators,
certification/registration bodies);
f) those internal or external to the organization who give advice or training on the quality
management system appropriate to that organization;
g) developers of related standards.
ISO 9001: 2008 Quality management systems Requirements specifies requirements for a quality
management system where an organization needs to demonstrate its ability to consistently
provide product that meets customer and applicable statutory and regulatory requirements, and
aims to enhance customer satisfaction through the effective application of the system, including
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Petroleum, petrochemical and natural gas industries - Sectorspecific quality management systems - Requirements for product
and service supply organizations
ISO 9004:2009 Managing for the sustained success of an organization - A quality management
approach provides guidance to organizations to support the achievement of sustained success by
a quality management approach. It is applicable to any organization, regardless of size, type and
activity.
ISO 9004:2009 is not intended for certification, regulatory or contractual use.
ISO 10005:2005 Quality management systems - Guidelines for quality plans provides guidelines for the
development, review, acceptance, application and revision of quality plans. It is applicable
whether or not the organization has a management system in conformity with ISO 9001. It is
applicable to quality plans for a process, product, project or contract, any product category
(hardware, software, processed materials and services) and any industry. It is focused primarily
on product realization and is not a guide to organizational quality management system planning.
ISO 10005:2005 is a guidance document and is not intended to be used for certification or
registration purposes.
ISO 19011:2002 Guidelines for quality and/or environmental management systems auditing provides
guidance on the principles of auditing, managing audit programmes, conducting quality
management system audits and environmental management system audits, as well as guidance on
the competence of quality and environmental management system auditors. It is applicable to all
organizations needing to conduct internal or external audits of quality and/or environmental
management systems or to manage an audit programme. The application of ISO 19011 to other
types of audits is possible in principle provided that special consideration is paid to identifying
the competence needed by the audit team members in such cases.
ISO/TS 29001:2010 Petroleum, petrochemical and natural gas industries -- Sector-specific quality
management systems -- Requirements for product and service supply organizations defines the
quality management system for product and service supply organizations for the petroleum,
petrochemical and natural gas industries. Boxed text is original ISO 9001:2008 text unaltered and
in its entirety. The petroleum, petrochemical, and natural gas industry sector-specific
supplemental requirements are outside the boxes.
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Abstract of standards
ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
specifies the general requirements for the competence to carry out tests and/or calibrations,
including sampling. It covers testing and calibration performed using standard methods, nonstandard methods, and laboratory-developed methods. It is applicable to all organizations
performing tests and/or calibrations. These include, for example, first-, second- and third-party
laboratories, and laboratories where testing and/or calibration forms part of inspection and
product certification. ISO/IEC 17025:2005 is applicable to all laboratories regardless of the
number of personnel or the extent of the scope of testing and/or calibration activities. When a
laboratory does not undertake one or more of the activities covered by ISO/IEC 17025:2005, such
as sampling and the design/development of new methods, the requirements of those clauses do
not apply. ISO/IEC 17025:2005 is for use by laboratories in developing their management system
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ISO/IEC 17021:2011 Conformity assessment - Requirements for bodies providing audit and certification
of management systems contains principles and requirements for the competence, consistency
and impartiality of the audit and certification of management systems of all types (e.g. quality
management systems or environmental management systems) and for bodies providing these
activities. Certification bodies operating to ISO/IEC 17021:2011 need not offer all types of
management system certification. Certification of management systems is a third-party
conformity assessment activity. Bodies performing this activity are therefore third-party
conformity assessment bodies.
ISO/IEC Guide 28:2004 Conformity assessment - Guidance on a third-party certification system for
products gives general guidelines for a specific product certification system. It is applicable to a
third-party product certification system for determining the conformity of a product with
specified requirements through initial testing of samples of the product, assessment and
surveillance of the involved quality system, and surveillance by testing of product samples taken
from the factory or the open market, or both. ISO/IEC Guide 28:2004 addresses conditions for
use of a mark of conformity and conditions for granting a certificate of conformity.
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NFOGM Standards
NFOGM 2001
NFOGM 2003
Abstract of standards
ISO/IEC Guide 98-1:2009 Uncertainty of measurement -- Part 1: Introduction to the expression of
uncertainty in measurement provides a brief introduction to the Guide to the expression of
uncertainty in measurement (GUM) in order to indicate the relevance of that fundamental guide
and promote its use. It also outlines documents related to the GUM that are intended to extend the
application of that guide to broader categories and fields of practical problems. ISO/IEC Guide
98-1:2009 addresses measurement science at a level that is suitable for those readers who have
received training at least to the second year of a science- or engineering-based degree course
containing some teaching of probability theory and statistics. It also considers various concepts
used in measurement science. In particular, it covers the need to characterize the quality of a
measurement through appropriate statements of measurement uncertainty. This introductory
document also outlines the recent evolution of thinking regarding measurement uncertainty.
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ISO 6974-2: 2001 Natural gas -- Determination of composition with defined uncertainty by gas
chromatography -- Part 2: Measuring-system characteristics and statistics for processing of data
describes the data processing for the tailored analysis of natural gas. It includes the determination
of the measuring system characteristics and the statistical approach to data handling and error
calculation with the aim of defining the uncertainty in the mole fractions of the component
measured. This part of ISO 6974 is only applicable in conjunction with part 1 of ISO 6974.
ISO 6974-3: 2000 Natural gas -- Determination of composition with defined uncertainty by gas
chromatography -- Part 3: Determination of hydrogen, helium, oxygen, nitrogen, carbon dioxide
and hydrocarbons up to C8 using two packed columns describes a gas chromatographic method
for the quantitative determination of the content of helium, hydrogen, oxygen, nitrogen, carbon
dioxide and C1 to C8 hydrocarbons in natural gas samples using two packed columns. This
method is applicable to determinations made in on-line processes or in the laboratory. It is
applicable to the analysis of gases containing constituents within the mole fraction ranges given
in Table 1 and which do not contain any hydrocarbon condensate. These ranges do not represent
the limits of detection, but the limits within which the stated precision of the method applies.
Although one or more components in a sample may not be detected present, the method can still
be applicable. This part of ISO 6974 is only applicable in conjunction with parts 1 and 2 of ISO
6974.
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ISO 6974-4: 2000 Natural gas -- Determination of composition with defined uncertainty by gas
chromatography -- Part 4: Determination of nitrogen, carbon dioxide and C1 to C5 and C6+
hydrocarbons for a laboratory and on-line measuring system using two columns describes a gas
chromatographic method for the quantitative determination of natural gas constituents using a
two-column system. This method is applicable to determinations made in on-line processes or in
the laboratory. It is applicable to the analysis of gases containing constituents within the mole
fraction ranges given in Table 1. These ranges do not represent the limits of detection, but the
limits within which the stated precision of the method applies. Although one or more components
in a sample may not be detected present, the method can still be applicable. This part of ISO 6974
is only applicable if used in conjunction with parts 1 and 2 of ISO 6974.
Table 1 Application ranges
Component
Nitrogen
Carbon dioxide
Methane
Ethane
Propane
iso-Butane (2-methylpropane)
n-Butane
neo -Pentane (2,2dimethylpropane)
iso -Pentane (2-methylbutane)
n-Pentane
Hexanes _ sum of all C6 and
higher hydrocarbons
ISO 6974-5: 2000 Natural gas -- Determination of composition with defined uncertainty by gas
chromatography -- Part 5: Determination of nitrogen, carbon dioxide and C1 to C5 and C6+
hydrocarbons for a laboratory and on-line process application using three columns describes a
gas chromatographic method for the quantitative determination of natural gas constituents using a
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ISO 6974-6: 2002 Natural gas -- Determination of composition with defined uncertainty by gas
chromatography -- Part 6: Determination of hydrogen, helium, oxygen, nitrogen, carbon dioxide
and C1 to C8 hydrocarbons using three capillary columns describes a gas chromatographic
method for the quantitative determination of the content of helium, hydrogen, oxygen, nitrogen,
carbon dioxide and C1 to C8 hydrocarbons in natural gas samples using three capillary columns.
This method is applicable to the determination of these gases within the mole fraction ranges
varying from 0,000 1 % to 40 %, depending on the component analyzed, and is commonly used
for laboratory applications. However, it is only applicable to methane within the mole fraction
range of 40 % to 100 %. These ranges do not represent the limits of detection, but the limits
within which the stated precision of the method applies. Although one or more components in a
sample may not be present at detectable levels, the method can still be applicable. ISO 69746:2002 is only applicable if used in conjunction with ISO 6974-1:2000 and ISO 6974-2:2001.
This method can also be applicable to the analysis of natural gas substitutes. Additional
information on the applicability of this method to the determination of natural gas substitutes is
also given where relevant.
ISO/TR 7066-1:1997 Assessment of uncertainty in calibration and use of flow measurement devices -Part 1: Linear calibration relationships describes the procedures to be used in deriving the
calibration curve for methods of measuring the flowrate in closed conduits or open channels, and
for assessing the uncertainty associated with such calibrations. Replaces the first edition
published as an International Standard (ISO 7066-1).
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
All sections
OIML Recommendation
R117-1: 2007
API Standards
API MPMS 5.1: 2008
Abstract of standards
ISO 1998-6:2000 Petroleum industry -- Terminology -- Part 6: Measurement introduces a list of
equivalent English and French terms, in use in the petroleum industry to indicate the
measurement of crude oils and petroleum products, together with the corresponding definitions in
the two languages. ISO 1998 is intended to cover the purposes of this part of petroleum industry
dealing with crude oils and petroleum products that means all related operations arising from the
production field to the final user. It is not intended to cover either petroleum equipment, or any
operation in the field. However some pieces of equipment or some operations of exploration and
production are defined. The corresponding terms were introduced only when they appear in a
definition of a product or process and when their definition was found necessary for
understanding or for avoiding any ambiguity.
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 5.2.2.3: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Flowmeter design
Annex A: (Normative) Requirements for automated condition based maintenance
Annex F: (Normative) Statistical evaluation of repeatability
API Standards
API MPMS 5.3: 2009
API MPMS 5.4: 2005
API MPMS 5.5: 2010
Abstract of standards
ISO 2715:1981 Liquid hydrocarbons -- Volumetric measurement by turbine meter systems gives the
characteristics of such equipment and rules for systematically applying appropriate consideration
to the nature of the liquids to be measured, to the installation of a metering system, and to the
selection, performance, operation and maintenance of the same.
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 5.2.2.3: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Flowmeter design
API Standards
API MPMS 5.2: 2010
API MPMS 5.4: 2005
API MPMS 5.5: 2010
Abstract of standards
ISO 2714:1980 Liquid hydrocarbons -- Volumetric measurement by displacement meter systems other
than dispensing pumps gives the characteristics of such equipment and rules for systematically
applying appropriate consideration to the nature of the liquids to be measured, to the installation
of a metering system, and to the selection, performance, operation and maintenance of the same.
ISO 6551: 1982 Petroleum liquids and gases - Fidelity and security of dynamic measurement -- Cabled
transmission of electric and/or electronic pulsed data establishes guidelines for ensuring the
quantities stated, a main objective being to ensure the integrity of the primary indication. In order
to achieve different levels of security, criteria and recommendations for the design, installation,
use and maintenance of the relevant equipment are laid down. Regulatory requirements, including
those for safety, are not specifically covered in detail but certain general cautionary notes on
safety are included for guidance.
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 5.2.2.3: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Flowmeter design
Annex F: (Normative) Statistical evaluation of repeatability
API Standards
API MPMS 5.6: 2008
API MPMS 5.4: 2005
API MPMS 5.5: 2010
Abstract of standards
ISO 10790:1999 Measurement of fluid flow in closed conduits - Guidance to the selection, installation
and use of Coriolis meters (mass flow, density and volume flow measurements) gives guidelines
for the selection, installation, calibration, performance and operation of Coriolis meters for the
determination of mass flow, density, volume flow and other related parameters of fluids. It also
gives appropriate considerations regarding the fluids to be measured.
ISO 6551: 1982 Petroleum liquids and gases - Fidelity and security of dynamic measurement -- Cabled
transmission of electric and/or electronic pulsed data establishes guidelines for ensuring the
quantities stated, a main objective being to ensure the integrity of the primary indication. In order
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 5.1.8: Sales and allocation measurement Functional requirements Layout requirements
Section 5.2.2.3: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Flowmeter design
Section 5.2.2.8: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Thermal insulation
Section 5.2.4.8: Sales and allocation measurement Technical requirements Instrument part
Ultrasonic flowmeter
Section 5.2.5.6: Sales and allocation measurement Technical requirements Computer part Check
Annex A: (Normative) Requirements for automated condition based maintenance
Annex B: (Normative) Testing and commissioning
Annex F: (Normative) Statistical evaluation of repeatability
API Standards
API MPMS 5.8: 2005
API MPMS 5.4: 2005
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Abstract of standards
ISO 6551: 1982 Petroleum liquids and gases - Fidelity and security of dynamic measurement - Cabled
transmission of electric and/or electronic pulsed data establishes guidelines for ensuring the
quantities stated, a main objective being to ensure the integrity of the primary indication. In order
to achieve different levels of security, criteria and recommendations for the design, installation,
use and maintenance of the relevant equipment are laid down. Regulatory requirements, including
those for safety, are not specifically covered in detail but certain general cautionary notes on
safety are included for guidance.
API MPMS 5.8:2005 Measurement of Liquid Hydrocarbons by Ultrasonic Flowmeters Using Transit
Time Technology describes methods for obtaining custody transfer level measurements with
ultrasonic flow meters (UFMs) used to measure liquid hydrocarbons. This document includes
application criteria for UFM and includes considerations regarding the liquids being measured.
This document also address the installation, operation, proving and maintenance of UFMs in
liquid hydrocarbon service.
API MPMS 5.4:2005 Accessory Equipment for Liquid Meters describes the characteristics of accessory
equipment used with displacement and turbine meters in liquid hydrocarbon service. Includes
guidance on the use of electronic flow computers.
API MPMS 5.5: 2010 Fidelity and Security of Flow Measurement Pulsed-Data Transmission Systems
serves as a guide for the selection, operation, and maintenance of various types of pulsed-data,
cabled transmission systems for fluid metering systems to provide the desired level of fidelity and
security of transmitted flow pulse data. This publication does not endorse or advocate the
preferential use of any specific type of equipment or systems, nor is it intended to restrict future
development of such equipment.
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 5.1.3: Sales and allocation measurement Functional requirements Equipment/Schematic
Section 5.1.6.1: Sales and allocation measurement Functional requirements Operational requirements
- General
Section 5.1.7.2: Sales and allocation measurement Functional requirements Maintenance requirements
Calibration
Section 5.1.7.4: Sales and allocation measurement Functional requirements Maintenance requirements
Isolation and sectioning
Section 5.2.2.3: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Flowmeter design
Section 5.2.2.4: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Block valves
Section 5.2.3.1: Sales and allocation measurement Technical requirements Mechanical part, prover
Unit - General
Section 5.2.3.2: Sales and allocation measurement Technical requirements Mechanical part, prover
Unit Conventional pipe prover
Section 5.2.3.3: Sales and allocation measurement Technical requirements Mechanical part, prover
Unit Compact prover
Section 5.2.4.1: Sales and allocation measurement Technical requirements Instrument part Location
of sensors
Section 5.2.5.2: Sales and allocation measurement Technical requirements Computer part Computer
design
Annex A: (Normative) Requirements for automated condition based maintenance
Annex B: (Normative) Testing and commissioning
Annex F: (Normative) Statistical evaluation of repeatability
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API Standards
API MPMS 4.1: 2009
API MPMS 4.2: 2003
API MPMS 4.4: 2010
API MPMS 4.5: 2005
API MPMS 4.6: 2008
API MPMS 4.7: 2009
API MPMS 4.8: 2007
Abstract of standards
ISO 7278-1:1987 Liquid hydrocarbons - Dynamic measurement - Proving systems for volumetric meters
- Part 1: General principles. The purpose of proving a meter is to determine its relative error or
its meter factor as a function of flow rate and other parameters such as temperature, pressure and
viscosity. The following types of proving systems are in use: tank prover systems; pipe provers,
bidirectional and unidirectional; master meters. They can be used either connected (fixed or
mobile) to the metering station or in a central proving station.
ISO 7278-2:1988 Liquid hydrocarbons - Dynamic measurement - Proving systems for volumetric meters
- Part 2: Pipe provers provides guidance for the design, installation and calibration of these
provers. Calculation techniques for use when calibrating and operating provers are detailed in
ISO 4267-2. Most of the material is general in that it applies to provers for use with different
liquids and types of meters and for proving them in different services. Does not apply to the
newer "small volume" or "compact" provers.
ISO 7278-3:1998 Liquid hydrocarbons - Dynamic measurement - Proving systems for volumetric meters
- Part 3: Pulse interpolation techniques. The use of pipe provers to prove meters with pulsed
outputs requires that a minimum number of pulses be collected during the proving period. The
number of pulses which a meter can produce during a proving run is often limited to significantly
less than 10 000 pulses. Therefore, in many applications some means of increasing the meters
resolution has to be found. One way of overcoming this problem is to process the signal from the
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ISO 8222:2002 Petroleum measurement systems - Calibration - Temperature corrections for use when
calibrating volumetric proving tanks specifies multiplication factors for the correction of the
volume of water transferred from a primary measure to a tank for changes arising from
temperature differences during the determination of the capacity of the tank at reference
temperature.
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ISO 18132-1:2011
Abstract of standards
ISO 18132-1:2011 establishes general principles for the accuracy, installation, calibration and
verification of automatic tank gauges (ATGs) used for custody transfer measurement
of liquefied natural gas (LNG) on board an LNG carrier or floating storage.
The LNG described in the standard is either fully refrigerated (i.e. at the cryogenic
condition), or partially refrigerated, and therefore the fluid is at or near atmospheric
pressure.
ISO 18132-1:2011 also specifies the technical requirements for data collection,
transmission and reception. Specific technical requirements for various automatic tank
gauges and accuracy limitations are given in the annexes.
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 4.1: General requirements General
Section 4.3: General requirements Sampling and water fraction metering equipment
Section 5.1.6.2: Sales and allocation measurement Functional requirements Operational requirements
- Tanker loading measurement system
Section 5.1.9: Sales and allocation measurement Functional requirements Interface requirements
Section 5.2.2.8: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Thermal insulation
Section 7.1.1: Oil sampler systems Functional requirements General
Section 7.1.3: Oil sampler systems Functional requirements Equipment/Schematic
Section 7.1.4.1: Oil sampler systems Functional requirements Performance Capacity
Section 7.1.9: Oil sampler systems Functional requirements Layout requirements
Annex A: (Normative) Requirements for automated condition based maintenance
Annex E: (Informative) Guidelines to implementation of ISO 3171
API Standards
API MPMS 8.1: 2006
API MPMS 8.2: 2010
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API MPMS 8.3:2010 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and
Petroleum Products covers the handling, mixing, and conditioning procedures required to ensure
that a representative sample of the liquid petroleum or petroleum product is delivered from the
primary sample container/receiver into the analytical test apparatus or into intermediate
containers. For sampling procedures, refer to Chapters 8.1 and 8.2. Refer to Chapter 8.4 for the
mixing and handling of light fuels for volatility measurement
API MPMS 8.4:2009 Standard Practice for Sampling and Handling of Fuels for Volatility
Measurement covers procedures and equipment for obtaining, mixing, and handling
representative samples of volatile fuels for the purpose of testing for compliance with the
standards set forth for volatility related measurements applicable to light fuels. The applicable dry
vapor pressure equivalent range of this practice is 13 to 105 kPa (2 to 16 psia). This practice is
applicable to the sampling, mixing, and handling of reformulated fuels including those containing
oxygenates.
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 4.1: General requirements General
Section 5.1.2: Sales and allocation measurement - Functional requirements - Products/services
Section 5.1.8: Sales and allocation measurement - Functional requirements Layout requirements
Section 5.2.2.5: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Meter run flow control
Section 5.2.2.5: Sales and allocation measurement Technical requirements - Mechanical part, exclusive
prover unit Thermal insulation
Section 5.2.3.1: Sales and allocation measurement Technical requirements Mechanical part, prover
Unit General
Section 5.2.4.1: Sales and allocation measurement Technical requirements Instrument part Location
of sensor
Section 5.2.4.4: Sales and allocation measurement Technical requirements Instrument part Stability
for smart transmitters
Section 5.2.4.5: Sales and allocation measurement Technical requirements Instrument part
Temperature loop
Section 5.2.4.6: Sales and allocation measurement Technical requirements Instrument part
Thermowell
Section 5.2.4.11: Sales and allocation measurement Technical requirements Instrument part Local
pressure indication
Section 5.2.4.14: Sales and allocation measurement Technical requirements Instrument part
Enclosures
Section 5.2.5.2: Sales and allocation measurement Technical requirements Computer part Computer
design
Section 7.1.3: Oil sampler Functional requirements Equipment/Schematic
Annex A: (Normative) Requirements for automated condition based maintenance
Annex B: (Normative) Testing and commissioning
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API Standards
API MPMS 7: 2007
Temperature Determination
Abstract of standards
CEI 60751:2008 Industrial platinum resistance thermometers and platinum temperature sensors
specifies the requirements and temperature/resistance relationship for industrial platinum
resistance temperature sensors later referred to as platinum resistors or "resistors" and industrial
platinum resistance thermometers later referred to as "thermometers" whose electrical resistance
is a defined function of temperature.
API MPMS 7:2007 Temperature determination describes methods and practices that may be used to
obtain accurate measurements of temperature of petroleum and petroleum products in pipelines,
storage tanks, gathering tanks, ships, barges, tank cars, pipe provers, tank provers and test
measures under both static and dynamic conditions using electronic temperature measuring
devices or mercury-in glass thermometers. Describes the methods, equipment, and procedures for
determining the temperature of petroleum and petroleum products under both static and dynamic
conditions. This chapter discusses temperature measurement requirements in general for custody
transfer, inventory control, and marine measurements. The actual method and equipment selected
for temperature determination are left to the agreement of the parties involved.
Other relevant Standards
ISO 8310: 1991
ISO 8310:1991 Refrigerated light hydrocarbon fluids - Measurement of temperature in tanks containing
liquefied gases - Resistance thermometers and thermocouples specifies the essential
requirements and verification procedures for sensors, thermocouples and associated equipment to
be used for ship and shore tanks containing hydrocarbon fluids. Annexes A and B are for
information only.
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Crude petroleum and liquid or solid petroleum products Determination of density or relative density - Capillarystoppered pyknometer and graduated bicapillary pyknometer
methods
Oscillation-type density meters -- Part 1: Laboratory instruments
Oscillation-type density meters -- Part 2: Process instruments for
homogeneous liquids
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Abstract of standards
ISO 3838:2004 Crude petroleum and liquid or solid petroleum products -- Determination of density or
relative density -- Capillary-stoppered pyknometer and graduated bicapillary pyknometer
methods specifies methods for the determination of the density or relative density of crude
petroleum and of petroleum products handled as liquids. The capillary-stoppered pyknometer
method is also for use with solids and this method may also be used for coal tar products,
including road tars, creosote and tar pitches, or for mixtures of these with petroleum products.
This method is not suitable for the determination of the density or relative density of highly
volatile liquids having Reid vapour pressures greater than 50 kPa according to ISO 3007 or
having an initial boiling point below 40 degrees Celsius. The graduated bicapillary pyknometer
method is recommended for the accurate determination of the density or relative density of all
except the more viscous products, and is particularly useful. when only small amounts of samples
are available. The method is restricted to liquids having Reid vapour pressures of 130 kPa or less
according to ISO 3007 and having kinematic viscosities less than 50 mm2/s (50 centistokes (cSt))
at the test temperature. Special precautions are specified for the determination of the density or
relative density of highly volatile liquids.
API MPMS 9.1:2005 Standard Test Method for Density, Relative Density (Specific Gravity), or API
Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method describes
the methods and practices relating to the determination of the density, relative density, or API
gravity of crude petroleum and liquid petroleum products using the hydrometer method
(laboratory determination).
Other relevant Standards
ISO 3675: 1998
ISO 3993: 1984
ISO 10790: 1999
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 4.1: General requirements General
Section 4.3: General requirements Sampling and water fraction metering equipment
Section 6: Water in oil measurement
Section 6.1.1: Water in oil measurement Functional requirements General
Section 6.1.4.1: Water in oil measurement Functional requirements Performance - Capacity
Section 6.1.4.2: Water in oil measurement Functional requirements Performance Uncertainty
Section 6.1.5: Water in oil measurement Functional requirements Process/Ambient conditions
Section 6.1.6: Water in oil measurement Functional requirements Operational requirements
Section 6.1.7.3: Water in oil measurement Functional requirements Maintenance requirements
Layout requirements
Section 6.2.1: Water in oil measurement Technical requirements Mechanical part
Section 6.2.2: Water in oil measurement Technical requirements Instrument part
Section 6.2.3: Water in oil measurement Technical requirements Computer part
Annex D: (Informative) Water in oil calculations
API Standards
API MPMS 10.3: 2008
API MPMS 10.4: 2010
API MPMS TR 2570: 2010
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ISO 10307-1: 2009 Petroleum products - Total sediment in residual fuel oils - Part 1: Determination by
hot filtration specifies a method for the determination of total sediment in residual fuel oils
having a maximum viscosity of 55 mm2/s at 100 C, and for blends of distillate fuels containing
residual components.
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 4.1: General requirements General
Annex B: (Normative) Testing and commissioning
ASTM D341-03 Standard Test Method for Viscosity-Temperature Charts for Liquid Petroleum
Products. The kinematic viscosity-temperature charts covered by this standard are a convenient
means to ascertain the kinematic viscosity of a petroleum oil or liquid hydrocarbon at any
temperature within a limited range, provided that the kinematic viscosities at two temperatures
are known.
ISO 2909:2002 Petroleum products -- Calculation of viscosity index from kinematic viscosity describes
two procedures for calculating the viscosity index (VI) of petroleum products and related
materials, such as lubricating oils, from their kinematic viscosities at 40 C and 100 C.
Procedure A is applicable to petroleum products of viscosity index up to and including 100.
Procedure B is applicable to petroleum products of viscosity index 100 or greater. ISO 2909:2002
does not apply to petroleum products with kinematic viscosities less than 2,0 mm2/s at 100 C. It
applies to petroleum products with kinematic viscosities between 2 mm2/s and 70 mm2/s at 100
C. Equations are provided for calculating the viscosity index of petroleum products having
kinematic viscosities above 70 mm2/s at 100 C.
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NORSOK References
NORSOK Standard I-105: 2007 Fiscal measurement systems for hydrocarbon liquid
Section 4.2: General requirements - Uncertainty
Section 4.4: General requirements - Calibration
Section 5.1.3: Sales and allocation measurement - Functional requirements - Equipment/schematic
Section 5.1.7.2: Sales and allocation measurement - Functional requirements - Maintenance requirements
Calibration
Section 5.2.4.7: Sales and allocation measurement - Technical requirements - Instrument part - Density
Section 5.2.5.2: Sales and allocation measurement - Technical requirements - Computer part - Computer
design
Section 5.2.5.5: Sales and allocation measurement - Technical requirements - Computer part Calculations
Section 5.2.5.9: Sales and allocation measurement - Technical requirements - Computer part - Reporting
of data for continuous measurement system
Section 5.2.5.13: Sales and allocation measurement - Technical requirements - Computer part Availability
Section 5.2.5.14: Sales and allocation measurement - Technical requirements - Computer part - Network
protection/security
Section 5.2.5.15: Sales and allocation measurement - Technical requirements - Computer part - Spare
capacity
Section 5.2.5.17: Sales and allocation measurement - Technical requirements - Computer part Downloading of constants and ranges
Section 6.1.5: Water in oil measurement - Functional requirements - Process/ambient conditions
Section 6.1.8: Water in oil measurement - Functional requirements - Interface requirements
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API Standards
API MPMS 11.1: 2004
API MPMS 11.2.2: 2007
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Using
Positive
Abstract of standards
ISO 91-1:1992 Petroleum measurement tables - Part 1: Tables based on reference temperatures of 15
degrees C and 60 degrees F refers to petroleum measurement tables published by the American
Petroleum Institute (API, USA), the American Society for Testing and Materials (ASTM, USA)
and the Institute of Petroleum (IP, UK) and subsidiary documents, correcting the printing errors
in these publications, based on reference temperatures of 15 C and 60 F. The standard reference
temperature for petroleum measurement adopted in IS0 5024 is 15 C, and should be used for
international trade. However, it is recognized that its use is not yet universally accepted and
references to tables based on 60 F have therefore been included in IS0 91-1:1992 and tables
based on 20 C are covered in IS0 91-2.
ISO 91-2:1991 Petroleum measurement tables - Part 2: Tables based on a reference temperature of 20
degrees C refers to computer implementation procedures for the correction of densities and
volumes to the reference temperature of 20C. This first edition cancels and replaces ISO/TR
91:1970/Add.1:1975. Annex A is for information only.
ISO 4267-2:1988 Petroleum and liquid petroleum products - Calculation of oil quantities - Part 2:
Dynamic measurement defines the various terms employed in the calculation of metered
petroleum quantities. Also specifies the equations which allow the values of correction factors to
be computed. Also gives rules for the sequence, rounding and significant figures to be employed
in a calculation. Provides tables which may be used to look up specific correction factors should it
not be desired to calculate them by manual as well as computer methods. The field of application
is the volumetric measurement of liquid hydrocarbons, including liquefied petroleum gases, by
meter and prover. It does not include two-phase fluids.
ISO 9770:1989 Crude petroleum and petroleum products -- Compressibility factors for hydrocarbons in
the range 638 kg/m3 to 1 074 kg/m3 includes the contents of Manual of Petroleum Measurement
Standards, Chapter 11.2.1M published August 1984 by API. The purpose is to correct
hydrocarbon volumes metered under pressure to the corresponding volumes at the equilibrium
pressure for the metered temperature. Contains compressibility factors related to meter
temperature and density of metered material.
API MPMS 11.1: 2004 Petroleum measurement tables - Part 1: Tables based on reference temperatures
of 15 degrees C and 60 degrees F provides the algorithm and implementation procedure for the
correction of temperature and pressure effects on density and volume of liquid hydrocarbons
which fall within the categories of crude oil, refined products, or lubricating oils; NGLs and LPGs
are excluded from consideration in this Standard. This document is distributed on CD-ROM in
Portable Document Format (PDF). A utility program is included on the CD to allow users to
calculate corrections for temperature and pressure effects and to print pages of correction factors
for a user-defined range of temperature, pressure and density in both US Customary and Metric
units of measure. The utility is used within a supported web browser and uses the Java language.
Internet access is not required. (Printed tables are not available from either API or ASTM for this
edition of Chapter 11.1 Temperature and Pressure Volume Correction Factors for Generalized
Crude Oils, Refined Products, and Lubricating Oils.)
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ISO 4124: 1994 Liquid hydrocarbons -- Dynamic measurement -- Statistical control of volumetric
metering systems. In dynamic measuring systems the performance of meters for liquid
hydrocarbons will vary with changes in flow conditions, viz. flowrate, viscosity, temperature,
pressure, density of product, and with mechanical wear. Has been prepared as a guide for
establishing and monitoring the performance of such meters, using appropriate statistical control
procedures for both central and on-line proving. These procedures may be applied to
measurements made by any type of volumetric or mass metering systems. The procedures to be
followed for collecting data, on which the control limits are based, are described.
API MPMS 20.1:2006 Allocation Measurement provides design and operating guidelines for liquid and
gas allocation measurement systems. Included are recommendations for metering, static
measurement, sampling, proving, calibrating and calculating procedures.
OIML R117-1:2007 specifies the metrological and technical requirements applicable to dynamic
measuring systems for quantities (volume or mass) of liquids other than water subject to legal
metrology controls. It also provides requirements for the approval of parts of the measuring
systems (meter, etc.).
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Abstract of standard
OIML R140:2007 Measuring systems for gaseous fuel applies to measuring systems for gaseous fuel:
with a designed maximum flowrate Qmax equal to or greater than 100 m3/h at base
conditions and for operating pressures equal to or greater than 200 kPa (2 bar) absolute;
not fitted with diaphragm gas meters.
It may apply to very large measuring systems located at the border between two countries as well
as to smaller measuring systems, with the exception of measuring systems for compressed natural
gas for vehicles (CNG). However, the provisions of this Recommendation may be adapted to
other cases. This Recommendation lays down the metrological and technical requirements
applicable to the measuring systems subject to legal metrology controls.
Different types of measuring systems are considered:
measuring systems providing indications of volume at base conditions (as defined in this
Recommendation) or mass converted from a volume of gas determined at metering or base
conditions;
measuring systems directly providing the mass of gas;
measuring systems providing an indication of energy corresponding to a volume at base
conditions or a mass of gas.
The concept of a measuring system may involve data and figures provided according to
documented provisions. This is often necessary in particular for the determination of energy. In
this case the purpose of this Recommendation is to provide tools in order to manage energy on a
metrological basis (see examples in D.3). It is not intended to prohibit the use of other tools
allowing the management of energy (see examples in D.4).
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NS-EN 1776:1999 Gas supply systems - Natural gas measuring stations Functional requirements This
European standard specifies functional requirements for the design, construction, commissioning,
operation and maintenance of new gas measuring stations for non-domestic custody transfer of
natural gas as described in ISO 13686 with a design capacity equal to or greater than 500 m3/h (at
base conditions, see 4.1) and for operating pressures equal to or greater than 1 bar (gauge
pressure). NOTE: Installations using diaphragm gas meters as primary measuring instruments are
not covered by this standard. Except for safety and environmental aspects, the extent to which the
requirements of this standard are applied should be justified by the economics of the measuring
station. Therefore, stations with an annual throughput of equal to or smaller than 300 000 m3 (at
base conditions) are excluded from the scope of this standard. This European Standard specifies
common basic principles for gas supply systems. Users of this European Standard should be
aware that more detailed national standards and/or codes of practice may exist in the CEN
member countries. This European Standard is intended to be applied in association with these
national standards and/or codes of practice setting out the above mentioned basic principles.
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Abstract of standard
ISO 5167-1:2003 Measurement of fluid flow by means of pressure differential devices inserted in
circular cross-section conduits running full -- Part 1: General principles and requirements
defines terms and symbols and establishes the general principles for methods of measurement and
computation of the flowrate of fluid flowing in a conduit by means of pressure differential
devices (orifice plates, nozzles and Venturi tubes) when they are inserted into a circular crosssection conduit running full. ISO 5167-1:2003 also specifies the general requirements for
methods of measurement, installation and determination of the uncertainty of the measurement of
flowrate. It also defines the general specified limits of pipe size and Reynolds number for which
these pressure differential devices are to be used. ISO 5167 (all parts) is applicable only to flow
that remains subsonic throughout the measuring section and where the fluid can be considered as
single-phase. It is not applicable to the measurement of pulsating flow.
ISO 5167-2:2003 Measurement of fluid flow by means of pressure differential devices inserted in
circular cross-section conduits running full -- Part 2: Orifice plates specifies the geometry and
method of use (installation and operating conditions) of orifice plates when they are inserted in a
conduit running full to determine the flow-rate of the fluid flowing in the conduit. It also provides
background information for calculating the flow-rate and is applicable in conjunction with the
requirements given in ISO 5167-1. ISO 5167-2:2003 is applicable to primary devices having an
orifice plate used with flange pressure tappings, or with corner pressure tappings, or with D and
D/2 pressure tappings. Other pressure tappings such as vena contracta and pipe tappings have
been used with orifice plates but are not covered by ISO 5167-2:2003. ISO 5167-2:2003 is
applicable only to a flow which remains subsonic throughout the measuring section and where the
fluid can be considered as single phase. It is not applicable to the measurement of pulsating flow.
It does not cover the use of orifice plates in pipe sizes less than 50 mm or more than 1 000 mm, or
for pipe Reynolds numbers below 5000.
ISO 5167-3:2003 Measurement of fluid flow by means of pressure differential devices inserted in
circular cross-section conduits running full -- Part 3: Nozzles and Venturi nozzles specifies the
geometry and method of use (installation and operating conditions) of nozzles and Venturi
nozzles when they are inserted in a conduit running full to determine the flow-rate of the fluid
flowing in the conduit. ISO 5167-3:2003 also provides background information for calculating
the flow-rate and is applicable in conjunction with the requirements given in ISO 5167-1. ISO
5167-3:2003 is applicable to nozzles and Venturi nozzles in which the flow remains subsonic
throughout the measuring section and where the fluid can be considered as single-phase. In
addition, each of the devices can only be used within specified limits of pipe size and Reynolds
number. It is not applicable to the measurement of pulsating flow. It does not cover the use of
nozzles and Venturi nozzles in pipe sizes less than 50 mm or more than 630 mm, or for pipe
Reynolds numbers below 10 000. ISO 5167-3:2003 deals with two types of standard nozzles, the
ISA 1932 nozzle and the long radius nozzle, as well as the Venturi nozzle.
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Abstract of standard
ISO 17089-1:2010 Measurement of fluid flow in closed conduits - Ultrasonic meters for gas - Part 1:
Meters for custody transfer and allocation measurement specifies requirements and
recommendations for ultrasonic gas flowmeters (USMs), which utilize the transit time of acoustic
signals to measure the flow of single phase homogenous gases in closed conduits. ISO 170891:2010 applies to transit time ultrasonic gas flowmeters used for custody transfer and allocation
metering, such as full-bore, reduced-area, high-pressure, and low-pressure meters or any
combination of these. There are no limits on the minimum or maximum sizes of the meter. ISO
17089-1:2010 can be applied to the measurement of almost any type of gas, such as air, natural
gas, and ethane. Included are flow measurement performance requirements for meters of two
accuracy classes suitable for applications such as custody transfer and allocation measurement.
ISO 17089-1:2010 specifies construction, performance, calibration, and output characteristics of
ultrasonic meters for gas flow measurement and deals with installation conditions.
AGA Report Nr 9:2007 Measurement of Gas by Multipath Ultrasonic Meters. This report is for
multipath ultrasonic transit-time flow meters, typically 6" and larger in diameter, used for the
measurement of natural gas. It is written in the form of a performance-based specification.
AGA Report Nr 10:2005 Natural gas -- Calculation of thermodynamic properties -- Part 1: Gas phase
properties for transmission and distribution applications. This report outlines a method for the
calculation of the speed of sound in natural gas and the individual components that make up
natural gas. It also calculates the entropy, enthalpy and C* coefficient for sonic nozzles. It also
provides computer codes for programming calculations of speed of sound.
Other relevant Standards
ISO 20765-1: 2005
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AGA Report Nr 11: 2003
Abstract of standard
ISO 10790:1999 Measurement of fluid flow in closed conduits -- Guidance to the selection, installation
and use of Coriolis meters (mass flow, density and volume flow measurements) gives guidelines
for selection, installation, calibration, performance and operation of Coriolis meters for
determination of mass flow, density, volume flow and other related parameters of fluids. The
standard primarily concentrates on measurement of liquids. Amendment 1 (2003) extend the
standard to cover some aspects of gas measurement with Coriolis meters.
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AGA Standards
AGA Report Nr 7: 2006
Abstract of standard
ISO 9951:1993 Measurement of gas flow in closed conduits -- Turbine meters specifies dimensions,
ranges, construction, performance, calibration and output characteristics of the turbine meters.
Also deals with installation conditions, leakage testing und pressure testing and provides a series
of informative annexes A to E including recommendations for use, field checks, and perturbations
of the fluid flowing. In many countries, some or all of the items covered are subject to mandatory
regulations imposed by the laws of these countries. Where conflicts exist, the mandatory
regulations shall prevail.
AGA Report Nr 7:2006 Measurement of Natural Gas by Turbine Meter provides information on the
theory of operation, performance characteristics, and installation and maintenance of turbine
meters. Also includes technique for flow computation, calibration and field checks.
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ISO 6551: 1982 Petroleum liquids and gases - Fidelity and security of dynamic measurement - Cabled
transmission of electric and/or electronic pulsed data establishes guidelines for ensuring the
quantities stated, a main objective being to ensure the integrity of the primary indication. In order
to achieve different levels of security, criteria and recommendations for the design, installation,
use and maintenance of the relevant equipment are laid down. Regulatory requirements, including
those for safety, are not specifically covered in detail but certain general cautionary notes on
safety are included for guidance.
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Abstract of standards
ISO 15970:2008 Natural gas -- Measurement of properties -- Volumetric properties: density, pressure,
temperature and compression factor gives requirements and procedures for the measurement of
the properties of natural gas that are used mainly for volume calculation and volume conversion:
density at reference and at operating conditions, pressure, temperature and compression factor.
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ISO 2186:2007
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AGA Standards
AGA Report Nr 8: 1994
Abstract of standard
ISO 6976:1995 Natural gas -- Calculation of calorific values, density, relative density and Wobbe index
from composition Specifies methods for the calculation of the superior calorific value and the
inferior calorific value, density, relative density and Wobbe index of dry natural gas and other
combustible gaseous fuels, when the composition of the gas by mole fraction is known. Replaces
the first edition, which has been technically revised.
ISO 12213-1: 2006 Natural gas -- Calculation of compression factor -- Part 1: Introduction and
guidelines specifies methods for the calculation of compression factors of natural gases, natural
gases containing a synthetic admixture and similar mixtures at conditions under which the
mixture can exist only as a gas. It is divided into three parts: this part, ISO 12213-1:2006, gives
an introduction and provides guidelines for the methods of calculation described in Parts 2 and 3.
ISO 12213-2: 2006 Natural gas -- Calculation of compression factor -- Part 2: Calculation using molarcomposition analysis specifies methods for the calculation of compression factors of natural
gases, natural gases containing a synthetic admixture and similar mixtures at conditions under
which the mixture can exist only as a gas. It is divided into three parts: this part, ISO 122132:2006, specifies a method for the calculation of compression factors when the detailed
composition of the gas by mole fractions is known, together with the relevant pressures and
temperatures. The method is applicable to pipeline quality gases within the ranges of pressure p
and temperature T at which transmission and distribution operations normally take place, with an
uncertainty of about +/- 0,1 %. It can be applied, with greater uncertainty, to wider ranges of gas
composition, pressure and temperature.
ISO 12213-3: 2006 Natural gas -- Calculation of compression factor -- Part 3: Calculation using physical
properties specifies methods for the calculation of compression factors of natural gases, natural
gases containing a synthetic admixture and similar mixtures at conditions under which the
mixture can exist only as a gas. It is divided into three parts: this part, ISO 12213-3:2006,
specifies a method for the calculation of compression factors when the superior calorific value,
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AGA Standards
AGA Report Nr 5: 2009
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ISO 10715: 1997 Natural gas - Sampling guidelines provides concise guidelines for the collection,
conditioning and handling of representative samples of processed natural gas streams. It also
contains guidelines for sampling strategy, probe location and the handling and design of sampling
equipment. It considers spot, composite (incremental) and continuous sampling systems. This
document gives consideration to constituents such as oxygen, hydrogen sulfide, air, nitrogen and
carbon dioxide in the gas stream. This document does not include sampling of liquid streams or
streams with multiphase flow. Traces of liquid, such as glycol and compressor oil, if present, are
assumed to be intrusive and not a part of the gas to be sampled. Their removal is desirable to
protect the sampling and analytical equipment from contamination. This document can be used
for custody transfer measurement systems and allocation measurement systems.
Other relevant Standards
ISO 8943: 2007
ISO 8943: 2007 Refrigerated light hydrocarbon fluids -- Sampling of liquefied natural gas -- Continuous
and intermittent methods specifies methods for the continuous and the intermittent sampling of
LNG while it is being transferred through an LNG transfer line.
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ISO 6974-2: 2001 Natural gas -- Determination of composition with defined uncertainty by gas
chromatography -- Part 2: Measuring-system characteristics and statistics for processing of data
describes the data processing for the tailored analysis of natural gas. It includes the determination
of the measuring system characteristics and the statistical approach to data handling and error
calculation with the aim of defining the uncertainty in the mole fractions of the component
measured. This part of ISO 6974 is only applicable in conjunction with part 1 of ISO 6974.
ISO 6974-3: 2000 Natural gas -- Determination of composition with defined uncertainty by gas
chromatography -- Part 3: Determination of hydrogen, helium, oxygen, nitrogen, carbon dioxide
and hydrocarbons up to C8 using two packed columns describes a gas chromatographic method
for the quantitative determination of the content of helium, hydrogen, oxygen, nitrogen, carbon
dioxide and C1 to C8 hydrocarbons in natural gas samples using two packed columns. This
method is applicable to determinations made in on-line processes or in the laboratory. It is
applicable to the analysis of gases containing constituents within the mole fraction ranges given
in Table 1 and which do not contain any hydrocarbon condensate. These ranges do not represent
the limits of detection, but the limits within which the stated precision of the method applies.
Although one or more components in a sample may not be detected present, the method can still
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ISO 6974-4: 2000 Natural gas -- Determination of composition with defined uncertainty by gas
chromatography -- Part 4: Determination of nitrogen, carbon dioxide and C1 to C5 and C6+
hydrocarbons for a laboratory and on-line measuring system using two columns describes a gas
chromatographic method for the quantitative determination of natural gas constituents using a
two-column system. This method is applicable to determinations made in on-line processes or in
the laboratory. It is applicable to the analysis of gases containing constituents within the mole
fraction ranges given in Table 1. These ranges do not represent the limits of detection, but the
limits within which the stated precision of the method applies. Although one or more components
in a sample may not be detected present, the method can still be applicable. This part of ISO 6974
is only applicable if used in conjunction with parts 1 and 2 of ISO 6974.
Table 1 Application ranges
Component
Nitrogen
Carbon dioxide
Methane
Ethane
Propane
iso-Butane (2-methylpropane)
n-Butane
neo -Pentane (2,2dimethylpropane)
iso -Pentane (2-methylbutane)
n-Pentane
Hexanes _ sum of all C6 and
higher hydrocarbons
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ISO 6974-6: 2002 Natural gas -- Determination of composition with defined uncertainty by gas
chromatography -- Part 6: Determination of hydrogen, helium, oxygen, nitrogen, carbon dioxide
and C1 to C8 hydrocarbons using three capillary columns describes a gas chromatographic
method for the quantitative determination of the content of helium, hydrogen, oxygen, nitrogen,
carbon dioxide and C1 to C8 hydrocarbons in natural gas samples using three capillary columns.
This method is applicable to the determination of these gases within the mole fraction ranges
varying from 0,000 1 % to 40 %, depending on the component analyzed, and is commonly used
for laboratory applications. However, it is only applicable to methane within the mole fraction
range of 40 % to 100 %. These ranges do not represent the limits of detection, but the limits
within which the stated precision of the method applies. Although one or more components in a
sample may not be present at detectable levels, the method can still be applicable. ISO 69746:2002 is only applicable if used in conjunction with ISO 6974-1:2000 and ISO 6974-2:2001.
This method can also be applicable to the analysis of natural gas substitutes. Additional
information on the applicability of this method to the determination of natural gas substitutes is
also given where relevant.
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ISO 19739:2004 Natural gas -- Determination of sulfur compounds using gas chromatography specifies
the determination of hydrogen sulfide, carbonyl sulfide, C1 to C4 thiols, sulfides and
tetrahydrothiophene (THT) using gas chromatography (GC). Depending on the method chosen
from those given in its annexes, the application ranges for the determination of sulfur compounds
can vary, but whichever of the methods is used, its requirements apply.
ISO 6326-1:2007 Natural gas -- Determination of sulfur compounds -- Part 1: General introduction
gives a brief description of standardized methods that can be used for the determination of sulfur
compounds in natural gas. The principle of each method is described generally, the range of
concentrations for which the method is suitable is indicated, and the analytical range and
precision of each method is given. It should enable the user to select judiciously the proper
method for the application being considered. Sulfur analysis is performed in order to determine
total sulfur, sulfur contained in specific groups [e.g. thiols (mercaptans)], individual sulfur
compounds and specific groups of sulfur compounds. The available standardized methods in the
field of sulfur analysis are the Wickbold combustion method for total sulfur determination (ISO
4260); the Lingener combustion method for total sulfur determination (ISO 6326-5); gas
chromatography for determination of individual sulfur compounds (ISO 19739); potentiometry
for determination of hydrogen sulfide, carbonyl sulfide and thiol compounds (ISO 6326-3).
ASTM D 1945-03: 2010 Standard Test Method for Analysis of Natural Gas by Gas Chromatography
covers the determination of the chemical composition of natural gases and similar gaseous
mixtures within the range of composition shown in Table 1. This test method may be abbreviated
for the analysis of lean natural gases containing negligible amounts of hexanes and higher
hydrocarbons, or for the determination of one or more components, as required. The values stated
in inch-pound units are to be regarded as standard. The values given in parentheses are
mathematical conversions to SI units that are provided for information only and are not
considered standard. This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this standard to establish appropriate
safety and health practices and determine the applicability of regulatory limitations prior to use.
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Crude petroleum and liquid or solid petroleum products -Determination of density or relative density -- Capillarystoppered pyknometer and graduated bicapillary pyknometer
methods
Crude petroleum and petroleum products -- Determination of
density -- Oscillating U-tube method
Liquefied petroleum gas and light hydrocarbons -- Determination
of density or relative density -- Pressure hydrometer method
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API Standards
API MPMS 9.1: 2005
Abstract of standard
ISO 3838: 2004 Crude petroleum and liquid or solid petroleum products -- Determination of density or
relative density -- Capillary-stoppered pyknometer and graduated bicapillary pyknometer
methods specifies methods for the determination of the density or relative density of crude
petroleum and of petroleum products handled as liquids. The capillary-stoppered pyknometer
method is also for use with solids and this method may also be used for coal tar products,
including road tars, creosote and tar pitches, or for mixtures of these with petroleum products.
This method is not suitable for the determination of the density or relative density of highly
volatile liquids having Reid vapour pressures greater than 50 kPa according to ISO 3007 or
having an initial boiling point below 40 degrees Celsius. The graduated bicapillary pyknometer
method is recommended for the accurate determination of the density or relative density of all
except the more viscous products, and is particularly useful when only small amounts of samples
are available. The method is restricted to liquids having Reid vapour pressures of 130 kPa or less
according to ISO 3007 and having kinematic viscosities less than 50 mm2/s (50 centistokes (cSt))
at the test temperature. Special precautions are specified for the determination of the density or
relative density of highly volatile liquids.
ISO 12185: 1996 Crude petroleum and petroleum products -- Determination of density -- Oscillating Utube method gives a method for the determination, using an oscillation U-tube densitometer, of
the density of crude petroleum and related products within the range 600 kg/m3 to 1 100 kg/m3
which can be handled as single-phase liquids at the test temperature and pressure.
ISO 3993: 1984 Liquefied petroleum gas and light hydrocarbons -- Determination of density or relative
density -- Pressure hydrometer method prescribed apparatus shall not be used for materials
having gauge vapour pressures higher than 1,4 MPa (absolute vapour pressure 1,5 MPa) at the
test temperature. Alternative calibration procedures are described, but only the one using a
certified hydrometer is suitable for the determination of density to be used in calculations of
qualities for custody transfer or fiscal purposes.
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ISO 649-1: 1981 Laboratory glassware -- Density hydrometers for general purposes -- Part 1:
Specification specifies the requirements for basic series and sub-series of glass hydrometers of
constant mass without built-in thermometer. They are graduated to indicate density at 20 degrees
centigrade and 15 degrees centigrade, respectively. Standard categories of surface tension are
tabled in annex A, recommended stem diameters in annex B.
ISO 649-2: 1981 Laboratory glassware -- Density hydrometers for general purposes -- Part 2: Test
methods and use specifies the determination of the density considering general procedures.
Apparatus and readings of the density and temperature are described and also the application of
the corrections. In drawings the construction and the dimensions of suitable vessels are shown.
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Abstract of standard
ISO 9030: 1990 Crude petroleum -- Determination of water and sediment -- Centrifuge method
specifies a method for the laboratory determination. The precision data of this procedure have
only been determined for water contents up to 1 % (V/V). Includes principle, apparatus, reagents,
sampling, procedure, expression of results, precision and test report. A centrifuge tube is shown
in figure 1. The procedure for reading the volume of water and sediment is shown in figure 2. The
precision of the method is shown in figure 3. The sample handling is described in annex A.
ISO 9029: 1990 Crude petroleum -- Determination of water -- Distillation method. The precision data
of this procedure have only been determined for water contents up to 1 % (V/V). Includes
principle, apparatus, solvent, calibration and recovery test, sampling, procedure, expression of
results, precision and test report. The distillation apparatus is shown in figures 1 and 2. The
precision of the method is shown in figure 3. The sample handling is described in annex A.
API MPMS 10.3: 2008 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge
Method (Laboratory Procedure) describes a method of laboratory determination of water and
sediment in crude oil by means of the centrifuge procedure.
API MPMS 10.6: 2009 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge
Method (Laboratory Procedure) describes the laboratory determination of water and sediment in
fuel oils in the range from 0 to 30 % volume by means of the centrifuge procedure.
API MPMS 10.7: 2006 Standard Test Method for Water in Crude Oils by Potentiometric Karl Fischer
Titration describes the procedure for the determination of water in crude oils by Karl Fischer
titration (potentiometric.) This test method covers the determination of water in the range from
0.02 to 2 mass percent in crude oils. Mercaptan and sulfide (S or H2S) sulfur are known to
interfere with the method.
API MPMS 10.8: 2010 Standard Test Method for Sediment in Crude Oil by Membrane Filtration
covers the determination of sediment in crude oils by membrane filtration. This test method has
been validated for crude oils with sediments up to approximately 0.15 mass %. The accepted unit
of measure for this test method is mass %, but an equation to convert to volume % is provided.
API MPMS 10.9: 2010 Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer
Titration covers the determination of water in the range from 0.02 to 5.0 percent in crude oils.
The test method presents two procedures for the direct determination of water content in crude
oils; weight and volume.
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API Documents
API MPMS RP 86: 2005
API MPMS Publ 2566 : 2004
ISO Documents
ISO/PRF TR 11583: 2011 (1)
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Petroleum measurement tables -- Part 1: Tables based on reference temperatures of 15 degrees C and 60 degrees F
Petroleum measurement tables -- Part 2: Tables based on a reference temperature of 20 degrees C
Petroleum industry -- Terminology -- Part 6: Measurement
Measurement of fluid flow in closed conduits -- Connections for pressure signal transmissions between primary and
secondary elements
Liquid hydrocarbons -- Volumetric measurement by displacement meter systems other than dispensing pumps
Liquid hydrocarbons -- Volumetric measurement by turbine meter systems
Petroleum products -- Calculation of viscosity index from kinematic viscosity
Petroleum liquids - Manual sampling
Petroleum liquids -- Automatic pipeline sampling
Crude petroleum and liquid petroleum products - Laboratory determination of density - Hydrometer method
Petroleum products and bituminous materials -- Determination of water - Distillation method
Petroleum products - Determination of water and sediment in residual fuel oils - Centrifuge method
Crude petroleum and fuel oils - Determination of sediment - Extraction method
Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillarystoppered pyknometer and graduated bicapillary pyknometer methods
Liquefied petroleum gas and light hydrocarbons - Determination of density or relative density - Pressure hydrometer
method
Liquid hydrocarbons -- Dynamic measurement -- Statistical control of volumetric metering systems
Liquefied petroleum gases -- Method of sampling
Petroleum and liquid petroleum products - Calculation of oil quantities - Part 2: Dynamic measurement
Petroleum liquids and liquefied petroleum gases - Measurement - Standard reference conditions
Measurement of fluid flow by means of pressure differential devices inserted in circular cross-section conduits running
full -- Part 1: General principles and requirements
Measurement of fluid flow by means of pressure differential devices inserted in circular cross-section conduits running
full -- Part 2: Orifice plates
Measurement of fluid flow by means of pressure differential devices inserted in circular cross-section conduits running
full -- Part 3: Nozzles and Venturi nozzles
Measurement of fluid flow by means of pressure differential devices inserted in circular cross-section conduits running
full -- Part 4: Venturi tubes
Measurement of fluid flow - Procedures for the evaluation of uncertainties
Petroleum products -- Determination of water -- Potentiometric Karl Fischer titration method
Natural gas -- Determination of sulfur compounds -- Part 1: General introduction
Petroleum liquids and gases -- Fidelity and security of dynamic measurement -- Cabled transmission of electric and/or
electronic pulsed data
Natural gas - Determination of composition with defined uncertainty by gas chromatography - Part 1: Guidelines for
tailored analysis
Natural gas - Determination of composition with defined uncertainty by gas chromatography - Part 2: Measuringsystem characteristics and statistics for processing of data
Revision 2
23, 28
23, 26
48
37
37
43, 86
90
46, 90
46
42, 85
43, 85
23, 52
38
50
6
56,71
56, 71
56, 71
56, 71
15
88
84
26, 28,
30,
32, 67
15, 80
15, 80
80
Natural gas - Determination of composition with defined uncertainty by gas chromatography - Part 3: Determination of
hydrogen, helium, oxygen, nitrogen, carbon dioxide and hydrocarbons up to C8 using two packed columns
Natural gas - Determination of composition with defined uncertainty by gas chromatography - Part 4: Determination of
nitrogen, carbon dioxide and C1 to C5 and C6+ hydrocarbons for a laboratory and on-line measuring system using
two columns
Natural gas - Determination of composition with defined uncertainty by gas chromatography - Part 5: Determination of
nitrogen, carbon dioxide and C1 to C5 and C6+ hydrocarbons for a laboratory and on-line process application using
three columns
71
80
23, 50
23, 50
22
15, 80
15, 80
15, 80
80
Natural gas - Determination of composition with defined uncertainty by gas chromatography - Part 6: Determination of
hydrogen, helium, oxygen, nitrogen, carbon dioxide and C1 to C8 hydrocarbons using three capillary columns
Natural gas -- Calculation of calorific values, density, relative density and Wobbe index from composition
Assessment of uncertainty in calibration and use of flow measurement devices - Part 1: Linear calibration
relationships
Assessment of uncertainty in the calibration and use of flow measurement devices - Part 2: Non-linear calibration
relationships
Liquid hydrocarbons - Dynamic measurement - Proving systems for volumetric meters -- Part 1: General principles
Liquid hydrocarbons - Dynamic measurement -- Proving systems for volumetric meters -- Part 2: Pipe provers
Liquid hydrocarbons - Dynamic measurement - Proving systems for volumetric meters -- Part 3: Pulse interpolation
techniques
Liquid hydrocarbons - Dynamic measurement - Proving systems for volumetric meters - Part 4: Guide for operators of
pipe provers
16, 80
72, 75
16
16
35
35
35
35
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Petroleum measurement systems - Calibration -- Temperature corrections for use when calibrating volumetric proving
tanks
Refrigerated light hydrocarbon fluids - Measurement of temperature in tanks containing liquefied gases - Resistance
thermometers and thermocouples
Refrigerated light hydrocarbon fluids -- Sampling of liquefied natural gas -- Continuous and intermittent methods
Quality management systems -- Fundamentals and vocabulary
Quality management systems - Requirements
Managing for the sustained success of an organization - A quality management approach.
Crude petroleum -- Determination of water -- Distillation method
Crude petroleum - Determination of water and sediment - Centrifuge method
Measurement of gas flow by means of critical flow Venturi nozzles
Guidelines for the use of ISO 5167:2003
3
Crude petroleum and petroleum products -- Compressibility factors for hydrocarbons in the range 638 kg/m to 1 074
3
kg/m
Measurement of gas flow in closed conduits -- Turbine meters
Quality management systems - Guidelines for quality plans
Guidelines for quality management system documentation
Petroleum products - Total sediment in residual fuel oils - Part 1: Determination by hot filtration
Petroleum products - Total sediment in residual fuel oils - Part 2: Determination using standard procedures for ageing
Crude petroleum -- Determination of water -- Potentiometric Karl Fischer titration method
Crude petroleum -- Determination of water -- Coulometric Karl Fischer titration method
Natural gas -- Sampling guidelines
Natural gas -- Performance evaluation for on-line analytical systems
Measurement of fluid flow in closed conduits -- Guidance to the selection, installation and use of Coriolis meters
(mass flow, density and volume flow measurements)
33
41
78
8
8
9
88
45, 88
58
58
23, 50
66
9
9
46
46
88
88
78
80
23, 30,
43, 64
Measurement of wet gas flow by means of pressure differential devices inserted in circular cross-section conduits
91
22
43, 85
73
73
73
32
58
88
6
15
80
54
75
42, 86
42, 86
58
69, 73
75
12
11
62
62
9
84
62, 73
8
16
80
9
41, 69
6
12
14
15
14
16
15
15
International vocabulary of metrology - Basic and general concepts and associated terms (VIM)
35
35
35
35
35
35
35
22
23, 28
23, 26
26, 28,
30, 32
26, 28,
30, 32
23, 30
23, 32
41
37
37
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38
38
43, 86
43, 86
37, 79
46
46
45, 89
45
46
46, 89
46, 89
46, 89
46, 89
50
50
50
50
50
50
50
50
16, 38
16, 38
7
52
50
45
91
91
58
75
66
73
62
62
64
ASTM D341-03
ASTM D 1945-03: 2010
Standard Test Method for Viscosity-Temperature Charts for Liquid Petroleum Products
Standard Test Method for Analysis of Natural Gas by Gas Chromatography
48
84
NFOGM 2001
NFOGM 2003
NFOGM Handbook 2005
Handbook Revision 2: 2005
14
14
46
91
55
22, 52
54
54
Revision 2
Orifice Metering of Natural Gas Part 1: General Equations & Uncertainty Guidelines
58
58
58