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Liquid/Liquid and Gas/Liquid/Liquid Separators - Type Selection and Design Rules

The copyright of this document is vested in this company. Calculation example an existing horizontal open two-phase settler has to be checked to establish whether it can separate oil and water properly under given process conditions. If required, its separation performance has to be upgraded by the installation of internals.

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337 views

Liquid/Liquid and Gas/Liquid/Liquid Separators - Type Selection and Design Rules

The copyright of this document is vested in this company. Calculation example an existing horizontal open two-phase settler has to be checked to establish whether it can separate oil and water properly under given process conditions. If required, its separation performance has to be upgraded by the installation of internals.

Uploaded by

bldp03
Copyright
© © All Rights Reserved
Available Formats
Download as PDF, TXT or read online on Scribd
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MANUAL

LIQUID/LIQUID AND GAS/LIQUID/LIQUID SEPARATORS -


TYPE SELECTION AND DESIGN RULES



DEP 31.22.05.12-Gen.
January 2008
DESIGN AND ENGINEERING PRACTICE
USED BY
COMPANIES OF THE ROYAL DUTCH/SHELL GROUP

This document is restricted. Neither the whole nor any part of this document may be disclosed to any third party without the prior written consent of Shell Global
Solutions International B.V., The Netherlands. The copyright of this document is vested in this company. All rights reserved. Neither the whole nor any part of this
document may be reproduced, stored in any retrieval system or transmitted in any form or by any means (electronic, mechanical , reprographic, recording or otherwise)
without the prior written consent of the copyright owner.
DEP 31.22.05.12-Gen.
January 2008
Page 74
IV.1.3 Calculation example
An existing horizontal open two-phase settler has to be checked to establish whether it can
separate oil and water properly under given process conditions.
If required, its separation performance has to be upgraded by the installation of internals.
Flow conditions are:
Oil: mass flow rate of 500 t/d with a density of 750 kg/m
3
and a dynamic viscosity of
0.5 mPa.s.
Water: mass flow rate of 320 t/d with a density of 990 kg/m
3
and a dynamic viscosity of
0.9 mPa.s.
Design margin is 1.2
No dispersion band expected in the oil/water interface
Level control (based on water flow rate):
3 minutes between high and low level (pre-alarms)
1 minute between pre-alarm and trip
Further information:
Vessel: diameter 1.5 m and T/T of 5 m (heads semi-elliptical with a ratio of 2:1)
Nozzles: feed inlet is a top inlet located 0.25 m from the "left" vessel tangent line;
distance of oil and water outlets from "right" vessel tangent line is 0.4 m; diameters of
feed inlet, oil outlet and water outlet are 0.15, 0.15 and 0.10 m respectively
Internals: only vortex breakers on the oil and water outlet are present
Check
To optimise the settling conditions, it is proposed to convert the vessel layout to the layout
shown in the top part of Figure 3.1.
It is proposed to fit the feed nozzle with an elbowed pipe directed to the nearest vessel head
and to install a double calming baffle (30 % NFA and 50 % NFA respectively), the second
baffle to be located at 0.75 m (0.45 vessel diameter) from the left tangent line with a
distance of 0.3 m (0.2 D
ves
diameter) between the baffles. The distance from the vertical TL
to the first baffle is taken slightly larger than the minimum (0.25 vessel diameter) to
accommodate the inlet nozzle with sufficient clearance from left tangent line and baffle. This
distance is 150+ ID
nozzle
+ max(150, 0.5xID
nozzle
) = 0.45 m.
This will result in an effective settling length to the nozzles of 5 - 0.4 - 0.75 = 3.85 m.
The distance between pre-alarm and trip level in each set is at least 0.1 m (no allowance for
dispersion band necessary) and the distance between high and low IL is minimal 0.35 m.
This results in a total control band of minimal 0.55 m.
As a starting point it is assumed that the control band has this minimum width of 0.55 m.
It should be located in the vessel so that in both the oil and the water layer proper bulk
separation takes place i.e. all droplets larger than 150 m diameter shall be removed.
Initially three locations of this control band in the vessel have been considered:
Position I: At the lowest location (LZA(LL)
int
= 0.2
*
D
ves
= 0.3 m)
Position II: In the centre (A
l
= A
h
)
Position III: At the highest location (LZA(HH)
int
= 0.8
*
D
ves
= 1.2 m)
For these three positions the various quantities (e.g. cross-sectional areas, velocities, cut-
off diameters, control time and maximum allowable axial velocities) have been calculated
according to the calculation scheme presented in Appendix IV.3.
DEP 31.22.05.12-Gen.
January 2008
Page 75
They are listed in the following table.
Nozzle velocities (including design margin!) have also been calculated and listed.
In this table it has been indicated (by bold italic and border) where the various requirements
for this type of separator are not satisfied (see Appendix IV.1.2).

location of control band position
I
(low)
position
II
(medium)
position
III
(high)
position
IV

limits of LZA(LL)
int
(m) 0.300 0.475 0.650 0.380
control band LZA(HH)
int
(m) 0.850 1.025 1.200 0.930
step 1
A
l
(m
2
)
0.734 0.480 0.252 0.616

A
h
(m
2
)
0.252 0.480 0.734 0.352
v
l,ax
(mm/s) 12.6 19.3 36.8 15.0
v
h,ax
(mm/s) 17.8 9.3 6.1 12.8
step 2 L
set
(m) 3.85 3.85 3.85 3.85
step 3 v
dh,set
(mm/s) 2.1 2.4 2.9 2.2
v
dl,set
(mm/s) 1.4 1.2 1.1 1.3
d
h
(m) 103 113 134 107
d
l
(m) 125 106 96 114
step 4
A
con
(m
2
)
0.505 0.520 0.505 0.516

V
hd
(m
3
)
0.143 0.152 0.143 0.149

V
con
(m
3
)
2.813 2.905 2.813 2.878
t
con,H_L
(sec) 627 647 627 641
t
con,HH_H
(sec) 186 177 155 184
t
con,L_LL
(sec) 155 177 186 167
nozzle feed: v
N1
(m/s) 0.74 0.74 0.74 0.74
velocities oil out: v
N3
(m/s) 0.50 0.50 0.50 0.50
water out: v
N4
(m/s) 0.55 0.55 0.55 0.55

The check of the settler leads to the following conclusions:
The calculations show that for the low, medium and high control band position, adequate
bulk separation takes place for both liquid phases (cut-off diameter smaller than
150 m).
However, the axial velocity in the light phase exceeds the upper limit of 0.015 m/s when
the control band is in the medium or high position. The axial velocity in the heavy phase
exceeds the limit of 0.015 m/s when the control band is in the low position. Therefore, for
optimum settler performance, a control band position between the low and medium
position should be selected.
The table shows that if LZA(LL)
int
is at 0.38 m (position IV; 0.08 m above the low
position) the velocity requirement for both phases has been satisfied.
The available time for the various control bands is in all cases much more than the
minimum requirements, so the selected width of the control band of 0.55 m is more than
sufficient.
The nozzle inlet and outlet velocities are well below the maximum of 1 m/s.
As i m trying to size settler as per
this shell DEP, i m unable to
understand how vdh and vdl for
all positions are calculated ?
Please help me in this regard i
will be very thankful to you. You
immediate response is highly
appreciated.

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