IS 4031 - Part2
IS 4031 - Part2
HYDRAULIC CEMENT
PART 2 DETERMINATION OF FINENESS BY BLAINE AIR PERMEABILITY METHOD
( Second Revision )
ICS 91.100.10
0 BIS 1999
FOREWORD
This Indian Standard (Part 2) (Secorrd Revision) was adopted by the Bureau of Indian Standards, after the draft
finalized by the Cement and Concrete Sectional Committee had been approved by the Civil Engineering Division
Council.
Standard methods of testing cement are essential adjunct to the cement specifications. This standard in different,
parts lays down the procedure for the tests to evaluate the physical properties of different types of hydraulic
cement. The procedure for conducting chemical test is covered in IS 4032 : 1985 ‘Methods of chemical analysis
of hydraulic cement Cfirst revision)‘. Originally all the tests to evaluate the physical properties of hydraulic
cement were covered in one standard but for facilitating the use of the standard and future revisions, the revised
standard was brought out into different parts, each part covering different tests. This part covers determination
of fineness by specific surface by Blaine air permeability apparatus.
The second revision of this standard has been prepared with a view to aligning this test method with European
Standard EN 196 (Part 6) ‘Method of testing cement: Determination of fineness’.
In reporting the result of a test or analysis made in accordance with this standard, if the final value, observed or
calculated, is to be rounded off, it shall be done in accordance with IS 2 : 1960 ‘Rules for rounding off numerical
values (revised)‘.
IS 4031( Part 2 ) : 1999
Indian Standard
METHODSOFPHYSICALTESTSFOR
HYDRAULICCEMENT
PART 2 DETERMINATION OF FINENESS BY BLAINE AIR PERMEABILITY METHOD
( Second Revision )
1 SCOPE 4.2 Timer
This standard (Part 2) covers the procedure for The timer shall have a positive starting and stopping
determining by Blaine air permeability apparatus, the mechanism and shall be capable of being read to the
fineness of cement as represented by specific surface nearest 0.2 s or better. The timer shall be accurate to
expressed as total surface area in cm2/g. 1 percent or better over time intervals up to 300 s.
NOTE - This method is also being used for determination of
fineness of various other materials. However, it should be
4.3 Balances
understood that the values obtained are relative rather than
Balances capable of weighing about 3 g to the nearest
absolute.
1 mg for the cement and about 50 g to 110 g to the
2 REFERENCES nearest 10 mg for the mercury.
The Indian Standards listed below contain provisions 4.4 Standard Weights
which through reference in this text, constitute
4.5 Pyknometer
provision of this standard. At the time of publication
the editions indicated were valid. All standards are Pyknometer or other convenient means of determining
subject to revision and parties to agreements based on the density of cement.
this standard are encouraged to investigate the
4.6 Manometer Liquid
possibility of applying the most recent editions of the
standards indicated below: The manometer shall be filled to the level of the lowest
etched line with a non-volatile, non-hygroscopic
IS No. Title
liquid of low viscosity and density, such as dibutyl
3535 : 1980 Methods of sampling hydraulic phthalate or light mineral oil.
cement first revision)
5516 : 1996 Specification for variable flow type 4.7 Mercury
air permeability apparatus (Blaine
type) (first revision) Mercury of reagent grade or better.
1
IS 4031( Part 2 ) : 1999
27 f 2°C and a relative humidity not exceeding Tap the cell to level the cement. Place a second new
65 percent. All materials for test and calibration shall filter paper disc on the levelled cement. Insert the
be at the laboratory temperature when used and shall plunger to make contact with the filter paper disc.
be protected from absorption of atmospheric moisture Press the plunger gently but firmly until the lower face
during storage. A laboratory temperature of 20 f 2°C of the cap is in contact with the cell. Slowly withdraw
may be maintained, if desired by the purchaser. the plunger about 5 mm, rotate it through 90” and
5.2 Compacted Cement Bed gently but firmly press the bed once again until the
plunger cap is in contact with the cell. The bed is now
5.2.1 Busis compacted and ready for the permeability test. Slowly
The compacted cement bed comprises a reproducible withdraw the plunger.
arrangement of cement particles with a specified NOTE - Too rapid and vigorous pressing may change the
volume of air included between the particles. This air particle size distribution and therefore change the specific
volume is defined as a fraction of the total volume of surface of the bed. The maximum pressure should be that
comfortably exerted by a thumb on the plunger.
the bed and is termed the porosity, e.
It follows that the volume fraction occupied by the 5.3 Air Permeability Test
cement particles is (l-e). If Vis the total volume of the 5.3.1 Basis
bed, the absolute volume of cement is V( l-e) (cm3),
and the mass of cement m is pV(l-e) (g) where p is The specific surface, S, is given in 5.6.1 but is
the solid density of the cement particles p (g/cm3). conveniently expressed as:
2
IS 4031( Part 2 ) : 1999
3
IS 4031( Part 2 ) : 1999
-another type of filter paper, and e is the porosity of the bed of cement under test,
-a new manometer tube; and e0 is the porosity of the bed of reference cement,
c) at systematic deviations of the secondary
t is the measured time for the cement under test(s),
reference cement.
to is the mean of the three times measured on the
5.5 Special Cements reference cement(s),
Certain cements having unusual particle size p is the density of the cement under test (g/cm”),
distributions and in particular, fine cements of higher
po is the density of the reference cement (g/cm3>,
strength grades may prove difficult to form into a
compacted bed of porosity e = 0.500 by the method TJ is the air viscosity at the test temperature taken
of 5.2.4. Should thumb pressure on the plunger cap fail from Table 1 (Pa.s), and
to bring it in contact with the top of the cell or if, after qa’is the air viscosity at the mean of the three
making contact and removing the pressure the plunger temperatures (Table 1) for the reference cement
moves upwards, the porosity of e = 0.500 shall be (Pa.s).
considered unattainable.
5.6.2 Eflect of Specified Porosity
For such cases the porosity required for a
Use of the specified porosity, e = 0.500 for both the
well-compacted bed shall be determined
reference and test cements simplifies formula, 5 to
eljperimentally. The mass of cement, rnq weighed to
make the bed as in 5.2.4 then becomes
. ..(6)
m4=U-ed PI V(g) . ..(4)
Where el is the porosity determined experimentally. In the case of cements requiring a porosity other than
e = 0.500 formula 6 cannot be used unless a reference
5.6 Simplification of the Calculation cement has been tested at that porosity.
5.6.1 Basic Formula
5.6.3 Effect of Density of Cement
The specific surface, S, of the cement under t&t is
calculated from the formula: The only remaining possibility of simplification is the
elimination of the density (p) terms. This has
Pox(l-eOl “;7x4iTx 47 previously been done where the only cements in
s3”
s =
p (1-e) O.lqo Gyso question were pure portland cements for which a value
of p of 3.15 was assumed to apply.That assumption is
(cm2k> ...(5) known to produce errors of up to 1 percent.
where 5.6.4 The formulae given in Table 2 may be used,
So is the specific surface of the reference cement calculate appropriate apparatus constant (KY)as shown
(cm2/g), in co1 3 of Table 2.
KG 0.001 36 x So
ii) 0.5 0.5 Outside?3’C
Jo7i;; Cl
KG42 1.414x&
iii) 0.5 Otherthan 0.5 Within +3’C Cements other than OPC
l-e to
KWF 0.001 92 x So
iv) 0.5 do Outsidef3OC do
dO.ln (t-e) to
K-FL? 4.455 x so
v) 0.5 do Within &3”C
P(1 -e) Cl
KdX7 0.006 05 x so
vi) 0.5 Outside+3’C do
p (1 -e)llO.ln 4,
4
IS 4031( Part 2 ) : 1999
5
IS 4031( Part 2 ) : 1999
ANNEX A
(FUFWW-d)
COMMITTEE COMPOSITION
Chairman
DR H. C. VISVESVARYA
Chandrika, 63-64 East Park Road,
Malleswaran, Bangalore 56OG03
Membem Representing
SHRIH. BHATTACHARYA Orissa Cement Limited, New Delhi
StIRIG. R. BHARITKAR B. G. Shirke & Co, Pune
DR A. K. CHA~RIEE The Associated Cement Companies Ltd. Mumbai
SHRIS. H. SUBRAMANIAN ( Alternate )
CHIEFENGINEER (DESIGN) Central Public Works Department, New Delhi
Suproc ENGINEER (S & S) ( Alternate )
CHIEFENGINEER, NAVAGAMDAM Sardar Sarovar Narman Nigam Ltd. Gandhinagar
SUPTDCENGINEER, QCC ( Alternate )
CHIEFENGINEER (RESEARCH-CIJM-DIRECR) Irrigation and Power Research Institute, Amritsar
RESEARCH OFFICER CONCRETE TECHMOUX~Y ( Alternate )
DIRECTOR A.P. Engineering Research Laboratories, Hyderabad
JT DIRECTOR ( Alternate )
DIRECTOR (CMDD) (N&W) Central Water Commission, New Delhi
DY DIRECTOR (CMDD) (NW&S) ( Alternate )
SHRI K. H. GANGWAL Hyderabad Industries Ltd. Hyderabad
SHRIV. PATTABHI (Alternate )
SHRIV.K. GHANEKAR Srructural Engineering Research Centre (CSIR), Ghaziabad
SHRIS. GOPINAM The India Cements Ltd. Chennai
StiRIIi. TAMILAKARAN (Alternate )
SHRIS. K. GUHATHAKURTA Gannon Dunkerley & Co Ltd, Mumbai
SHRI S. P. SANKARANARAYANAN ( Alternute )
SHRIN. S. BHAL Central Building Research Institute (CSIR), Roorkee
DR IRWAD MASOOD( Alternate )
DR IRSHADMASSED Cement Corporation of India, New Delhi
SHRIN. C. JAIN(Alternate )
JOINTDIRECTOR STDS(B&S) (CB-I) Research, Designs & Standards Organization (Ministry of Railways),
Lucknow
JOINTDIRECTOR STDS(B & S) (CB-II) (Alternate )
SHRIN. G. JOSHI Indian Hume Pipes Co Ltd, Mumbai
SI~RIP. D. KELKAR(Alternate )
SHRID. K. KANUNFO National Test House, Caicutta
SHRIB. R. MEENA(Alternote)
SHRIP. KRISHNAMURTHY Larsen and Toubro Limited, Mumbai
SHRIS. CHAKRAVARTHY (Alternate 1)
SHRIC. REDDY(Alternate II )
DR A. G. MADHAVARAO Structural Engineering Research Centre (CSIR). Chennai
SHRIK. MANI ( Alternate )
SHRIG. K. MAJUMDAR Hospital Services Consultancy Corporation (India) Ltd. New Delhi
SHRIJ. SARUP( Alternute )
SIIRIPRAFULLAKUMAR Ministry of Transport, Department of Surface Transport Roads Wing,
New Delhi
SHRIP. P. NAIR ( Alternute )
MEMBERSECRETARY Central Board of Irrigation and Power, New Delhi
DIRECTOR (CIVIL)(Alternute )
SHRI S. K. NATHANI,SO 1 Engineer-in-Chief’s Branch, Army Headquarters, New Delhi
DR A. S. GoE~EE ( Alternate )
SHRIY. R. PHULL Central Road Research Institute (CSIR), New Delhi
StIRIS. S. SEEHRA( Alrernafe )
SHRIY. R. PWLL Indian Roads Congress, New Delhi
SHRIA. K. SHARMA( Alternute )
DR C. RAJKUMAR National Council for Cement and Building Materials, New Delhi
DR S. C. AHLUWALIA(Alternate)
SNRIG. RAMDAS Directorate General of Supplies and Disposals, New Delhi
SHRIR. C. SHARMA( Alternute )
SHRIS. A. REDDI Gammon India Ltd. Mumbai
REPRESENTATIVE Builder’s Association of India, Mumbai
SI-~RI
J. S. SANGANERIA Geological Survey of India, Calcutta
SHRIL. N. AGARWAL( A/tern&e )
(Continued on page 7)
6
IS 4031( Part 2 ) : 1999
(Continued.from page 6)
Members Representing
SHRIS. B. Sum Central Soil and Materials Research Station, New Delhi
SHRIN. CHANDRASEKARAN
( Alternate )
SUFTDGENGINEER(DESIGN) Public Works Department, Govt of Tamil Nadu, Chennai
EXECUTIVE (S.M.R. DIVISION)(Alternate )
SHRIA. K. CHADHA Hindustan Prefab Ltd. New Delhi
SHRIJ. R. SIL (Alternate )
DR H. C. VISVE.WARAYA The Institution of Engineers (India), Calcutta
SHRID. C. CHATURVEDI( Alternate )
SHRI VINOD KUMAR. Director General, BIS (Ex-officio Member)
Director (Civ Engg)
Member Secretary
SHRI J. K. PRASAD
Additional Director (Civ Engg), BIS
7
Bureau of Indian Standards
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harmonious development of the activities of star ‘ardization, marking and quality certification of goods and
attending to connected matters in the country.
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Enquiries relating to copyright be addressed to the Director (Publication), BIS.
Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed
periodically; a standard along with amendments is reaffirmed when such review indicates that no changes are
needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards
should ascertain that they are in possession of the latest amendments or edition by referring to the latest issue
of ‘BIS Handbook’ and ‘Standards Monthly Addition..’
This Indian Standard has been developed from Dot: No. CED 2 ( 5171 ),
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