Modelling and Simulation of Rougher Flotation Circuits
Modelling and Simulation of Rougher Flotation Circuits
Automation and Supervision Centre for the Mining Industry, CASIM, Chemical and Environmental Engineering Department, Federico Santa Mara Technical University, Valparaso, Chile
Divisin El Teniente, Codelco, Rancagua, Chile
a r t i c l e
i n f o
Article history:
Received 7 June 2011
Received in revised form 9 June 2012
Accepted 14 June 2012
Available online 21 June 2012
Keywords:
Flotation
Modelling
Simulation
Rougher cells
a b s t r a c t
At present, large mechanical otation cells of 100 to 300 m3 are used in rougher operation in different industrial otation plants around the world. However, in spite of the advances in fundamental research and the
notable growth in equipment size, there is still a lack of reliable data for industrial otation modelling and
simulation. In this work, a procedure for modelling and simulating rougher otation banks that is based on
operating variables and parameters tted by empirical data from plant measurements is presented.
Recently, a new methodology for describing industrial otation by separating the collection and froth zones
has been developed. This approach consists of using a new apparatus for direct bubble load measurement
below the pulpfroth interface in industrial cells. The procedure allows independently estimating the froth
recovery and the collection zone recovery. Metallurgical characterisation is developed by plant sampling,
mass balance adjustment and applying a short-cut method for kinetic characterisation of otation banks. In
addition, the effect of grinding is characterised using otation models with distributed otation rates (for
each particle size class) and a low number of parameters.
From the experimental data, a non-linear distributed model to simulate rougher otation banks was developed, which allows describing the industrial operation as a function of the main operating variables
(e.g., mass ow rate, solid percentage, grinding degree, pulp level and supercial air rate). The simulator
was calibrated and validated using experimental data from the rougher operation at El Teniente Division,
Codelco-Chile.
The new approach is a practical tool that is useful for otation operation diagnosis, for robust design and
analysis of new control and optimisation strategies and for evaluation of the effect that design and operating
variables have upon the collection and froth zone performance in large otation cells. This methodology can
be applied to other otation operations, such as cleaner and scavenger circuits that use mechanical otation
cells.
2012 Elsevier B.V. All rights reserved.
1. Introduction
Two types of mechanical otation cells are employed in industrial
applications: self-aspirated and forced-air otation cells. The main
differences between the cells are the type and location of the rotor
and the mechanism used for the air input. In self-aspirated cells, the
rotor is located near the top of the cell, whereas in forced-air cells,
the rotor is located near the bottom.
Mechanical cell designs have included some modications, such as
the use of froth-crowders and internal radial launders. These modications have been focused on improving the froth transport and consequently the mineral recovery.
The minimum number of cells per bank can be estimated from a
hydrodynamic analysis assuming perfectly mixed cells. For example,
it has been observed that when using four or more cells in series,
Corresponding author.
E-mail address: [email protected] (J. Yianatos).
0301-7516/$ see front matter 2012 Elsevier B.V. All rights reserved.
doi:10.1016/j.minpro.2012.06.005
64
RC RF
1RC 1RF
0 0
exptP =S exptP = L
S P
where L is the mean residence time of the large tank, S is the mean
residence time of the small tank and p is the dead time. In addition,
the ratio S/L is usually close to 0.1 in mechanical cells (Yianatos et
al., 2005). Eq. (3) was considered for the simulator implementation.
65
Fig. 1 shows good agreement between the LSTS model and the experimental data recorded in a Wemco cell of 130 m 3.
2.1.2. Flotation rate distribution, F(k)
Several models have been proposed in order to evaluate the
otation rate distribution in otation cells. The Dirac delta function, (k kB), and rectangular models correspond to single parameter models, where (k kB) represents a single otation
rate constant, kB.
The rectangular model for the i-th size class (+100#, 100+ 325#,
325#, where # means mesh) and for the n-th cell, given by Eq. (4), was
used for simulating the otation rate distribution in a distributed manner
n
because of its exibility and low number of parameters, kmax,i
.
n
F i k
8
<
1
knmax;i
:
0
; if
0bkbknmax;i
; if
k > knmax;i
4
Fig. 2. Recovery prediction model for batch tests.
Then, the mineral recovery in the collection zone of class i and cell
n
n,RCi
, was calculated by means of Eq. (5):
n
RC;i RC
MAX;i
kt
n
Et F i kdt dk
1e
0 0
where RnC MAX,i is the maximum collection zone recovery of the i-th class
in the n-th cell. Notice that because of the amount of valuable mineral
decreases along the otation bank, the maximum recovery value in
each size class (i.e., ne, intermediate and coarse) also decreases. If
this change is not taken into account, the otation rate distribution
in each cell will be hindered by the variation of RnC MAX,i.
Therefore, the valuable mineral was described by a fraction with a
probability (> 0) of being oated and a non-oatable fraction. Thus,
the amount of oatable, valuable and non-valuable material feeding
a single cell in a bank was obtained from a mass balance in the previous cell, where the recoveries were known. To estimate the maximum recovery of the raw material entering the rougher circuit,
batch tests for each size class were carried out using the same feed
samples from the mass balance measurements. Fig. 2 shows a batch
test result along with the RMAX estimation per size class.
The same residence time distribution was considered in Eq. (5) for
each size class because the empirical data showed no signicant differences in the mean residence time and the distribution shape.
Samples for the mass balances per size class were obtained for a
complete description of the rst 3 cells and the overall bank. The results for the global and froth recovery in each cell allowed estimating
Fig. 1. Model t to industrial data (non-oatable tracer), L = 5.5 min, S = 0.5 min,
p = 0.8 min.
knmax;i
k1max;i
n1
exp
i
Eq. (6) allows obtaining the rectangular model parameters for the
n-th cell as a function of the rst one. The i parameter depends on
the characteristic size of the i-th size class, and is a t parameter.
Fig. 3 shows a comparison between the proposed model and the
plant data in three size classes for a chalcopyrite mineral.
2.2. Cleaning zone, RF
The cleaning zone was characterised by means of the froth recovery, which can be estimated from bubble load measurement along
Fig. 3. Plant data and model describing changes in the collection rate along the otation
bank.
66
with a mass balance around the cell. Thus, the froth recovery, RF, was
calculated by Eq. (7) (Yianatos et al., 2008b):
C X C
RF
B J G AC X B
H F;n G
JG
where HF,n is the froth height and G is the mean gas concentration
(hold-up) in the froth.
The empirical evidence showed that the froth stability of each cell
downstream from the bank is reduced, i.e., the froth selectivity
increases along the cells arrangement. Therefore, the n parameter
in Eq. (8) was modelled as follows:
n Mn RC;n :
where B is the bubble load, JG is the supercial gas rate, AC the crosssectional area of the cell, C is the solid mass ow in the concentrate
and XC and XB are the concentrate and bubble load grade,
respectively.
It has been shown that Eq. (7) is useful for calculating the froth
recovery and the valuable minerals collected by true otation
from experimental data (Yianatos et al., 2008b). In addition, Eq. (8)
is usually employed for modelling the froth zone (Gorain et al.,
1998; Mathe et al., 1998; Zheng et al., 2004).
RF;n exp n F;n
10
where Mn is the amount of valuable mineral entering the n-th cell, RC,
n is the overall recovery of the collection zone and is a t parameter.
Notice that MnRC, n corresponds to the overall amount of valuable
mineral entering the froth zone by true otation.
Fig. 4 shows the Cu grade of the bubble load and at the top of froth
in a single cell, for different size classes. Based on these results, a
rather non-selective froth was observed, which is consistent with the results reported by Yianatos et al., 2008b. Therefore, the same froth
recovery per size class was assumed.
WC
WF
11
F;n n
JG
12
where is the maximum water recovery, and and are t parameters. Notice that Eq. (12) is similar to the froth recovery relationship
in Eq. (8). In addition, this equation considers the inuence of the
froth behaviour in the water recovery as a distributed system.
2.4. Gangue recovery
The gangue is recovered into the concentrate by entrainment caused by the water reported to the concentrate stream. The gangue ren
covered per size class in the n-th cell, RG,i
, was estimated by means of
Eq. (13) (Yianatos and Contreras, 2010).
n
RG;i EF i RW;n
13
where EFi is the entrainment factor per size class. The gangue recovery
per size class can then be obtained from RW measurements and
empirical EFi values.
3. Single-cell simulation
In order to evaluate the contribution of each individual cell in the
otation bank recovery, the collection zone recovery by true otation,
RC, the froth recovery of oatable minerals, RF, the water recovery, RW,
and the gangue recovery, RG, were calculated for each cell. In addition,
the mass ow rate of water and solids per size class in the tailings of
each cell were obtained by means of a mass balance.
The global recovery of mineral m, size class i, in cell n is given by
m
Ri;n
RC;i :RF;i
1RC;i RC;i :RF;i
14
C;m
X i;n
2
P
3
P
m1 i1
Fig. 4. Comparison between Cu grade in the bubble load (CB) and at the top of froth (TOF).
15
m
F i;n X F;m
i;n Ri;n
67
4. Summary
The general procedure for developing and calibration of the simulator includes the following steps:
i) Sampling the rst, second and third cells of the bank together
with sampling the otation bank as a whole.
ii) Characterise the streams in terms of solid percentage by
weight, and mass and grades (Cu, Mo and Fe) per size class.
iii) Carry out mass balance adjustment per size class and estimate
mineral recoveries.
iv) Using the feed sample, conduct batch test to determine the
RMAX values per size class.
v) Estimate froth recovery, Eq. (7), using the measured values of
XC, XB, B and JG. The adjusted value of concentrate C and the
cross sectional area is also required.
vi) Using results from steps iii) and v), obtain the collection zone
recovery per size class from Eq. (1).
vii) Estimate the otation rate parameters per size classes from
Eq. (5) based on the RTD model, the distributed RMAX,i n along
the bank per size class and the collection zone recovery results
from step vi).
viii) Characterise the decrease of the otation rate distribution per
size class along the rougher bank using Eq. (6).
ix) From Eqs. (8), (9) and (10) and results from step v), determine
the froth recovery parameter using HF, n, G and JG data along
the bank together with the amount of valuable mineral entering the froth by true otation. An value of 92% was assumed
in Eq. (8).
x) Estimate gangue recovery from water recovery. First, obtain
water recovery using the mass balance results together with
the solid percentage by weight. Second, estimate parameters
of Eq. (12) using the JG, and HF, n, and n values along the
bank. Determine gangue recovery from mass balances and
bubble load measurements (Yianatos and Contreras, 2010)
and estimate EFi factors per size class.
xi) Based on the previously adjusted parameters (by regression),
Eqs. (3) to (13), the overall mineral recovery and the concentrate
grade can be computed from Eqs. (14) and (15), respectively.
The rougher otation circuit (SAG plant) at El Teniente, CodelcoChile, was considered. The rougher circuit consists of four banks
with seven self-aspirated Wemco cells (130 m 3) in series, in a 1-22-2 array.
For the simulator calibration, measurements of feed, tail and concentrate grades per size class, supercial gas rate, bubble load, solid
percentage, gas hold-up, residence time distribution and froth depth
proles along the rougher bank were carried out in the rougher otation SAG plant (Carrasco, 2010). These results allowed obtaining the
simulator parameters as well as to validate them. Table 1 shows the
simulation results for Cu performance corresponding to a feed tonnage of 900 tph, a feed grade of 1%, a solid percentage by weight of
42% and 18% particle size (% + 100#) in a rougher bank.
Table 2 presents a comparison between the simulator outputs
based on operational parameters and plant results for two tests conducted in the rougher bank. The operational parameters of Test 1
were as follows: feed tonnage 790 tph, Cu feed grade 0.99%, Mo
feed grade 0.021%, Fe feed grade 5.0%, percentage + 100# 19.8%,
solids percentage by weight 41.5% and froth height (rst cell) 5 cm.
For Test 2, the operational parameters were: feed tonnage 650 tph,
Cu feed grade 0.95%, Mo feed grade 0.020%, Fe feed grade 5.5%, percentage +100# 22.0%, solids percentage by weight 40.0% and froth
height (rst cell) 3 cm. A reasonable agreement between the simulated data and the plant performance was observed.
5.2. Sensitivity analysis
For visualisation of the simulation responses, a sensitivity analysis
for different operating conditions was carried out. The main variables
for this analysis were particle size distribution (PSD), froth depth in
the rst cell of the bank, feed tonnage, feed grade and solid percentage. These variables are interesting for control purposes because of
the economic impact in terms of mineral recovery and concentrate
grade in industrial otation banks.
5.2.1. Effect of particle size distribution (PSD)
The effect of changes in the PSD on the cumulative Cu recovery
and the incremental grade along the otation bank was studied. The
Table 2
Comparison between plant performance and simulation results.
Test 1
Rougher recovery %
Final concentrate
07/12/2009
Cu
Mo
Cu grade %
Mo grade %
Solid %
Cu/Fe ratio
% 325 #
Plant data
Simulation
% Error
90.8
91.0
0.2
80.00
83.76
4.7
5.5
5.3
3.6
0.09
0.084
6.7
27.2
27.1
0.4
0.63
0.64
1.6
69.8
69.2
0.9
Test 2
Rougher recovery %
Final concentrate
14/12/2009
Cu
Mo
Cu grade %
Mo grade %
Solid %
Cu/Fe ratio
% 325 #
Plant data
Simulation
Error (%)
91.2
91.6
0.4
81.0
83.4
3.0
5.00
5.03
0.6
0.071
0.070
1.4
24.5
25.3
3.3
0.61
0.60
1.6
67.4
66.9
0.7
68
Fig. 5. Comparison of (a) the cumulative Cu recovery and (b) the incremental Cu grade
as a function of the coarser feed content.
Fig. 6. Effect of froth depth change in the rst cell on (a) the cumulative Cu recovery
and (b) the incremental Cu grade.
Fig. 7. Effect of feed tonnage change on (a) the cumulative Cu recovery and (b) the
incremental Cu grade.
69
Fig. 8. Comparison of (a) the cumulative Cu recovery and (b) the incremental Cu grade
as a function of the feed grade.
70
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