ASTM D-2513 - 04 Thermoplastic Gas Pressure Pipe, Tubing, and Fittings PDF
ASTM D-2513 - 04 Thermoplastic Gas Pressure Pipe, Tubing, and Fittings PDF
Designation: D 2513 04
1. Scope
1.1 This specification covers requirements and test methods
for material (see Appendix X1) dimensions and tolerances,
hydrostatic burst strength, chemical resistance, and impact
resistance of plastic pipe, tubing, and fittings for use in fuel gas
mains and services for direct burial and reliner applications.
The annexes provide specific requirements and test methods
for each of the materials currently approved. If and when
additional materials are available, specific annex requirements
will be added. The pipe and fittings covered by this specification are intended for use in the distribution of natural gas.
Requirements for the qualifying of polyethylene systems for
use with liquefied petroleum gas are covered in Annex A1.
1.1.1 This specification does not cover threaded pipe. Design considerations are discussed in Appendix X2. In-plant
quality control programs are specified in Annex A3 and Annex
A4.
1.2 The text of this specification references notes, footnotes,
and appendixes which provide explanatory material. These
notes and footnotes (excluding those in tables and figures) shall
not be considered as requirements of the specification.
1.3 The values stated in inch-pound units are to be regarded
as the standard. The values given in parentheses are provided
for information purposes only.
1.4 The following is an index of the annexes and appendixes
in this specification:
Subject
Polyethylene (PE) Pipe and Fittings
Poly (Vinyl Chloride) (PVC) Pipe and Fittings for Maintenance or
Repair
A3
In-Plant Quality Control for all materials up to 12 in.
A4
In-Plant Quality Control for PE materials between 14 and 24 in.
A5
Polyamide (PA) Pipe and Fittings
A6
Magnetic-detectable Polyethylene Pipe
A7
Crosslinked Polyethylene (PEX) Pipe
Appendixes
Subject
X1
New Materials
X2
Design Consideration
X3
Gas Pressure Pipe and Fittings Produced from Polyethylene (PE)
materials with Minimum Required Strength (MRS) Designation
2. Referenced Documents
2.1 ASTM Standards: 2
2.1.1 Terminology:
D 1600 for Abbreviated Terms Relating to Plastics
F 412 Relating to Plastic Piping Systems
2.1.2 Test Methods for:
D 638 Tensile Properties of Plastics
D 1238 Melt Flow Rates of Thermoplastics by Extrusion
Plastometer
D 1598 Time-to-Failure of Plastic Pipe Under Constant
Internal Pressure
D 1599 Resistance to Short-Time Hydraulic Pressure of
Plastic Pipe, Tubing, and Fittings
D 2122 Determining Dimensions of Thermoplastic Pipe
and Fittings
D 2290 Apparent Hoop Tensile Strength of Plastic or Reinforced Plastic Pipe by Split Disk Method
D 2837 Obtaining Hydrostatic Design Basis for Thermoplastic Pipe Materials
F 1473 Notch Tensile Test to Measure the Resistance to
Slow Crack Growth of Polyethylene Pipes and Resins
2.1.3 Practices for:
D 543 Evaluating the Resistance of Plastics to Chemical
Reagents
D 618 Conditioning Plastics for Testing
D 1898 Sampling of Plastics
D 2657 Heat Fusion Joining of Polyolefin Pipe and Fittings
D 2774 Underground Installation of Thermoplastic Pressure
Piping
1
This specification is under the jurisdiction of ASTM Committee F17 on Plastic
Piping Systems and is the direct responsibility of Subcommittee F17.60 on Gas.
Current edition approved Jan. 1, 2004. Published February 2004. Originally
approved in 1966. Last previous edition approved in 2003 as D 2513 03b.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at [email protected]. For Annual Book of ASTM
Standards volume information, refer to the standards Document Summary page on
the ASTM website.
Annex
A1
A2
Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D 2513 04
with a 630 psi design stress for water at 73.4F (23C). The
hydrostatic design stresses for gas are not used in this designation code.
3.7 thermoplastic pipe dimension ratio (DR)the ratio of
pipe diameter to wall thickness. It is calculated by dividing the
specified outside diameter of the pipe, in inches, by the
minimum specified wall thickness, in inches. The standard
dimension ratio (SDR) is a common numbering system which
is derived from the ANSI preferred number series R 10.
3.8 toe-ina small reduction of the outside diameter at the
cut end of a length of thermoplastic pipe.
4. Materials
4.1 GeneralThe plastic used to make pipe and fittings
shall be virgin plastic or reworked plastic (see 4.2) as specified
in the Annexes and shall have a Plastics Pipe Institute (PPI)
long-term hydrostatic design stress and hydrostatic design
basis rating.
4.2 Rework MaterialClean rework material of the same
commercial designation, generated from the manufacturers
own pipe and fitting production shall not be used unless the
pipe and fitting produced meet all the requirements of this
specification.
NOTE 1References and material descriptions for ABS, CAB, PB,
PE2306, PE3306 and PE3406 have been removed from D 2513. Elimination of these materials does not affect the pipelines that are in service.
They can still be used for gas distribution. The main reason for removing
these materials from this standard is to reflect the current state of the art
in gas distribution plastic piping.
3. Terminology
3.1 DefinitionsDefinitions are in accordance with Terminology F 412, and abbreviations are in accordance with Terminology D 1600, unless otherwise specified.
3.2 The gas industry terminology used in this specification
is in accordance with ANSI B31.8 or 49 CFR Part 192, unless
otherwise indicated.
3.3 The term pipe used herein refers to both pipe and tubing
unless specifically stated otherwise.
3.4 re-rounding equipmentequipment used to reform the
pipe and permanently reduce ovality to 5% or less.
3.5 rounding equipmentequipment, devices, clamps, and
so forth, used to temporarily hold the pipe round while
out-of-roundness measurements are made, or a joining procedure (heat fusion, electrofusion, or mechanical) is performed.
3.6 standard thermoplastic material designated codethe
pipe material designation code shall consist of the abbreviation
for the type of plastic (PE, PVC, or PA) followed by Arabic
numerals which describe the short term properties in accordance with applicable ASTM standards, the hydrostatic design
stress for water at 73.4F (23C) in units of 100 psi with any
decimal figures dropped. Where the hydrostatic design stress
code contains less than two figures, a zero is used before the
number. Thus, a complete material designation code shall
consist of two or three letters and four figures for plastic pipe
materials. For example, PE 2406 is a grade P24 polyethylene
5. Requirements
5.1 GeneralSee the annexes for specific product requirements in addition to the following. Pipe shall be supplied in
either coils or straight lengths. Any pipe supplied in coils must
meet the same requirements before and after coiling.
5.2 WorkmanshipThe pipe and fittings shall be homogeneous throughout and free of visible cracks, holes, foreign
inclusion, blisters, and dents, or other injurious defects. The
pipe and fittings shall be as uniform as commercially practicable in color, opacity, density, and other physical properties.
5.3 Pipe and Tubing Dimensions and Tolerances:
5.3.1 DimensionThe dimensions shall be specified by
wall thickness and outside diameter.
5.3.1.1 DiametersThe outside diameter shall meet the
requirements given in Table 1 or Table 2 when measured in
accordance with 6.5.
5.3.1.2 Toe-InWhen measured in accordance with 6.5.1.1,
the outside diameter at the cut end of the pipe shall not be more
than 1.5 % smaller than the undistorted outside diameter.
Measurement of the undistorted outside diameter shall be made
no closer than 1.5 pipe diameters or 11.8 in. (300 mm),
whichever distance is less, from the cut end of the pipe.
Undistorted outside diameter shall meet the requirements of
Table 1 or Table 2.
5.3.1.3 Wall ThicknessThe wall thickness shall be as
specified in Table 2 or Table 3 when measured in accordance
with 6.5.1.2. The minimum wall thickness at any point of
measurement shall be not less than the minimum wall thickness
specified in Table 2 or Table 3.
3
Available from American National Standards Institute, 1430 Broadway, New
York, NY 10018.
4
Available from Standardization Documents Order Desk, Bldg. 4 Section D, 700
Robbins Ave., Philadelphia, PA 19111 5094, Attn: NPODS.
5
National Fire Protection Association, 470 Atlantic Avenue, Boston, MA 02210.
6
Plastic Pipe Institute, Inc., 1825 Connecticut Avenue NW, Suite 680, Washington, DC 20009
D 2513 04
TABLE 1 Outside Diameters and Tolerances for Plastic Pipe, in. (mm)
Maximum Out-of-Roundness
Nominal
Pipe
Size
Outside Diameter
1
114
112
2
212
3
312
4
5
6
8
10
12
0.840 (21.3)
1.050 (26.7)
1.315 (33.4)
1.660 (42.1)
1.900 (48.3)
2.375 (60.3)
2.875 (73.0)
3.500 (88.9)
4.000 (101.6)
4.500 (114.3)
5.563 (141.3)
6.625 (168.3)
8.625 (219.1)
10.750 (273.0)
12.750 (323.8)
12
34
Tolerance
60.004 (60.102)
60.004 (60.102)
60.005 (60.127)
60.005 (60.127)
60.006 (60.152)
60.006 (60.152)
60.007 (60.179)
60.008 (60.203)
60.008 (60.203)
60.009 (60.229)
60.010 (60.254)
60.011 (60.279)
60.013 (60.330)
60.015 (60.381)
60.017 (60.432)
SDR 32.5
...
...
...
...
...
...
...
...
...
...
...
0.12(3)
0.24(6.1)
0.24(6.1)
0.28(7.12)
12
12
12
34
34
34
1
1
1
1
1
114
114
114
134
14
38
Outside
Diameter
0.375
0.500
0.625
0.625
0.625
0.875
0.875
0.875
1.125
1.125
1.125
1.125
1.125
1.375
1.375
1.375
1.875
(9.52)
(12.7)
(15.9)
(15.9)
(15.9)
(22.2)
(22.2)
(22.2)
(28.6)
(28.6)
(28.6)
(28.6)
(28.6)
(34.9)
(34.9)
(34.9)
(47.6)
Tolerance
60.004
60.004
60.004
60.004
60.004
60.004
60.004
60.004
60.005
60.005
60.005
60.005
60.005
60.005
60.005
60.005
60.006
(60.10)
(60.10)
(60.10)
(60.10)
(60.10)
(60.10)
(60.10)
(60.10)
(60.13)
(60.13)
(60.13)
(60.13)
(60.13)
(60.13)
(60.13)
(60.13)
(60.15)
Minimum
Wall
Thickness
0.062
0.062
0.062
0.090
0.104
0.062
0.077
0.090
0.062
0.090
0.099
0.101
0.121
0.062
0.090
0.121
0.062
(1.58)
(1.58)
(1.58)
(2.27)
(2.64)
(1.58)
(1.95)
(2.27)
(1.58)
(2.27)
(2.51)
(2.56)
(3.07)
(1.58)
(2.27)
(3.07)
(1.58)
SDR 26
SDR 21
SDR 17
SDR 13.5
SDR 11
...
...
...
...
...
...
...
...
...
...
...
0.11(2.74)
0.16(4.06)
0.2(5.08)
0.2(5.08)
0.03(0.762)
0.03(0.762)
0.03(0.762)
0.03(0.762)
0.06(1.524)
0.06(1.524)
0.06(1.524)
0.06(1.524)
0.1(2.5)
0.1(2.5)
0.1(2.5)
0.1(2.5)
0.12(3)
0.14(3.58)
0.14(3.58)
0.016(0.406)
0.02(0.508)
0.02(0.508)
0.024(0.61)
0.024(0.61)
0.024(0.61)
0.03(0.762)
0.03(0.762)
0.03(0.762)
0.03(0.762)
0.06(1.524)
0.07(1.778)
0.08(2.04)
0.1(2.5)
0.1(2.5)
Wall
Thickness
Tolerance
+0.006 (+0.15)
+0.006 (+0.15)
+0.006 (+0.15)
+0.009 (+0.23)
+0.010 (+0.25)
+0.006 (+0.15)
+0.008 (+0.20)
+0.009 (+0.23)
+0.007 (+0.18)
+0.011 (+0.28)
+0.012 (+0.31)
+0.012 (+0.31)
+0.015 (+0.38)
+0.007 (+0.18)
+0.011 (+0.28)
+0.015 (+0.38)
+0.007 (+0.18)
7
The boldface numbers in parentheses refer to the list of references at the end of
this standard.
D 2513 04
be covered in this specification. Users should consult applicable codes for
limitations on pertinent maximum temperatures.
NOTE 6In the absence of an HDB established at the specified
temperature, the HDB of a higher temperature may be used in determining
DRC
Minimum
Tolerance
0.062 (1.58)
0.076 (1.93)
0.090 (2.29)
+0.007 (+0.178)
+0.009 (+0.229)
+0.011 (+0.279)
0.090 (2.29)
0.095 (2.41)
0.113 (2.87)
+0.011 (+0.279)
+0.011 (+0.279)
+0.014 (+0.356)
0.090
0.097
0.120
0.133
0.140
(2.29)
(2.46)
(3.05)
(3.38)
(3.56)
+0.011 (+0.279)
+0.012 (+0.305)
+0.014 (+0.356)
+0.016 (+0.406)
+0.017 (+0.432)
0.090
0.098
0.123
0.140
0.151
0.166
0.178
0.277
(2.29)
(2.49)
(3.12)
(3.56)
(3.84)
(4.22)
(4.52)
(7.04)
+0.011 (+0.279)
+0.012 (+0.305)
+0.015 (+0.381)
+0.017 (+0.432)
+0.018 (+0.457)
+0.020 (+0.508)
+0.021 (+0.533)
+0.033 (+0.838)
17
13.5
Sch 40
11
0.090 (2.29)
0.112 (2.85)
0.141 (3.58)
0.145 (3.68)
0.173 (4.39)
+0.011 (+0.279)
+0.013 (+0.330)
+0.017 (+0.432)
+0.017 (+0.432)
+0.021 (+0.533)
21
17
Sch 40
13.5
11
9.33
0.113 (2.87)
0.140 (3.56)
0.154 (3.91)
0.176 (4.47)
0.216 (5.49)
0.255 (6.48)
+0.014
+0.017
+0.018
+0.021
+0.026
+0.031
(+0.356)
(+0.432)
(+0.457)
(+0.533)
(+0.660)
(+0.787)
212
21
17
13.5
11
0.137
0.169
0.213
0.261
(3.48)
(4.29)
(5.41)
(6.63)
+0.016
+0.020
+0.026
+0.031
(+0.406)
(+0.508)
(+0.660)
(+0.787)
21
17
Sch 40
13.5
11.5
11
9.33
0.167
0.206
0.216
0.259
0.304
0.318
0.375
(4.24)
(5.23)
(5.49)
(6.58)
(7.72)
(8.08)
(9.53)
+0.020
+0.025
+0.026
+0.031
+0.036
+0.038
+0.045
(+0.508)
(+0.635)
(+0.660)
(+0.787)
(+0.914)
(+0.965)
(+1.143)
312
21
17
13.5
11
21
19
17
13.5
11.5
11.0
9.33
0.190
0.236
0.296
0.363
0.214
0.237
0.265
0.333
0.391
0.409
0.482
(4.83)
(5.99)
(7.52)
(9.22)
(5.44)
(6.02)
(6.73)
(8.46)
(9.93)
(10.39)
(12.24)
+0.023 (+0.584)
+0.028 (+0.711)
+0.036 (+0.914)
+0.044 (+1.118)
+0.026 (+0.660)
+0.028 (+0.711)
+0.032 (+0.813)
+0.040 (+1.016)
+0.047 (+1.194)
+0.049 (+1.246)
+0.058 (+1.473)
21.6
21
17
13.5
11
0.258
0.265
0.327
0.412
0.506
(6.55)
(6.73)
(8.31)
(10.46)
(12.85)
+0.031
+0.032
+0.039
+0.050
+0.061
12
11.0
9.33
34
11.0
Sch 40
1
13.5
11.0
9.9
9.33
114
17.0
13.5
Sch 40
11.0
10.0
9.33
6.0
112
(+0.787)
(+0.813)
(+0.991)
(+1.270)
(+1.549)
D 2513 04
TABLE 3 Continued
DRC
Minimum
32.5
26
23.7
21
17
13.5
11.5
11.0
0.204 (5.18)
0.255 (6.48)
0.280 (7.11)
0.315 (8.00)
0.390 (9.91)
0.491 (12.47)
0.576 (14.63)
0.602 (15.29)
+0.024
+0.031
+0.034
+0.038
+0.047
+0.059
+0.069
+0.072
(+0.610)
(+0.787)
(+0.864)
(+0.965)
(+1.194)
(+1.499)
(+1.753)
(+1.829)
32.5
26
21
17
13.5
11.5
11
0.265 (6.73)
0.332 (8.43)
0.411 (10.44)
0.507 (12.90)
0.639 (16.23)
0.750 (19.05)
0.784 (19.91)
+0.032
+0.040
+0.049
+0.061
+0.077
+0.090
+0.094
(+0.813)
(+1.016)
(+1.245)
(+1.549)
(+1.956)
(+2.286)
(+2.388)
10
32.5
26
21
17
13.5
11.5
11
0.331
0.413
0.512
0.632
0.796
0.935
0.977
(8.41)
(10.49)
(13.00)
(16.05)
(20.22)
(23.75)
(24.82)
+0.040 (+1.016)
+0.050 (+1.270)
+0.061 (+1.549)
+0.076 (+1.930)
+0.096 (+2.438)
+0.112 (+2.845)
+0.117 (+2.972)
12
32.5
26
21
17
13.5
11.5
11
0.392
0.490
0.607
0.750
0.944
1.109
1.159
(9.96)
(12.45)
(15.42)
(19.05)
(23.98)
(28.17)
(29.44)
+0.047 (+1.194)
+0.059 (+1.499)
+0.073 (+1.854)
+0.090 (+2.286)
+0.113 (+2.870)
+0.133 (+3.378)
+0.139 (+3.531)
Tolerance
The sizes listed in Table 3 are those commercially available sizes used by the gas industry.
The minimum is the lowest wall thickness of the pipe at any cross section. The maximum permitted wall thickness, at any cross section, is the minimum wall thickness
plus the stated tolerance. All tolerances are on the plus side of the minimum requirement.
C
The DR shown are designations commonly accepted by the gas industry and do not calculate exactly.
These wall thicknesses are minimum and are not a function of the dimension ratios.
Test Method
A
100 (38)
B
120 (49)
C
140 (60)
Category
D
160 (71)
E
F
Temperature,
...
180 (82)
...
F (C)
Hydrostatic
D 2837
400 (2.8)
500 (3.4)
630 (4.3)
800 (5.5)
1000 (6.9)
1250 (8.6)
Design
Basis, psi
(MPa)
C
D 1238
>0.5
0.20.5
0.010.3
<0.01B
...
Melt IndexA
Examples: CDB - At 140F (60C) the HDB is 800 psi (5.5 MPa). The approximate melt index range is 0.2 to 0.5 g/10 min for this PE pipe.
A
DF - At 160F (71C) the HDB is 1250 psi (8.6 MPa) .
G
...
1600 (11.0)
...
A
The melt Index information in this table is intended to provide guidance relating to heat fusion joining of PE materials, not for classification of materials. This property
is not applicable to non-PE materials or to mechanical fittings. See 7.3.
B
Typically melt flow measured under condition 190/21.6 is less than 4.01 g/10 min.
When a PE pipe or fitting is marked per 7.2 or 7.3 with the letter E, it affirms that the manufacturer has verified the applicability of generic fusion joining with their
products in accordance with PPI TR-33 and PPI TR-41 by joining to itself and to other E materials and testing the joints in accordance with applicable regulations.
However, qualification of joining procedures by operators in accordance with applicable regulations may still be required. Information about manufacturers who have
verified PPI TR-33 and PPI TR-41 generic fusion joining with their products is found in PPI TR-33 and PPI TR-41. Consult PPI and the manufacturer for additional
information.
5.7 Minimum Hydrostatic Burst PressureThe burst requirements for plastic pipe shall be as given in the appropriate
annexes.
5.8 Apparent Tensile Strength At Yield The minimum
apparent tensile strengths at yield for plastic pipe are given in
the annexes when determined in accordance with 6.8.
5.9 Joints:
D 2513 04
5.9.2.2 PE butt fusion joining shall be between components
(pipes, fittings, or valves) having the same SDR or DR. Butt
fusion between unlike SDR or DR components shall be
allowed only if it has been demonstrated that long term
performance is not adversely affected. The minimum requirement to demonstrate long term performance shall be the
validation procedure for PE in Test Method D 2837. The
Hydrostatic Design Basis (HDB) of the PE material shall be
validated using specimens containing butt fusion joints resulting from different SDRs or DRs. Pipe/pipe joints of the given
PE material that pass shall validate pipe/pipe, pipe/fitting, or
fitting/fitting joints of the same SDR ratio for that PE material.
5.9.3 MechanicalMechanical fittings shall be installed in
accordance with the users written procedures and the fitting
manufacturers installation instructions. The joint shall be
tested in accordance with the specific design category as
outlined in 6.10.
5.10 Plastic ValvesAll plastic gas valves shall meet the
requirements of ANSI Standard B 16.40.
5.11 Excess Flow ValvesAll excess flow valves shall meet
the requirements of Specification F 2138.
6. Test Methods
6.1 GeneralThe test methods in this specification cover
plastic pipe and fittings to be used for gas distribution. Test
methods that are applicable from other specifications will be
referenced in the paragraph pertaining to that particular test.
6.2 SamplingTake a representative sample of the pipe and
fittings sufficient to determine conformance with this specification. About 40 ft (12 m) of pipe is required to perform all the
tests prescribed. The number of fittings required varies, depending upon the size and type of fitting. A sampling plan shall
be agreed upon by the purchaser and the manufacturer (see
Practice D 1898).
6.2.1 Pipe Test SpecimensNot less than 50 % of the test
specimens required for any pressure test shall have at least a
part of the marking in their central sections. The central section
is that portion of pipe which is at least one pipe diameter away
from an end closure.
6.3 ConditioningUnless otherwise specified, condition
the specimens prior to test at 73.4 6 3.6F (23 6 2C) and 50
6 5 % relative humidity for not less than 40 h, in accordance
with Procedure A of Practice D 618 for those tests where
conditioning is required and in all cases of disagreement.
6.4 Test ConditionsConduct the test in the standard laboratory atmosphere of 73.4 6 3.6F (23 6 2C) and 50 6 5 %
relative humidity, unless otherwise specified.
6.5 Dimensions and Tolerances:
6.5.1 PipeAny length of pipe is used to determine the
dimensions. Coiled pipe shall be measured in the natural
springback condition, unless specified otherwise.
6.5.1.1 DiameterMeasure the diameter of the pipe in
accordance with Test Method D 2122. The average outside
diameter for nonroundable pipe is the arithmetic average of the
maximum and minimum diameters at any cross section on the
length of the pipe. For roundable pipe, out-of-roundness
tolerance applies to measurements made while the pipe is
rounded with the manufacturers recommended equipment.
Measure out-of-roundness within one-half pipe diameter or 2
6.5.1.4 LengthMeasure pipe length and other linear dimensions with a steel tape or other device, accurate to 6132 in.
(61 mm) in 10 ft (3 m).
6.5.2 FittingsMeasure the dimensions of fittings in accordance with Test Method D 2122.
6.5.3 Ovality:
6.5.3.1 ApparatusA micrometer or vernier caliper accurate to within 60.001 in. (60.02 mm).
6.5.3.2 ProcedureTake a series of outside diameter (OD)
measurements at closely spaced intervals around the circumference to ensure that the minimum and maximum diameters
have been determined.
6.5.3.3 CalculationCalculate the percent ovality as follows:
6.5.1.2 Wall ThicknessMake a minimum of six measurements at each cross section in accordance with Test Method
D 2122.
6.5.1.3 Wall Thickness Eccentricity Range Measure in a
manner such that the maximum, A, and the minimum, B, wall
thickness at single points of each cross section measured are
obtained. Calculate the wall thickness eccentricity range, E, in
percent for each cross section as follows:
E 5 [~A 2 B!/A#
3 100
maximum OD 2 minimum OD
ovality 5 minimum OD 1 maximum OD 3 200
(1)
(2)
D 2513 04
6.10.1.1 The apparatus and report shall be as specified in
Test Method D 638. The test shall be conducted at ambient
temperatures, that is, 67 6 10F (19.4 6 5.6C). The speed of
the testing shall be 0.2 in. (5 mm)/min 625 %. Five specimens
shall be prepared following the manufacturers published
installation instructions. Length of the specimens shall be such
that the unreinforced distance between the grip of the apparatus
and the end of the stiffener is at least five times the nominal
outside diameter of the pipe size being tested. Apply a load
until permanent deformation (yield) occurs in the unreinforced
area of the piping.
6.10.1.2 Results obtained from the above method pertain
only to the specific outside diameter, wall thickness, and
compound of the piping used in the test and specific fitting
design tested.
NOTE 9The ability to restrain pipe to its yield as specified above does
not guarantee that a properly installed joint will prevent pullout under
actual long-term field conditions. Joints that cannot pass this test would be
expected to pullout under actual long term field conditions. To date, this
test is the best available for disqualifying unsound joints.
Concentration (% by volume)
100
5 in mineral oil
100
100
15 in methanol
Test five specimens with each chemical. Weigh the specimens to the nearest 0.005 g and completely immerse them in
the chemicals for 72 h. On removal from the chemicals, wipe
the specimens with a clean dry cloth. Condition in air for 2 to
214 h and reweigh. Calculate the increase in weight to the
nearest 0.01 % on the basis of initial weight. Test the specimen
in tension in accordance with 6.8 within 12 h after weighing.
Examine the weight and apparent tensile strength of each
specimen for conformance to the requirement in 5.4.
(WarningBecause of the possible toxicity of these reagents,
refer to the Material Safety Data Sheet on each of these
reagents before using or handling them.)
6.10 Categorization of Mechanical JointsThe following
test methods provide a uniform procedure for qualification or
categorization of mechanical joints using short term pullout
resistance tests and burst tests. The mechanical joint categories
and test methods are as follows:
6.10.1 Category 1A mechanical joint design that provides
a seal plus a resistance to a force on the pipe end equal to or
greater than that which will cause a permanent deformation of
the pipe.
7. Marking
7.1 PipeAll required marking shall be legible, visible,
and permanent. To ensure permanence, marking shall be
applied so it can only be removed by physically removing part
of the pipe wall. The marking shall (1) not reduce the wall
thickness to less than the minimum value for the pipe, (2) not
have any effect on the long-term strength of the pipe, and (3)
not provide leakage channels when elastomeric gasket compression fittings are used to make the joints. These marking
shall consist of the word GAS, the designation ASTM D 2513,
the manufacturers name or trademark, the normal pipe size
including the sizing system used (IPS, CTS, or OD), DR or
minimum wall thickness, material designation, and date of
manufacture.
7.1.1 In addition to 7.1, the pipe marking shall include a
coding that will enable the manufacturer to determine the
location of manufacture, pipe production and resin lots, and
any additional information which is agreed upon between the
7
D 2513 04
manufacturer and purchaser. The manufacturer shall maintain
such records for fifty years or for the design service life of the
pipe, whichever is longer.
7.1.2 All the markings in 7.1 and 7.1.1 shall be repeated at
intervals not exceeding 5 ft (1.5 m). For indented printing,
either the indented print line shall be in a color that contrasts
with that of the pipe, or a separate print line shall be in a color
that contrasts with the pipe. See Annex A1 and Annex A2 for
additional specific marking requirements. When color is applied to identify gas service, such as with color stripes, a color
shell or solid color pipe, yellow color shall be used.
7.2 Pipe intended for natural gas service at elevated temperatures greater than 73F (23C) shall be marked with
additional code letters from Table 4 (the first code letter to
identify the temperature of pressure rating, the second code
letter to identify HDB at highest rated temperature, and the
third code letter to identify the melt index).
NOTE 11The non-mandatory, preferred order for all the items required in the print line in the marking sections 7.1 and 7.2 are:
(1) Pipe size including sizing system (IPS, CTS or OD),
(2) SDR (DR) or minimum wall thickness,
(3) Manufacturers name or trademark,
(4) GAS,
(5) Pipe material designation code,
(6) Elevated temperature code from Table 4,
(7) ASTM D 2513,
8. Quality Assurance
8.1 When the product is marked with this designation,
D 2513, the manufacturer affirms that the product was manufactured, inspected, sampled, and tested in accordance with this
specification and has been found to meet the requirements of
this specification.
SUPPLEMENTARY REQUIREMENTS
GOVERNMENT/MILITARY PROCUREMENT
These requirements apply only to federal/military procurement, not domestic sales or transfers.
S2.1 PackagingUnless otherwise specified in the contract, the materials shall be packaged in accordance with the
suppliers standard practices in a manner ensuring arrival at
destination in satisfactory condition and which will be acceptable to the carrier at lowest rates. Containers and packing shall
comply with Uniform Freight Classification rules or National
Motor Freight Classification rules.
S2.2 MarkingMarking for shipment shall be in accordance with Fed. Std. No. 123 for civil agencies and MIL-STD
129 for military agencies.
S1. Responsibility for InspectionUnless otherwise specified in the contract or purchase order, the producer is responsible for performance of all inspection and test requirements
specified herein. The producer shall use his own or any other
suitable facilities for the performance of the inspection and test
requirements specified herein, unless the purchaser disapproves. The purchaser shall have the right to perform any of the
inspections and tests set forth in this specification where such
inspections are deemed necessary to ensure that material
conforms to prescribed requirements.
NOTE S00001In U.S. federal contracts, the contractor is responsible
for inspection.
NOTE S00002The inclusion of U.S. Government procurement requirements should not be construed as an indication that the U.S.
Government uses or endorses the products described in this specification.
D 2513 04
ANNEXES
(Mandatory Information)
A1. SUPPLEMENTAL REQUIREMENTS FOR GAS PRESSURE PIPE AND FITTINGS PRODUCED FROM
POLYETHYLENE (PE) MATERIAL
TABLE A1.2 Specification D 3350 Cell Classifications of
Polyethylene Pipe and Fittings Materials
A1.1 Scope
A1.1.1 This annex covers requirements for PE pipe and
fittings. These requirements are in addition to those in the main
body of this specification.
8
Available from International Organization for Standardization 1 Rue de
Varemb, Case Postale 56, CH-1211, Geneva 20, Switzerland
14
16
18
20
22
24
14.000
16.000
18.000
20.000
22.000
24.000
(355.6)
(406.4)
(457.2)
(508.0)
(558.8)
(609.6)
3
3, 4, or 5
4 or 5
4 or 5
6
Tolerance
60.063
60.072
60.081
60.090
60.099
60.108
2
1, 2, 3, or 4
3 or 4
3 or 4
6
NOTE A1.2The long-term hydrostatic strength at 50 years in accordance with Test Method D 2837 is not to be used for any pressure rating
calculations. The MAOP is still calculated using the HDB obtained from
Test Method D 2837 long-term hydrostatic strength at 100 000 h.
PE 3408
A1.3 Materials
A1.3.1 ClassificationPolyethylene materials suitable for
use in the manufacture of pipe and fittings under this specification shall be classified in accordance with Specification
D 3350, and as shown in Table A1.2. Example: for a polyethylene material having an HDB of 1250 psi (8.6 MPa), Cell
Nominal
Pipe Size
PE 2406
PE Material
Designation Code
(61.60)
(61.83)
(62.06)
(62.29)
(62.51)
(62.74)
PE 2406
PE 3408
Short-Term
in Accordance
with D 3350
Grade PE 24
Grade PE 34
Long-Term
in Accordance
with D 2837A
HDB of 1250 psi for 73F
HDB of 1600 psi for 73F
A
The hydrostatic design basis (HDB) shall be established using water or natural
gas as the pressurizing fluid.
D 2513 04
A1.5.5 Squeeze-OffThis requirement is limited to pipe
sizes, wall thicknesses, squeeze procedures, and conditions
deemed suitable for squeeze-off in service by the pipe manufacturer. There shall be no leakage or visual evidence of
splitting, cracking, breaking or reduction in 1000-h sustained
pressure category when pipe is tested as follows:
A1.5.5.1 Prepare six randomly selected pipe specimens in
accordance with Test Method D 1598 except they shall be
unfilled.
A1.5.5.2 The squeeze-off shall be effected at the mid-point
of the test specimen, 90 to the point of the measured minimum
wall thickness. Close the squeeze bars to the gap stop in
Specification F 1563 and hold in constraint for 4 h. Remove
squeeze bars and reround pipe by closing squeeze bars at a
point 90 from the squeeze area.
A1.5.5.3 Immediately upon removal of the squeeze-off tool,
fill the specimens with ambient temperature water, that is, 67 6
10F (19.4 6 5.6C), condition, and test in accordance with
6.6.
A1.5.6 Thermal StabilityThe PE material shall contain
sufficient antioxidant so that the minimum induction temperature shall be 428F (220C) when tested in accordance with
Specification D 3350. The sample shall be representative of the
cross section of the pipe or fittings.
A1.5.7 Outdoor Storage StabilityPE pipe stored outdoors
and unprotected for at least two years from date of manufacture
shall meet all the requirements of this specification. PE pipe
stored outdoors for over two years from date of manufacture is
suitable for use if it meets the requirements of this specification.
A1.5.8 Dimensions and TolerancesThe outside diameter
shall meet the requirements in Table 1 and Table 2 in the main
body for sizes through 12 in., or in Table A1.1 for larger sizes
or in Table A1.4 for metric sizes. The wall thickness shall meet
the requirements in Table 2 and Table 3 in the main body for
sizes through 12 in., or in Table A1.5 for larger sizes or in Table
A1.4 for metric sizes. When sizes other than those listed in
these tables are used, the tolerances of the next lower size shall
be used.
A1.5.9 Short Term Pressurization for Sizes Above 12 in.
Pipe and molded or fabricated fittings shall not fail when tested
in accordance with Test Method D 1599 with the hoop stress of
2500 psi for Class 2 density materials or 2900 psi for Class 3
density materials. Hoop stress calculation shall be based on the
DR of the fitting at the point of fusion. (Warning
Pressurization of pipe specimens above 12 in. nominal diameter being tested in accordance with A1.5.8 should not commence until it is certain that all entrapped air has been bled
from the water-filled specimens.)
D 2513 04
TABLE A1.4 Outside Diameter and Wall Thickness for Metric SizesA
Nominal
Size
minimum
Maximum Out of
RoundnessB
maximum
minimum
DR 11 Wall Thickness
maximum
minimum
maximum
mm
mm
(in.)
mm
(in.)
mm
(in.)
mm
(in.)
mm
(in.)
mm
(in.)
mm
(in.)
16
20
25
32
40
50
63
75
90
110
125
140
160
180
200
225
250
280
315
355
400
450
500
560
630
16.0
20.0
25.0
32.0
40.0
50.0
63.0
75.0
90.0
110.0
125.0
140.0
160.0
180.0
200.0
225.0
250.0
280.0
315.0
355.0
400.0
450.0
500.0
560.0
630.0
(0.630)
(0.787)
(0.984)
(1.260)
(1.575)
(1.969)
(2.480)
(2.953)
(3.543)
(4.331)
(4.921)
(5.512)
(6.299)
(7.087)
(7.874)
(8.858)
(9.843)
(11.024)
(12.402)
(13.976)
(15.748)
(17.717)
(19.685)
(22.047)
(24.803)
16.3
20.3
25.3
32.3
40.4
50.4
63.4
75.5
90.6
110.7
125.8
140.9
161.0
181.1
201.2
226.4
251.5
281.7
316.9
357.2
402.4
452.7
503.0
563.4
633.8
(0.642)
(0.799)
(0.996)
(1.272)
(1.591)
(1.984)
(2.496)
(2.972)
(3.567)
(4.358)
(4.953)
(5.547)
(6.339)
(7.130)
(7.921)
(8.913)
(9.902)
(11.091)
(12.476)
(14.063)
(15.843)
(17.823)
(19.803)
(22.181)
(24.953)
1.2
1.2
1.2
1.3
1.4
1.4
1.5
1.6
1.8
2.2
2.5
2.8
3.2
3.6
4.0
4.5
5.0
9.8
11.1
12.5
14.0
15.6
17.5
19.6
22.1
(0.047)
(0.047)
(0.047)
(0.051)
(0.055)
(0.055)
(0.059)
(0.063)
(0.071)
(0.087)
(0.098)
(0.110)
(0.126)
(0.142)
(0.157)
(0.177)
(0.197)
(0.386)
(0.437)
(0.492)
(0.551)
(0.614)
(0.689)
(0.772)
(0.870)
2.3
2.3
2.3
2.3
2.3
2.9
3.6
4.3
5.2
6.3
7.1
8.0
9.1
10.3
11.4
12.8
14.2
15.9
17.9
20.2
22.8
25.6
28.4
31.9
35.8
(0.091)
(0.091)
(0.091)
(0.091)
(0.091)
(0.114)
(0.142)
(0.169)
(0.205)
(0.248)
(0.280)
(0.315)
(0.358)
(0.406)
(0.449)
(0.504)
(0.559)
(0.626)
(0.705)
(0.795)
(0.898)
(1.008)
(1.118)
(1.256)
(1.409)
2.7
2.7
2.7
2.7
2.7
3.3
4.1
4.9
5.9
7.1
8.0
9.0
10.2
11.5
12.7
14.2
15.8
17.6
19.8
22.4
25.2
28.3
31.4
35.2
39.5
(0.106)
(0.106)
(0.106)
(0.106)
(0.106)
(0.130)
(0.161)
(0.193)
(0.232)
(0.280)
(0.315)
(0.354)
(0.402)
(0.453)
(0.500)
(0.599)
(0.622)
(0.693)
(0.780)
(0.822)
(0.922)
(1.114)
(1.236)
(1.386)
(1.555)
3.0
3.0
3.0
3.0
3.7
4.6
5.8
6.8
8.2
10.0
11.4
12.7
14.6
16.4
18.2
20.5
22.7
25.4
28.6
32.2
36.4
40.9
45.5
50.9
57.3
(0.118)
(0.118)
(0.118)
(0.118)
(0.146)
(0.181)
(0.228)
(0.268)
(0.323)
(0.394)
(0.449)
(0.500)
(0.575)
(0.646)
(0.717)
(0.807)
(0.894)
(1.000)
(1.126)
(1.268)
(1.433)
(1.610)
(1.791)
(2.004)
(2.256)
3.5
3.5
3.5
3.5
4.2
5.2
6.5
7.6
9.2
11.2
12.7
14.1
16.2
18.2
20.2
22.7
26.1
28.1
31.6
35.6
40.2
45.1
50.2
56.1
63.1
(0.138)
(0.138)
(0.138)
(0.138)
(0.165)
(0.205)
(0.256)
(0.299)
(0.362)
(0.441)
(0.500)
(0.555)
(0.638)
(0.717)
(0.795)
(0.894)
(1.028)
(1.106)
(1.244)
(1.402)
(1.583)
(1.776)
(1.976)
(2.209)
(2.484)
Outside Diameter and maximum out of roundness are in accordance with ISO 4437. Wall thickness is in accordance with ISO 4437 and ISO 119221.
Maximum out of roundness applies to straight pipe and pipe prior to coiling for sizes that are packages in coils. Measure out of roundness in accordance with 6.5.1.1
but without rounding equipment applied. See 5.3.1.5 for ovality.
B
TABLE A1.5 Minimum Wall Thickness and Tolerance, 14 in. and Larger Pipe, in.
Nominal
Pipe
Size
14
16
18
20
22
24
SDR
32.5
SDR
26
SDR
21
SDR
17
DR
15.5
SDR
13.5
SDR
11
SDR
9
SDR
7.3
0.431
+0.052
0.492
+0.059
0.554
+0.066
0.615
+0.074
0.677
+0.081
0.738
+0.089
0.538
+0.065
0.615
+0.074
0.692
+0.083
0.769
+0.092
0.846
+0.102
0.923
+0.111
0.667
+0.080
0.762
+0.091
0.857
+0.103
0.952
+0.114
1.048
+0.126
1.143
+1.137
0.824
+0.099
0.941
+0.113
1.059
+0.127
1.176
+0.141
1.294
+0.155
1.412
+0.169
0.903
+0.108
1.032
+0.124
1.161
+0.139
1.290
+0.155
1.419
+0.170
1.548
+0.186
1.037
+0.124
1.185
+0.142
1.333
+0.160
1.481
+0.178
1.630
+0.196
1.778
+0.213
1.273
+0.153
1.455
+0.175
1.636
+0.196
1.818
+0.218
2.000
+0.240
2.182
+0.262
1.556
+0.187
1.778
+0.213
2.000
+0.240
...
1.918
+0.230
...
...
...
...
...
...
...
NOTE A1.6The ring may be tested in its entirety, or may be cut into
representative sectors to produce bend-back test specimens.
11
D 2513 04
protrude 1 to 114 in. (25 to 32 mm) or two wall thicknesses,
whichever is greater, above the point of closure (jaws). (c) With
the unaided (naked) eye, visually examine the protruding
reverse-bent pipe ID surface for signs of brittle cracking or
crazing.
(3) Any indication of brittle cracking or crazing indicates
failure.
A1.5.11.2 Elongation-at-Break Test Method:
(1) Five Test Method D 638 Type IV specimens cut in the
longitudinal direction from locations equally spaced around the
circumference of the pipe shall be tested in accordance with
Test Method D 638 at a cross-head separation speed of 2 in.
(50.8 mm) min, and at 73.4 6 3.6F (23 6 2C). If the
specimen thickness must be reduced by machining, the pipe ID
surface shall be left unaltered.
A2. SUPPLEMENTAL REQUIREMENTS FOR GAS PRESSURE PIPE AND FITTINGS PRODUCED FROM POLY
(VINYL CHLORIDE) (PVC) COMPOUNDS FOR MAINTENANCE OR REPAIR
A2.1 Scope
A2.1.1 This annex covers requirements for PVC pipe for
use only to maintain or repair existing PVC gas piping. These
requirements are in addition to those in the main body of this
specification. All PVC pipe for gas shall be marked per 7.1 (the
words GAS and ASTM D 2513 on pipe, etc.) and A2.4.1.7.
A2.1.2 This annex covers requirements for PVC fittings for
use to maintain or repair exisiting gas piping. These requirements are in addition to those in the main body of this
specification. All PVC fittings for gas shall be marked per 7.2
(the words ASTM D 2513 on fittings, etc.).
D 2513 04
TABLE A2.1 Impact Requirements for PVC Pipe at 32 to 35F (0
to 2C) for SDR 17 and 21 Pipe
Impact
Classification
Cell
Nominal Pipe
Size, in.
1
1
14
112
2
3
4
6
ftlbf (J)
IC-1
IC-2
IC-3
30 to 50
(41 to 68)
30 to 51
(41 to 68)
40 to 60
(54 to 81)
70 to 90
(95 to 122)
120 to 140
(163 to 190)
160 to 200
(217 to 271)
200 to 260
(271 to 353)
>50 to 65
(68 to 88)
>50 to 65
(68 to 88)
>60 to 75
(81 to 102)
>90 to 100
(122 to 136)
>140 to 180
(190 to 244)
>200 to 240
(271 to 326)
>260 to 300
(353 to 407)
>65 (88)
>65 (88)
>75 (102)
>100 (122)
>180 (244)
>240 (326)
>300 (407)
Standard
Demension
Ratio
PVC 1120
PVC 2110
PVC 2116
11
13.5
17
21
1250
1000
800
630
1000
800
630
500
(8.6)
(6.9)
(5.5)
(4.3)
(6.9)
(5.5)
(4.3)
(3.4)
PVC
PVC
PVC
PVC
1120
1220
2110
2116
6400
6400
5000
5000
(44.1)
(44.1)
(34.5)
(34.5)
A3. IN-PLANT QUALITY CONTROL PROGRAM FOR PLASTIC PIPE AND FITTINGS UP TO
AND INCLUDING 12 IN. NOMINAL DIAMETER
13
Sustained
Pressure Test
4200 (29.0)
4200 (29.0)
2300 (15.9)
3650 (23.2)
D 2513 04
TABLE A3.2 Product Quality Control Tests
Property
Diameter
Wall thickness
Ring tensile or burst pressure
NOTE A3.1When the pipe fails to meet this specification in any test,
additional tests shall be made on the pipe produced back to the previous
acceptable result to select the pipe produced in the interim that does pass
the requirement. Pipe that does not meet the requirement shall be rejected.
NOTE A3.2For pipe sizes above 4-in. nominal diameter, the quick
burst test (Test Method D 1599) may be replaced by the Apparent Ring
Tensile Strength Test (Test Method D 2290) if agreed to between the
purchaser and the manufacturer.
A3.3.2 Dimensions:
A3.3.2.1 Socket Fittings:
(a) Socket Entrance, Bottom and Minimum Internal
DiametersOnce an hour or one out of ten fittings, whichever
is less frequent.
(b) Wall ThicknessAt the beginning of each production
setup for each cavity.
A3.3.2.2 Butt Fusion Fittings:
(a) Outside Diameter and Wall ThicknessOnce an hour or
one out of ten fittings, whichever is less frequent.
A3.3.3 Other Tests:
A3.3.3.1 PVC FittingsThe burst pressure shall be measured on one fitting per 8-h production.
A3.3.3.2 PE and PB FittingsAt the start of each production run, whenever production conditions have changed, or
when the resin lot is changed, but not less frequently than once
per 500 fittings thereafter, the following tests shall be made:
(a) The knit line strength for at least one fitting from each
cavity shall be demonstrated by one of the following tests:
Stress
580 6 10 psi
(4.0 6 0.07 MPa)
670 6 10 psi
(4.6 6 0.07 MPa)
Frequency
once every hour or every coil,
whichever is less frequent
once every hour or every coil,
whichever is less frequent
Once every 8 h or once every coil,
whichever is less frequent, or
multilevel plan described in A3.2.3
once every 8 h
once every 2 h
once every hour
Time Requirement
1000 h
170 h
9
Supporting data are available from ASTM Headquarters. Request RR: F171018.
Methane should not be substituted for water in this 176F (80C) test.
14
D 2513 04
(b) The integrity of at least one part from each mold cavity
shall be verified, using a method selected by the manufacturer
as appropriate for this specific product and process.
NOTE A3.4Separation in the knit constitutes a failure.
NOTE A3.5In tests 2 and 3 the strength requirements shown in the
annexes must be met.
A4. IN-PLANT QUALITY CONTROL PROGRAM FOR 14-IN. AND LARGER DIAMETER
POLYETHYLENE PIPE
A4.1 Visual inspection of every length of pipe for workmanship defects shall be carried out at the manufacturers
plant. Measurements of outside diameter and wall thickness
shall be made for each hours production or each length of
pipe, whichever is less frequent.
A4.2 Lengths of pipe that are shorter than standard shipping lengths are butt-fused to produce standard lengths. Such
build-up lengths must otherwise meet all of the product
requirements of this specification.
15
D 2513 04
A5. SUPPLEMENTAL REQUIREMENTS FOR GAS PRESSURE PIPE AND FITTINGS PRODUCED FROM POLYAMIDE
MATERIAL
TABLE A5.2 Short and Long Term Property Requirements
A5.1 Scope
A5.1.1 This annex covers requirements for PA pipe and heat
fusion fittings. These requirements are in addition to those in
the main body of this specification.
A5.2 Referenced Documents
A5.2.1 ASTM Standards: 2
D 4066 Specification for Nylon Injection and Extrusion
Materials (PA)
F 1563 Specification for Tools to Squeeze-Off Polyethylene
(PE) Gas Pipe or Tubing
Short-Term in
Accordance with
D 4066
PA32312
PA323
Long-Term in Accordance
with D 2837
HDB of 2500 psi for
73F (23C)
A5.3 Materials
A5.3.1 ClassificationPolyamide materials suitable for use
in the manufacturing of pipe and fittings under this specification shall be classified in accordance with Specification
D 4066, as shown in Table A5.1.
A5.3.2 Short- and Long-Term PropertiesPolyamide pipe
and fittings shall be made from a PA material which also
satisfies the combinations of short- and long-term property
requirements shown in Table A5.2.
Classification
PA Material
Designation Code
Designation
1.83
185195
1.031.06
48
A5.5 Marking
200
A5.5.1 PA pipe shall be marked with the elevated temperature code letters EF CG in accordance with Table 4 in addition
to the marking requirements of 7.1.
E = maximum temperature of 180F (82C),
F = 1250 psi HDB at 180F (82C),
C = temperature of 140F (60C), and
G = 1600 psi HDB at 140F (60C).
900
55
40
0.08
16
D 2513 04
TABLE A5.3 Chemical Resistance
Weight
Change,
max
Chemical
%
Mineral
oil
Tertiary-butyl
mercaptan
(5 %)
Methanol
Ethylene
glycol
Toluene
(5 %)
Yield
Strength
Inherent
Viscosity,
%
Change,
max
%
+0.5
12
63
+0.5
12
63
+5
+0.5
35
12
63
63
+7
40
63
A6. SUPPLEMENTAL REQUIREMENTS FOR GAS PRESSURE PIPE PRODUCED FROM MAGNETIC-DETECTABLE
POLYETHYLENE MATERIAL (MDPEMAG/HDPEMAG) WITH UP TO 24 % CONCENTRATION (WEIGHT PERCENT) OF
STRONTIUM FERRITE (SrFe)
A6.1 Scope
A6.3 Materials
A6.3.1 Cell Classification and Strontium Ferrite
BlendingPolyethylene materials for blending with strontium
ferrite shall be PE2406 (MDPE) material meeting a cell
classification of 234363C or 234263E per specification
D 3350, or PE3408 (HDPE) material meeting a cell classification of 345464C or 345464E per specification D 3350. These
materials shall be blended with up to a maximum of 24 %
concentration level by weight of strontium ferrite (SrFe)
A6.3.1.1 MDPEMAGPE2406 material that is blended
with a maximum of 24 % concentration level by weight of
strontium ferrite, shall be listed by PPI TR4 with a minimum
hydrostatic design basis (HDB) ratings of 1250 psi (8.62 MPa)
at 73F (23C) and 800 psi (5.52MPa) at 140F (60C)
A6.3.1.2 HDPEMAGPE3408 material that is blended
with a maximum of 24 % concentration level by weight of
strontium ferrite, shall be listed by PPI TR4 with a minimum
hydrostatic design basis (HDB) ratings of 1600 psi (11.03
MPa) at 73F (23C) and 800 psi (5.52MPa) at 140F (60C)
A6.3.1.3 Strontium Ferrite (SrFe)Strontium Ferrite materials must conform to typical powder characteristics shown in
Table A6.1.
A6.3.2 Short and Long Term PropertiesPolyethylene pipe
and tubing shall be made from magnetic-detectable PE materials which also satisfy the combinations of short- and longterm property requirements shown in Table A5.2.
A6.3.3 Hydrostatic Design Basis (HDB) Substantiation
The HDB for magnetic-detectable PE materials at 73F (23C)
A6.1.1 This annex covers requirements for magneticdetectable PE pipe and tubing with up to 24 % concentration
by weight of Strontium Ferrite (SrFe). These requirements are
in addition to those in the main body of this specification.
NOTE A6.1The use of the term Magnetic-detectable Polyethylene
(Magnetic-detectable PE) throughout the body of this annex refers to only
conventional grades of PE (medium and high density) blended with up to
24 % (by weight) concentration of Strontium Ferrite (SrFe) only. While
other fillers can be added, this annex is restricted to SrFe only on the basis
of the comprehensive testing and evaluation on the chemical, physical,
and mechanical properties of the magnetic-detectable PE. Magneticdetectable PE is a patented technology exclusively owned by Gas
Technology Institute (formerly Gas Research Institute).
17
Units
Value
g/cm3
kg/m3
wt. %
microns
SrFe12O19
5.09
2243
5
3.5
D 2513 04
A6.5.1.1 MagnetizerFor less than 2 in. IPS (60.3 mm)
pipe and tubing, AILM 2.375 magnetizer unit must be used.
For pipe and tubing larger than 2 in. IPS (60.3 mm) and less
than 4 in. IPS (114.3 mm), AILM 4.0 magnetizer unit must be
used. For 2 in. IPS (60.3 mm), either AILM 2.375 or AILM 4.0
can be used.
A6.5.1.2 Magnetizer Rotation SpeedsThe rotation speed
of the magnet core contained within the magnetizer unit shall
be calculated for each pipe size as a function of the line speed
using the following equation:
v 5 V/~12l!
(A6.1)
where:
v = rotation speed of the magnet core, r/min
V = line speed, in./min.
l = one single period as measure from peak to peak on a
sin function graph. For gas distribution application, l =
10 ft.
A6.5.2 ConditioningFor those tests where conditioning is
required or unless otherwise specified, condition the specimens
prior to testing for a minimum of 1 h in water or 4 h in air at
73.4 6 3.6F (23 6 2C) or in accordance with 6.3. The
conditioning requirements of 6.3 shall be used in all cases of
disagreement.
A6.5.3 Minimum Hydrostatic Burst Pressure/Apparent Tensile Strength (Quick Burst)The pipe or system shall fail in a
ductile manner when tested in accordance with Test Method
D 1599. For pipe size above 4-in. nominal diameter, the quick
burst test (Test Method D 1599) may be replaced by the
apparent ring tensile strength test (Test Method D 2290). The
minimum apparent tensile strength at yield when determined in
accordance with 6.8 shall be 2520 psi (17.4 MPa).
A6.5.4 Sustained Pressure 73F (23C)The pipe or system shall not fail in less than 1000 h when tested in accordance
with Test Method D 1598. For MDPEMAG material, the stress
shall be 1320 psi, for HDPEMAG materials, the stress shall be
1600 psi.
A6.5.5 Melt IndexMelt index is the flow rate of Magneticdetectable PE material when measured in accordance with Test
Method D 1238, condition 190/2.16 (formerly Condition E).
Materials that record zero flow under condition 190/2.16 shall
be measured in accordance with condition 190/21.6 (formerly
condition F). The melt index of pipe shall meet the designated
category in Table 4. The sample shall be representative of the
cross section of the pipe and diced to an appropriate size by a
method not producing heat.
A6.5.6 Squeeze-offThis requirement is limited to pipe
sizes, wall thicknesses, squeeze procedures and conditions
deemed suitable for squeeze-off in service by the pipe manufacturer. There shall be no leakage or visual evidence of
splitting, cracking, breading or reduction in 1000-h sustained
pressure category when pipe is tested as follows:
A6.5.6.1 Prepare six randomly selected pipe specimens in
accordance with Test method D 1598.
A6.5.6.2 The squeeze-off shall be effected at the midpoint
of test specimen, 90 to the point of the measured minimum
wall thickness. Close the squeeze bars to the gap stop recommended in Specification F 1563 and hold in constraint for 4 h.
NOTE A6.2For less than 2 in. IPS (60.3 mm) pipe and tubing that has
been magnetized to induce a characteristic sinusoidal signature, a maximum of 24 % concentration level by weight of strontium ferrite (SrFe) in
polyethylene has been identified as effectively detectable at typical burial
depths. For 2 in. IPS (60.3 mm) and larger pipe and tubing that has been
magnetized to induce a characteristic sinusoidal signature, a 17 %
concentration level by weight of strontium ferrite (SrFe) in polyethylene
has been identified as effectively detectable at burial depths of 3 to 5 feet
(0.9 to 1.5 m). Supporting information in a Research Report. RR-F171018, has been filed with ASTM headquarters.
NOTE A6.3For more information on the AILM Magnetizer Unit
contact Gas Technology Institute (GTI) 1700 S. Prospect Rd., Des Plaines,
IL 60018
NOTE A6.4Melt index ranges for magnetic detectable PE with up to
24 % concentration by weight of strontium ferrite are summarized in Table
4.
NOTE A6.5The long term hydrostatic strength at 50 years in accordance with Test Method D 2837 is not to be used for any pressure rating
calculations. The MAOP is still calculated using the HDB obtained from
Test Method D 2837 long term hydrostatic strength at 100 000 hours.
D 2513 04
2500 psi for MDPEMAG materials or 2900 psi for HDPEMAG
materials. Hoop stress calculation shall be based on the DR.
(WarningPressurization of pipe specimens above 12 in.
nominal diameter being tested in accordance with A6.5.9
should not commence until it is certain that all entrapped air
has been bled from water-filled specimens.)
A7.1 Scope
A7.1.1 This annex covers requirements for PEX pipe. These
requirements are in addition to those in the main body of this
specification.
A7.2 Referenced Documents
A7.2.1 ASTM Standards: 2
A7.2.1.1 Test Methods for:
D 792 Density and Specific Gravity (Relative Density) of
Plastics by Displacement
D 1505 Density of Plastics by Density-Gradient Technique
D 2765 Determination of Gel Content and Swell Ratio of
Crosslinked Ethylene Plastics
D 4883 Density of Polyethylene by Ultrasound Technique
A7.3 Materials
A7.3.1 GeneralPEX pipe are primarily defined by means
of three criteria, namely, (1) nominal density, (2) degree of
crosslinking, and (3) long-term strength tests. There is a strong
correlation between nominal density and results of short-term
strength tests.
19
D 2513 04
deemed suitable for squeeze-off in service by the pipe manufacturer. There shall be no leakage or visual evidence of
splitting, cracking, breaking or reduction in 1000-h sustained
pressure category when pipe is tested as follows:
A7.4.6.1 Prepare six randomly selected pipe specimens in
accordance with Test Method D 1598 except they shall be
unfilled.
A7.4.6.2 The squeeze-off shall be effected at the mid-point
of the test specimen, 90 to the point of the measured minimum
wall thickness. Close the squeeze bars to the gap stop in
Specification F 1563 and hold in constraint for 4 h. Remove
squeeze bar and reround pipe by closing squeeze bars at a point
90 from the squeeze area.
A7.4.6.3 Immediately upon removal of the squeeze-off tool,
fill the specimens with ambient temperature water, that is 67 6
10F (19.4 6 5.6C), condition, and test in accordance with
6.6.
A7.4.7 Thermal StabilitySpecimens of the pipe inside
wall surface not more than 0.005 in. (0.13 mm) thick shall
demonstrate a minimum induction temperature of 428F
(220C) when tested in accordance with the Test Method for
Thermal Stability in Specification D 3350.
A7.4.8 Outdoor Storage StabilityPEX pipe stored outdoors and unprotected for at least two years from date of
manufacture shall meet all the requirements of this specification. PE pipe stored outdoors for over two years from date of
manufacture is suitable for use if it meets the requirements of
this specification.
A7.4.9 Apparent Tensile Strength at YieldWhen tested in
accordance to 6.8, the PEX pipe shall demonstrate a minimum
of 2600 psi for PEX 0006 materials and 3000 psi for PEX 0008
materials.
A7.4.10 Slow Crack Growth ResistanceTest Method is
F 1473 on compression molded plaques or PEX pipe sample.
Stress is 2.4 MPa based on unnotched area. Temperature is
80C. Notch depth in accordance with Table 1 in Test Method
F 1473. The minimum of the average of the two tests shall be
100 h. Do at least four tests in case of a dispute.
A7.5 Marking
A7.5.1 PEX pipe shall be marked with the marking requirements of 7.1.
20
D 2513 04
APPENDIXES
(Nonmandatory Information)
X1. NEW MATERIALS
X2.1 General
X2.1.1 The design of a plastic piping system for natural gas
service must include consideration of the combined effects of
time, internal and external stress, and environment as an
overall basis for selecting a specific kind and size of plastic
pipe. The design stress for plastic pipe used for distribution of
natural gas and petroleum fuels is regulated by the U.S.
Department of Transportation as published in Part 192 Title 49
of the Code of Federal Regulations. The American Gas
Association Plastic Materials Committee, the Fuel Gas Division of PPI, and members of ASTM Committee F17 are
cooperating with the ASME Gas Piping Technology Committee to provide assistance in selecting safe design stress levels
for the various kinds of plastic pipe.
where:
P b = burst pressure, psig (MPa),
Sy
= yield stress, psi (MPa), and
DR = dimension ratio.
Ps 5 2Sf /~ DR 2 1!
(X2.3)
where:
P s = sustained pressure, psig (MPa),
= fiber stress psi (MPa), and
Sf
DR = dimension ratio.
X2.2.3 Relation between Hydrostatic Design Basis (HDB)
and Hydrostatic Design Stress (HDS)The HDS is determined
by multiplying the HDB by a design factor, f. The design factor,
f, has a value less than 1.0.
(X2.2)
(X2.4)
(X2.1)
NOTE X2.1The actual choice of design factor for a given installation
must be reviewed by the design engineer taking into account federal, state,
and local code requirements. For example, the design factor for gas
pipelines under the jurisdiction of the Department of Transportation is
0.32.
where:
S
= stress in the circumferential or hoop direction, psi
(MPa),
P
= internal pressure, psig (MPa),
DR = dimension ratio,
Do = average outside diameter, in. (mm), and
t
= minimum wall thickness, in. (mm).
X2.2.2 The following expression can be used to determine
the burst pressure or sustained pressures needed in testing:
D 2513 04
Dt
Hydrostatic Design
Basis at
73F (23C), psi (MPa)
2500 (17.2)
1250 (8.6)
1600 (11.0)
4000 (27.6)
2000 (13.8)
3150 (24.8)
PA 32312
PE 2406
PE 3408
PVC 1120
PVC 2110
PVC 2116
F5S 3A
where:
F = force, lbf (N),
S = stress, psi (MPa), and
A = cross-sectional pipe wall area, in.2 (mm2).
X2.4.3 Calculate pipe contraction in unrestrained pipe
caused by a reduction in temperature as follows:
DL 5 k 3 L 3 C 3 Dt
where:
DL =
k
=
k
=
L
=
C
=
Dt
=
(X2.7)
change in length,
1000 for DL (mm), L (m), C (C1), Dt (C), or
12 for DL (in.), L (ft), C (F 1), Dt (F),
original length,
coefficient of linear expansion, and
temperature change.
(X2.6)
(X2.5)
where:
S = stress, psi (MPa),
E = modulus of elasticity, psi (MPa), instantaneous, at
73F (23C),
C = coefficient of expansion, in./in./F, (mm/mm/C), and
X2.5.3 Internal pressure, earth settlement, ground movement, and thermal contraction impose stresses on the pipe that
can be transmitted to joints. These stresses are additive.
Installation practices should reflect the need for continuous
22
D 2513 04
X2.7 Environmental Effects
X3. GAS PRESSURE PIPE AND FITTINGS PRODUCED FROM POLYETHYLENE (PE) MATERIALS WITH MINIMUM
REQUIRED STRENGTH (MRS) DESIGNATION
X3.1 Scope
X3.1.1 This appendix covers information for PE pipe and
fittings produced from polyethylene material with MRS designations. The intent for this Appendix is to utilize the information as a guideline for specifying product to take to the DOT
(Department of Transportation). In conjunction with this Appendix, the AGA-PMC (American Gas Association Plastics
Materials Committee) has a project to petition the DOT for
recognition and use of MRS rated materials in gas pressure
pipe and fittings. Gas utilities may obtain waivers from
appropriate governing bodies to use MRS rated materials in gas
pressure pipe and fittings. The non-mandatory information in
23
D 2513 04
cation may be classified in accordance with Specification
D 3350 as noted in Table X3.1.
X3.4.3 Substantiation of long-term hydrostatic strength at
50 years is not required when the MRS time, t, is 50 years or
greater. However, the manufacturer shall assure that in determining MRS at u = 23C and t = 50 years, any ductile to brittle
transition occurs after the 50-year intercept.
X3.5 Requirements
X3.5.1 Elevated Temperature ServiceIn addition to MRS
classification using the ISO 12162 standard conditions of 20C
and 50 years, the MRS can be determined at other desired
temperature or time conditions as denoted by MRS (u, t). The
MRS (u, t) is the categorized MRS value for a material at a
temperature of u C and a time of t years. Consult the
manufacturer for elevated temperature MRS values. In addition
to the pipe category per table 4 of ASTM D 2513, the pipe
category using the MRS designation as noted in Table X3.2
may be used.
NOTE X3.1For more information on hydrostatic strength classification, refer to PPI TN-7 or contact the Hydrostatic Stress Board Chairman.
X3.3 Terminology
X3.3.1 long-term hydrostatic strength (sLTHS), na quantity obtained in accordance with ISO 9080 with the dimensions
of stress which represents the predicted mean strength at a
temperature u and time t and can be considered as a property
of the material under consideration.
X3.3.2 lower predictive limit (LPL), na pipe materials
97.5 % lower confidence level of the extrapolated value
(typically at 20C and 50 years) obtained in accordance with
ISO 9080.
X3.3.3 minimum required strength (MRS), nthe categorized lower predictive limit (LPL) of the ISO 9080 long-term
strength at 20C and 50 years as defined in ISO 12162.
X3.5.2.2 Testing at 176F (80C)Alternatively, the sustained pressure testing may be performed at 176F (80C)
under the following stress and minimum failure times as noted
in Table X3.3.
TABLE X3.3 Hydrostatic Strength176F (80C) Stress/Minimum
Failure Time Correlation
X3.4 Materials
X3.4.1 Materials with PPI recommended MRS ratings are
listed in PPI TR-4. Grades of recommendation and data
requirements for PPI recommended MRS ratings are specified
in part B of PPI TR-3.
X3.4.2 ClassificationPolyethylene materials suitable for
use in the manufacture of pipe and fittings under this specifi-
PE 80
PE 80
PE 100
PE 100
Stress,
psi (MPa)
Minimum Failure
Time, h
Stress,
psi (MPa)
Minimum Failure
Time, h
667
653
638
624
609
595
580
(4.6)
(4.5)
(4.4)
(4.3)
(4.2)
(4.1)
(4.0)
165
219
283
394
533
727
1000
798
783
769
754
740
725
(5.5)
(5.4)
(5.3)
(5.2)
(5.1)
(5.0)
165
233
332
476
688
1000
PE 100
2, 3 or 4
3 ,4, or 5
3, 4, 5, or 6
3, 4, or 5
6
3 or 4
3, 4, or 5
4, 5, or 6
4, 5, or 6
6
3 or 4 and 5
4 and 6
X3.6 Marking
X3.6.1 Material DesignationThe ISO thermoplastic material designation code PE 80 or PE 100 may be utilized for
material designation in addition to PE 2406 or PE 3408.
24
D 2513 04
TABLE X3.2 Pipe Category
Property
Test
Method
Temperature, F (C)
Minimum Required Strength (MRS)
Melt Index
ISO 12162
D 1238
100 (38)
> 0.5
120 (49)
0.2 to 0.5
140 (60)
0.01 to 0.3
160 (71)
< 0.01A
180 (82)
0.07 to 0.20B
3.2
4.0
6.3
8.0
10.0
Typically melt flow measured under condition 190/21.6 is less than 4.01 g/10 min.
When a PE pipe or fitting is marked per 7.2 or 7.3 with this melt index range, it affirms that the manufacturer has verified generic fusion joining in accordance with PPI
TR-33. Information about manufacturers who have verified PPI TR-33 generic fusion joining with their products is found in PPI TR-33. Consult PPI and the manufacturer
for additional information.
B
(23C) may be marked with the three letter code from Table
X3.2 in addition to the three letter code from Table 4.
REFERENCES
(1) Allman, W.B., Earthloading Design Considerations for Polyethylene
Gas Distribution Systems, Proceedings of the Fifth Plastic Pipe
Symposium, November 1315, 1974, Houston, TX, A.G.A., 1515
Wilson Blvd., Arlington, VA 22209, pp. 55171.
(2) Spangler, M.G., Secondary Stresses in Buried High Pressure Lines,
Iowa State College Bulletin, Engineering Report 23 of the Iowa
Engineering Experiment Station, 1954, 1955.
(3) Kuhlman, H. W., Leninger, R. I., and Wolter, Fritz, Investigation of
Engineering and Design Concepts for Plastics Pipe for Gas Distribution Application, presented at ANSI B31.8 meeting in St. Charles, IL,
October 19, 1965.
(4) Palermo, E. F., and Cassady, M. J., Comparison of Long-Term Effect
ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned
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25