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Test Method For The Determination of Chlorides by Potentiometric Titration

cloruro en aminas

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Nicola Margarelli
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37 views1 page

Test Method For The Determination of Chlorides by Potentiometric Titration

cloruro en aminas

Uploaded by

Nicola Margarelli
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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LUBRIZOL TEST PROCEDURE

TP-ACM-4
Edition: September 14, 2010
Original Date: April 7, 2008

Test Method for the Determination of


Chlorides by Potentiometric Titration
Purpose: Procedure:
This procedure is used to determine the chloride 1. Weigh a 4 - 5 gram sample (1 - 2 grams if the
salts in Lubrizol Surfactants, using a potentio- Chloride content is greater than 5) to the
metric titrator. nearest 0.1 mg into a 250 ml beaker.
2. Add 110 mls of deionized water.
3. Using a stir bar and stirrer, titrate with 0.1N
Abstract:
AgNO 3 to the potentiometric end point.
A solution of the surfactant is titrated
potentiometrically with silver nitrate to determine
the weight percentage of chloride salt. Review Calculations:
MSDS for each material before handling.
% Sodium Chloride= N x ml x 58.5
Sample wt. (g) x 10
Safety Precautions:
% Ammonium Chloride = N x ml x 53.5
1. Proper personal protective equipment should Sample wt. (g) x 10
be worn during transfer of materials so that
injury due to spillage is avoided. % Diethanolamine Hydrochloride = N x ml x 142.6
Sample wt. (g) x 10
2. Refer to MSDS for each material for handling
and storage information. % Triethanolamine Hydrochloride = N x ml x 185.7
Sample wt. (g) x10

Reagents:
1. Deionized Water
2. 0.1N Silver Nitrate (AgNO3)

Apparatus:
1. AgCl electrode
2. Potentiometric Titrator

Lubrizol Advanced Materials, Inc. / 9911 Brecksville Road, Cleveland, Ohio 44141-3247 / TEL: 800.379.5389 or 216.447.5000
The information contained herein is being furnished combination with other substances or in the User’s process. THE IMPLIED WARRANTIES OF MERCHANTABILITY
for informational purposes only, upon the express condition Due to variations in methods, conditions and equipment OR FITNESS FOR A PARTICULAR PURPOSE. It is the
that the User makes its own assessment of the appropriate used commercially in processing these materials, no User’s sole responsibility to determine if there are any
use of such information. While the information contained warranties or guarantees are made as to the suitability of issues relating to patent infringement of any component or
herein is believed to be reliable, no representations, the information or products for the applications combination of components relating to the supplied
guarantees or warranties of any kind are made as to its disclosed. Lubrizol shall not be liable and the User information. Nothing contained herein is to be
accuracy, suitability for a particular application or the assumes all risk and responsibility for any use or considered as permission, recommendation, nor as
results to be obtained herefrom. Lubrizol Advanced handling of any material beyond Lubrizol's direct an inducement to practice any patented invention
Materials, Inc. ("Lubrizol") cannot guarantee how any control. LUBRIZOL MAKES NO WARRANTIES, EXPRESS without permission of the patent owner.
products associated with this information will perform in OR IMPLIED, INCLUDING, BUT NOT LIMITED TO,
For further information, please visit: www.lubrizol.com/personalcare
Lubrizol Advanced Materials, Inc. is a wholly owned subsidiary of The Lubrizol Corporation
All trademarks owned by The Lubrizol Corporation
© Copyright 2013 / The Lubrizol Corporation

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