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Estimation of Total Dissolved Solids in Water Samples: Revision Summary GTP Number Date Revised Reason For Revision

This document outlines a procedure for estimating total dissolved solids in water samples. It involves filtering a well-mixed 100 mL water sample through a filter paper, then evaporating and drying the filtrate in a weighed crucible at 180°C. The increase in weight of the crucible represents the total dissolved solids. The procedure is calculated by subtracting the initial crucible weight from the final weight after drying, then multiplying by 1000 and dividing by the sample volume of 100 mL to obtain mg/L total dissolved solids. The document provides the purpose, apparatus, step-by-step procedure, calculation, and reference.

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138 views3 pages

Estimation of Total Dissolved Solids in Water Samples: Revision Summary GTP Number Date Revised Reason For Revision

This document outlines a procedure for estimating total dissolved solids in water samples. It involves filtering a well-mixed 100 mL water sample through a filter paper, then evaporating and drying the filtrate in a weighed crucible at 180°C. The increase in weight of the crucible represents the total dissolved solids. The procedure is calculated by subtracting the initial crucible weight from the final weight after drying, then multiplying by 1000 and dividing by the sample volume of 100 mL to obtain mg/L total dissolved solids. The document provides the purpose, apparatus, step-by-step procedure, calculation, and reference.

Uploaded by

depardieu1973
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© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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GENERAL TEST PROCEDURE (GTP) Page 1 of 3

Estimation of Total Dissolved Solids In Water


Title Effective Date 04/01/05
Samples
GTP Number GTP 119-02 Review Date 03/01/07

REVISION SUMMARY

GTP Number Date Revised Reason for Revision


GTP 059 - 00 01/07/2002 First Issue
GTP 119 - 01 05/03/2003 Renumbering of GTP and Format Changed
GTP 119 - 02 04/01/05 The format of the GTP is changed as per SOP QA
030-00 and the procedure is revised.

1.0 PURPOSE
1.1 To lay down the procedure for determining the total dissolved solids in water
samples.
Prepared By Checked By Approved By
Name M. SRIHARI N. RAJENDRA KUMAR SANJAY SHAH K. R. PRAKASH

Signature

Date
GENERAL TEST PROCEDURE (GTP) Page 2 of 3
Estimation of Total Dissolved Solids In Water
Title Effective Date 04/01/05
Samples
GTP Number GTP 119-02 Review Date 03/01/07

1.2 A well mixed sample is filtered through whatman filter paper, and filtrate is
evaporated to dryness in a weighed dish and dried to constant weight at180º
C.The increase in the dish weight represents the Total Dissolved Solids

2.0 APPARATUS
2.1 Glass Crucible
2.2 Oven for drying
2.3 Analytical Balance
2.4 100 ml measuring cylinder
2.5 Whatman filter paper and funnel

3.0 PROCEDURE
3.1 Sample 100 ml of water in a clean and dried standard glass bottle.
3.2 Cut a small piece of Whatman Filter paper so as so to accommodate in the
funnel.
3.3 Take the filter paper and form a cone shape and place it in the funnel.
3.4 Slowly pour the sample through the side wall of the filter placed in the funnel filter
the entire sample.
3.5 Take the weight of the Empty crucible (A)
3.6 Pour the filtrate into the crucible and keep it at 180º C for evaporation.
3.7 After complete evaporation place the crucible in the desiccator.
3.8 After the temperature of the crucible is reduced to room temperature weigh the
crucible. (B)
3.9 The increase in the weight of the dish will represent the total dissolved solids.
4.0 CALCULATION

i. Weight of the Crucible after drying. - B


ii. Initial Weight of the crucible - A
iii. Volume of the sample taken - 100 ml

Prepared By Checked By Approved By


Name M. SRIHARI N. RAJENDRA KUMAR SANJAY SHAH K. R. PRAKASH

Signature

Date
GENERAL TEST PROCEDURE (GTP) Page 3 of 3
Estimation of Total Dissolved Solids In Water
Title Effective Date 04/01/05
Samples
GTP Number GTP 119-02 Review Date 03/01/07

 Total Dissolved Solids = (B - A) x 1000


----------------------- = mg / liter
100

5.0 REFERENCE

5.1 American Public Health Association page number 2-56 to 2-57

END OF DOCUMENT

Prepared By Checked By Approved By


Name M. SRIHARI N. RAJENDRA KUMAR SANJAY SHAH K. R. PRAKASH

Signature

Date

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