75%(4)75% found this document useful (4 votes) 3K views222 pagesRichard Vernon Parish - NMR, NQR, Epr, and Mossbauer Spectroscopy in Inorganic Chemistry (Ellis Horwood Series in Inorganic Chemistry) (1991) PDF
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NMR, NQR, EPR,
AND MOSSBAUER
SPECTROSCOPY
IN INORGANIC
CHEMISTRY
R. V. PARISH ph.v..p.Se.(London), D.Se(Manchester). C.Chem., F.R.S.C.
Department of Chemistry
n :
‘The University of Manchester Institute of Science and Technology First published in 1990 by
ELLIS HORWOOD LIMITED
Market Cross House, Cooper Street,
Chichester, West Sussex, PO19 1EB, England
A sion of.
Simon & Schuster International Group
‘A Paras Communictions Company
© Ellis Horwood Limited, 1990
All rights reserved. No part of this publication may be
reproduced. stored in a retrieval system, or transmitted,
in any form. or by any means, electronic, mechanical.
photocopying, recording or otherwise, without the prior
permission, in writing, of the publisher
‘Typeset in Times by Ellis Horwood Limited
Printed and bound in Great Britain
by Hartnolls, Bodmin, Cornwall
British Library Cataloguing in Publication Data
Parish, RV.
NMR, NOR. EPR and Méssbauer spectroscopy in inorganic
chemistry.
1. Tnorganic compounds
L Title
541.28
ISBN 0-13-625518-3
Library of Congress Cataloging-in-Publication Data
Parish, R. V. (Richard Vernon), 1934
NMR, NOR, EPR, and Massbauer spectroscopy in inorganic
chemistry /R. V. Parish
p. cm. — (Ellis Horwood series in inorganic chemistry)
ISBN 0-13-625518-3
1. Spectrum analysis. 2. Chemistry. Inorganic. 1. Title
IL. Series.
QD95.P25 1990
543.087—e20 90-4873
ce Table of Contents
1 Introduction .......--.-.---
1.1 Hyperfine interactions ... . .
1.2 Common features of the spectra.
1.2.1. Energy ranges.
1.2.2. Numbers of lines
1.2.3 Intensities . .
1.2.4 Line widths . . . 7
1.2.5 Types of spectrometer
1.3 Quantum numbers . .
1.4 Restrictions
2 Nuclear magnetic resonance . .
2.1 Experimental considerations .
2.1.1 Thesample ......
2.1.2 The spectrometer . .
2.2 Fundamentals
2.2.1 Chemical shift.
2.2.2 Coupling constants.
2.2.3 Complications .
2.2.3.1 Satellites . . A
2.2.3.2 Second-order spectra .
2.2.3.3 Exchange. . :
2.3 'Hspectra.......
2.3.1 Organometallics
2.3.1.1 Chemical shifts . .
2.3.1.2 Coupling effects. :
23.2 Phosphine and arsine ligands . -
23.3 Hydrides........--00005
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