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Analisis Data Absorbsi

1. The document analyzes data from experiments measuring the addition of BaCl2 to two tanks (S5 and S4) over time and the standardization of a NaOH solution. 2. Calculations are shown to determine the normality of solutions used in the experiments, including a 0.1 N NaOH solution that required 120 grams of NaOH. 3. Data and calculations at 0, 10, 20, 30, and 40 minutes show concentrations of NaOH and Na2CO3 at the inlet and outlet of a reactor as well as the amount of CO2 absorbed over time.

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Annyssa Maylia
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0% found this document useful (0 votes)
64 views6 pages

Analisis Data Absorbsi

1. The document analyzes data from experiments measuring the addition of BaCl2 to two tanks (S5 and S4) over time and the standardization of a NaOH solution. 2. Calculations are shown to determine the normality of solutions used in the experiments, including a 0.1 N NaOH solution that required 120 grams of NaOH. 3. Data and calculations at 0, 10, 20, 30, and 40 minutes show concentrations of NaOH and Na2CO3 at the inlet and outlet of a reactor as well as the amount of CO2 absorbed over time.

Uploaded by

Annyssa Maylia
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© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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I.

Analisis Data
 Penambahan BaCl2
Tangki Umpan (S5)
Waktu 0 : T2-T1 = 30.4 - 26.7 = 3.7 x 10/100 = 0.37 mL BaCl2
Waktu 10 : T2-T1 = 33.3 – 27.5 = 5.8 x 10/100 = 0.58 mL BaCl2
Waktu 20 : T2-T1 = 35.5 – 26.2 = 9.3 x 10/100 = 0.93 mL BaCl2
Waktu 30 : T2-T1 = 37.5 – 26.5 = 11 x 10/100 = 1.1 mL BaCl2
Waktu 40 : T2-T1 = 44 – 22.5 = 21.5 x 10/100 = 2.15 mL BaCl2
Tangki Umpan (S4)
Waktu 10 : T2-T1 = 45.8 – 17.3 = 28.5 x 10/100 = 2.85 mL BaCl2
Waktu 20 : T2-T1 = 46 – 10 = 36 x 10/100 = 3.6 mL BaCl2
Waktu 30 : T2-T1 = 46.5 – 5.3 = 41.2 x 10/100 = 4.12 mL BaCl2
Waktu 40 : T2-T1 = 50 – 3 = 47 x 10/100 = 4.7 mL BaCl2
 Pembuatan Larutan NaOH 0,1 N 30 liter
N=Mxi
0,1 = M x 1, M= 0,1 M
M = (g/Mr) x (1000/V)
0,1 = (g/40) / (1000/30000)
120 gram = g (massa NaOH yang dibutuhkan)
 Pembuatan Larutan Asam Oksalat
Massa A.oksalat = 0,633 gram
V = 100 mL
BE = Mr / 2 = 126 / 2 = 63 g/ml
N = (m/BE) x (1000/V)
N = (0.633/126) x (1000/100)
N = 0,1 N
 Standarisasi Larutan NaOH dengan Asam Oksalat
V1 = volume larutan NaOH rata-rata titrasi = 25,55 mL
V2 = volume larutan A.oksalat = 25 mL
N1 = Normalitas larutan NaOH (yang dicari)
N2 = Normalitas larutan asam oksalat = 0,1 N
N1 V1 = N2 V2
N1 x 25,55 = 25 x 0,1 N
N1 = 0,098 N

Saat t = 0

1. Inlet
𝑇3
CNaOH = (50 𝑚𝑙) × 0,1 M
26,1
= (50 𝑚𝑙) × 0,1 M

= 0,0522
𝑇2−𝑇3
CNa2CO3 = ( 50 𝑚𝑙 ) × 0,1 M × 0,5
30,4−26,1
=( ) × 0,1 M × 0,5
50 𝑚𝑙

= 4,3 × 10−3
Outlet
𝑇3
CNaOH = (50 𝑚𝑙) × 0,1 M
0
=( ) × 0,1 M
50 𝑚𝑙

=0
𝑇2−𝑇3
CNa2CO3 = ( 50 𝑚𝑙 ) × 0,1 M × 0,5
0
= (50 𝑚𝑙) × 0,1 M × 0,5

=0
CO2 absorbed = laju alir × [(CN)o-(CN)i]
= 0,033 × [0-4,3 × 10−3]
= -1,419 × 10−4
1
= laju alir × 2 ×[(Cc)i-(Cc)o]
1
= 0,033 × 2 ×[0,022-0]

= 3,63 × 10−4
Saat t = 10

2. Inlet
𝑇3
CNaOH (Cc)i = (50 𝑚𝑙) × 0,1 M
28,2
= (50 𝑚𝑙) × 0,1 M

= 0,0564
𝑇2−𝑇3
CNa2CO3 (CN)i= ( 50 𝑚𝑙 ) × 0,1 M × 0,5
33,3−28,2
=( ) × 0,1 M × 0,5
50 𝑚𝑙

= 5,1 × 10−3
Outlet
𝑇3
CNaOH (Cc)i = (50 𝑚𝑙) × 0,1 M
11,6
= (50 𝑚𝑙) × 0,1 M

= 0,0232
𝑇2−𝑇3
CNa2CO3 (CN)o= ( 50 𝑚𝑙 ) × 0,1 M × 0,5
45,8−11,6
=( ) × 0,1 M × 0,5
50 𝑚𝑙

= 0,0342
CO2 absorbed = laju alir × [(CN)o-(CN)i]
= 0,033 × [0,0342-5,1 × 10−3]
= 9,603 × 10−4
1
= laju alir × 2 ×[(Cc)i-(Cc)o]
1
= 0,033 × 2 ×[0,0564-0,0342]

= 3,663 × 10−4

Saat t = 20

3. Inlet
𝑇3
CNaOH = (50 𝑚𝑙) × 0,1 M
25,6
= (50 𝑚𝑙) × 0,1 M

= 0,0512
𝑇2−𝑇3
CNa2CO3 = ( 50 𝑚𝑙 ) × 0,1 M × 0,5
35,4−25,6
=( ) × 0,1 M × 0,5
50 𝑚𝑙

= 9,8 × 10−3
Outlet
𝑇3
CNaOH = (50 𝑚𝑙) × 0,1 M
4,6
= (50 𝑚𝑙) × 0,1 M

= 9,2 × 10−3
𝑇2−𝑇3
CNa2CO3 = ( 50 𝑚𝑙 ) × 0,1 M × 0,5
46−4,6
= ( 50 𝑚𝑙 ) × 0,1 M × 0,5

= 0,0414
CO2 absorbed = laju alir × [(CN)o-(CN)i]
= 0,033 × [0,0414-9,8 × 10−3]
= 1,0428 × 10−3
1
= laju alir × 2 ×[(Cc)i-(Cc)o]
1
= 0,033 × 2 ×[0,0512-9,2 × 10−3 ]

= 6,93 × 10−4

Saat t = 30

4. Inlet
𝑇3
CNaOH = (50 𝑚𝑙) × 0,1 M
23,5
= (50 𝑚𝑙) × 0,1 M

= 0,047
𝑇2−𝑇3
CNa2CO3 = ( 50 𝑚𝑙 ) × 0,1 M × 0,5
37,5−23,5
=( ) × 0,1 M × 0,5
50 𝑚𝑙

= 0,014
Outlet
𝑇3
CNaOH = (50 𝑚𝑙) × 0,1 M
10
= (50 𝑚𝑙) × 0,1 M

= 9,2 × 10−3
𝑇2−𝑇3
CNa2CO3 = ( 50 𝑚𝑙 ) × 0,1 M × 0,5
46,5−10
=( ) × 0,1 M × 0,5
50 𝑚𝑙

= 0,0365
CO2 absorbed = laju alir × [(CN)o-(CN)i]
= 0,033 × [0,0365-0,014]
= 7,425 × 10−4
1
= laju alir × 2 ×[(Cc)i-(Cc)o]
1
= 0,033 × 2 ×[0,047-0,02]

= 4,455 × 10−4

Saat t = 40
5. Inlet
𝑇3
CNaOH = (50 𝑚𝑙) × 0,1 M
18
= (50 𝑚𝑙) × 0,1 M

= 0,036
𝑇2−𝑇3
CNa2CO3 = ( 50 𝑚𝑙 ) × 0,1 M × 0,5
44−18
= ( 50 𝑚𝑙 ) × 0,1 M × 0,5

= 0,026
Outlet
𝑇3
CNaOH = (50 𝑚𝑙) × 0,1 M
14
= (50 𝑚𝑙) × 0,1 M

= 0,028
𝑇2−𝑇3
CNa2CO3 = ( 50 𝑚𝑙 ) × 0,1 M × 0,5
50−14
= ( 50 𝑚𝑙 ) × 0,1 M × 0,5

= 0,036
CO2 absorbed = laju alir × [(CN)o-(CN)i]
= 0,033 × [0,036-0,026]
= 3,3 × 10−4
1
= laju alir × 2 ×[(Cc)i-(Cc)o]
1
= 0,033 × 2 ×[0,036-0,028]

= 1,32 × 10−4

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