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Autoprep: Spectrometer Page. This Is The Location For The Reference Solution That The System Uses To

This document discusses emission spectroscopy settings and autodilution parameters. It explains that the emission setup location specifies the reference solution used to calibrate the instrument for emission measurements. It also describes autodilution options for preparing calibration standards and diluting samples above the calibration range, including selecting the autodiluter, initial dilution factor for all samples, and pump filling speed.

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Edder Alvarezz Rodriguez
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30 views

Autoprep: Spectrometer Page. This Is The Location For The Reference Solution That The System Uses To

This document discusses emission spectroscopy settings and autodilution parameters. It explains that the emission setup location specifies the reference solution used to calibrate the instrument for emission measurements. It also describes autodilution options for preparing calibration standards and diluting samples above the calibration range, including selecting the autodiluter, initial dilution factor for all samples, and pump filling speed.

Uploaded by

Edder Alvarezz Rodriguez
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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Emission Setup Location

This parameter appears only if you have selected Emission for the measurement
technique on the
Spectrometer page. This is the location for the reference solution that the system uses to
set up
the instrument to make emission measurements. This reference solution is usually the
most
concentrated calibration standard.
AutoPrep
Use this page to select online dilution for the flame technique. If this page appears, make
sure that
the diluter is switched on even if you do not intend to use the diluter, otherwise the system
will
report communication errors.
You can use the diluter to prepare the calibration standards from a stock standard solution.
You
select this option on the Calibration > Standard Concentrations page.
You can also use the diluter to dilute samples that have an analyte concentration higher
than that
of the most concentrated calibration standard. You select the parameters for this on the
Checks >
Beyond Calibration page.
AutoPrep
Select this if you want the AutoPrep to perform dilutions. Even if you do not generally want
to
dilute the samples, you must select this option if you intend to use the option on the
Checks >
Beyond Calibration page to dilute samples that have an analyte concentration higher than
that of
the most concentrated calibration standard.
Dilution factor for all samples
Select the dilution factor that the diluter will initially use for all the sample solutions. The
diluter
does not dilute user-prepared calibration blanks and standards. Select None if you do not
generally want to dilute the samples, but intend to use the option on the Checks > Beyond
Calibration page to dilute samples that have an analyte concentration higher than that of
the most
concentrated calibration standard

Pump Filling Speed


This is the speed at which the pump draws solutions from the autosampler containers into
the
holding coil, expressed as a percentage of the maximum pump speed. If you have viscous
sample
solutions, you may want to reduce the speed. The default pump speed is 50%, you may
increase
the speed above the default value by increments of 10%. Make sure there are no gas
bubbles
entering the sample loop.
Calibration curve technique (see page 213 for more information)

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