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Bpharm 1 Sem Pharmaceutical Analysis 1 Bop 114 2017 18

This document contains the questions from a Pharmaceutical Analysis exam. It covers several key topics: 1) Definitions of pharmaceutical analysis, acid/base theories, molarity, normality and titration concepts. 2) Methods of expressing concentration, classifying acid-base titrations, weak acid/base theory and titration techniques. 3) Differences between iodimetry and iodometry, mass action law, buffer mechanisms, thermogravimetric analysis and salt hydrolysis. 4) Roles of quantitative analysis, precipitation titrations, organic precipitants, primary/secondary standards, solvents in acid-base titrations and redox indicators.

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189 views1 page

Bpharm 1 Sem Pharmaceutical Analysis 1 Bop 114 2017 18

This document contains the questions from a Pharmaceutical Analysis exam. It covers several key topics: 1) Definitions of pharmaceutical analysis, acid/base theories, molarity, normality and titration concepts. 2) Methods of expressing concentration, classifying acid-base titrations, weak acid/base theory and titration techniques. 3) Differences between iodimetry and iodometry, mass action law, buffer mechanisms, thermogravimetric analysis and salt hydrolysis. 4) Roles of quantitative analysis, precipitation titrations, organic precipitants, primary/secondary standards, solvents in acid-base titrations and redox indicators.

Uploaded by

Fuhyjji
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Printed pages: 01 Sub Code: BOP114

Paper Id: 5 0 4 0 Roll No:


B PHARM
(SEM I) THEORY EXAMINATION 2017-18
PHARMACEUTICAL ANALYSIS-I
Time: 3 Hours Total Marks: 100
Notes: Attempt all Sections. Assume any missing data.
SECTION A
1. Attempt all questions in brief. 2 x10 = 20
a. Define pharmaceutical analysis.
b. Define Acid and Base according to lewis theory.
c. Write a formula of Molarity and Normality.
d. Draw the structure of phenolphthalein in two different medium.
e. Define solubility product and show its relation with ionic product.
f. Differentiate between Titrant and Titrand.
g. Define Supersaturation, Co-precipitation, Post-precipitation and Digestion.
h. Define concept of Oxidation and Reduction.
i. Calculate Equivalent weight of Kmno4 in different medium.
j. Differentiate between determinate and indeterminate error.

SECTION B
2. Attempt any three of the following: 10 x 3 = 30
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a. Discuss the method of expressing concentration of solution.


b. Classify Acid-Base titration along their neutralization curve.
c. Explain the theory of weak base or weak acid in non aqueous titration.
d. Discuss titrations involving ceric ammonium sulphate and potassium permanganate.
e. Write a short note on Mohr’s, Volhard’s and Fajan’s method in precipitation titration.

SECTION C
3. Attempt any one part of the following: 10 x 1 = 10
a. Differentiate between iodimetry and iodometry.
b. Write a short note on Law of mass action and Common ion effect.
4. Attempt any one part of the following: 10 x 1 = 10
a. What are Buffers? Explain the mechanism of action of buffer.
b. What are thermogravimetric curves? Explain with example barium as barium sulphate.
5. Attempt any two parts of the following: 5 x 2 = 10
a. Describe the significance of quantitative analysis in quality control.
b. What are precipitation titrations? Discuss effect of Acid, temperature
and solvent on solubility of precipitates.
c. What is salt hydrolysis? Discuss the classification of salt hydrolysis.
6. Attempt any one part of the following: 10 x 1 = 10
a. What are organic precipitants? Also discuss their role in gravimetry.
b. What are primary standards? And how they are differ from secondary standards?
7. Attempt any one part of the following: 10 x 1 = 10
a. What are role of solvents in Acid base titrations?
b. What are Redox indicators? Briefly describe Oxidation-reduction curves.

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