Lab Thesis
Lab Thesis
TIRUCHIRAPPALLI-620015
i
ACKNOWLEDGEMENT
ii
EXPERIMENT DETAILS
EXPT PAGE
DATE DESCRIPTION
NO NO
iii
LIST OF TABLES
iv
LIST OF FIGURES
v
1. IMPACT SENSITIVENESS TEST
1.1 AIM: To determine the impact sensitivity of the given energetic material using
ball fall hammer.
The diagram of the drop weight apparatus used in this study for impact
sensitiveness measurement is shown in Figure 1.1. The equipment was supplied by
Electro Ceramics Private Limited, Pune, India. The design and principle of the
equipment is similar to that of the drop fall hammer equipment of BAM standards. It
consists of a cast steel block with a base, an anvil, supporting columns, guide rods, a
drop mass with release device and an impact device. A steel anvil is screwed on to the
steel block and cast base. The two supporting columns (made from a seamless drawn
steel tube), are bolted to the back of the steel block. The two guide rods fixed to the
column are used to limit the rebound of the drop mass. The apparatus is fixed on to a
concrete block by means of four anchoring screws secured in concrete, so that the
base is in contact with the concrete over its whole area and guides are exactly vertical.
1
1.3 SPECIFICATION:
2kg, 5kg, 10kg weight give the desired impact load range.
Solid cast steel hard bar block.
Hardened steel anvil.
Control column with graduated scale reading to set and calibrated.
1.4 STANDARD:
As per the United Nations (UN) guidelines for Transport of Dangerous Goods
(TDG), the sample exhibiting limiting impact energy of 2J or less is considered too
sensitive.
Limiting Impact Energy: The lowest energy at which at least one explosion occurs in
six trials.
1.5 PROCEDURE:
1.6 OBSERVATIONS:
Height Trial
(in cm) 1 2 3 4 5 6
40
35
30
28
27
25
2
24
23.5
1.7 CALCULATIONS:
3
2. FRICTION SENSITIVENESS TEST
2.1 AIM: To determine the friction sensitivity of an energetic material (match stick
composition is used)
2.3 APPARATUS:
The diagram of the BAM friction tester used in this study for friction
sensitiveness measurements is shown in the Figure 2.1. It consists of a cast steel base,
on which a friction device is mounted. The friction device comprises a fixed porcelain
pin and a moving porcelain plate. The porcelain plate is held in a carriage which runs
in two guides. The carriage is connected to an electric motor via a connecting rod, an
eccentric cam and suitable gearing such that the porcelain plate could retract and
move forward to a distance of 10 mm beneath the porcelain pin. The loading device
pivots on an axis so that the porcelain pin can be changed; it is extended by a loading
arm which is fitted with 6 notches for the attachment of a weight. Zero load is
obtained by adjusting a counter weight. When the loading device is lowered onto the
porcelain plate, the longitudinal axis of the porcelain pin is perpendicular to the plate.
There are different weights of masses up to 10kg. The loading arm is fitted with 6
notches of distances of 11cm, 16 cm, 21cm, 31cm and 36cm from the axis of the
porcelain pin. A weight is hung onto a notch on the loading arm by means of ring and
hook. The use of different weight in different notches results in loads on the pin of 5-
10-20-40-60-80-120-160-240-360 N. Provisions are available for using intermediate
loads, if needed.
4
2.4 STANDARD:
As per the United Nations (UN) guidelines for Transport of Dangerous Goods
(TDG), in a BAM friction tester, a sample is subjected to a frictional load between the
porcelain plate and pin. Samples exhibiting a limiting load of 80N or less are
considered too sensitive.
Limiting frictional load: The lowest frictional load at which atleast one explosion
occurs in six trials
2.5 PROCEDURE:
Load 1 2 3 4 5 6
128
120
108
96
84
80
2.7 RESULT:
6
3. DIFFERENTIAL SCANNING CALORIMETRY (DSC)
3.1 AIM
3.2 THEORY
7
Fig 3.1 a standard output for a polymer from a DSC machine.
From the fig 3.1, it can be seen that a sudden upward jump in the curve signifies an
exothermic process. A sudden drop in heat flux indicates an endothermic process.
It is possible to approximate the heat flow into the sample holder using the following
equation:
K Tb T ……………..(1)
dQ
dT
Tb T0 qt ……………..(2)
The heat capacity is defined as the amount of heat energy required to raise the
temperature of a body by 1K. For a substance with a constant heat capacity:
Q C P T T0 ……………..(3)
It is possible to derive an equation from equations 2 and 3 that forms the basis for the
DSC experiment. This is as follows:
8
CP
T q ……………..(4)
K
ΔT is the difference in temperature between the reference material and the sample.
C P mcP ……………..(5)
Where cp is the specific heat (Amount of heat required to raise the temperature of unit
mass by 1K).
The enthalpy change for a given phase transition may be found by integrating over the
area in which the transition is seen to occur on the DSC plot. This change may be
described by the following integral:
Tf Tf
KT
H C P dt dT ……………..(6)
Ti Ti
q
Where the limits of integration Ti and Tf are the initial and final temperatures over
which the graph is integrated. Therefore it is the area under the curve that gives
information about the enthalpy changes involved in the various transitions.
3.3 APPARATUS
9
As shown in fig 3.3, the reference pan is to remain empty at all times. Signals from
both pans provide information to the computer. This allows it to regulate the
temperature and provide a constant heating rate. Not shown are the gas inlets and
outlets, using these, a chemically inert gas such as Argon or nitrogen may be pumped
through the machine in order to prevent the accumulation of dust. The gas also serves
to remove any volatile chemicals that may be present.
3.4 PROCEDURE
Prepare the samples for analysis. Extreme care should be taken not to
contaminate samples or sample pans with either other chemicals or matter
from human skin. This meant that all equipment is to be handled with
tweezers. Prepare Samples as follows:
Obtain tare weight of the sample pan and lid. Select Sample pans with flat
undersides so as to make the maximum contact possible with the bottom of the
calorimeter. Following this, place between 5 and 10 milligrams of sample in
10
the sample pan and find the mass of the filled sample pan and lid. This is the
mass of sample to be used. Again using tweezers, move the sample pan and lid
to the crimping press where upon crimping the lid sealed the pan. Weigh
another sample pan along with its lid. This, however, leave as empty and seal
using the crimping device, forming the reference pan to be heated along with
the sample.
Place the first sample in the left hand side of the furnace in the calorimeter
while the reference pan should place in the right hand position, where it should
remain for the duration of the experiment.
Avg Heating cycle:
Nitrogen atmosphere, with a gas flow rate of 10Cm3/min, heating rate of
10oC/min from 120oC to 180oC.
Maintain the same gas flow rate, along with the heating rate of 10oC/min. The
only change is that the range of temperature was modified so that it ranged
from 30oC to 250oC. Following this, the furnace was allowed cool to room
temperature before the next sample could be introduced.
Then analyse resulting graphs and information about onset, peak and endpoint
temperatures and changes in enthalpy for the various processes obtained using
the computer software.
3.5 OBSERVATION
The resultant graphs are shown on the next few pages along with the enthalpy changes
and temperature range of each transition. The first of these graphs is for the Indium
reference material.
11
Fig 3.4: Graph between TG % and Temperature
12
3.6 RESULTS
13
4. HAND ARM VIBRATION MEASUREMENT
4.1 AIM
To carry out hand-arm vibration measurements in order to investigate the
Hand Arm vibration of operator and to assess vibration exposure risk assessments
from acquired vibration data.
4.2 THEORY
HAV is vibration transmitted from work processes into workers’ hands and
arms. It can be caused by operating hand-held power tools such as road breakers,
hand-guided equipment such as lawn mowers, or by holding materials being
processed by machines such as pedestal grinders. Regular and frequent exposure to
high levels of vibration can lead to permanent injury. This is most likely when contact
with a vibrating tool or process is a regular part of a person’s job. Occasional
exposure is unlikely to cause injury. Jobs requiring regular and frequent use of
vibrating tools and equipment are found in a wide range of industries, for example:
Building and maintenance of roads and railway, concrete products, Construction,
Concrete products, Foundries etc.
Aim should be to buy the lowest vibration equipment suitable for the job.
Manufacturers identify vibration levels in units of meters per second squared (m/s2).
4.2.1 Effects
Regular exposure to HAV can cause a range of permanent injuries to hands
and arms, collectively known as hand-arm vibration syndrome (HAVS). The injuries
can include damage to the:
1. Blood circulatory system (e.g. vibration white finger)
2. Sensory nerves
3. Muscles
4. Bones
5. Joints
Vibration-induced white finger (VWF) is the most common condition among the
operators of hand-held vibrating tools. Vibration can cause changes in tendons,
muscles, bones and joints, and can affect the nervous system. Collectively, these
14
effects are known as Hand-Arm Vibration Syndrome (HAVS). The symptoms of
VWF are aggravated when the hands are exposed to cold. Workers affected by HAVS
commonly report symptoms such as:
1. Attacks of whitening (blanching) of one or more fingers when exposed to
cold
4.2.2.3 ACIGH
Table 4.1-ACGIH HAV (2006) TLV values
Maximum value of frequency weighted
Total Daily Exposure Duration (hours)
acceleration (m/s2) in any direction
4 to less than 8 hours 4
2 to less than 4 hours 6
1 to less than 2 hours 8
less than 1hour 12
15
4.2.2.4 EU directive
Table 4.2-EU exposure guidelines
Exposure limit value (ELV) 5 m/s2
Exposure action value (EAV) 2.5 m/s2.
4.3 PROCEDURE
3. Mount the accelerometers at the proper hand locations so that they can
measure the vibration transmitted to the hands from the vibrating equipment.
5. Process the outputs from the accelerometers via charge amplifiers and input
to a vibration analyser (Brüel & Kjær PULSE system) for real-time analysis.
6. Activate the vibration analyser a few seconds after the start of equipment
(once stable operation had been achieved) and take measurement for the
duration of 1 minute for free operation.
4.4 MEASUREMENTS
Calculate ax in free air and calculate frequency weighted acceleration along x-axis
(ahwx ) as shown in fig 4.1.
16
4.5 OBSERVATIONS
Plot graph for sensitive frequency range of 8 to 16 Hz and 6.3 to 1250 Hz and take
acceleration on Y-axis and frequency on X-axis.
Table 4.3: Showing calculations for frequency weighted acceleration for a particular
axis from 6.3 to 1250 Hz
Weighting Acceleration
Frequency
Sl No. W i * Ai (Wi * Ai) 2
(Hz) factor (Wi) A i (m/s2)
1 6.3 0.727 0.0109971 0.007995 6.39183E-05
2 8 0.873 0.00778094 0.006793 4.61416E-05
3 10 0.951 0.0200502 0.019068 0.000363579
4 12.5 0.958 0.0084266 0.008073 6.51682E-05
5 16 0.896 0.00845172 0.007573 5.73464E-05
6 20 0.782 0.00673668 0.005268 2.77527E-05
7 25 0.647 0.00892324 0.005773 3.33314E-05
8 31.5 0.519 0.0435089 0.022581 0.000509907
9 40 0.411 0.0165603 0.006806 4.63255E-05
10 50 0.324 0.0420336 0.013619 0.000185474
11 63 0.256 0.0974421 0.024945 0.000622262
12 80 0.202 0.0885625 0.01789 0.000320039
13 100 0.16 0.120538 0.019286 0.000371953
14 125 0.127 0.38796 0.049271 0.002427624
15 160 0.101 0.30932 0.031241 0.00097602
16 200 0.0799 0.279184 0.022307 0.000497593
17 250 0.0634 1.02861 0.065214 0.004252849
18 315 0.0503 2.16501 0.1089 0.011859211
19 400 0.0398 1.45485 0.057903 0.003352761
20 500 0.0314 1.31738 0.041366 0.001711124
21 630 0.0245 0.675726 0.016555 0.000274078
22 800 0.0186 0.571784 0.010635 0.000113107
23 1000 0.0135 0.768718 0.010378 0.000107697
24 1250 0.00894 0.528929 0.004729 2.23599E-05
Σ (Wi * Ai) 2
=0.02830762
17
Table 4.4: Showing calculations for frequency weighted acceleration for a particular
axis from 8 to 16 Hz
4.6 CALCULATIONS
ahw is frequency weighted rms acceleration. Whj is weighting factor for the jth
1/3rd octave band. ahj is the rms acceleration in the jth 1/3rd octave band in
m/s2(given by vibration analyser) n is the number of 1/3rd octave band considered.
18
11 12.5 0.958
12 16 0.896
13 20 0.782
14 25 0.647
15 31.5 0.519
16 40 0.411
17 50 0.324
18 63 0.256
19 80 0.202
20 100 0.160
21 125 0.127
22 160 0.101
23 200 0.0799
24 250 0.0634
25 315 0.0503
26 400 0.0398
27 500 0.0314
28 630 0.0245
29 800 0.0186
30 1000 0.0135
31 1250 0.00894
32 1600 0.00536
33 2000 0.00295
Note: Calculate frequency weighted rms acceleration for both the frequency ranges
i.e.
1) for 6.3 Hz to 1.25 kHz
2) for 8 Hz to 16 Hz
4.7 RESULTS-
19
HAND ARM VIBRATION 6.3 TO 1250 Hz
Acceleration axis in Logarithemic scale
10
1
ACCELERATION (m/s2)
0.1
0.01
0.001
100
125
160
200
250
315
400
500
630
800
12.5
31.5
1000
1250
8
10
16
20
25
40
50
63
80
6.3
FREQUENCY (Hz)
0.012
ACCELERATION (m/s2)
0.01
0.008
0.006
0.004
0.002
0
8 10 12.5 16
FREQUENCY (Hz)
Frequency Peak-rms
Sl No.
in air(Hz) acceleration (m/s2)
1 6.3 to 1250 0.1682
2 8 to 16 0.014004
20
5. WHOLE BODY VIBRATION MEASUREMENT
5.1 AIM
To carry out Whole Body vibration measurements in order to investigate the Whole
Body vibration of operator and to assess vibration exposure risk assessments from
acquired vibration data.
5.2 THEORY
WBV is defined as the vibration experienced by the human body as a result of direct
contact with the vibrating surface. Vibration arises from various mechanical sources
with which humans have physical contact. Vibration energy can be passed on to
operators from vehicles on rough roads; vibrating tools; vibrating machinery; or
vibrating work platforms. It can be transmitted through the feet and legs, the hands
and arms but most commonly through the buttocks in a driving vehicle. If a human
body is subjected to strong vertical vibration it may cause fracturing of spine,
discomfort and adverse effects on health. Regular and frequent exposure to high
levels of vibration can lead to permanent injury. This is most likely when contact with
a vibrating tool or process is a regular part of a person’s job. Occasional exposure is
unlikely to cause injury. Before you buy new equipment, consider any alternative way
of working without using vibrating equipment. If not, introduce a low vibration
purchasing policy in consultation with your managers and safety or employee
representatives and let potential suppliers know about it. We should aim to buy the
lowest vibration equipment suitable for the job. Manufacturers identify vibration
levels in units of meters per second squared (m/s2).
5.2.1 Effects
21
5.2.2.1 Indian Standard- Mechanical vibration and shock- evaluation of human
exposure to whole body vibration IS 2631-2: 2003.
This part of ISO 2631 concerns human exposure to whole-body vibration and shock
in buildings with respect to the comfort and annoyance of the occupants. It specifies a
method for measurement and evaluation, comprising the determination of the
measurement direction and measurement location. It defines the frequency weighting
Wm which is applicable in the frequency range 1 Hz to 80 Hz where the posture of an
occupant does not need to be defined.
5.2.2.2 EU directive
Pulse labshop is a vibration measuring software. The whole body vibrations and hand
arm vibrations can be measured using this software. This software is developed by the
Bruel & Kjaer. The most basic vibrations measurements that can be made are Time
signal and Spectrum analysis. The accelerometer can be attached to anything that the
vibration spectrum or time response can be measured. As shown in fig 5.1, a simple
setup may involve mounting an accelerometer to a table and the response of the
tapping the table can be measured. In order for measurements to be made with Pulse,
a transducer has to be connected to one of the inputs of the analyser.
22
Fig 5.1- Accelerometer with cable & connector and Vibrational analyser
5.3 PROCEDURE
5. Process the outputs from the accelerometers via charge amplifiers and
input to a vibration analyser (Brüel & Kjær PULSE system) for real-time
analysis.
6. Activate the vibration analyser few seconds after the start of vehicle
(once stable operation had been achieved) and take measurement for the
duration of 1 minute.
23
7. The vibration analyser produces a frequency spectrum of acceleration
for z-axis.
5.4 OBSERVATIONS-
Note: Get the value of weighting factor (Wk) and divide the value by 1000 from IS
2631-1: General requirements Table-5.3 corresponding to the required frequencies.
Table 5.2: Showing calculations for frequency weighted acceleration for a particular
axis 1 to 80 Hz on floor
24
5 2.5 0.00398732 0.91 0.003628 1.31657E-05
Σ (Wk * aj)2=
0.006526789
Table 5.3: Showing calculations for frequency weighted acceleration for a particular
axis 2 to 5 Hz on floor
25
4 4 0.00577507 0.818 0.004724 2.23162E-05
Σ (Wk * aj)2
= 0.00005176
Table 5.4: Showing calculations for frequency weighted acceleration for a particular
axis 1 to 80 Hz on seat
26
18 50 0.210461 0.109 0.02294 0.000526255
Σ (Wk * aj)2=
0.004449808
Table 5.5: Showing calculations for frequency weighted acceleration for a particular
axis 2 to 5 Hz on seat
=0.00004113
5.5 CALCULATIONS-
aw is frequency-weighted acceleration.
27
Wk is weighting factor for the jth 1/3rd octave band.
aj is the rms acceleration in the jth 1/3rd octave band in m/s2 (given by vibration
analyser)
2) for 2 Hz to 5 Hz
28
5.6 RESULTS-
Frequency weighted acceleration along z-axis is 0.079 m/s2 for frequency range of 1
Hz to 80 Hz.
0.06
0.05
0.04
0.03
0.02
0.01
0
FREQUENCY (Hz)
2) Frequency weighted acceleration along z-axis 0.0071 m/s2 for frequency range
of 2 Hz to 5 Hz.
0.005
0.004
0.003
0.002
0.001
0
2 2.5 3.15 4 5
FREQUENCY (Hz)
29
3) When accelerometer is placed at seat
Frequency weighted acceleration along z-axis 0.0667 m/s2 for frequency range of 1
Hz to 80 Hz.
0.35
0.3
0.25
0.2
0.15
0.1
0.05
0
1.25
3.15
12.5
31.5
1
4
5
8
10
16
20
25
40
50
63
80
1.6
2.5
6.3
FREQUENCY (Hz)
4) Frequency weighted acceleration along z-axis 0.0064 m/s2 for frequency range
of 2 Hz to 5 Hz.
0.004
0.0035
0.003
0.0025
0.002
0.0015
0.001
0.0005
0
2 2.5 3.15 4 5
FREQUENCY (Hz)
30
5) Comfort reaction to vibration environment for all the frequency ranges are in
the comfortable limit.
31
6. Application of ErgoMaster software in Ergonomic analysis
6.1 AIM: To learn the ErgoMaster Software and to understand its applications
Ergonomic analysis.
ErgoMaster enables users with minimal computer expertise to easily utilize the
system. The user can customize various reports and analysis. The system also includes
detailed on-line help and instructions.
The system allows users to obtain images from a variety of popular packages and
receive such images even via the Internet. The system includes a database, which
enables users to easily save and retrieve their studies including the images.
32
Task Analyst: includes various tools to evaluate task design and perform job
analysis. These tools include Task Assessment, Tool Assessment, RULA,
Work/Rest Cycles, and Discomfort Survey.
Biomechanics Analyst: enables users to easily interface with the University of
Michigan's 3D SSPP in 2D mode (which is purchased directly from the
University of Michigan Software) by simply clicking on the joint positions in
the digital image.
Posture Analyst: provides tools to evaluate an individual's posture as it
pertains to range-of-motion, biomechanics and anthropometrics. These tools
include Posture Assessment, RULA, Dimensional Analysis, and Discomfort
Survey.
Workstation Analyst: provides tools for the evaluation of industrial and/or
office environments for ergonomic risk factors. This includes the assessment
of furniture and equipment. These tools include Workstation Assessment,
Video Display Assessment, Tool/Product Assessment, and Discomfort Survey.
Ergo Product Database: is a resource of ergonomic related products that may
be used as recommendations to environmental layout or tool/equipment
selection. This database does contain sample products but is encouraged to be
user defined.
Getting Started: contains general tools to begin an ergonomic evaluation.
General Information, Discomfort Survey.
Many of the modules have image digitization capability. Users have a variety of tools
to enter information (text and basic drawings) in the image area and obtain
information from the image itself (such as distances and angles) as well as edit the
image itself.
These modules include the capability to digitize any digital image converted from
video frames and other digital and scanned images (captured using a variety of
popular packages). Users can also capture images from an AVI file. Images or AVI
files can be received from clients or plants by sending them over the Internet and then
simply importing them into ErgoMaster's image areas.
The ability to incorporate the image of the job greatly increases the effectiveness in
the presentation of the final report and recommendations.
33
Discomfort Survey
Posture Assessment
The Posture Assessment function allows the user to select various joints of interest
and easily perform angular and distance calculations. The user has the ability to
customize the evaluation of risk associated with various work postures.
34
RULA
The RULA posture analysis is used to investigate the exposure of workers to the risk
of upper limb disorders. RULA provides a record of each operator's general posture
with particular reference to the trunk, neck and upper limbs. RULA examines several
risk factors associated with the body posture, loads, and muscle use and compiles
these factors into a posture score.
Dimensional Assessment
The Dimensional Assessment function easily calculates linear and angular dimensions
from the captured image. The software includes a calibration feature to properly
calculate linear distances. Users can also enter text and basic drawings in the image
area as well as edit the image.
6.3 RESULT-
ErgoMaster Software is studied and its various applications in Ergonomic analysis has
been understood.
35
7. DETERMINATION OF FUME EMISSION RATE DURING
ARC WELDING
7.1 AIM: To measure the fume emission rate from arc welding.
7.2 APPARATUS REQUIRED: Fume Test Chamber, Filter Paper, and Precision
Weighing Balance.
7.3 THEORY:
Welding fumes are small particles formed by the condensation of metals and
metal oxides that become volatile due to the intense heat of the arc; whose presence
poses great health risks to the people inhaling it. The mass rate of these fumes
depends on the following: base material, filler metal, welding process adopted and
chemical composition of the shielding gas mixture. The acute and chronic health
effects due to exposure to welding fumes are dependent on the exposure duration and
its severity. Despite the automation in welding and control technology, welders are
still exposed to hazardous fumes and gases. Further, the concern of industries to
reduce the costs related to the worker’s sick leave (both short and long terms) and the
need to increase worker’s productivity is also increasing nowadays. The revision of
Permissible exposure limits in recent years has resulted in recent years has resulted in
even lower limits on the release of toxic substances during welding, and this
downward trend can be expected to continue in the coming years as a way to reduce
the incidence of work-related diseases in welders. Accurate Fume generation data is
thus necessary for sophisticated control strategies.
International Standard: The collection of welding fumes using the “Fume Test
Chamber” conforms to the ISO 10511-1 standard.
a. Test Chamber: Having a top section in which a filter is positioned to capture all
fume produced, of a construction that minimizes the deposition of fume on the
internal surface and attached to a suitable extraction unit.
36
b. Filters: Manufactured from glass or quartz fibre for emission rate testing. The
filters shall be sufficiently robust that they do not tear or perforate during testing and
shall not be friable that fibres can be lost from the filter during handling.
c. Extraction Unit: Capable of maintaining an adequate flow rate through the filter.
d. Turn Table: Variable speed and Capable of providing rotation to the base plate
7.5 PROCEDURE:
a. Weigh the filter paper in a precision weighing balance and mount it in the Fume
Test Chamber.
b. Adjust the speed of rotation of the turn table to approx. 10rev/hr corresponding to
the normal speed of welding.
d. Turn ON the welding power supply and start welding. Do welding for a period of
60 s and leave the extraction unit running for another 90s to ensure maximum fume
collection efficiency.
37
f. Take out the filter paper and weigh it again in the precision weighing balance.
g. Note the difference in weight of the filter paper before and after fume collection.
7.6 CALCULATIONS:
0.0986
= g/min = 98.6 mg/min
1
7.7 OBSERVATIONS
7.8 RESULT:
38
8. PERSONAL EXPOSURE MEASUREMENTS TO WELDING
FUMES
8.1 AIM:
To find out the breathing zone concentration of fumes for an automatic welding
process
8.3 THEORY:
Welding is the principal industrial process used for joining metals. The form
welding refers to the joining process of two materials that coalesced at their
contacting surface by the application of pressure and heat.
Fumes are formed when hot metal vapor’s cool and condense into very small
particles that stay suspended in gas. The particle may be metal or metal compound
and are often smaller than one micrometer.
The PCXR8 (as shown in fig 8.1) Universal Sample Pump is a constant flow
air sampler suitable for a broad range of applications. It is ideal for industrial hygiene
studies as well as environmental testing.
39
Fig 8.1 PCXR8 Universal Sample Pump
Compensation Range:
1000 to 2500 ml/min at 40 inches water back pressure
3000 ml/min at 35 inches water back pressure
4000 ml/min at 20 inches water back pressure
5000 ml/min at 10 inches water back pressure
40
Compare the information in this table to pump compensation range to determine
appropriate applications
8.5 STANDARDS:
Conforms to the procedure for sampling airborne particles in the breathing zone of a person
who performs welding and allied processes ISO 10882-1:2011
8.6 PROCEDURE:
1. Calibrate the pump of the sampler for a standard flow rate of 2 l/min.
2. Prior to welding those parameters which likely influence the mass and composition
of fumes were selected and it ranges were based on initial experiment trials.
3. Attach one end of the personal air sampler having a filter paper-cassette
arrangement to the lapel of the welder behind his face shield.
5. Measure the filter paper prior to and after sampling and find out its difference to get
the mass of fumes collected.
8.7 OBSERVATIONS:
Initial Final
Trial Current BZC
weight weight
no. (A) mg/m3
(g) (g)
1 120 0.0165 0.0168 12.5
41
8.8 CALCULATIONS:
For Trial No 1:
0.0003 x 1000
= mg/l
2 x 12
= 12.5 mg/m3
8.9 RESULT: The average air borne particle concentration in the breathing zone of
the welder = 72.925 mg/m3
42
9. HIGH-VOLUME SAMPLER
9.1 AIM: To determine the amount of suspended particles in air using respirable dust
sampler.
9.3.1 Specifications:
9.3.2 Standards: 40 CFR Part 50, Appendix B - Reference Method for the
Determination of Suspended Particulate Matter in the Atmosphere (High-Volume
Method)
9.4 PROCEDURE:
1) Mount the pre-weighted filter paper on the filter holder as shown in fig 9.1.
2) Check whether auxiliary power and cord provided with the system is plugged
off when blower unit is off.
3) Put the sub main switch of the flow controller on “manual” mode.
4) Place the auto switch of the timer in the leftmost position.
5) Note down the initial time.
6) Switch on the power to the flow controller unit which is real sacked and
provided on the panel.
7) Power ON the blower unit using the MCB.
8) Slowly turn the flow control knot until you reach a reading of 1mg/min.
9) Put the auto manual switch of the flow controller in the “auto” mode. This
enables the auto slowdown features.
43
Fig. 9.1 Schematic of a high volume sampler
9.5 PRECAUTIONS
44
9.6 CALCULATION:
= 1.275 mg/m3
= 0.85 mg/m3
9.7 RESULT:
45
10. STUDY OF PERSONAL PROTECTIVE EQUIPMENTS (PPE)
10.1 INTRODUCTION
As a safety engineer, you must assess your workplace to determine if hazards are
present that require the use of PPE. If such hazards are present, you must select PPE
and require employees to use it, communicate your PPE selection decisions to your
employees, and select PPE that properly fits your workers.
You must also train employees who are required to wear PPE on how do the
following:
46
10.2 TYPES OF PPE:
Wearing earplugs or earmuffs can help prevent damage to hearing. Exposure to high
noise levels can cause irreversible hearing loss or impairments well as physical and
psychological stress. Earplugs made from foam, waxed cotton, or fiber glass wool is
self-forming and usually fit well. A professional should fit employees individually for
moulded or preformed earplugs. Clean earplugs regularly, and replace those you
cannot clean. Hearing protectors are required to be tested according to the
International Organization for Standardization (ISO) acoustical testing standard, ISO
4869 Part 1 and the Single Number Rating (SNR) or High/Middle/Low (HML)
ratings are calculated according to ISO 4869 Part 2. An SNR is a single number
rating system determined according to International Standard ISO 4869. The tests are
carried out by commercial laboratories that are independent of the manufacturers.
Like NRRs, SNRs are expressed in dB's and are used as a guide for comparing the
potential noise reduction capability of different hearing protection devices. A typical
ear plug and earmuff is shown in the fig 10.1.
47
The amount of on-the-job noise exposure can be determined through various testing
devices; excessive noise is generally defined as exposure to 85 or more decibels of
sound over an 8 hour period. According to OSHA, hearing protection is required for
all employees at this degree of exposure as in table 10.1. This OSHA Action Level,
however, will vary depending upon the decibel level of the surrounding environment.
For example, if a worker is exposed to 100dB in a 2 hour period, he or she is also
required to wear hearing protection.
6 92
4 95
3 97
2 100
1.5 102
1 105
.5 110
<.25 115
A typical Comparison of hearing protection between Ear plug and Ear Muff is given
in Table 10.2.
48
Table 10.2: Comparison of hearing protection.
49
Fig10.2: Cross section of a safety helmet.
The brim shall be continuous around the dome. The position of ventilation holes shall
be such that the central axis of the holes is almost horizontal when the helmet is in
normal wearing position. The diameter of any hole shall not exceed 6 mm nor the
edges of adjacent holes closer than 15 mm. The minimum number of holes on each of
the two sides shall be not less than 3 and total aggregate area of holes shall not less
than 180 mm2 and not exceeds 300 mm2. The mass of a complete helmet without
attachments and with or without peak (where not provided) may not exceed 400 g. If
the mass exceeds 400 g, this mass determined to the nearest 35 g shall be shown on a
label attached to the helmet.
Other international standards for safety helmets, Each hard hat is specified by both
Type and Class:
i. Types:
ANSI Type I / CSA Type 1 hard hats meet stringent vertical impact and
penetration requirements.
ANSI Type II / CSA Type 2 hard hats meet both vertical and lateral impact and
penetration requirements and have a foam inner liner made of expanded
polystyrene (EPS).
ii. Classes:
c. Water flowing over the whole outer surface of the shell at room temperature
for 4 hours at a rate of 1 l/min.
51
measurement of the depth of a penetration or dent including the
thickness of the material of the shell shall not exceed 10 mm.
III. Flammability Resistance
Helmet shell shall be tested with the helmet upside down, and the
burner angled at 45° to the vertical, the end of the flame shall be applied
to the outside of the shell at any suitable point between 50 and 100 mm
from the crown for a period of 10 seconds. The plane tangential to the
test point shall be horizontal. The shell shall be examined for flaming 5
seconds removal of the flame. The material of the shell shall not burn
with emission of flame after a period of 5 seconds following removal of
flame.
IV. Electrical Resistance
Invert the helmet and place it on a frame in a suitable container with a
solution of 6 g/l of sodium chloride in water, in the container and the
helmet to within 12 mm of the junction of the brim and the dome, or, if
the helmet is provided with holes to a depth of 12 mm below the holes.
10Allow the helmet to remain in the solution for a period of 18 to 24
hours. Maintain the temperature of 25° to 35°C during this period. Then
apply an alternating voltage of 2 000 V (rev/s) at 50 Hz and of
approximately sine wave form, for one minute between electrodes
placed in the solution inside and outside the helmet respectively. If no
electrical breakdown occurs, disconnect the high voltage supply and
connect a milliammeter in the circuit on each side of the electrode.
Raise the test voltage slowly observing the ammeter reading, until the
applied voltage is 2000 V. An automatic tripping device may be used in
the circuit in addition to the milliammeter.
V. Water Absorption
Weigh the sample (full shell). Immerse for 24 hours in water, at a
temperature of 25° to 35°C. Remove from water, dry the surfaces by
wiping them, and weigh them again. Report the average gain in mass as
a percentage and shall not absorb water more than 5 percent of its mass.
VI. Heat Resistance
Place the shell for 15 minutes in an oven maintained at a temperature of
93 ± 5°C. The shell shall be shielded from direct radiation during the
52
test. Remove the shell from the oven and examine for separation,
distortion or softening and the shell shall not separate, distort or soften.
53
tangential to a point not less than 10mm posterior to the corneal plane and not less
than 10mm in height (8mm for the small head form) above/below the horizontal plane
as in fig 10.3.
High Mass and High Velocity Impact forces to be tested remain essentially the same
as the prior standard. The high mass pointed projectile is pointed and weighs 500
grams and is dropped from a height of 50 inches. The high velocity test uses a steel
ball.25 inches in diameter that is fired at 150 feet per second at the lens in the test
frame.
I. Safety shoes:
Safety Footwear Standards EN345 / EN ISO 20345:2007 / EN ISO 20345:2011. The
EN ISO 20345:2007 standard sets out minimum requirements that safety footwear
must be successfully tested against .The EN ISO 20345:2011 standard sets out new
tougher minimum requirements that safety footwear must be successfully tested
against. The standard specifies all safety footwear must have toe protection. In
addition to different protective features footwear can be represented by a combination
of letters. Cross section of safety boot is given in fig 10.4.
54
Fig10.4: Cross section of safety boot
a) Toe protection (SB): Toes are a very vulnerable part of your body, especially
in a work place. Toe protection must withstand a 200 joule impact..
Something heavy falling from a low height could have a lot less energy than
something lighter from a much higher height. As well as impacts the toe area
must withstand a resting mass of well over 1000kg. Most people have heard
of steel toe cap boots but the protection doesn't have to be steel. In fact there
are advantages to alternatives. Non-metallic protection can be equally as
strong but lighter.
b) Antistatic protection (A): Clothing, seating materials, and climate factors can
cause a build up a static charge of electricity in the body. Some materials in
footwear can over insulate the body causing the charge to be held. When you
then touch something the charge can rush from your body quickly causing a
spark and a small uncomfortable shock. Antistatic footwear will significantly
reduce this effect but does not offer full protection for exposure to electronics
and explosives work. You will need Electro-Static Protection (ESD) for this.
c) Midsole penetration protection (P) - SB-P, S1-P, S3, S5: Sharp objects where
we walk and stand are significant risk not only in the workplace but also
outdoors and at home. Midsole protection will guard against nails and other
objects. To meet this standard the footwear must be able to resist a
penetration force of 1100N. Midsole protection is provided in one of these
methods: a stainless steel insert in the sole, aluminium insert in the sole, or by
55
Kevlar insole. The Aluminium and Kevlar solutions are the most flexible and
lightest and cover the greatest area of the foot. Kevlar insoles also offer much
higher thermal insulation.
e) Water Resistant Upper (WRU): Water resistant upper, not used on all rubber
or polymeric footwear.
g) Insulation against Cold (CI): Insulation against cold: tested for 30 minutes at
1 -20°C.
h) Insulation against heat (HI): Insulation against heat: tested for 30 minutes at
150°C.
Respirators serve to protect the user from breathing in contaminants in the air, thus
preserving the health of one's respiratory tract. There are two main types of
respirators. One type of respirator functions by filtering out chemicals and gases or
airborne particles from the air breathed by the user. Gas masks and particulate
respirators are examples of this type of respirator. A second type of respirator
protects users by providing clean, respirable air from another source. This type
includes airline respirators and self-contained breathing apparatus (SCBA). OSHA's
Respiratory Protection Standard 29 CFR 1910.134 gives the standards for major
requirements of respiratory protection standards. Fit tests are required to be
conducted to ensure the compatibility with users.
56
10.2.6. Hand and Arm protection:
It depends on
-Nature of contact
-Grip requirement
It includes
-temperature protectives
Types are:
-Laboratory coats
-Jackets
-Apron
-Surgical gown
57