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GC Ion Trap

GC

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0% found this document useful (0 votes)
138 views

GC Ion Trap

GC

Uploaded by

Suwaibah AH
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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chromatography

The Thermo Scientific ITQ™ Series

Product Specifications
of ion trap mass spectrometers
comprises a family of fully
upgradeable systems designed to
provide high performance and
high specificity. Developed for a
wide range of applications from
routine GC/MS to research-grade
ion trap MS, these new GC/MS
systems address your lab’s analyt-
ical needs now, while providing
ITQ Series GC/MS Ion Trap clear pathways for upgrading to
Mass Spectrometers meet your future needs.
Mass spectrometer performance that meets
your lab’s needs – now and in the future

ITQ Series of Ion Trap Mass Thermo Scientific ITQ 1100™ GC/MSn
Spectrometers • Mass range to 1100 amu in full scan
mode covers most GC-able compounds
Thermo Scientific ITQ 700 GC/MS

• Standard with the best full scan EI
• Rugged performance for routine full scan
performance, plus MSn, vacuum interlock,
applications
and Data Dependent™ scanning
• Combined with Thermo Scientific FOCUS™
• Features advanced MSn modes new for
GC to create a system perfect for labs
the ITQ Series – Automated Collision
with small spaces and tight budgets
Energy (ACE) and our patented Pulsed Q
• Standard with best full scan EI perform- Dissociation Mode (PQD)
ance – upgrade to MSn, chemical ionization,
• Upgrade to chemical ionization and direct
vacuum interlock, direct sample probe
sample probe
Thermo Scientific ITQ 900™ GC/MS
External Ion Source
• Expanded mass range extends the number
of compounds that can be analyzed • External ionization standard on all
• Step up to the Thermo Scientific TRACE GC ITQ systems
Ultra™ gas chromatograph for versatile • EI and optional CI or EI/CI sources, with
options for injection and detection exchangeable ion volumes
• Standard with best full scan EI perform- • Electron energy adjustable between 0 and
ance – upgrade to MSn, chemical ionization, 130 eV and emission current up to 850 µA
vacuum interlock, direct sample probe • Independently-controlled heating from
125 °C to 300 °C for stable operation and
superior chromatographic integrity

Part of Thermo Fisher Scientific


Product Specifications

Quadrupole Ion Trap Mass Analyzer ITQ 900 and ITQ 1100 Gas Data System Software & Options
• Unit mass resolution throughout the Chromatograph Features • Xcalibur™ Data system, common platform
mass range for all MS systems
Thermo Scientific TRACE GC Ultra
• Scan rate of 5555 amu/sec • EnviroLab™ Forms Software
• Multiple-level temperature program with
• Patented Automatic Gain Control (AGC) – seven ramps and eight levels settable • QuanLab™ Forms Software
the ion trap is always filled with the from 0.1 °C to 120 °C/min • ToxLab™ Forms Software
optimum number of ions
• Eight independent heated zones for indi- • NIST, Wiley, Pfleger-Maurer-Weber and
• Durable, inert materials guarantee long vidual control of injectors and detectors Pesticide libraries
life and simple maintenance plus auxiliary zones
• No tools required for analyzer maintenance • Superior oven cooldown for increased Installation Requirements
• Independently pressurized for stable sample throughput – typically 450 °C to
operation 50 °C in 250 seconds Supplies
• Capillary split/splitless injectors with • Power: 120 Vac +6%/-10% or 230 Vac
Detection System Digital Pressure and Flow Control (DPFC) ± 10%, 50/60 Hz
• Post-acceleration ± 10 kV conversion including gas saver and septum purge • Helium: purity 99.999% with less than
dynode for efficient positive and negative • Maximum oven temperature 450 °C one ppm each of water, oxygen, and total
ion detection hydrocarbons
• Off-axis, discrete dynode electron multiplier TRACE GC Ultra Options • CI reagent gases: methane, isobutane,
with extended dynamic range ammonia or carbon dioxide with
• Sub-ambient cooling to -99 °C with LN2
• Digital electronic noise discrimination purity 99.99%
or -55 °C with CO2
• Proprietary Pulsed Positive Ion/Negative • Programmable Temperature Vaporizer Environment
Ion Chemical Ionization option to acquire (PTV) for split, cold split, splitless and • Complete system averages 3940 W
positive and negative CI spectra on alter- large volume injection (13,450 Btu/h) output when considering
nating scans in the same injection • Cold on-column injector for true on-column air conditioning needs
and large volume injections • Operating environment must be 15 – 31 °C
Inlet/Vacuum Interlock Option • Additional GC detector(s) (59 – 88 °F) and relative humidity must be
• Standard with ITQ 1100, optional with 40 – 80% with no condensation. Optimum
ITQ 700 and 900 systems operating temperature is 18 – 26 °C
Standard Installation
• Easily remove ion volumes for fast (65 – 78 °F)
Specifications
switching from EI to CI, from GC to
probe analysis, and for routine source Electron Ionization System Dimensions/Weights
maintenance Hot splitless injection of 1 pg octafluoro- Complete GC/MS system requires 2 m (6')
naphthalene (OFN) in isooctane produces of linear workbench space. Allow 16 cm (6")
ITQ 700 Gas a signal to noise of 100:1 for m/z 272 in of clearance behind the instrument (32 cm if
Chromatograph Features full scan. using autosampler). Additional space should
Thermo Scientific FOCUS GC be allotted for data system and printer.
• Small footprint for optimal bench utilization Negative Chemical Ionization
Mass Spectrometer
• Temperature programmable with seven Hot splitless injection of 1 pg of decafluoro-
ramps and eight levels, settable from (height x width x depth)
benzophenone (DFBZ) in methylene chloride
0.1 °C to 120 °C/min 44 x 33 x 68 cm (17 x 13 x 27 in)
produces a signal to noise of 1000:1 for
• Compatible with standard capillary Weight: 45 kg (98 lbs)
m/z 362 in full scan using methane as a
column cages TRACE GC Ultra
reagent gas.
• Oven cool-down: 350 °C to 50 °C in 44 x 61 x 65 cm (17 x 24 x 25.5 in)
270 seconds Positive Chemical Ionization Weight: 55 kg (120 lbs)
• Capillary split/splitless injector with
Digital Pressure and Flow Control (DPFC) Hot splitless injection of 100 pg of DFBZ in FOCUS GC
with gas saver and septum purge methylene chloride produces a signal to
44 x 35 x 51 cm (17 x 14 x 20 in)
noise of 100:1 for m/z 363 in full scan using
Weight: 30 kg (66 lbs)
Direct Probe System Option methane as a reagent gas. Methane adduct
• Switch to probe in under three minutes ion [M+ 29]+ must be present.
with GC interface undisturbed
• Available in two styles: rapid heating
filament Direct-Exposure Probe (DEP) or
slower volatilization Direct-Insertion
Probe (DIP)

Thermo Fisher Scientific,


Austin, TX USA is ISO Certified.
©2008 Thermo Fisher Scientific Inc. All rights reserved. All trademarks are the property of Thermo Fisher Scientific Inc. and its subsidiaries.
Specifications, terms and pricing are subject to change. Not all products are available in all countries. Please consult your local sales representative for details. PS10235_E 02/08M

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