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The Empirical Formula of Magnesium Oxide

The experiment aimed to determine the empirical formula of magnesium oxide. Magnesium ribbon was burned in a crucible and the mass of the resulting magnesium oxide was measured. Based on the data collected, the empirical formula was determined to be MgO, with a ratio of 1 magnesium atom to 1 oxygen atom. Key steps in the procedure included cleaning the magnesium to remove any initial oxide layer, covering the crucible during burning to contain the reaction, and repeating the heating/cooling/weighing steps until the mass remained constant to ensure full reaction of the magnesium.

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1K views3 pages

The Empirical Formula of Magnesium Oxide

The experiment aimed to determine the empirical formula of magnesium oxide. Magnesium ribbon was burned in a crucible and the mass of the resulting magnesium oxide was measured. Based on the data collected, the empirical formula was determined to be MgO, with a ratio of 1 magnesium atom to 1 oxygen atom. Key steps in the procedure included cleaning the magnesium to remove any initial oxide layer, covering the crucible during burning to contain the reaction, and repeating the heating/cooling/weighing steps until the mass remained constant to ensure full reaction of the magnesium.

Uploaded by

みゆ マイクロ
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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EXPERIMENT:

THE EMPIRICAL FORMULA OF MAGNESIUM OXIDE.


To determine the empirical formula of magnesium
AIM
oxide.
Problem
What is the empirical formula of magnesium oxide ?
Statement

Hypothesis The empirical formula for magnesium oxide is MgO.

Manipulated variable : Magnesium ribbon


Variables Responding variable : Mass of magnesium oxide
Fixed variables : Excess water / Magnesium ribbon

Crucible with lid, tongs, Bunsen burner, Tripod stand,


Apparatus
Pipe-clay triangle and balance.

Materials 10 cm magnesium ribbon, Sandpaper

Figure

1. A crucible and its lid are weighed.


2. A 10 cm length of magnesium ribbon is cleaned with
氧 化 物
sandpaper to remove the oxide layer on its surface.
3. The ribbon is rolled up / coiled loosely and put inside
Procedure
the crucible. The crucible and its lid and content are
weighed.
4. The apparatus is set up as shown in Figure.
5. The crucible is heated strongly without its lid.
6. When the magnesium starts to burn, the crucible is
covered with its lid.
7. Using a pair of tongs, the lid is carefully raised a little at
间 隔
intervals.
8. When the burning is complete, the lid is removed and
the crucible is heated strongly for 1 to 2 minutes.
9. The crucible with its lid still on is allowed to cool to room
temperature.
10. The crucible with its lid and content are weighed again.
11. The processes of heating, cooling and weighing are
repeated until a constant mass is obtained. The constant
mass obtained is recorded.
Description Mass(g)
Crucible + lid x
Crucible + lid + magnesium y
Crucible + lid + magnesium oxide z
Magnesium y-x
Oxygen z–y
Data &
Observation
Element Magnesium, Mg Oxygen, O
Mass (g) y–x z-y
Number of y–x z–y
moles of atoms 24 16
Simplest ratio of
moles
1) Magnesium reacts with oxygen in the air to form
white fumes ( magnesium oxide ).
Mg + O2 → 2MgO

2) Why is the magnesium ribbon cleaned with


Discussion
sandpaper before use ?
to remove the oxide layer on the surface of
magnesium ribbon.

3) State the reasons for the following.


a) Covering the crucible with lid as soon as the
magnesium starts burning to prevent the
escaping of white fumes.

b) Raising the lid at intervals during heating to allow


oxygen to enter to react with magnesium.

c) Heating, cooling, weighing process is repeated


until a constant mass is obtained to ensure all the
magnesium had reacted completely.

4) This method can also be used to determine the


empirical formulae of oxides of other high reactivity
metals such as calcium oxide, aluminium oxide and
zinc oxide.

Conclusion The empirical formula for magnesium oxide is MgO.

o Magnesium ribbon is cleaned with sandpaper.


- to remove the oxide layer on the surface of
magnesium ribbon.

o Covered the crucible with lid immediately when


magnesium starts to burn.
- to prevent the escaping of white fume.
Precautions
o The lid is raised a little at intervals.
- allow oxygen gas to enter to react with
magnesium.

o Heating, Cooling, Weighing process is repeated


until a constant mass is obtained.
- ensure all the magnesium had reacted completely
with oxygen.

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