Experiment On Basic Concepts: Experiment 4.1 Measurement of Viscosity by Redwood Viscometer
Experiment On Basic Concepts: Experiment 4.1 Measurement of Viscosity by Redwood Viscometer
EXPERIMENT 4.1
Measurement of Viscosity by Redwood Viscometer
Learning Objectives
Determine the kinematic and dynamic viscosity of fluid using Redwood viscometer.
Apparatus
1. Redwood viscometer
2. 50 mL measuring flask
3. Thermometers (2)
4. Weighing balance.
Experimental Set-up
Figure 4.1 shows the experimental set-up of Redwood viscometer.
Theory
Viscosity is the property of the fluid that offers resistance to the relative motion between layers of fluid.
It represents fluidity of the fluid. The fluidity and viscosity are inversely proportional. That is, highly
viscous fluid is less fluidic and low viscous fluid (thin fluid) is highly fluidic.
Figure 4.1 Experimental set-up of Redwood viscometer.
According to Newton’s law of viscosity, the shear stress, τ, developed between two layers of the
fluid is proportion to the velocity gradient du/dy. That is,
du
τ∝ (4.1)
dy
du
τ =μ (4.2)
dy
where μ is the dynamic viscosity, absolute viscosity or simply viscosity of the fluid. It is expressed in N∙
s/m2 or in poise (P). Another way of defining the viscosity is the kinematic viscosity, v, defined as
μ
v¿ (4.3)
ρ
where ρ is the mass density of fluid. Kinematic viscosity is expressed in m2/s in SI units.
Redwood viscometer is the standard commercial viscometer used to measure viscosity of liquids.
It works on the principle that the quality of a certain volume liquid flowing through the orifice is
proportional to the time of flow. The rate of flow will be proportional to kinematic viscosity and hence
kinematic viscosity, v, is determined using the time, t. the kinematic viscosity, v, is given by
B
v¿ At− (4.4)
t
where A and B are constants determined by calibration. The values of A and B are supplied by the
suppliers.
Procedure
1. Place the Redwood viscometer on a level platform and level it with the help of leveling
screws.
2. Fill the water bath with sufficient water.
3. Close the orifice valve by the ball fitted with wire. Fill the oil cup with required quantity of
oil.
4. Note down the mass of empty flask, m1.
5. Place the empty flask below the orifice.
6. Fix the thermometers one in each oil cup and water bath.
7. Switch on the heater and maintain a particular temperature in the water bath by continuous
stirring.
8. Once the constant temperature is reached, lift the ball valve and allow the liquid to drain
into the flask. Start the stop watch simultaneously.
9. Once the flask is filled up to 50 mL marking, stop the stop watch and record the time.
10. Take out the flask and find its mass, m2.
11. Repeat the procedure for various temperatures.
Observations
1. Mass of empty flask, m1 = . . . . . . . . . . g
2. Volume of the liquid, V = 50 cc.
3. Redwood constants, A = 0.0026 and B = 1.79 for 34 < t < 100 s.
A = 0.00247 and B = 0.5 for t > 100 s.
Graphs
1. Plot temperature versus Kinematic viscosity.
2. Plot temperature versus Absolute viscosity.
Nature of Graphs
The typical nature of graphs shown in figure 4.4.
Possible Errors
1. Error in the measurement of the weight of the flask.
2. Mistake in noting the time of the collection of the liquid.
3. Error in measurement of the temperature of the liquids.
Precaution
1. Properly level the viscometer.
2. Stir the liquid properly and note the temperatures.
3. Open the orifice correctly so as to avoid wastage of liquid.
4. Maintain proper earthing of electrical connections.
5. Operate the equipment under the supervision of laboratory technical staff.
6. In case of emergency, contact the laboratory technical staff.