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Parameter Name EPA Approved Method Reference

Standard Operating Procedures (SOPs) are written instructions that explain how to perform analytical methods and tasks in the field or laboratory. SOPs describe all aspects of an analysis, including sample collection and preservation, instrumentation, reagents, calibration, sample analysis, quality control, data handling, and safety. The document provides a standardized format for developing technical SOPs, which includes sections for scope, summary of method, definitions, health and safety, interferences, sample handling, instrumentation, reagents, standards preparation, calibration, sample analysis, quality control, data management, references, waste disposal, revision history, and appendices. Adhering to a consistent SOP format helps to ensure procedures are performed correctly and results

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36 views

Parameter Name EPA Approved Method Reference

Standard Operating Procedures (SOPs) are written instructions that explain how to perform analytical methods and tasks in the field or laboratory. SOPs describe all aspects of an analysis, including sample collection and preservation, instrumentation, reagents, calibration, sample analysis, quality control, data handling, and safety. The document provides a standardized format for developing technical SOPs, which includes sections for scope, summary of method, definitions, health and safety, interferences, sample handling, instrumentation, reagents, standards preparation, calibration, sample analysis, quality control, data management, references, waste disposal, revision history, and appendices. Adhering to a consistent SOP format helps to ensure procedures are performed correctly and results

Uploaded by

BIPL REPORT
Copyright
© © All Rights Reserved
Available Formats
Download as PDF, TXT or read online on Scribd
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Standard Operating Procedures (SOPs) Format

Technical SOPs are written instructions on how to perform a specific analytical method and/or
task in the field or laboratory. SOPs are also used to explain how to collect a sample and
preserve it to maintain the sample integrity. The SOP must explain all aspects associated with an
analysis. More information concerning technical SOPs can be found at
http://www.epa.gov/sites/production/files/2015-06/documents/g6-final.pdf.

Use the following format for developing a technical SOP. Include on the title page and in the
header of each method the following information:

Laboratory Name: Revision Date:


SOP ID Number: Revision Number:
Issue Date:

Parameter Name
EPA Approved Method Reference

A. Scope and Applicability


Describes the purpose of the process or procedure, types of samples analyzed, and any
organization or regulatory requirements, as well as any limits to the use of the procedure.

B. Summary of the Method


Provides a brief explanation of the procedure.

C. Definitions
Defines any acronyms, abbreviations, or specialized terms used in the methodology and
SOP.

D. Health & Safety


Indicates operations and/or chemicals that could result in personal injury or loss of life
and explains what will happen if the procedure is not followed or is followed incorrectly.

E. Interferences
Describes any component of the process that may interfere with the accuracy of the final
product. Includes physical or chemical properties of the sample.

F. Sample Handling, Preservation, and Storage


Documents the sampling and collection requirements for each type of sample (NPDES,
Drinking Water, and Solid and/or Hazardous Waste). Specifies the maximum required
holding time from the time of collection along with the temperature and chemical
preservative. Documents the storage conditions for samples before analysis.

G. Instrumentation and Equipment


Lists all instrumentation and equipment that are necessary to perform the analysis/test.
Specifies the manufacturer and model number of all instruments.
H. Reagents, Standards, and Consumable Materials
Lists all reagents, standards, and materials needed to perform the analysis/test. Specifies
the source by documenting the manufacturer, catalog number, concentration, and any
other pertinent information.

I. Standard and/or Reagent Preparation


Documents the preparation procedure for all standards and reagents. Specifies the
concentration at which all standards and/or reagents are prepared and the storage
conditions and maximum holding times for all standards and reagents. Specifies the
procedure for necessary standardization of reagents and the frequency performed.

J. Instrument Calibration Procedures


Documents the calibration procedures and frequency of calibration for each instrument.
Includes initial calibration, and calibration verification procedures along with the
acceptance criteria for a valid calibration.

K. Sample Analysis Procedures


Documents step-by-step procedures for analyzing routine and quality control samples.

L. Quality Control
Includes all laboratory quality control practices along with the frequency and acceptance
criteria for all QC samples and calibration verifications. Describes the initial
Demonstration of Capability (DOC) and on-going demonstration of capability for all
analysts. Includes the procedures for the determination of Method Detection Limits
(MDLs), if applicable.

M. Data Reduction, Validation, and Reporting


Describes data reduction, calculations, and reporting procedures.

N. References
Includes the references used to develop the SOP and any pertinent instrument manuals.

O. Waste Management
Provides information concerning proper waste disposal procedures for samples and/or
reagents and supplies.

P. Revision History
Documents the section(s) that have been modified since the last revision. Provides an
ongoing history of the SOP modifications.
SOP Revision
Section Modified Modification Reason Changed
Revision # Date

Q. Appendix
Includes all appendices, tables, diagrams, etc.

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