1.1 CV Analyser - Manual
1.1 CV Analyser - Manual
3-9000-521
April 2012
ROSEMOUNT ANALYTICAL, INC. AND DANIEL MEASUREMENT AND CONTROL, INC. (COLLECTIVELY,
“SELLER”) SHALL NOT BE LIABLE FOR TECHNICAL OR EDITORIAL ERRORS IN THIS MANUAL OR OMISSIONS
FROM THIS MANUAL. SELLER MAKES NO WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING THE IMPLIED
WARRANTIES OF MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE WITH RESPECT TO THIS
MANUAL AND, IN NO EVENT, SHALL SELLER BE LIABLE FOR ANY SPECIAL OR CONSEQUENTIAL DAMAGES
INCLUDING, BUT NOT LIMITED TO, LOSS OF PRODUCTION, LOSS OF PROFITS, ETC.
PRODUCT NAMES USED HEREIN ARE FOR MANUFACTURER OR SUPPLIER IDENTIFICATION ONLY AND MAY
BE TRADEMARKS/REGISTERED TRADEMARKS OF THESE COMPANIES.
THE CONTENTS OF THIS PUBLICATION ARE PRESENTED FOR INFORMATIONAL PURPOSES ONLY, AND
WHILE EVERY EFFORT HAS BEEN MADE TO ENSURE THEIR ACCURACY, THEY ARE NOT TO BE CONSTRUED
AS WARRANTIES OR GUARANTEES, EXPRESSED OR IMPLIED, REGARDING THE PRODUCTS OR SERVICES
DESCRIBED HEREIN OR THEIR USE OR APPLICABILITY. WE RESERVE THE RIGHT TO MODIFY OR IMPROVE
THE DESIGNS OR SPECIFICATIONS OF SUCH PRODUCTS AT ANY TIME.
SELLER DOES NOT ASSUME RESPONSIBILITY FOR THE SELECTION, USE OR MAINTENANCE OF ANY
PRODUCT. RESPONSIBILITY FOR PROPER SELECTION, USE AND MAINTENANCE OF ANY SELLER PRODUCT
REMAINS SOLELY WITH THE PURCHASER AND END-USER.
DANIEL AND THE DANIEL LOGO ARE REGISTERED TRADEMARKS OF DANIEL MEASUREMENT AND
CONTROL, INC. ROSEMOUNT AND THE ROSEMOUNT ANALYTICAL LOGO ARE REGISTERED TRADEMARKS
OF ROSEMOUNT ANALYTICAL. THE EMERSON LOGO IS A TRADEMARK AND SERVICE MARK OF EMERSON
ELECTRIC CO.
©2012
HOUSTON, TX
USA
All rights reserved. No part of this work may be reproduced or copied in any form or by any means–graphic,
electronic, or mechanical–without first receiving the written permission of Rosemount Analytical Inc. or Daniel
Measurement and Control, Inc., Houston, Texas, U.S.A.
WARRANTY
1. LIMITED WARRANTY: Subject to the limitations contained in Section 2 herein and except as otherwise
expressly provided herein, Rosemount Analytical and Daniel Measurement and Control, Inc., (collectively
“Seller”) warrants that the firmware will execute the programming instructions provided by Seller, and that
the Goods manufactured or Services provided by Seller will be free from defects in materials or
workmanship under normal use and care until the expiration of the applicable warranty period. Goods are
warranted for twelve (12) months from the date of initial installation or eighteen (18) months from the
date of shipment by Seller, whichever period expires first. Consumables and Services are warranted for a
period of 90 days from the date of shipment or completion of the Services. Products purchased by Seller
from a third party for resale to Buyer (“Resale Products”) shall carry only the warranty extended by the
original manufacturer. Buyer agrees that Seller has no liability for Resale Products beyond making a
reasonable commercial effort to arrange for procurement and shipping of the Resale Products. If Buyer
discovers any warranty defects and notifies Seller thereof in writing during the applicable warranty period,
Seller shall, at its option, promptly correct any errors that are found by Seller in the firmware or Services, or
repair or replace F.O.B. point of manufacture that portion of the Goods or firmware found by Seller to be
defective, or refund the purchase price of the defective portion of the Goods/Services. All replacements or
repairs necessitated by inadequate maintenance, normal wear and usage, unsuitable power sources,
unsuitable environmental conditions, accident, misuse, improper installation, modification, repair, storage
or handling, or any other cause not the fault of Seller are not covered by this limited warranty, and shall be
at Buyer's expense. Seller shall not be obligated to pay any costs or charges incurred by Buyer or any other
party except as may be agreed upon in writing in advance by an authorized Seller representative. All costs
of dismantling, reinstallation and freight and the time and expenses of Seller's personnel for site travel and
diagnosis under this warranty clause shall be borne by Buyer unless accepted in writing by Seller. Goods
repaired and parts replaced during the warranty period shall be in warranty for the remainder of the
original warranty period or ninety (90) days, whichever is longer. This limited warranty is the only warranty
made by Seller and can be amended only in a writing signed by an authorized representative of Seller.
Except as otherwise expressly provided in the Agreement, THERE ARE NO REPRESENTATIONS OR
WARRANTIES OF ANY KIND, EXPRESSED OR IMPLIED, AS TO MERCHANTABILITY, FITNESS FOR PARTICULAR
PURPOSE, OR ANY OTHER MATTER WITH RESPECT TO ANY OF THE GOODS OR SERVICES. It is understood
that corrosion or erosion of materials is not covered by our guarantee.
2. LIMITATION OF REMEDY AND LIABILITY: SELLER SHALL NOT BE LIABLE FOR DAMAGES CAUSED BY DELAY
IN PERFORMANCE. THE SOLE AND EXCLUSIVE REMEDY FOR BREACH OF WARRANTY HEREUNDER SHALL BE
LIMITED TO REPAIR, CORRECTION, REPLACEMENT OR REFUND OF PURCHASE PRICE UNDER THE LIMITED
WARRANTY CLAUSE IN SECTION 1 HEREIN. IN NO EVENT, REGARDLESS OF THE FORM OF THE CLAIM OR
CAUSE OF ACTION (WHETHER BASED IN CONTRACT, INFRINGEMENT, NEGLIGENCE, STRICT LIABILITY,
OTHER TORT OR OTHERWISE), SHALL SELLER'S LIABILITY TO BUYER AND/OR ITS CUSTOMERS EXCEED THE
PRICE TO BUYER OF THE SPECIFIC GOODS MANUFACTURED OR SERVICES PROVIDED BY SELLER GIVING
RISE TO THE CLAIM OR CAUSE OF ACTION. BUYER AGREES THAT IN NO EVENT SHALL SELLER'S LIABILITY TO
BUYER AND/OR ITS CUSTOMERS EXTEND TO INCLUDE INCIDENTAL, CONSEQUENTIAL OR PUNITIVE
DAMAGES. THE TERM “CONSEQUENTIAL DAMAGES” SHALL INCLUDE, BUT NOT BE LIMITED TO, LOSS OF
ANTICIPATED PROFITS, LOSS OF USE, LOSS OF REVENUE AND COST OF CAPITAL.
IMPORTANT INSTRUCTIONS
• Read all instructions prior to installing, operating, and servicing this product.
• Follow all warnings, cautions, and instructions marked on and supplied with this
product.
• Inspect the equipment packing case and if damage exists, notify your local carrier
for liability.
• Open the packing list and carefully remove equipment and spare or replacement
parts from the case. Inspect all equipment for damage and missing parts.
• Install equipment as specified per the installation instructions and per applicable
local and national codes. All connections shall be made to proper electrical and
pressure sources.
• Ensure that all equipment doors are closed and protective covers are in place,
except when maintenance is being performed by qualified persons, to prevent
personal injury.
• Use of this product for any purpose other than its intended purpose may result in
property damage and/or serious injury or death.
• When installing or servicing ATEX-certified units, the ATEX approval applies only
to equipment without cable glands. When mounting the flameproof enclosures in
a hazardous area, only flameproof cable glands certified to IEC 60079-1 must be
used.
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LIST OF FIGURES
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Figure A-15 DB 9-pin connector (P2 and P3) and pinout for jacks..................................... A-24
Figure A-17 GC DB 9-pin Port to PC DB 25-pin Port .......................................................... A-26
Figure A-18 GC DB 9-pin Port to PC DB 25-pin Port .......................................................... A-27
Figure A-19 GC Phoenix Plug Port to PC DB 25-pin Port ................................................... A-28
Figure A-21 GC Phoenix Plug Port to External Modem DB 25-pin Port.............................. A-30
Figure A-22 Example RS-422 Serial Cable Terminations ................................................... A-31
Figure A-23 Example RS-485 Serial Cable Terminations, Line Driver to GC
Controller Com3 .......................................................................................... A-33
Figure A-24 Example RS-485 Serial Cable Terminations, Line Driver to GC
Controller Com4........................................................................................... A-34
Figure C-1 Manifold for two carrier gas bottles to GC system........................................... C-2
Figure D-2. Selecting a check box ..................................................................................... D-9
Figure D-3. Selecting a list box........................................................................................ D-10
Figure D-4. Selecting a combo box ................................................................................. D-11
Figure D-5. Entering a date and time .............................................................................. D-12
Figure D-6. Navigate to the Application menu ................................................................ D-14
Figure D-7. The System screen ....................................................................................... D-15
Figure D-8. You must log in to the GC before editing a screen ........................................ D-16
Figure D-9. The Enter the data dialog allows you to edit the selected field ...................... D-17
Figure D-10. The field now holds new data ....................................................................... D-18
Figure D-11. The Is Multi User Write Enabled? check box .................................................. D-19
Figure D-12. The Is Multi User Write Enabled? check box, no longer checked.................... D-20
Figure D-13. The GC Mode field ........................................................................................ D-21
Figure D-14. The Select an Item combo box...................................................................... D-22
Figure D-15. The Chromatogram menu............................................................................ D-26
Figure D-16. The Chromatogram Settings screen ............................................................. D-26
Figure D-17. The Live Chromatogram View (Status Mode) screen..................................... D-27
Figure D-18. The Live Chromatogram View (Advanced Mode) screen ............................... D-28
Figure D-19. The Archived Chromatogram (Advanced Mode) screen................................ D-29
Figure D-20. The Live & Archived Chromatogram Viewer Options screen ......................... D-29
Figure D-21. The CGM Scaling screen ............................................................................... D-30
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LIST OF TABLES
Table 3-1. Modbus slave address (COM ID) dip switch settings ......................................3-34
Table 3-2. Switch positions for cold start........................................................................3-34
Table 3-3. FTB discrete digital inputs..............................................................................3-49
Table 3-4. FTB discrete digital outputs ...........................................................................3-50
Table 3-5. FTB analog inputs ..........................................................................................3-51
Table 3-6. FTB analog outputs........................................................................................3-51
Table 3-7. Optional analog outputs................................................................................3-52
Table 3-8. J8 Modem Board Jumper Settings ..................................................................3-53
Table 3-9. J9 Modem Board Jumper Settings ..................................................................3-53
Table 3-10. J10 Modem Board Jumper Settings ................................................................3-54
Table 3-11. J26 Radicom Modem Jumper Settings ...........................................................3-54
Table 3-12. J27Radicom Modem Jumper Settings ............................................................3-54
Table 3-13. J30 Radicom Modem Jumper Settings ...........................................................3-54
Table 3-14. J31 Radicom Modem Jumper Settings ...........................................................3-55
Table 4-1. Basic Hardware Troubleshooting via Alarms ..................................................4-10
Table 4-2. Troubleshooting Checklist.............................................................................4-13
Table 4-3. Temperature Control Dialog..........................................................................4-21
Table A-1 Matrix of possible TCD configurations field termination board ....................... A-1
Table A-2 Matrix of possible FID configurations field termination board ......................... A-6
Table A-3 Communication with WinSystems CPU ........................................................ A-14
Table A-4 Communication with WinSystems CPU ........................................................ A-15
Table A-5 Communication with WinSystems CPU ........................................................ A-15
Table A-6 Communication with WinSystems CPU ........................................................ A-16
Table A-7 Communication with WinSystems
MCM/LPM — Com4A Board (Optional) .......................................................... A-17
Table A-8 J10 Jumper Settings ...................................................................................... A-19
Table A-9 J7 Jumper Settings ........................................................................................ A-19
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Section 1: Introduction
1
This section describes the contents and purpose of the Model 700 Gas
Chromatograph System Reference Manual, a description of the Model 700
system, an explanation of the theory of operation, and a glossary of
chromatograph terminology.
Use this section to get acquainted with the basic engineering of the
Model 700 product.
The Model 700 system consists of three major parts: the analyzer
assembly, controller assembly, and sample conditioning system (SCS).
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PREAMPLIFIER PCB
PREAMPLIFIER P/S PCB
INPUTS:
DC-DC CONVERTERS
1 TCD DETECTOR
24VDC INPUT 1 FID DETECTOR
24VDC POWER
OUTPUTS OUTPUTS:
+20VDC -20VDC COM (1)
100VDC (RS-232 OR RS-485)
5VDC
3.3 VDC
SERIAL I/O
SOLENOID/HEATER
DRIVER PCB
DC-DC CONVERTERS
24 VDC INPUT
OUTPUTS
5VDC
SOLENOID DRIVERS (16)
HEATERS (4 ZONES)
DIGITAL INPUTS.................(5)
COM RS-232......................(1)
RTD INPUTS.......................(4)
ANALOG INPUTS 4-20mA....(4)
DIGITAL OUTPUTS..............(5) SERIAL PERIPHEERAL INTERFAC
SERIAL DAC CONTROL........(SPI)
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See Figure and Figure 1-4 for lower enclosure block diagrams.
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INPUT OPTIONAL
AC POWER AC-DC
POWER SUPPLY
CPU
MULTIFUNCTION COM 3
COM4A PCB
COM 5-8
FID & TCD PREAMPLIFIER COM 4
ETHERNET PCB
INTERNAL MODEM
OPTIONAL PC104
BOARD STACK
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The GC-PC interface provides the user with the greatest capability, ease-
of-use, and flexibility. One PC running MON2000 can connect with up to
32 chromatographs (via RS-485 serial communications links). MON2000
is used to edit applications, monitor operations, calibrate streams, and
display analysis chromatograms and reports, which can then be stored
to files on the PC hard drive or printed from either the PC printer port or
the GC printer port.
The Model 700 electronics and hardware are housed in two explosion-
proof enclosures and meet IEC Class I, Zone 1, Ex d IIB+H2, T4 (NEC Class
1, Division 1, Groups B, C, and D) approval for use in a hazardous
environment.
WARNING
Do not use a PC or a printer in a hazardous area. Serial port and Modbus
communications links are provided to connect the unit to the PC and to connect to
other computers and printers in a safe area. Failure to follow this warning may result in
injury or death to personnel or cause damage to the equipment.
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Note
For additional information, see "Section 1.5: Theory of operation".
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The MON2000 uses three distinct types of software. This enables total
flexibility in defining the calculation sequence, printed report content,
format, type and amount of data for viewing, control and/or
transmission to another computer or Controller Assembly. The three
types are:
• Baseline Operating System (BOS)
• Application configuration software
• Maintenance and Operations software (MON2000 version 2.2 or
later)
The BOS and the Application configuration software are installed when
the Model 700 system is shipped. The application configuration is
tailored to the customer’s process and shipped on a floppy disk. Note
that the hardware and software are tested together as a unit before the
equipment leaves the factory. MON2000 communicates with the Model
700 system and allows an initial site system setup (i.e., operational
parameters, application modifications, and maintenance).
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1.4.1 BOS
1.4.2 MON2000
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The following sections discuss the theory of operation for the Model
700, the engineering principles and concepts used.
Note
See "Section 1.8: Glossary" for definitions of the terminology used in the following
explanations.
One thermistor is designated the reference element and the other the
measurement element. See Figure 1-5 for a schematic diagram of the
thermal conductivity detector (TCD).
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The analysis begins when a fixed volume of sample is injected into the
column by operation of the sample valve. The sample is moved through
the column by the continuous flow of carrier gas. As successive
components elute from the column, the temperature of the
measurement element changes.
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1 2 1
The signals from the preamplifier are sent to the Controller Assembly for
computation, recording on a printer, or viewing on a PC monitor (via
MON2000).
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1.5.3 LSIV
The Liquid Sample Inject Valve (LSIV) penetrates the wall of the upper
enclosure and is held in place by a retaining ring. The mounting
arrangement is designed to ensure integrity of the flameproof enclosure.
Retraction Actuation
Air Inlet Air Inlet
The next section houses an auxiliary stem seal assist. A piston driven by
air at 80 to 100 psi keeps adequate load on the stem seal to counteract
wear at the high temperatures and pressures that might be encountered.
There are two ¼npt ports in this section; one port retracts the sample
piston and the other port activates the seal assist.
The innermost section houses the stem seals and the sample chamber.
There are five ¼ npt ports in this section.
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The tip of the LSIV is the port where flashed sample is taken to the oven
system.
The port at right angles to the length of the LSIV is the input for carrier
gas.
1.5.4 Methanator
After all other components have been separated from the sample,
normally undetectable CO and CO2 are sent through the methanator.
They are combined with hydrogen to make methane in a heat generated
catalytic reaction. The methanator is also known as a methanizer or a
catalytic converter.
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Methanator
Assembly
Every second, exactly 40 equi-spaced data samples are taken (i.e., one
data sample every 25 milliseconds) for analysis by the Controller
Assembly. The sampling frequency of 40 Hertz (Hz) was chosen to
reduce normal mode noise (at 60 Hz).
Because the data analysis is done as the signal is sampled (in real-time),
only a limited number of past data samples is required to analyze any
signal.
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N = PW
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Note
The Controller Assemblysoftware assumes that aregion of signal quiescenceand
stability will exist.
In a single peak situation, peak area is the area of the component peak
between the curve and the zero reference line. The peak height is the
distance from the zero reference line to the maximum point on the
component curve. The value and location of the maximum point is
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For fused peak sequences, this interpolation technique is used both for
peaks, as well as, valleys (minimum points). In the latter case, lines are
dropped from the interpolated valley points to the zero reference line to
partition the fused peak areas into individual peaks.
Note
For additional information about other calculations performed, see the MON2000
Software for Gas Chromatographs User Manual (P/N 3-9000-522).
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Area n Ht n
ARF n = --------------- or HRF n = -----------
Cal n Cal n
where
ARFn area response factor for component “n” in area per mole percent
Arean area associated with component “n” in calibration gas
Caln amount of component “n” in mole percent in calibration gas
Htn peak height associated with component “n” mole percent in calibration
gas
HRFn peak height response factor for component “n”
RFi
RFAVG n = i------------------
=1
k
where
RF new – RF old
deviation = ----------------------------------- 100
RF old
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Area n Ht n
CONC n = --------------- or CONC n = --------------
ARF n HRF n
where
ARFn area response factor for component “n” in area per mole percent
Arean area associated with component “n” in unknown sample
CONCn concentration of component “n” in mole percent
Htn peak height associated with component “n” mole percent in unknown
sample
HRFn peak height response factor for component “n”
CONC n
- 100
CONCN n = ---------------------------
k
CONCi
i=1
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Note
The average concentration of each component will also be calculated when data
averaging is requested.
where
CONCNn normalized concentration of component “n” in percent of total gas
concentration
CONCi non-normalized concentration of component “n” in mole percent for
each “k” component
CONCn non-normalized concentration of component “n” in mole percent
k number of components to be included in the normalization
1.8 Glossary
Auto Zero
The FID is automatically zeroed at each new analysis run and can be
configured to take place anytime during the analysis when either the
component is not eluting or the baseline is steady. The TCD is only
automatically zeroed at the start of a new analysis.
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Baseline
Signal output when there is only carrier gas going across the detectors.
In a chromatogram you should only see Baseline when running an
analysis without injecting a sample.
Carrier Gas
The gas used to push the sample through the system during an analysis.
In C6+ analysis we use Ultra Pure (zero grade) Carrier Gas for the carrier.
This gas is 99.995 percent pure.
Chromatogram
Component
Any one of several different gases that may appear in a sample mixture
Condulet
CTS
Clear to send
DCD
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DSR
DTR
FID
LSIV
Liquid Sample Inject Valve - The optional LSIV is used to convert a liquid
sample to a gas sample by vaporizing the liquid in a heated chamber,
then analyzing the flashed sample.
Methanator
Response Factor
RawArea
RF = ----------------------------------------------------------------------
CalibrationConcentration
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Retention Time
Time (in seconds) that elapses between the start of analysis (0 seconds)
and the sensing of the maximum concentration of each component by
the detector.
RI
Ring indicator
RLSD
RTS
Request to send
TCD
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Section 2: Equipment description and
2
specifications
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Note
All circuit boards are connected through a common ground via the enclosure.
Insulating Cover
Preamplifier Assembly
Multifunction Board
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• Micro-FID
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Micro-FID
The optional flame ionization detector may be used in place of one TCD
for the detection of trace levels of compounds.
• Methanator
Methanator
ssembly
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The optional liquid sample inject valve (LSIV) is used to convert a liquid
sample to a gas sample for analysis on the Model 700 Gas
Chromatograph.
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• TCD Electronics
- Dual Methods Adapter Board
- Driver I/O Board
- Multifunction Board
- Preamplifier Board
- External Locking Device
• FID Electronics
- Solenoid/Heater Driver Board
- Multifunction Board
- Preamplifier Power supply
- Driver I/O Board
- Multifunction Board
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The Model 700 lower enclosure consists of the Card cage assembly,
which contains the following:
• CPU board
• Com4A board (optional)
• Analog board
• Additional analog board (optional)
• Digital I/O
• Internal modem (optional)
• Ethernet card (optional)
• Field termination board (FTB)
• Connection for AC/DC power supply
(converter)
• Internal and external ground
Note
The Model 700 CSA-certified unit is equipped with 3/4 inch cross-over adapters.
WARNING
See power supply label prior to connection. Check the unit power design to determine
if it is equipped for AC or DC power. Applying 110/ 220 VAC to a DC power input unit
will severely damage the unit. Failure to do so may result in injury or death to personnel
or cause damage to the equipment.
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The flow panel assembly is attached to the front of the upper enclosure
and consists of the following: (see Figure 2-2):
• Carrier pressure regulator(s) and gauge(s)
• Sample flow meter
• Sample Vent (SV)
• Measure Vent (MV)
• Actuation pressure limiting regulator
• Pressure switch, mounted internally
CAUTION
If the carrier gas pressure drops below a set point, this switch causes the analysis to stop
and activates the analyzer failure alarm.
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2.2.1 Utilities
Type Specification
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Type Specification
power • 24VDC standard (24.5 - 26.5 VDC operating voltage range); 80 watts
• AC optional 90-130/180-264 VAC; 47-63 Hz; 80 watts
80 watts start-up; 33 watts nominal
• 47-63Hz (single phase)
• 75W (Model 700 w/TCD)
• 150W (Model 700 w/Methanator or LSIV)
• 36VDC, Sol/Drv PCB Transorb
Note: Voltage range includes line voltage variations. Ensure the GC receives at
least 24.5 VDC at the terminals. If the power supply is located more than 164 feet
(50 meters) from the GC, a voltage drop may occur across the cable and cause the
solenoids to fail. If your GC installation is more than 164 feet (50 meters) away
from the power supply, use an AC power supply to avoid problems with a voltage
drop across the cable.
instrument not required; optional for valve actuation, minimum pressure of 90 psig
air
environment • -18 to 55 oC (0 to 130 oF)
• 0 to 95% RH (non-condensing)
• indoor/outdoor
• pollution - degree 2 (the unit can withstand some non conductive
environmental pollutants e.g., humidity)
• max altitude 2000m
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Type Specification
approvals
0518
SIRA 04ATEX1055X
II 2 G
Ex d IIC T4 Gb
Tamb = +60oC
IECEx SIR 08.0008X
Ex d IIC T4 Gb
Tamb = 60oC
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PREAMPLIFIER PCB
PREAMPLIFIER P/S PCB
INPUTS:
DC-DC CONVERTERS 1 TCD DETECTOR
24VDC INPUT 1 FID DETECTOR
24VDC POWER
OUTPUTS OUTPUTS:
+20VDC -20VDC COM (1)
100VDC (RS-232 OR RS-485)
5VDC
3.3 VDC
SERIAL I/O
SOLENOID/HEATER
DRIVER PCB
DC-DC CONVERTERS
24 VDC INPUT
OUTPUTS
5VDC
SOLENOID DRIVERS (16)
HEATERS (4 ZONES)
DIGITAL INPUTS.................(5)
COM RS-232......................(1)
RTD INPUTS.......................(4)
ANALOG INPUTS 4-20mA....(4)
DIGITAL OUTPUTS..............(5) SERIAL PERIPHEERAL INTERFACE
SERIAL DAC CONTROL.........(SPI)
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INPUT OPTIONAL
AC POWER AC-DC
POWER SUPPLY
24 VDC
CPU
MULTIFUNCTION COM 3
COM4A PCB
COM 5-8
FID & TCD PREAMPLIFIER COM 4
ETHERNET PCB
INTERNAL MODEM
OPTIONAL PC104
BOARD STACK
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Type Specification
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2.2.4 Software
Note
The Model 700 has its own applications and is not compatible with 2350/2350A
applications.
Type Specification
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Section 3: Installation and setup
3-
This section provides instructions for installing and setting up the Model
700 gas chromatograph (GC) system for Zone 1/ Division I
environments.
WARNING
Install and operate all equipment as designed and is compliant with all safety
requirements. The “Seller” does not accept any responsibility for installations of the
Model 700, or any attached equipment, in which the installation or operation thereof
has been performed in a manner that is negligent and/or non-compliant with
applicable safety requirements.
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WARNING
Observe all precautionary signs posted on the Model 700 enclosure. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.
WARNING
Observe all precautionary signs posted on the Model 700 enclosure.
WARNING
The Model 700 enclosures are certified by CSA for Class I, Zone 1, Ex d IIB+H2 T4,
Enclosure Type 4 and Class I, Division 1, Groups B,C,D. The Model 700 enclosures are
certified by ATEX for ATEX Ex d IIC T4 and IEC-Ex Ex dIIC T4.
WARNING
ATEX certified units must be installed strictly in compliance with the requirements of
IEC 60079-14.
Special conditions for safe use must be met. The maximum constructional gap (ic) is
less than that required by Table 2 of EN 60079-1:2007.
Before opening the Model 700 enclosure, reduce the risk of igniting hazardous
atmospheres by disconnecting the equipment from all power supplies. Keep the
assembly closed tightly when in operation to reduce the risk of igniting hazardous
atmospheres. Inlet (incoming) wiring must meet local standards (i.e. in conduit with
seal fitting within 18 or via cable glands certified to IEC 60079-1). Upper enclosure
threaded entry is ¾ NPT. Lower enclosure threaded entries are M32-1.5.
Observe all precautionary signs posted on the Model 700 enclosure. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.
Please direct all health, safety and certification related questions to: Emerson Process
Management, Gas Chromatographs, Applications Engineering Group, 713-827-6380 or
1-866-GC Center (1-866-422-3683).
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1. All wiring must conform to the CEC or NEC, local state or other
jurisdiction, and company standards and practices.
CAUTION
15 amps is the maximum current for 14 AWG (wire).
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Note
Card cage removal is not necessary for I/O connections.
1. Remove the lower enclosure cover and the front flow panel
assembly or LOI.
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Cover
LOI
Note
Note the location of the ribbon cables for ease of reassembly.
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Flow Panel
3. Use a Phillips head screw driver and remove the two screws
located at the top of the card cage and one screw on the bottom
left side of the card cage (not visible in the figure).
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Card Cage
Screws
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5. User power and signal connections may be made with the card
cage removed from the lower enclosure.
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Figure 3-5. Card cage disassembly for power and signal wiring
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Follow these general precautions for field wiring digital and analog
input/output (I/O) lines:
CAUTION
Observe all precautionary signs posted on the Model 700 enclosure. Applicable to all
digital and analog I/O lines connecting to the GC: Any loop of extra cable left for service
purposes inside the GC housing must not be placed near any AC power lines. If this
precaution is not followed, the data and control signals to and from the GC can be
adversely affected.
• Metal conduit must be used for all process signal wiring (assuming
operation in a Class 1, Division 1 Explosive Area). Metal conduit is not
required for use in general purpose areas.
• Metal conduit or cable (in compliance with EN 60079-14) used for
process signal wiring must be grounded at conduit support points
(intermittent grounding of conduit helps prevent induction of
magnetic loops between the conduit and cable shielding).
• All process signal wiring should be a single, continuous length
between field devices and the GC. If, however, length or conduit runs
require that multiple wiring pulls be made, the individual conductors
must be interconnected with suitable terminal blocks.
• Use suitable lubrication for wire pulls in conduit to prevent wire
stress.
• Use separate conduits for AC voltage and DC voltage circuits.
• Do not place digital or analog I/O lines in same conduit as AC power
circuits.
• Use only shielded cable for digital I/O line connections.
- Ground the shield at only one end.
- Shield-drain wires must not be more than two AWG sizes smaller
than the conductors for the cable.
• When inductive loads (relay coils) are driven by digital output lines,
the inductive transients must be diode-clamped directly at the coil.
• Any auxiliary equipment wired to the GC must have its signal
common isolated from earth/chassis ground.
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• Resistance between the copper-clad steel ground rod and the earth
ground must not exceed 25 Ohms.
• On ATEX certified units, the external ground lug must be connected
to the customer’s protective ground system via AWG 9 (6mm2)
ground wire. After the connection is made, apply a non-acidic grease
to the surface of the external ground lug to prevent corrosion.
• The equipment-grounding conductors used between the GC and the
copper-clad steel ground rod must be sized according to the
following specifications:
Length Wire
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Length Wire
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WARNING
Observe all precautionary signs posted on the equipment. Consult your company
policies and procedures and other applicable requirements documents to determine
wiring and installation practices that are appropriate for hazardous areas. Failure to do
so may result in injury or death to personnel or cause damage to the equipment.
Line length:
If possible, avoid long sample lines. In case of a long sample line, flow
velocity can be increased by decreasing downstream pressure and using
by-pass flow via a speed loop.
Note
Stream switching requires a sample pressure of 20 psig.
Note
The calibration gas stream inlet is the last stream inlet following the sample gas.
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Stream 1 - 8
Gas Connections
Use small sizes to minimize time lag and prevent back diffusion.
Note
Install the probe/regulator first, immediately followed by the coalescing filter and then
the membrane filter. See Appendix C for a recommended natural gas installation.
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Valving:
3.2 Preparation
Your Model 700 GC was started and checked out before it left the
factory. Program parameters were installed and documented in the PC
Config Report furnished with your Model 700.
Install the GC as close as possible to the sample system but allow for
adequate access space for maintenance tasks and adjustments. Allow a
minimum of 14 inches (36 cm) in front for enclosure opening and access.
• Allow a minimum of 14 inches (36 cm) above the top of the dome
enclosure for dome removal and access.
• Ensure that exposure to radio frequency (RF) interference is minimal.
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See the following checklist for unpacking the unit and inspecting for
damage:
4. If an FID is present, remove the vent plug from the FID outlet. The
vent plug has a tag attached to it that reads “REMOVE VENT
PLUGS PRIOR TO OPERATION”. Failure to remove the cap could
result in a performance failure or in damage to the detector.
Installation and startup should proceed only if all required materials are
on hand and free from obvious defects.
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Note
The wall should be strong enough to support the 200-pound load.
• Wall mount
• Pole mount
• Floor mount
The uppermost of the holes should be about 30 inches from the floor for
the most efficient use of the unit.
The space between the enclosures and the wall (1.3 inches) allows
adequate access above and around the unit.
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You will need these tools and components to install the Model 700:
• Zero grade carrier gas (99.995% pure, with less than 5 ppm water,
and less than 0.5 ppm hydrocarbons)
• High pressure dual-stage regulator for the carrier gas cylinder, high
side up to 3000 pounds per square inch, gauge (psig), low side
capable of controlling pressure up to 150 psig
• Calibration standard gas with correct number of components and
concentrations. See Appendix Table C-1.
• Single-stage regulator for the calibration gas cylinder, low pressure
side capable of controlling pressure up to 30 psig
• Sample probe regulator (fixture for procuring the stream, or sample
gas for chromatographic analysis)
• Coalescing filter
• Membrane filter
• 1/8-inch stainless steel (SS) tubing for connecting calibration
standard to GC, 1/8 inch SS tubing for connecting carrier gas to the
GC, 1/8-inch SS tubing for connecting stream gas to the GC
• Heat tracing (as required) for sample transport and calibration lines
• Miscellaneous Swagelok tube fittings, tubing benders and tubing
cutter
• 14 AWG (18 MWG) or larger electrical wiring and conduit to provide
115 or 230 volts AC, single phase, 50 to 60 Hertz, from an
appropriate circuit breaker and power disconnect switch. See
guidelines in “Power source wiring” on page 3-3.
• Liquid leak detector (Snoop® or equivalent)
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WARNING
Do not use a PC or a printer in a hazardous area. Serial port and Modbus
communications links are provided to connect the unit to the PC and to connect to
other computers and printers in a safe area. Failure to follow this warning may result in
injury or death to personnel or cause damage to the equipment.
Note
You can use the serial cable installed for the Model 700. For straight-through serial
cable installation and fabrication instructions, see Appendix A.
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WARNING
Ensure that the DC power source is switched OFF before connecting the wires. Also,
ensure that the DC power is S.E.L.V. compliant by suitable electrical separation from
other circuits. Failure to follow these warnings may result in injury or death to personnel
or cause damage to the equipment.
CAUTION
Check the unit prior to wiring to determine if it is equipped for DC power. Failure to
observe this precaution may damage equipment.
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2. Bring the two leads in through the entry on the left side of the
lower enclosure. Connect to the termination plug provided with
the unit. See Appendix H Drawing DE- 20993.
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+ (positive) red
— (negative) black
Note
A new version of the Solenoid/Heater Driver Board that includes the Diode protection
will soon be released.
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WARNING
Check the unit prior to wiring to determine if it is equipped for optional AC power.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.
AC / DC Power
Converter
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WARNING
Do not connect AC power leads without first ensuring that AC power source is switched
OFF. Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.
CAUTION
Do not apply electrical power to the GC until all interconnections and external signal
connections have been verified, and proper grounds have been made. Failure to
observe this precaution may cause damage to equipment.
2. Bring the power leads in through the left entry on the bottom of
the enclosure.
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Note
Use SS tubing. Keep tubing clean and dry internally to avoid contamination. Before
connecting the sample and gas lines, flow clean air or gas through them. Blow out
internal moisture, dust, or other contaminants.
1. Remove the plug from the Sample Vent (SV) line (1/16-inch
tubing marked “SV” located on the Flow Panel Assembly).
• If desired, connect the SV line to an external (ambient
pressure) vent. If the vent line is terminated in an area exposed
to wind, protect the exposed vent with a metal shield.
• Use 1/4-inch or 3/8-inch tubing for vent lines longer than 10
feet.
SV
MV
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2. Connect carrier gas to the GC. (The carrier gas inlet is a 1/8-inch
tee fitting located on the left side of the upper enclosure.)
CAUTION
Do not turn on gas until you have completed leak checking the carrier and sample lines
(see Step 5). Failure to follow this precaution may cause injury to personnel or damage
equipment.
Carrier Gas
Inlet
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Note
The first stream is the calibration gas stream.
Note
When installing the calibration standard gas line, ensure that the correct
tubing connection is made.
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Calibration
Gas Inlet
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Streams 1 - 7 Calibration
Gas Inlets Gas Inlet
5. After all lines have been installed, proceed with leak checking the
carrier and sample lines. See Section 3.5.1; note that it requires
the AC power to be turned on at the GC.
Note
Follow the steps in this section only if you wish to change the Com ID setting or visually
inspect and verify the DIP switch settings.
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In most cases, the Com ID configuration made at the factory will not
need to be changed. The factory DIP switch settings produce a Com ID of
1.
To visually inspect and verify the DIP switch settings or to change the
Com ID settings on the multifunction board,
CAUTION
Use caution when accessing an enclosure. A voltage of 115 to 230 VAC, along with
various DC voltages, are present. Failure to follow this precaution may cause injury to
personnel or damage equipment.
Note
Note that MON2000 Com I.D. settings will override the hardware settings. To
use the hardware Com I.D. configuration, enter a zero in the MON2000 Com
I.D. settings. For details, refer to MON2000 Software for Gas Chromatographs
User Manual (P/N 3-9000-522).
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Mounting Bracket
Thumb Screw
Multifunction
Board
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Table 3-1. Modbus slave address (COM ID) dip switch settings
Com ID 1 2 3 4 5
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Note
Model 700 software upgrades can be installed via any available
communications port.
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Note
You can buy this cable from most computer supply retailers. If, however, it is
necessary to custom-wire a cable because of circumstances, see guidelines
provided in Appendix B.
2. Connect the serial cable plugs to the appropriate serial port jacks
at the PC and GC. Use the MON2000 software to monitor and
operate the GC as needed.
Note
For detailed information concerning serial communications, refer to Appendix A.
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If the length of cable can be 50 feet or less, connect the serial cable to
one of the GC serial ports configured for RS-232. (Recall that output
from a standard PC serial port follows RS-232 serial definition.) Cable
that is longer than 50 feet, when used for RS-232 serial transmission, can
result in spurious loss or corruption of data.
1. Access the GC’s field termination board, located on the right wall
of the lower enclosure.
FTB
Note
Model 700, standard configuration, has three communications ports available
on the FTB: Com1, Com2 and Com5.
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Note
Com 4 is dedicated to the Micro-FID/TCD Preamplifier.
Multifunction FID/TCD
Board Preamplifier Board
Com3 (1) Com4
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Com4A
Com5 Com5
Com6 Com6
Com7 Com7
Com8 Com8
(1) optional
Note
Model 700, with the Com 4A board installed, has six communications ports
available on the FTB; Com1 and Com2, and Com5, Com6, Com7, and Com8.
Note
Com 4 is dedicated to the Micro-FID/TCD Preamplifier.
Note
See Appendix A for instructions on fabricating a direct serial cable.
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5
RI 1 9
DSR 1 4
RTS 1 8
RXD 1 3
CTS 1 7
TXD 1 2
DTR 1 6
DCD 1 1
GND Com2
P3
5
RI 2 9
DSR 2 4
RTS 2 8
RXD 2 3
CTS 2 7
TXD 2 2
DTR 2 6
DCD 2 1
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Com2
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Com7
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the twisted pair cable to the RS-422/RS-485 serial port of the line
driver.
4. Access the GC FTB (see Figure 3-20 in "Section 3.4.2: Preparing for
serial connections").
Note
Serial ports Com1 through Com3 are configured by default for RS-232. For
further details or instructions on how to configure these ports to RS- 422/485,
see Appendix A.
Note
The GC uses only a generic printer driver. The PC printer allows more control and better
quality output.
1. Access the GC FTB (see Figure 3-20 in "Section 3.4.2: Preparing for
serial connections").
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Note
See Appendix A for a complete listing of the serial ports and corresponding
pinouts to fabricate a serial printer cable.
The Field Termination Board (P/N 3-0700-010) has five discrete outputs
and four discrete inputs. Refer to the MON2000 Software for Gas
Chromatographs Manual (P/N 3-9000-522) and use the Application>User
Defined>Selection menu to to configure the Digital Outputs.
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Note
Configure the Digital Output using the MON2000 Software, from the Application >
User Defined>Selections, set the enable the Common Alarm either Normally Open or
Normally Closed.
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J14
J10
The FTB has five discrete outputs and four discrete inputs. The
discrete input, DIG_IN4, is dedicated to a pressure switch. The
discrete inputs are located on J10 (10 pin Phoenix connector).
Pin 1 DIG_IN1
Pin 2 GND
Pin 3 DIG_IN2
Pin 4 GND
Pin 5 DIG_IN3 to customer
Pin 6 GND
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The discrete outputs are located on J14 (P/N 3-0700-010) (Phoenix 10-
pin connector) have two “Form A” relays on the FTB. Outputs 3-5 are
Solid State switches with a rating of .375A @30 VDC. The relays, with
sealed enclosures, have a contact current rating of 1.0 Amperes each.
J14 Function
Pin 1 DIG_OUT
Pin 2 DIG_OUT
Pin 3 DIG_OUT
Pin 4 DIG_OUT
Pin 5 DIG_OUT_ 3+
Pin 6 DIG_OUT_ 3-
Pin 7 DIG_OUT_ 4+
Pin 8 DIG_OUT_ 4-
Pin 9 DIG_OUT_ 5+
Pin 10 DIG_OUT_ 5-
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There are four analog inputs on the Field Termination Board (P/N 3-0700-
010 and drawing CE-21157) located at J4 (12-pin Phoenix connector).
Table 3-5. FTB analog inputs
J4 Function
Pin 1 VIN+_1
Pin 2 VIN-_1
Pin 3 Shield
Pin 4 VIN+_2
Pin 5 VIN-_1
Pin 6 Shield
Pin 7 VIN+_3
Pin 8 VIN-_1
Pin 9 Shield
Pin 10 VIN+_4
Pin 11 VIN-_1
Pin 12 Shield
There are four standard analog outputs on the standard FTB (P/N 3-
0700-010 and drawing CE-21157); located at J8 (12-pin Phoenix
connector). Additionally, if installed, the optional analog board has eight
analog outputs
Table 3-6. FTB analog outputs
J8 Function
Pin 1 IOUT+_1
Pin 2 IOUT-_1
Pin 3 Shield
Pin 4 IOUT+_2
Pin 5 IOUT-_2
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J8 Function
Pin 6 Shield
Pin 7 IOUT+_3
Pin 8 IOUT-_3
Pin 9 Shield
Pin 10 IOUT+_4
Pin 11 IOUT-_4
Pin 12 Shield
There are eight analog outputs on the optional analog output board (P/N
2-3-0580-037 and drawing CE-21157); located at J3 (24-pin Phoenix
connector):
Table 3-7. Optional analog outputs
J3 Function
Pin 1 IOUT+_5
Pin 13 IOUT-_5
Pin 2 Shield
Pin 14 IOUT+_6
Pin 3 IOUT-_6
Pin 15 Shield
Pin 4 IOUT+_7
Pin 16 IOUT-_7
Pin 5 Shield
Pin 17 IOUT+_8
Pin 6 IOUT-_8
Pin 18 Shield
Pin 7 IOUT+_9
Pin 19 IOUT-_9
Pin 8 Shield
Pin 20 IOUT+_10
Pin 9 IOUT-_10
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J3 Function
Pin 21 Shield
Pin 10 IOUT+_11
Pin 22 IOUT-_11
Pin 11 Shield
Pin 23 IOUT+_12
Pin 12 IOUT+_12
Pin 24 Shield
Optional modem boards are available for the Model 700 GC.
The jumper settings and pinouts for each board is shown below.
Pin(s) Position
1 and 2 In
3 and 4 In
5 and 6 In
7 and 8 In
Pin(s) Position
1 and 2 In
5 and 6 In
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Pin(s) Position
1 and 2 In
3 and 4 In
5 and 6 In
9 and 10 In
15 and 16 In
Pin(s) Position
1 and 2 In
Pin(s) Position
1 and 2 In
Pin(s) Position
1 and 2 In
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Pin(s) Position
2 and 3 In
The focus of this section is for field connections to the analyzer, during
the installation process. See “Leak checks” on page 4-26 for an in depth
discussion of analyzer leak checks.
1. Plug the Measure Vent (labeled “MV”) to block the free flow of
Carrier Gas through the GC.
Note
The GC does not have an inline Block Valve to shut off the Carrier Gas flow.
2. Slowly pressurize the “GC side” of the Carrier Gas to 110 psig (±2
percent) with the dual-stage regulator at the Carrier Gas cylinder.
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3. After two minutes, shut off the Carrier Gas bottle valve by turning
it clockwise. Then, observe the high-side regulator gauge on the
Carrier Gas bottle.
• The gauge should not bleed down more than 200 psig in 10
minutes.
• If Carrier Gas is lost at a faster rate, then all tube fittings
between the Carrier Gas bottle and the GC (including the
dual-stage regulator) must be checked for leaks and
tightened if necessary.
Most leaks at this stage (Installation and Setup) are usually
found between the Carrier Gas bottle and the GC.
The dual-stage regulator fitting connecting to the Carrier
bottle, may not seat properly with some Carrier Gas bottles
and allow a leak. If this occurs, carefully wrap a small length of
Teflon tape around the tip of the inlet tube on the dual-stage
regulator (which sits against the Carrier Gas bottle valve seat).
4. Once the GC passes the “Initial leak check”, reopen the Carrier
Gas bottle valve and remove the Measurement Vent (MV) plug.
3. Shut off the Calibration gas at the gas bottle by turning the valve
clockwise.
5. When the GC passes the “Initial Calibration Gas leak check”, re-
open the Calibration gas bottle valve and the in-line “Cal Stream”
block valve.
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4. When the GC passes the “Initial Sample Gas leak check”, re-open
the Sample Gas lines.
Purging carrier and calibration gas lines requires AC power. Use Helium
that is 99.995% pure and that has less than 5ppm water and less than
0.5ppm hydrocarbons.
Note
Tubing should be clean and dry internally. During installation, the tubing should have
been blown free of internal moisture, dust, or other contaminants.
1. Ensure that the MV vent line plug has been removed, and the vent
line is open.
3. Set the carrier gas line pressure at 110 psig. Use the dual stage
regulator at the carrier gas bottle to adjust pressure.
Note
Do not use the “Carrier Pressure Adjust” regulator adjustment (on the Flow Panel
Assembly) to adjust carrier gas line pressure. This pressure is factory-set and should not
be adjusted.
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8. Select the Auto Sequence Function. Use the Control > Auto
Sequence menu path described in Section 4 of the MON2000
Software for Gas Chromatographs User Manual (P/N 3-9000-522).
Note
A period of 4 to 8 hours (or overnight) is recommended, during which all of the
settings described in Steps 1 through 7 are maintained. No other settings
should be made.
1. Ensure that the Carrier Gas lines have been fully purged, as
described in the previous section, and that the SV plug has been
removed.
3. Fully open the block valve associated with calibration gas feed
(the block valve should be located on lower right-hand corner of
the front panel).
See Section 5.8 in the MON2000 Software for Gas Chromatographs
User Manual (P/N 3-9000-522) for instructions on selecting
streams.
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7. Let both gauges on the calibration gas bottle valve bleed down to
0 (zero) psig.
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Section 4: Maintenance and troubleshooting
4--
WARNING
Observe all precautionary signs posted on the Model 700 enclosure. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.
WARNING
ATEX certified units must be installed strictly in compliance with the requirements of
IEC 60079-14.
Special conditions for safe use must be met. The maximum constructional gap (ic) is
less than that required by Table 2 of EN 60079-1:2007.
Before opening the Model 700 enclosure, reduce the risk of igniting hazardous
atmospheres by disconnecting the equipment from all power supplies. Keep the
assembly closed tightly when in operation to reduce the risk of igniting hazardous
atmospheres. Inlet (incoming) wiring must meet local standards (i.e. in conduit with
seal fitting within 18 or via cable glands certified to IEC 60079-1). Upper enclosure
threaded entry is ¾ NPT. Lower enclosure threaded entries are M32-1.5.
Observe all precautionary signs posted on the Model 700 enclosure. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.
Please direct all health, safety and certification related questions to: Emerson Process
Management, Gas Chromatographs, Applications Engineering Group, 713-827-6380 or
1-866-GC Center (1-866-422-3683).
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The most efficient method for maintaining and repairing the Model 700
GC system is a component-replacement concept that allows you to
return the system to operation as quickly as possible. Sources of trouble,
such as printed-circuit assemblies, valves, etc., are identified during
troubleshooting test procedures and are replaced at the lowest level
practical with units in known working order. The defective components
are then either repaired in the field or returned to Measurement Services
for repair or replacement.
The Model 700 GC system will perform accurately for long periods with
very little attention (except for maintaining the Carrier Gas cylinders). A
bimonthly record of certain parameters will assist greatly in assuring that
your Model 700 is operating to specifications. The maintenance checklist
should be filled out bimonthly, dated, and kept on file for access by
maintenance technicians as necessary.This gives you a historical record
of the operation of your Model 700, enables a maintenance technician to
schedule replacement of gas cylinders at a convenient time, and allows
quick troubleshooting and repair when it becomes necessary.
Copy the sample maintenance checklist as necessary for your files. If you
have a problem, please complete the checklist and reports, and have the
results available when calling Measurement Services with a problem.
Also have the Sales Order number. The Sales Order number can be found
on the nameplate located on the left side wall of the upper housing of
the Model 700. The chromatograms and reports archived when your
Model 700 left the factory are filed by this number.
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MAINTENANCE CHECKLIST
Sample System
Sample Line Pressure(s) (1)_____ psig _____ psig
(2)_____ psig _____ psig
(3)_____ psig _____ psig
(4)_____ psig _____ psig
(5)_____ psig _____ psig
Calibration Gas
High Pressure Reading _____ psig _____ psig
Outlet Pressure Reading _____ psig _____ psig
Flow ___ cc/min ___ cc/min
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WARNING
The explosion-proof housing should not be opened when the unit is exposed to an
explosive environment. If access to the explosion-proof housing is required,
precautions must be taken to ensure that an explosive environment is not present.
Failure to do so may result in injury or death to personnel or cause damage to the
equipment.
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• Multifunction Board
• Dual Methods Adapter Board
• Dual Methods Preamplifier Board
• Solenoid Heater/Driver Board
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• Multifunction Board
• Solenoid/Heater Driver Board
• FID/TCD Preamplifier Board
• FID/TCD Preamplifier Power Supply Board
• FID Connector Board
Note
The optional Radicom Modem is always mounted on top of the PC/104 card
stack.
The detector elements, heater elements, valves and columns are located
in the upper explosion-proof housing of the Danalyzer Pro GC.
Remove the thermal cover and insulating shield to gain access to these
components.
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Thermal
Cover
The detector elements, including the FID, are located in the block (TCD)
and on the FID Base attached to the valve block.
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Thermal
Conductivity
Detectors
FID
FID Block
There are five heater elements: three valve block heaters, the column
heater, and the stream switching system heater.
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The block heaters are cartridge heaters located in the corners of the
block. Column and block heaters are identical and are installed from the
underside of the manifold (plastic base) of the oven.
Note
Correct ALL alarms before re-calibration.
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Use the following table to identify the alarm and possible cause to
remedy the problem.
Table 4-1. Basic Hardware Troubleshooting via Alarms
Micro-FID/TCD Preamplifier
Alarms
extinguished flame
Micro-FID Temperature High
Micro-FID Comm. Failure
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Preamp Input 1 Out of Range Indicates either Carrier Gas gone; air not purged
from carrier lines; power failure; bad
thermistors; preamp out of balance or failed;
analyzer temperature low; interconnection
wiring.
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TCD
Fused Peak Overflow - Noisy Air not purged from carrier lines; bad
Baseline thermistors; shields.
Use the MON2000 software in the offline mode and select Logs >
Parameter List from the drop-down menu and open a saved *.par file.
Do not adjust any values if they are within the nominal tolerance values
on the Checklist. Compare the values with those obtained in preceding
weeks. This may pinpoint your problem immediately.
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Analyzer
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Controller Inputs
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Chromatogram
Check baseline
Number of peaks
Retention times
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Note
Refer to System Operational Parameters.
This section applies to Model 700 GCs with the TCD and 2350A
Controllers. If your Model 700 GC is equipped with an FID or LSIV this
section does not apply.
Use the test points in Figure 4-5 through Figure 4-8 to ensure that the
voltage meets specifications on the dual methods adapter board and the
field termination board. See Table 4-2 for voltage specifications.
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Test Points
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4.6.4 Preamplifier
Ensure that the flow panel gauge is properly set. Refer to the Model 700
Troubleshooting Checklist for values. Do not adjust; check with
Measurement Services if your reading is abnormal.
4.6.6 Temperature
The settings and values shown in Figure 4-9 and described in Table 4-3
are preset at the factory and are based on the specific customer
application. These values should not be changed unless recommended
by Application Engineering or Customer Service Personnel, or it is a
factory application requirement.
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Use the pull down menu to select the appropriate mode setting (e.g.
AUTOMATIC, MANUAL, or OUT OF SERVICE). Ensure that the
temperature is constant for the Oven (i.e. Multivalve System block and
column module kit) and the SSS.
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4 Spare N/A
Or, Methanator 300 oC (572 oF)
150 oC (302 oF)
Or, LSIV
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• Igniter ON duration
• Flame ON sense temperature Degrees C
• Flame OUT sense temperature Degrees C
• Electrometer (TCD) gain
Short term noise results from baseline upsets that have frequencies
significantly higher than those of an eluted peak. Short term noise is not
a serious problem as it is easily removed by appropriate noise filters
without significantly affecting the profiles of the peaks. Its source usually
originates from either the detector sensor system or the preamplifier.
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Long term noise results from baseline upsets that have frequencies similar
to those of an eluted peak. This type of noise is the most damaging
because it can not be differentiated from very small peaks. Long term
noise cannot be removed by electronic filtering without affecting the
profiles of the eluted peaks. Long term noise usually arises from
temperature, pressure or flow rate changes in the sensing cell. It is this
noise that ultimately limits the sensitivity of the detector.
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Baseline drift results from baseline upsets that have frequencies that are
significantly larger than those of the eluted peak. Drift is almost always
due to either changes in ambient temperature, changes in mobile flow
rate, detector cell pressure or column bleed in the GC. Drift is easily
controlled by choosing operating parameters that are within detector
and column specifications.
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To ensure that the baseline is not drifting, compare the baseline upsets
caused by valve actuations with those of the spectrum chromatogram
provided with the Operational Parameters Sheet.
2. Make sure the setting of the carrier cylinder regulator is 115 psig
(pounds per square inch, gauge).
3. Check all fittings at the pressure regulator flow panel and at the
carrier cylinder regulator with a leak detector. Correct any leaks
detected by a bubble indication.
4. Turn the Carrier Gas shut-off valve clockwise to close. Observe the
carrier pressure for ten minutes to check for a drop in carrier
pressure.
The drop should be less than 200 psig on the high side of
the regulator/gauge. If the carrier pressure remains
constant, no leaks are present.
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Note
When the valves are switched, some pressure change is normal because of
carrier loss. Momentarily open the cylinder valve to restore pressure if
necessary.
6. If the pressure does not hold constant, check all valve fittings for
tightness.
Note
Do not use a liquid leak detector on the valve or components within the MVS
insulated cover.
The following steps are performed to leak-check the Model 700 at the
factory when the unit is quality-checked prior to release. This procedure
is more thorough and is designed to isolate specific zones where a leak
may occur.
Leak check the Carrier Gas line first, according to the steps that follow.
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Note
Do not use the “Carrier Pressure Adjust” valve (on the Flow Panel of the Model
700 GC) to adjust Carrier Gas line pressure. The valve is factory-set and should
not be adjusted.
Next, leak check the calibration gas feed line, per the following steps:
Note
Calibration gas line pressure of 50 psig is for leak check and test purposes only. For
normal operation, the calibration gas line pressure is maintained at 20-30 psig.
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Next, leak check the sample gas lines, per the following steps:
Note
Calibration gas line pressure of 50 psig is for leak check and test purposes only.
For normal operation, the calibration gas line pressure is maintained at 20-30
psig.
2. Leak test all other sample stream lines by connecting gas to each
of the sample streams and repeating Step 1(a) through 1(b).
Finish the test and set up the Model 700 for normal operation, as follows:
3. If the calibration gas bottle was used to leak check the sample
stream lines, reconnect the calibration gas bottle to the
calibration gas line on the flow panel assembly. Reconnect the
sample stream lines.
To ensure that lines, columns, and valves are not plugged, check the gas
flow at valve ports. For a reference, use the flow diagram in the drawing
package, and remember these points about flow diagrams:
• Port-to-port flow paths are indicated by solid or dashed lines.
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• A dashed line indicates flow direction when the valve is ON, that is,
energized.
• A solid line indicates flow direction when the valve is OFF, i.e., not
energized.
• A combination of solid and dashed lines indicates a constant flow
path regardless of the ON/OFF state of the valve.
The tools required for performing repair and general maintenance on the
valve assemblies are:
• Torque wrench, scaled in foot-pounds
• 1/2” socket
• 1/4” open-end wrench
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• #1 flat screwdriver
Note
If an existing unit has a teflon gasket between the lower actuation diaphragms and the
kiosk block, install gasket P/N 2-4-0700-064 (for 6-port valves) and P/N 2-4-0700-160
(for 10-port valves). Otherwise, the teflon gasket is not required.
To disassemble a valve, unscrew the torque bolt and then flip the valve
over so that the bolt is pointed toward the floor.
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torque bolt
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Blow clean and dry valve parts with nitrogen before reassembling.
1. Inspect the primary plate (Item #9, refer to Figure 4-15) to insure
that the tubing parts are clean and that the sealing surface has no
scratches or pits.
2. Insert guide pins (#2 and #3) in the locating holes in the primary
plate (#9).
3. Place the sealing diaphragm over the guide pins and onto the
primary plate.
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4. Place the cushion diaphragm over the guide pins and onto the
sealing diaphragm and the primary plate.
5. Slide the upper piston plate (#5) over the guide pins.
6. Set the three short pistons (#6) into their respect places in the
upper piston plate.
7. Place the two upper actuator diaphragms over the guide pins and
onto the upper piston plate, covering the short pistons.
8. Slide the lower piston plate (#1) over the guide pins and onto the
upper actuator diaphragms.
9. Set the three long pistons (#4) into their respect places in the
lower piston plate.
10. Place the two lower actuator diaphragms over the guide pins and
onto the lower piston plate, covering the long pistons.
11. Install the torque bolt and washer (#8 and #7) up through the
primary plate and tighten the bolt to 30 ft. lbs.
12. Holding the bolthead and retainer with one hand, install the
plastic retainer disk and cap to hold the assembly together until
the valve is installed onto the GC.
Note
Do not use an oil-based cleaner on the valve.
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Use the following procedure for removing the Oven System from the
Model 700 unit:
Note
The Oven System may be removed and repaired at a bench. However, it is not necessary
to remove the oven.
WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.
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Thermal
Cover
3. Loosen the screw on the mounting bracket that secures the Oven
Plate to the support post (see Figure 4-17).
4. Lift up slightly and rotate the oven forward one quarter turn so
that the components are accessible.
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Oven System
Wiring Plug
Connector
Blocks
6. Unplug the heat control wiring from the driver board side.
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10. Lift the oven assembly from the unit for bench maintenance and
repairs.
Use the following procedure for removing the FID from the Model 700
unit.
WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.
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CAUTION
This unit operates at high temperature. Allow a cool-down period of at least 10 minutes
after shutdown and handle the unit carefully. Failure to follow this precaution may
result in injury to personnel.
FID
Oven System
Connector Blocks
4. Grasp the edges of the Connector Board on top of the unit and
pull and wiggle to remove the six socket tubes that extend onto
the pins in the cap (see Figure 4-20).
5. Remove the exhaust tube from the side by pulling the 'U' shaped
retainer from the top of the exhaust body and moving the
exhaust tube away from the FID. Take care not to lose the clip.
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7. Grasp the shielded section and lift it over the burner. Pull the cap
out of the shield. Remove the body from the shield, if necessary.
The FID cap has no replaceable parts. Damage like a broken RTD or
broken igniter coil requires a replacement cap.
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2. Gently lift out the burner tip tube. Use short needle nose pliers if
it is stubborn, taking care not to bend the tube. The alternative is
to unscrew the assembly and clean as an assembly.
1. Insert burner tip tube into the isolating nut. Be certain it is fully
seated. There should be about .350 of tube visible.
2. Tighten the isolating nut in small increments until the tube ceases
to pull free. Slight additional tightening will ensure proper
sealing.
3. Place the cap onto the end of the body with the deep cavity.
Once the alignment pin is in its mating hole, gently press the two
parts together and ensure the o-ring is seated properly.
4. Slide the FID shield onto the body from the bottom. Align the
notch with the exhaust fitting and insert the two screws.
5. Lower the FID body assembly onto the base, placing the
alignment pin in its hole. Press the body into place, seating the o-
ring. Tighten the screws slightly more than 'finger tight.'
7. Press the FID exhaust tube onto the fitting and anchor with the
‘U’ shaped clip. (1/16 tubing makes an adequate clip.)
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Thermal
Cover
CAUTION
This unit operates at high temperature. Allow a cool-down period of at least 10 minutes
after shut-down and handle the unit carefully. Failure to follow this precaution may
result in injury or death to personnel.
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3. Disconnect sample and air tubing from the outer portions of the
LSIV.
CAUTION
Use of wrenches other than a strap wrench to disassemble the LSIV can damage the
valve beyond repair. Failure to follow this precaution may damage equipment.
2. There are two seals with a central packing gland between them to
be removed, either from the stem or the bore in the body. Use
care to avoid scratching the stem or bore surfaces.
3. Replace the two seals with the central packing gland between
them onto the stem. Carefully align the two assemblies and insert
the seals into the bore.
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Use the following procedure to disassemble the LSIV and refer to Figure
4-22.
1. Use the one (1) inch strap wrenches and unscrew the piston
housing (counter-clockwise) from the seal assist housing (use one
strap wrench on the piston housing and one strap wrench on the
seal assist housing).
CAUTION
Use care when disassembling the LSIV to prevent bending the valve stem. Failure to
follow this precaution may cause damage to the equipment.
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3. Separate the piston and valve stem assembly from the piston
housing or seal assist housing by carefully pulling it straight out.
7. Push out the football seals and the central packing gland from the
body.
10. Unscrew the seal nut from the upper piston packing gland.
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A. Case
B. Insulation
C. Tube
D. Catalytic Column
E. Heater
F. RTD (temperature detector)
G. Two #6-20 x 1/2 stainless steel screws
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1. Disconnect the tubing and wiring, then lift the Methanator from
the enclosure.
2. Remove the two screws and open the box (enclosure). The
catalytic column assembly is housed inside this insulation-filled
box.
Note
Replacement factory-built valves are available. We recommend returning and replacing
the 6-port valve for extensive repairs or complete replacement.
1. Shut off carrier and sample gas streams entering the unit.
3. If the faulty valve is not easily accessible, loosen the thumb screw
and rotate the oven forward (see Figure 4-17 and Figure 4-18).
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Note
The Oven System may be removed and repaired at a bench. However, it is not
necessary to remove the oven.
4. Disconnect tubing and fittings that attach to the valve from other
locations.
Valve
Attaching
Bolt
Fitting
Tubing
6. Holding the lower piston plate, pull the valve straight off the
block. The alignment pins may stick slightly.
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Note
Ensure that the primary seal diaphragm is correctly installed on the primary
plate.
Note
Do not scratch the primary plate surface.
Note
Do not use an oil base cleaner on the valve.
(b.) Align the pins with holes in the block and push the valve
assembly into place.
(c.) Tighten the valve “attaching bolt” to 30 lbs./ft. (40 N-m)
(d.) Reconnect all fittings and tubing
(see Figure 4-24).
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Both the oven system and the stream switching system use the same
solenoid valves. The solenoids are replaced in both systems using the
same procedure.
WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.
Replace the oven system and stream switching system (SSS) solenoids
using the following steps.
Note
Carrier Gas leaks may be caused by the SSS solenoids See “Leak checks” on page 4-26
for leak check procedures.
2. Loosen the mounting bracket thumb screw that secures the oven
to the chassis, see Figure 4-25.
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Thumb Screw
3. Holding the left side of the oven mounting plate, gently lift up the
assembly and rotate it so that the enclosure opening is accessible.
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7. Disconnect the wire leads and remove the gasket from the
bottom of the solenoid block.
8. Replace the old leads at the connector plug or splice the wires
from the new solenoid to the old leads.
Note
The solenoids are not polarity sensitive.
The following procedure should be performed if the Model 700 does not
produce a chromatogram.
1. Remove the cover of the upper explosion- proof housing and the
thermal cover on the Model 700 for access the preamplifier.
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Detector 1 Detector 2
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Detector 1
1. Attach a flow meter to the vent output on the right side of the
Model 700 “MV1”(marked on the tag).
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MV1
(Marked on tags)
MV2
WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.
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2. Remove the lower enclosure cover and access the card cage
assembly holding the circuit boards.
Explosion-proof Cover
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Note
After removing the cable(s), any board may be replaced without removing the
card cage assembly.
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The DC/DC power supply is mounted on the left wall of the lower
enclosure (see Figure 4-35) and is accessible by removing the threaded
cover plate from the housing.
WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.
DC Power
Supply
Note
Needle nose pliers may be used to turn rear thumbscrews.
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1. Disconnect the cables from the CPU, the Com4A board (if
installed), and the modem board.
2. Unscrew the card cage thumb screws and remove the card cage
assembly.
7. Align the power supply bracket and tighten the two thumb
screws.
8. Reinstall the card cage assembly, tighten the thumb screws and
reconnect all cables.
4.11 Communications
The Model 700 with the TCD has up to six communications channels
available; up to three communications ports from the WinSystems CPU
board and four communications ports from the Com4A board.
Note
See Appendix A for a list of the ports and terminals (pins) assigned to serial communica-
tions.
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The communication protocols are selected inside the Model 700 GC with
jumpers. The protocols are normally specified by the customer and then
set at the factory.
WARNING
The enclosure should not be opened when hazardous gases are present. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.
The jumpers to be changed are located on the CPU board and the
Com4A board.
When the desired GC address (Com ID) is known, it will be set before the
unit leaves the factory. If the address (Com ID) needs to be changed in
the field, it will be necessary to change the arrangement of an 8-position
DIP switch on the multifunction board.
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Ensure the cables are replaced in the exact order and positions.
Note
See “Inspect or change the Com ID” on page 3-31 for an explanation of DIP switch
settings and their determination of the GC Controller Modbus slave address (Com ID).
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The analog outputs can be calibrated and or adjusted via the MON2000
software. However, these outputs should be measured with a good
digital meter upon initial installation at zero scale and full scale. Then the
span can be set with MON2000 software so that it represents values
from zero to 100 percent of the user-defined units in use.
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There are four analog inputs available on the Field Termination Board (J4
- 12-pin Phoenix connector).
The initial analog output adjustment will be set at the factory, before
shipment, at standard values (4-20 mA). It may be necessary to check
and/or adjust these values depending on output cabling/impedance.
The adjustment may require two persons if the units are some distance
apart. It will require a good digital meter to check the zero and full scale
values at the receiving end. The scale or span value can be adjusted by a
PC with the Model 700 when the values are known at the receiving end.
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The Model 700 has four standard analog outputs (J8 - 12-pin Phoenix
connector) on the Field Termination board (P/N 3-0700-010).
J4
J8
Analog
Outputs
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The analog outputs for the optional analog board (P/N 2-3-0580-037)
are configured as follows:
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2-3-2350-098 Ethernet PCA (If replacing faulty Ethernet board; if a Optional Optional
new kit is needed, purchase 2-3-2350-143)
2-4-0700-152 Solenoid valve, Srs 3 3
2-4-0700-171 Repair Kit, 10-Port Valve (For use on Model 700 GCs Application Application
only) dependent dependent
2-4-0700-187 Repair Kit, 6-Port Valve 3 6
2-4-5000-113 Filter Element 2 Micron, Swagelok SS-2F-K4-2 1/stream 2/stream
2-4-5000-938 Membrane Kit, Genie® Model 120 Filter/Bypass/LSO 1/stream 2/stream
Note
Refer to the MON2000 Software for Gas Chromatographs User Manual (P/N 3-9000-522)
for BOS upgrade procedures.
BOS provides the basic resources and interfaces to run the user's tasks.
Unlike DOS or Windows or Linux, since BOS is an embedded real-time
multi-tasking preemptive operating system, there is no direct user level
interface to it. If a BOS upgrade is required to your system, refer to the
MON2000 Software for Gas Chromatographs User Manual (P/N 3-9000-
522) for additional BOS information.
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4.15.2 Applications
The GC application, which runs under BOS, utilizes the tools provided by
BOS to perform the desired gas chromatograph functions for the user.
There are different applications to provide for different gas
chromatographic needs. To load a new application or to upgrade an
existing application refer to the MON2000 Software for Gas
Chromatographs User Manual (P/N 3-9000-522) for details.
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Appendix A: Communications specifications
A
The MON2020 Software for Gas Chromatographs with a TCD has three
standard CPU serial communications ports: Com1, Com2, and Com4;
and four optional Com4A board serial ports: Com5 Com6, Com7, Com8
and Com9 for the optional internal modem. Per the matrix below,
jumper settings can be configured for either RS-232, RS-422, or
RS-485 serial signal definitions.
Note
Com3 is reserved for the multifunction board.
Com1 and Com2 (WinSys CPU RS-232, RS-422 or RS-485 PC, Flow Computer, Modem
Board) J1 to FTB (external)
Com3 (WinSys CPU Board) J6 to RS-232 Reserved for Multifunction Board
Multifunction Board
Com4 (WinSys CPU Board) RS-232, RS-422 or RS-485
J6 to FTB
Com5 (WinSys Com4A Board) RS-232, RS-422 or RS-485 Modem (External)
J9 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com6 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J13 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com7 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J17 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
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The CPU board has three communications ports that can be used for the
PC or the Flow Computer, as the customer desires.
Note
A telephone modem can be connected to any of the GC serial ports configured for RS-
232. If an internal modem (WinSystems P/N 3-0580-042) or (P/N 3- 0700-029
Radicom) is installed, it is assigned to serial port Com9. If the Com4A board is installed,
the modem is assigned to Com9. With or without the Com4A board, the internal
modem is assigned to Com9.
Serial ports configured for RS-232 are most commonly used for direct
serial communication between the GC and a PC or modem.
Serial ports configured for RS-422 or RS-485 are most commonly used
for long distance serial communications systems, such as a DCS or a
network. For these systems, the GC can communicate as a Modbus slave
device.
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Note
In any Modbus host-slave DCS or network, there must only be one host to which any
one of the GC serial ports can respond as a Modbus slave. To use MON2000 to configure
the GC for Modbus communication, see the MON2000 Software for Gas Chromatographs
User Manual (P/N 3-9000- 522).
Note
The Model 700, standard configuration, has three ports available on the FTB: Com 1,
Com 2, and Com 5.
Multifunction
Board
Com3
CPU
Field Termination
Com1
Board
Com2
Com1
Com3 Com2
Com4
Com5
Com6
Com7
Com8
Note
The Model 700 with the Com4A board installed has six communications ports available
on the FTB: Com1 and Com2, and Com5, Com6, Com7, and Com8.
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Com1
Field Termination
Com2 Board
Com3
Com1
Com4 Not
Connected Com2
Com5
Com 4A Com6
Com7
Com5
Com8
Com6
Com7
Com8
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Com1
P2
5
RI 1 9
DSR 1 4
RTS 1 8
RXD 1 3
CTS 1 7
TXD 1 2
DTR 1 6
DCD 1 1
GND Com2
P3
5
RI 2 9
DSR 2 4
RTS 2 8
RXD 2 3
CTS 2 7
TXD 2 2
DTR 2 6
DCD 2 1
Note
Com3 is reserved for Multifunction board. Com4 is reserved for the FID/TCD board.
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Com1 and Com2 (WinSys CPU Board) J1 RS-232, RS-422 or RS-485 PC, Flow Computer, Modem
to FTB (external)
Com3 (WinSys CPU Board) J6 to RS-232 Reserved for Multifunction
Multifunction Board PCB
Com4 (WinSys CPU Board) RS-232 Reserved for FID/TCD
J6 to FID/TCD Preamplifier Preamplifier PCB
Com5 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J9 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com6 (WinSys CPU Board) RS-232, RS-422 or RS-485
J13 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com7 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J17 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com8 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J18 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com9 Reserved for internal modem
Note
In any Modbus host-slave DCS or network, there must only be one host to which any
one of the GC serial ports can respond as a Modbus slave. To use MON2000 to configure
the GC for Modbus communication, see the MON2000 Software for Gas Chromatographs
User Manual (P/N 3-9000- 522).
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Serial ports configured for RS-232 are most commonly used for direct
serial communication between the GC and a PC or modem.
Serial ports configured for RS-422 or RS-485 are most commonly used
for long distance serial communications systems, such as a DCS or a
network. For these systems, the GC can communicate as a Modbus slave
device.
Note
The Model 700, standard configuration, has two communications ports available on
the FTB: Com1 and Com2.
Multifunction FID/TCD
Board Preamplifier Board
Com3 Com4
Note
Com4 is dedicated to the FID/TCD Preamplifier. When the LOI becomes available, it will
use a video board instead of a serial port connection.
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Com4A
Com5 Com5
Com6 Com6
Com7 Com7
Com8 Com8
Note
The Model 700, with the Com 4A board installed, has six communications ports
available on the FTB: Com1 and Com2, Com5, Com6, Com7, and Com8.
Note
Com4 is dedicated to the Micro-FID/TCD Preamplifier. When the LOI becomes available,
it will use a video board instead of a serial port connection.
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Note
Serial communications for FTB (Com1- Com4) is standard. Com3 reserved for the
Multifunction board. Serial communications with optional Com4A board are available
on ports Com5 - Com8.
Note
If you are changing or adding serial communications to the GC, ensure that the
correct jumpers are set.
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Com2
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Com7
Com8
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This section applies only to GCs not installed with the WinSystems LX-
800 CPU board (P/N #2-3-0700-036).
Com1
RS-232 Mode
J8 — Jumpers Pins 1 and 2
J13 — No jumpers
U2 — Installed (Standard)
U5 — Removed
U6 — Removed
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Com2
RS-232 Mode
J9 — Jumpers Pins 1 and 2
J16 — No jumpers
U9 — Installed (Standard)
U11 — Removed
U12 — Removed
RS-232 Mode
J12 — Jumpers Pins 1 and 2
J14 — No jumpers
U4 — Installed (Standard)
U7 — Removed
U8 — Removed
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RS-232 Mode
J15 — Jumpers Pins 1 and 2
J17 — No jumpers
U10 — Installed (Standard)
U13 — Removed
U14 — Removed
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Jumper settings and pinouts for the four serial communications ports
(COM5 - COM8) on the optional WinSystems Com4A board are defined
in the following tables.
Table A-7 Communication with WinSystems
MCM/LPM — Com4A Board (Optional)
Com5
RS-232 Mode
J2 — No jumpers
U6 — Installed (Standard)
U3 — Removed
U4 — Removed
J2 — No jumpers
U6 — Removed
U3 — Installed
U4 — Installed
Com6
RS-232 Mode
J5 — No jumpers
U13 — Installed (Standard)
U10 — Removed
U14 — Removed
J5 — No jumpers
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Com6
U13 — Removed
U10 — Installed
U14 — Installed
Com7
RS-232 Mode
J4 — No jumper
U11 — Installed (Standard)
U9 — Removed
U12 — Removed
J4 — No jumpers
U11 — Removed
U9 — Installed
U12 — Installed
Com8
RS-232 Mode
J1 — No jumpers
U5 — Installed (Standard)
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Com8
U1 — Removed
U2 — Removed
J1 — No jumpers
U5 — Removed
U1 — Installed
U2 — Installed
Pin(s) Position
1 and 2 In
3 and 4 In
7 and 8 In
9 and 10 In
Pin(s) Position
1 and 2 Open
3 and 4 Open
5 and 6 Open
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Pin(s) Position
1 and 2 In
3 and 4 In
5 and 6 In
7 and 8 In
Pin(s) Position
1 and 2 In
5 and 6 In
Jumper settings and pinouts used on the MON2020 Software for Gas
Chromatographs for the PCM-NE-2000-16 PC-104 Ethernet board
(optional) are defined in the following table:
Table A-12 Ethernet Board Pin Settings
J1 13 and 14
15 and 16
17 and 18
23 and 24
27 and 28
J2 1 and 2
J3 1 and 2
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The jumper settings and pinouts for the Radicom Modem (P/N 3-0700-
029) are shown below:
Table A-13 J26 Radicom Modem Jumper Settings
Pin(s) Position
1 and 2 In
Pin(s) Position
1 and 2 In
Pin(s) Position
1 and 2 In
Pin(s) Position
2 and 3 In
This section provides more detailed information about local serial port
connections for the Model 700. It identifies serial port pin assignments
and diagrams for designing
RS-232 serial cables.
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GC serial ports are found on the Field Termination Board and the
connection points for external devices are as follows:
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Phoenix Plug
Port Comments (bare-wire)
connection
Phoenix plug (bare-wire) connections are available to all four serial ports.
Pin-outs are identical for all four serial port Phoenix plugs and jacks. Each
Phoenix plug/jack (male) combination allows a bare-wire connection and
uses 9-Pins as illustrated:
Figure A-14 Phoenix Connector (J5, J6, J10, and J11) Pinout
Null modem connections (DB 9-pin) are available for Serial Ports 1 and 2
only, as noted in Table A-17.
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Note
PC-to-GC connections, direct serial: The GC serial ports were wired to appear as DCE, so
a straight-through serial cable is used for a direct serial connection between the GC and
the PC. (The PC is Data Terminal Equipment, or DTE.) See “GC DB 9-pin serial port to PC
DB 9-pin port” on page A-25.
External modem-to-GC connections, serial: a null modem cable and gender changes
may be purchased from any computer products store, for the GC to external modem
connection. However, a custom serial cable may be built to emulate a null-modem
cable for a connection between the GC Controller and an external modem. (The
modem is Data Communications Equipment, or DCE.) See “Wiring remote RS-232
communications” on page A-28.
Both of the GC DB 9-pin jacks are female and have identical pin
assignments. Note that a DB 9-pin male numbering scheme is also
illustrated, but for reference purposes only as follows.
Figure A-15 DB 9-pin connector (P2 and P3) and pinout for jacks
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9 6 6 9 6
9
9 RI 9 RI 9 RI
8 RTS 8 CTS 8 CTS
7 CTS 7 RTS 7 RTS
6 DTR 6 DSR 6 DSR
5 GND 5 GND 5 GND
4 DSR 4 DTR 4 DTR
3 RxD 3 TxD 3 TxD
2 TxD 2 RxD 2 RxD
1 RLSD 1RLSD 1RLSD
(DCD) (DCD) Straight-through serial cable(DCD)
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Note
The cable for this application is also available(P/N 3-2350-068) in a customer-specified
length with six exposed leads and a female DB 9-pin connector.
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Note
Data Communications Equipment (DCE). Use a custom nullmodem type cable to make
the connection between the GC and an external modem. GC serial ports were wired to
appear as DCE so that a straight-through serial cable could be used for a direct serial
connection between the GC Controller and the PC, which is Data Terminal Equipment
[DTE].
5 1 1 5 1 13
9 6 6 9 14 25
9 RI 9 RI 22 RI
8 RTS 8 CTS 4 RTS
7 CTS 7 RTS 5 CTS
6 DTR 6 DSR 20 DTR
5 GND 5 GND 7 GND
4 DSR 4 DTR 6 DSR
3 RxD 3 TxD 3 RxD
2 TxD 2 RxD 2 TxD
1 RLSD 1 DCD 8 DCD
(DCD) Null Modem cable
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Note
See “Setting the Com ID” on page 3-30 for additional details about serial
communication setups.
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Note
For this example, a straightthrough RS-232 serial cable is used to connect between the
PC and the line driver.
Front Panel Switch NORMAL / DLB NORMAL Uses normal operation, instead of
loopback testing.
DIP Switch Bank XW1A DCE / XW1A DCE Sets line driver to operate as data
communications equipment (DCE).
XW1B DTE
DIP Switch Bank S2 UNTERM Eliminates need for resistor network
termination to connect one PC directly
to one GC.
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Note
See “Setting the Com ID” on page 3-30 for additional details about serial
communication setups.
Refer to Figure A-23 and Figure A-24 for RS-485 line terminations,
jumpers and switch settings to configure the line driver device (also
listed in Table A-19).
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Note
For this example, a straightthrough RS-232 serial cable is used to connect between the
PC and the line driver.
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Front Panel NORMAL / DLB NORMAL Normal operation used, instead of loopback
Switch testing.
DIP Switch Banks XW1A DCE / XW1A DCE Sets line driver to operate as data
communications equipment (DCE).
XW1B DTE
DIP Switch Banks S2 UNTERM Eliminates need for resistor network
termination to connect one PC directly to
one GC.
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Appendix B: Modem installation
B
Note
Revision C of the Internal Modem requires MON2000 software, version 2.2 or later.
WARNING
Before removing the cover from the GC, ensure that the power supply switch is OFF and
the AC power cord is disconnected. Failure to follow this warning may result in injury or
death to personnel or cause damage to the equipment.
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J26 1-2
J27 1-2
J30 1-2
J31 2-3
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2. Remove the CPU assembly and install the Ethernet assembly with
associated hardware into J19 and J20 PC/104 Bus connector on
the CPU assembly. If an option board is already plugged into the
PC/104 Bus on the CPU, install the Ethernet assembly and
mounting hardware into the PC/104 Bus connector on the option
board.
4. Run the Ethernet line through the conduit into the lower
enclosure and connect it to the Ethernet extension cable.
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B-4
Appendix C: Manifold Carrier for Gas Bottles
C
Note
The illustration and information in this appendix are adapted from drawing #AE-10098.
• When one bottle is nearly empty (i.e., 100 psig remaining), the other
bottle becomes the primary supply.
• Each bottle can be disconnected for refilling without interrupting GC
operation.
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6. Open V-1 (bleed valve) and let the carrier gas bleed to
atmosphere until both gauges read 0 psig, then close V-1.
7. Repeat Steps 4 and 5 two more times to purge the line to V-2.
9. With valves 1-4 closed, open both cylinder valves and regulate
both carriers to approximately 10 psig.
10. Open V-2 and V-3 simultaneously, then turn both cylinder valves
off and let the carrier gasses bleed through the line to the
Analyzer until all gauges read 0 psig.
11. Repeat steps (8) and (9) two more times to purge line to Analyzer.
13. Open cylinder valve of Carrier Cylinder 1 and, with carrier gas
flowing at 10 psig or below, connect carrier line to Analyzer.
15. Open V-3 and slowly regulate Carrier Cylinder 2 to 100 psig. (By
doing this, all but 100 pounds of Carrier Cylinder 1 will be used
before any of Carrier Cylinder 2 is used. When Carrier Cylinder 1
gets to 100 pounds, replace the cylinder). Leak-check all of the
fittings carefully.
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4. Open the appropriate block valve to the Analyzer (V-2 or V-3) and
regulate outlet pressure to appropriate level. (See Steps 14 and
15 of Installation Instructions, "Section C.2: Installation and line
purging".)
The calibration gas used for BTU analysis should be blended of gases
specified as Primary Standards. Primary Standard gases are blended
using weights that are traceable to the National Institute of Standards
and Technology (N.I.S.T). For other applications, the calibration gas
should be blended to the specifications detailed in the analyzer’s
Application Data Sheets.
The calibration gas should not have any component that could drop out
at the coldest temperature to which the gas will be subjected. A typical
blend for a temperature of zero degrees Fahrenheit is listed in Table C-1.
No dropout will occur in this calibration gas if it is blended at a pressure
below 250 psig.
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Mole
Gas
Percent
Nitrogen 2.5
Carbon Dioxide 0.5
Methane Balance
Propane 1.0
Isobutane 0.3
N-butane 0.3
Neopentane 0.1
Isopentane 0.1
N-pentane 0.1
N-hexane 0.03
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C-6
Appendix D: Local operator interface
The local operator interface (LOI) has multiple components that you can
use to interact with the unit.
A. LCD screen
B. Keypads
C. LED indicators
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There are three light emitting diode (LED) status indicators on the LOI
that show the overall status of the gas chromatograph. These LEDs are
positioned to the right of the display screen. Each LED, when lit, indicates
a specific condition.
D.1.3 Keypad
The keypad consists of eight infrared keys. See “Navigating the screen”
on page D-5 for more information.
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The four keys located above the LCD screen are “command” keys.
The four keys below the LCD screen are arrow keys that allow you to
navigate within the screen by scrolling or moving the cursor from field to
field. These keys function in the same way as a computer keyboard’s
arrow keys.
A key is “pressed” by placing a finger on the glass over the associated key
hole and then removing the finger. Holding a finger over the key hole will
cause that key to repeat until the finger is removed.
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D.2.1 Start up
Upon starting the GC, the LOI automatically runs in Status Display
mode, in which it scrolls through a predefined series of screens,
displaying each screen for approximately 30 seconds.
Status Displays information about the operational state of the analyzer, including a
scrolling list of up to 25 user-selectable parameters that can be defined or
modified using the MON 2000 application.
NOTE: There may be more than one Status screen, depending upon the GC’s
mode of operation.
Live Chromatogram Displays the chromatogram for the current analysis in real time.
NOTE: There may be more than one Live Chromatogram screen, depending
upon the GC’s mode of operation.
NOTE: This screen does not display if the GC is not currently analyzing a
sample.
Active Alarms Lists active alarms, if any.
Heater Displays information about the PID temperature control loops.
Valves Displays the settings and states of the stream and analyzer valves.
In Status Display mode, you can manually scroll to the next screen
using the RIGHT arrow key, or to the previous screen using the LEFT
arrow key. You can pause automatic scrolling at any time by pressing the
EXIT key, and you can resume automatic scrolling by pressing either the
LEFT or the RIGHT arrow key. Automatic scrolling resumes after ten
minutes of keypad inactivity.
Pressing F1 when “MOVE” is displayed in the green box below it takes the
focus inside the screen so that you can navigate through the controls of
the screen using the LEFT, RIGHT, UP and DOWN keys. Pressing EXIT
returns the focus to the top level–that is, outside of the screen. Pressing
LEFT or RIGHT at the top level resumes automatic scrolling in addition
to moving to the previous or next screen.
At any time while in Status Display mode, you can press ENTER or F2 to
enter the Main Menu. Use the EXIT key to leave the Main Menu and
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return the LOI to Status Display mode. If you log onto the GC from the
Main Menu to perform operations or edit data, when you exit the menu
you will automatically be logged off the LOI.
At any time while in Status Display mode, you can press ENTER or F2 to
enter the Main Menu.
Use the UP and DOWN arrow keys to navigate between fields or controls
within each drop down menu. Pressing the DOWN arrow key while focus
is on the last field of a drop down menu moves the focus to the first field
on a screen. Alternatively, pressing the UP arrow key while focus is on the
first field of the drop down menu causes the focus to move to the last
field.
Use the ENTER key from the Main Menu to activate submenus and
individual menu items.
Press EXIT to leave the Main Menu and return the LOI to Status
Display mode, if no menu is dropped down. If a menu is dropped down
then pressing EXIT closes that menu.
If you log onto the GC from the Main Menu to perform operations or
edit data, when you exit the menu you will automatically be logged off
the LOI.
The Main Menu allows you access to all of the available LOI screens.;
however, you must be logged on to make changes. If you are not logged
on and you attempt to edit a field, the Login screen will appear first.
LOI screens have several functions. They can display data for review; they
can display data for editing; and they can be used to initiate activities.
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Within any given screen, the function of the ENTER key depends upon
the context. It can be used to validate and save changes or to initiate an
action.
Pressing EXIT closes the currently open screen. If you have made
changes to the screen, the LOI will display a confirmation message asking
if you want to save your changes. Use the arrow keys to select the
appropriate button and press ENTER. If you select No, your changes will
be discarded and the Main Menu will display; if you select Cancel, the
message window will close and you will be returned to the current
screen; if you select Yes, your changes will be validated and saved and
then you will be returned to the Main Menu.
Press F1 to open the edit dialog for the field that contains the
cursor. The type of dialog that displays depends upon the
type of field to be edited. See “Editing numeric fields” on
page D-7 and “Editing non-numeric fields” on page D-9 for
more information.
Press F1 to select the field to be edited.
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Note
Throughout this appendix, when referring to the F1 key, the key’s current valid
function will be indicated in parenthesis–for instance, F1 (MOVE) or F1 (SELECT).
The F2 key, when “MAIN” is displayed in the prompt box, closes all
screens and goes back to the Main Menu.
There is a navigation icon in the upper right corner of the screen that
indicates which navigation keys are active for the currently displayed
screen.
When you press a key, a green square will flash in the upper left corner if
the key is valid; if the key is not valid, a red box will flash in the upper left
corder.
When the focus is on an editable field, pressing F1 (EDIT) will display the
Edit Dialog containing the field’s original text.
Use the LEFT and RIGHT arrow keys to move through the individual
characters within the field and to select the character to be changed. Use
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the UP and DOWN arrows keys to select the value of each digit. The
possible values are 1, 2, 3, 4, 5, 6, 7, 8, 9, 0, “-” (minus), “.” (period), and
“E”.
The “.” and the “E” values are available for floating-point numbers,
except for retention times and timed event values.
The DOWN arrow key moves backward in the list from the current value
of the selected digit.
The UP arrow key moves forward in the list from the current value of the
selected digit.
The ENTER key validates and saves the entry, then closes the Edit
Dialog. The new entry will display in the field.
The EXIT key cancels any changes that were entered and closes the Edit
Dialog, restoring the previous value to the field.
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2. Use the UP and DOWN arrow keys to move through the various
radio buttons within the group.
2. Use the UP and DOWN arrows keys to move between the values
within the list box.
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1. Press F1 (SELECT) while focused on the Date and Time field and
the Enter the Date and Time dialog displays. By default, the
focus is set on the “Month” unit.
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2. Use the UP and DOWN arrow keys to change the value of the
unit–that is, to go from January to February, or from 1 to 2.
3. Use the LEFT and RIGHT arrow keys to change units–that is, to
go from months to years or hours to minutes.
Note
If the focus is on the left most section, the LEFT arrow key will be inactive and
similarly if the focus is on the right most section, the RIGHT arrow key will be
inactive.
1. Press F1 (SELECT) while focused on the Time field and the Enter
the Time dialog displays. By default, the focus is set on the “Hour”
unit.
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2. Use the UP and DOWN arrow keys to change the value of the unit.
3. Use the LEFT and RIGHT arrow keys to change units–to go from
hours to minutes, for example.
Note
If the focus is on the left most section, the LEFT arrow key will be inactive and
similarly if the focus is on the right most section, the RIGHT arrow key will be
inactive.
This tutorial, which guides you through the procedure for editing data on
a screen, will incorporate all of the preceding information to
demonstrate the typical method of navigating and interacting with the
LOI. You will learn how to perform the following actions:
• Opening and closing screens
• Navigating through tables
• Selecting fields for editing
• Saving data
1. From the Main Menu, click the RIGHT arrow key enough times
to navigate to the Application menu. The System submenu, since
it is the first item in the list, is already selected.
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Note
In this instance, the term “click” means to tap the glass on the spot directly
above the arrow’s keyhole.
Note
Notice the navigation icon in the upper right corner, which indicates that all
four arrow keys are active. This allows you to navigate to all of the menu items
and sub menu items.
Note
Notice that the green prompt boxes are empty. This means that the F1 and F2
keys are inactive from the Main Menu.
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Note
Notice the navigation icon in the upper right corner, which indicates that no
arrow keys are active.
4. Notice that the navigation icon in the upper right corner of the
screen indicates that the down arrow is active. Click the down
arrow once. Now the navigation icon indicates that both the up
and down arrows are active. Click the up arrow once to return to
the previous cell. The navigation icon again indicates that only the
down arrow is active.
5. Notice that the green F1 prompt box reads “EDIT”. Click F1.
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Note
Notice that there is also a navigation icon on the Login dialog.
Note
For the remainder of this tutorial, when referring to the F1 key, the key’s
current valid function will be indicated in parenthesis–for instance, F1
(MOVE) or F1 (SELECT).
8. Click ENTER.
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11. Now that your are logged in, you can edit the fields on the screen.
Click F1 (EDIT). The Enter the data dialog displays.
Figure D-9. The Enter the data dialog allows you to edit the selected field
13. When you are finished entering data, press ENTER to validate and
save the new information. To discard the information, press EXIT.
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Note
If a validation error is found after pressing ENTER, an “Invalid Entry” message
displays. Press ENTER to close the message and then re-enter your data.
14. Use the down arrow to move to the Is Multi User Write
Enabled? check box.
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Figure D-12. The Is Multi User Write Enabled? check box, no longer checked
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19. Use the DOWN arrow to scroll down to the last item in the combo
box. Press ENTER.
20. Press ENTER a second time to save all the changes that were
made to the table.
Note
If you neglect to press ENTER at this point, all of your changes will be lost.
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The table below lists the submenus and commands that are available
from the Main Menu.
Submenu Command Subcommands Reference
Chromatogram
View
Chromatogram Settings page 26
Live Chromatogram View Screen page 27
(Status Mode)
Live Chromatogram Screen (Advanced page 28
Mode)
Archived Chromatogram Screen page 29
(Advanced Mode)
Live & Archived Chromatogram Viewer page 29
Options Menu
CGM Scaling Screen page 30
Chromatogram CDT Table page 31
Chromatogram TEV Table page 32
Chromatogram Raw Data Table page 32
Hardware
Heaters page 34
Valves page 35
Electronic Pressure Ctrl page 36
Detectors page 36
Discrete Inputs page 37
Discrete Outputs page 37
Analog Inputs page 38
Analog Outputs page 38
Installed Hardware page 39
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Application
System page 40
Component Data page 41
CDT 1
CDT 2
CDT 3
CDT 4
Timed Events page 41
TEV 1
TEV 2
TEV 3
TEV 4
Streams page 43
Status page 44
DET1
DET2
Ethernet Ports page 44
Logs/Reports
Maintenance Log page 46
Event Log page 47
Alarm Log page 48
Unack Alarms page 48
Active Alarms page 49
Report Display page 50
Control
Auto Sequence page 52
Single Stream page 53
Halt page 54
Calibration page 55
Validation page 56
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Refer to the MON2020 Software for Gas Chromatographs User Manual for
detailed information regarding the commands listed in The table above.
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Note
The blue box displays the current analysis time.
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Note
The blue box displays the current analysis time.
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Figure D-20. The Live & Archived Chromatogram Viewer Options screen
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Note
The blue box displays the cursor’s x- (analysis time) and y- (amplitude) coordinates.
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The Hardware menu enables you to view and manage the GC’s
hardware components.
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Note
The usage (Sample/BF1, Dual Column), mode (Auto, Off), and state (green = on, black =
off, red = error) of each valve is displayed. See the “Configuring the valves” section of
the MON2020 Software for Gas Chromatographs User Manual for more information.
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The Application menu allows you to view the CDT, TEV and streams
tables for the GC. The System, Status, and Ethernet Ports screens are
also accessible from this menu.
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The Logs/Reports menu enables you to view the various reports that
are available from the GC.
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Refer to the “Control menu” section of the MON2020 Software for Gas
Chromatographs User Manual for detailed information regarding the
Control menu screens.
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The Manage menu enables you to change the LOI’s settings, change a
user’s password, and log off of the GC to which you are connected.
Refer to the “Manage menu” section of the MON2020 Software for Gas
Chromatographs User Manual for detailed information regarding the
Manage menu screens.
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If the LOI is powered up but the LCD screen is blank, do the following:
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D - 62
Appendix E: LX-800 CPU Board Retrofit Instructions
In addition to the new CPU board, the kit contains the following items:
• MON2000 Gas Chromatograph Software for Windows (P/N #2-3-2350-
400). This CD-ROM also contains the software’s user manual (P/N #3-
9000-522).
• Six replacement cables
- P/N #2-3-2350-083
- P/N #2-3-2350-077
- P/N #2-3-2350-087
- P/N #2-3-2350-084
- P/N #2-3-2350-080
- P/N #2-3-2350-081
• A extra fuse (P/N #2-5-4203-130)
• Two replacement card guides (P/N #2-4-5001-078)
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Due to the addition of the Flash Memory connector on the back of the
new CPU board, a new Analog board (P/N #2-3-0700-034) also must be
installed to prevent interference with the back of the CPU board when
inserted into the card cage. The new analog board is included with the
retrofit kit.
The LX-800 CPU assembly has been designed to include all digital I/O and
COM1 through COM4 serial ports.
The UniBOS file on the CompactFlash card can be upgraded in the field
with MON2000. Refer to the MON2000 Software for Gas Chromatographs
user manual, which is located on the MON2000 CD-ROM, for
information about downloading 2350A applications and UniBOS
upgrades.
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CAUTION
UniBOS is preloaded on this CPU board. Do not attempt to install BOS or an earlier
version of UniBOS. Doing so will irreversibly corrupt the firmware and will require the
purchase of a new CPU board. To learn the version level of the UniBOS loaded onto your
CPU board, refer to the label on the board’s back.
The protocol setup for serial ports COM1 through COM4 can now be
configured through MON2000 version 2.58 or later. Each serial port can
be set to RS-232, RS-422 or RS-485. Protocol changes to the serial ports
on the COM4A board still require different jumper settings and IC chip
changes.
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Before replacing a 16-bit CPU board with the new 32-bit version, you
must first upgrade the 16-bit application to its 32-bit equivalent.
Note
This procedure applies to MON2000 version 4.04 or later.
Before performing the upgrade, you need to know the file names of the
16-bit application and its 32-bit equivalent.
If you don’t know the filename of the 16-bit application that you intend
upgrade, you can call Customer Support at 1-713-827-6314 to learn it.
Be prepared to supply a sales order number or a GC serial number.
2. Locate the appropriate 16-bit application file and select it. Click
Open.
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The end result of this procedure will be a 32-bit version of the 16-bit
application using a 32-bit application template file.
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Note
The latest versions of these application template files were installed with
MON2000 and are typically located at C:\GC\APP\.
Note
If the application template file selected is not newer than the currently
installed application, or if it is not the same type of application, MON2000
displays the following error message:
The selected application is not a compatible upgrade
4. Type a new name for the upgraded application into the File name
field.
Note
It is recommended that you give the 32-bit application a name similar to the
name of the 16-bit application it will replace.
Note
It is recommended that you do not give the 32-bit application the same name
as the application template file on which it is based. Doing so will over-write
the application template file.
6. Click OK.
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1. Remove the front panel or the LOI and disconnect the cables
going to the card cage assembly.
3. Unplug all PC104 boards from the CPU board and set them aside.
4. Make note of the analog board’s slot number in the card cage and
then eject the analog board from the card cage.
7. If there is a video driver board for an LOI in the stack, replace the
'Panel Out' cable with the new cable (P/N #3-0700-098) that is
supplied with the kit.
8. Insert the CPU board into the slot above the analog board and
connect the remaining cables. If necessary, refer to “Internal
Cable Wiring” (DE-20991), which is located in the drawings
section at the back of the manual.
10. If there is a COM4A board in the stack that is not installed at the
top position, it may be necessary to remove the cable clamp on
the connector that plugs into the board to avoid interference with
the board above it. The clamp is not required and can be
discarded.
11. Reconnect all cables to the switch panel or LOI and the analog
card.
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13. Start MON2000. The four CPU serial ports, COM1 - COM4, can be
configured through MON2000.
Note
Make sure that MON2000 version 2.58 or later is installed.
14. Select Serial Ports... from the Application menu. The Serial Ports
window displays.
15. Use the Mode column to select the protocol for each serial port.
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E - 10
Appendix F: Shipping and long-term storage
recommendations
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F-2
Appendix G: Recommended spare parts
The following tables list the recommended spare parts that would allow
you to maintain a single GC gas chromatograph for one year.
5+ GCs or
1-5 GCs Critical Description Part No.
Installations
0 1 PCA, CPU 32-bit w/ (4) RS-232 & BOS - Requires 32-bit 2-3-0700-232
application file
0 1 PCA Analog I/O (8 in / 4 out) 2-3-2350-041
0 1 Preamplifier Board 2-3-0580-002
0 1 Field Termination Board 2-3-0700-010
1 2 Fuses, Assortment (5 each 1A, 3A and 6A) 2-3-0700-136
0 1 Dual Methods Adapter Board 2-3-0700-011
0 1 Driver I/O Board 2-3-0700-005
0 1 Multifunction Board 2-3-0700-004
0 Note 1 Modem Bd. PC104 - Board Only, Upgrade Kit is part 2- 2-3-0700-029
3-2350-142
0 Note 1 PCA, 4 Isolated Analog Outputs Board 2-3-0700-007
0 Note 3 Assembly, Power Supply 115/230 VAC - Model 700 and 2-3-0700-110
Model 1000A only
2 2 Solenoid Valve, Srs 2-4-0700-152
1/Valve 1/Valve Repair Kit, 6-port Valve - For use on Model 700 only 2-4-0700-187
1/Valve 1/Valve Repair Kit, 10-port Valve - For use on Model 700 only 2-4-0700-171
1 1 Column Set Note 4
0 1/Detector Kit, Thermistors (TCD) Note 4
1 1 Teflon Thermistor Seals (Set Of 10) 2-3-0500-391
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5+ GCs or
1-5 GCs Critical Description Part No.
Installations
5+ GCs or
1-5 GCs Critical Description Part No.
Installations
0 1 PCA, CPU 32-bit w/ (4) RS-232 & BOS - Requires 32-bit 2-3-0700-232
application file
0 1 PCA Analog I/O (8 in / 4 out) 2-3-2350-041
0 1 Preamplifier Board 2-3-0580-002
0 1 PCA ADC Main Board Modified for FID/FPD 2-3-0700-032
0 1 Field Termination Board 2-3-0700-010
1 2 Fuses, Assortment (5 each 1A, 3A and 6A) 2-3-0700-136
0 1 Dual Methods Adapter Board 2-3-0700-011
0 1 Driver I/O Board 2-3-0700-005
0 1 Multifunction Board 2-3-0700-004
0 Note1 Modem Bd. PC104 - Board Only, Upgrade Kit is part 2-3- 2-3-0700-029
2350-142
0 Note1 PCA, 4 Isolated Analog Outputs Board 2-3-0700-007
0 Note1 PCA - Board with 8 Non-Isolated Analog Outputs for use 2-3-0580-037
with the Model 700/1000A only
0 Note2 Power Supply 24 VDC 2-3-0700-117
0 Note3 Assembly, Power Supply 115/230 VAC - Model 700 and 2-3-0700-110
Model 1000A only
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5+ GCs or
1-5 GCs Critical Description Part No.
Installations
1
1 recommended if this option is installed on the Model 700.
2 1 recommended if Model 700 is powered with 24 VDC line.
3
1 recommended if Model 700 is powered with AC line.
4 Application dependent. Please contact customer service at 1-888-801-1452 and provide
sales order number for recommended part number and description.
5+ GCs or
1-5 GCs Critical Description Part No.
Installations
0 1 PCA, CPU 32-bit w/ (4) RS-232 & BOS - Requires 32-bit 2-3-0700-232
application file
0 1 PCA Analog I/O (8 in / 4 out) 2-3-2350-041
0 1 Preamplifier Board 2-3-0580-002
0 1 PCA ADC Main Board Modified for FID/FPD 2-3-0700-032
0 1 Field Termination Board 2-3-0700-010
1 2 Fuses, Assortment (5 each 1A, 3A and 6A) 2-3-0700-136
0 1 Dual Methods Adapter Board 2-3-0700-011
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5+ GCs or
1-5 GCs Critical Description Part No.
Installations
0 Note3 Assembly, Power Supply 115/230 VAC - Model 700 and 2-3-0700-110
Model 1000A only
2 2 Solenoid Valve, Srs 2-4-0700-152
1/Valve 1/Valve Repair Kit, 6-port Valve - For use on Model 700 only 2-4-0700-187
1/Valve 1/Valve Repair Kit, 10-port Valve - For use on Model 700 only 2-4-0700-171
1 1 Column Set Note4
0 1 Methanator Convertor Assembly Note4
0 1 Assembly, Micro-FID Detector and Connector Board 2-3-0700-148
complete, Model(s) 700 and 1000A
1/Stream 1/Stream Filter Element 2-micron,Swagelok SS-2F-K4-2 2-4-5000-113
1/Stream 1/Stream Membrane Kit, Genie® Model 120 Filter/Bypass/LSO 2-4-5000-938
G-4
Appendix H: Engineering Drawings
H
H-1
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H-2
(2) NOTES:
LOWER ACTUATOR PLASTIC RETAINER DISK 13. 6 PORT VALVE ASSEMBLY INSTRUCTIONS
DIAPHRAGMS 10
THIS PROCEDURE TO BE PERFORMED IN A CLEAN AND DRY
LARGE AREA. ALL PARTS TO BE BLOWN CLEAN AND DRY WITH
GUIDE NITROGEN BEFORE ASSEMBLY.
3
PIN 1. ASSEMBLY IS ACCOMPLISHED IN THE UPSIDE DOWN POSITION.
10 VITON GASKET
(3) 2. PLACE ITEM 9, PRIMARY PLATE INTO SHOP ASSEMBLY FIXTURE AND
LONG INSTALL ITEM 3, LARGE DOWEL PIN AND ITEM 2, SMALL DOWEL PIN.
PISTON 4
3. PLACE ITEM 10, AMBER SEALING DIAPHRAGM ( HAVING NO ACTUATOR
2 SMALL GUIDE PIN HOLES) ALIGN LARGE AND SMALL DOWEL PIN HOLES.
(3) 10 NOMEX CUSHION DIAPHRAGM 6. PLACE ITEM 6, SHORT PISTONS IN PISTON PLATE 3 PLACES.
SHORT PISTON SHAFT MUST FALL THROUGH HOLES. DO NOT FORCE.
6
PISTONS
7. PLACE ITEM 10, AMBER UPPER ACTUATOR DIAPHRAGMS WITH
10 LARGE ACTUATOR HOLES OVER DOWEL PINS 2 PLACES. ALIGN
SEALING DIAPHRAGM WITH LARGE AND SMALL DOWEL PINS.
UPPER
PISTON 5 8. PLACE ITEM 1, LOWER PISTON PLATE OVER DOWEL PINS.
PLATE 9 PRIMARY PLATE
9. PLACE ITEM 4, LONG PISTONS IN PISTON PLATE 3 PLACES.
PISTON SHAFT MUST FALL FREELY THROUGH HOLES.
DO NOT FORCE.
7 FLAT WASHER
13. 10. PLACE ITEM 10, AMBER LOWER ACTUATOR DIAPHRAGMS WITH
SMALL ACTUATOR HOLES OVER DOWEL PINS 2 PLACES. ALIGN
WITH LARGE AND SMALL DOWEL PINS.
8 TORQUE BOLT
11. PLACE ITEM 10, BLACK VITON GASKET, OVER DOWEL PINS. ALIGN WITH
LARGE AND SMALL DOWEL PINS.
12. INSTALL ITEM 8, BOLT AND ITEM 7, FLAT WASHER UP THRU
PRIMARY PLATE. REMOVE FROM FIXTURE AND INSTALL INTO UNIT.
14. TORQUE THE BOLT (ITEM 8) TO 30 FT. LBS. WHEN THE VALVE IS
INSTALLLED ON THE ANALYZER.
SI METRIC G 08/13/10 CC ECO-XX-5005838 EM HS THIS DRAWING IN DESIGN AND DETAIL IS OUR PROPERTY AND MUST NOT BE USED EXCEPT IN CONNECTION WITH OUR
WORK. IT SHALL NOT BE REPRODUCED AND SHALL BE RETURNED TO US ON DEMAND. ALL RIGHTS ARE RESERVED.
THIRD ANGLE PROJECTION F 7-6-06 HM ECO-XX-5001969 EM NP TITLE
GEOMETRIC TOLERANCES &
E 4-2-06 HM ECO-XX-5001716 EM NP DIMENSIONS PER
ANSI Y14.5
D 2-25-05 HM ECO-XX-5000518 EM BLB LATEST REVISION ASSEMBLY
MATERIAL: C 8-3-04 HM ECO-XX-212474 EM HS RADIAL 6 PORT VALVE, KIOSK OVEN
B 6-29-04
UNLESS OTHERWISE NOTED MODEL 700 G.C.
SEE ORDER DLT ECO-XX-209763 EM DLT ALL DIMENSIONS IN INCHES
X.XX ±.015
(2)
7 LOWER ACTUATOR DIAPHRAGMS
(5)
5 LONG PISTON
LOWER
PISTON 3 .156 DIA.
PLATE 6 GUIDE PIN
14.
(2)
.093 DIA. 10
GUIDE PIN 7 UPPER ACTUATOR DIAPHRAGMS
(5)
SHORT
PISTONS 4
(2)
CUSHION 7
DIAPHRAGM
14.
SEALING 7 15.
DIAPHRAGM
1 PRIMARY PLATE
9 FLAT WASHER
8 TORQUE BOLT
SI METRIC H 08/13/10 CC ECO-XX-5005838 EM HS THIS DRAWING IN DESIGN AND DETAIL IS OUR PROPERTY AND MUST NOT BE USED EXCEPT IN CONNECTION WITH OUR
WORK. IT SHALL NOT BE REPRODUCED AND SHALL BE RETURNED TO US ON DEMAND. ALL RIGHTS ARE RESERVED.
THIRD ANGLE PROJECTION G 7-6-06 HM ECO-XX-5001969 EM NP TITLE
GEOMETRIC TOLERANCES &
F 4-2-06 HM ECO-XX-5001716 EM NP DIMENSIONS PER
FINISH:
B 11-11-03 HM ECO-XX-190965 EM BLB X.XXX
ANGULAR
±.005
±0° 30'
FINISH 200 RA MAX
REV DATE
DRN HM DATE 10/1/03 DWG NO. REV
BLOCK N/A DRN DESCRIPTION CHKD APPD
CE-20958
BREAK ALL SHARP CORNERS TO
.003-.015 RADIUS AND REMOVE
CHKD DLT DATE 10-17-03 H
PROJ. FILE NO. G-00001 FILE NAME: CE20958H1.SLDDRW, DATE: 08/13/10, TIME: 8:15 A.M. ALL BURRS APPD BLB DATE 10-17-03 SCALE
1:1 P/N 2-3-0700-118 SHT
1OF1
ITEM PART DESCRIPTION QTY. METHANATOR ASSEMBLY:
NO. NUMBER
1. INSERT & ALIGN HEATER (ITEM 7) INSIDE HEATER ADAPTER TUBE
1 2-4-0710-181 METHANATOR CASE 1 (ITEM 11).
BE-22201
METHANATOR CAP 2. CENTER & ALIGN THE HEATER ADAPTER TUBE (ITEM11) IN THE
2 2-4-0710-180 BE-22200 1 COLUMN (ITEM 5) WITH THE HEATER WIRES AT THE SHORT END
OF THE COLUMN.
3 2-4-9214-016 RETAINING RING 1
WH_275 (2) 3. SLIDE INSULATOR (ITEM12) THRU THE HEATER WIRES TO FLUSH WITH HEATER
AS SHOWN IN VIEW A-A
4 2-4-9326-911 BUSHING, 1 10
NIAGARA SB437-5 4. CENTER & ALIGN HEATER (ITEM 7) & INSULATOR (ITEM12), FROM ABOVE
ALONG WITH HEATER ADAPTER TUBE (ITEM11) & COLUMN ASSEMBLY (ITEM
5 2-4-0700-207 COLUMN, METH 1 5)IN THE ISOLATOR METHANATOR WITH THE HEATER WIRES AT THE END
BE-21339 WITH THE RTD HOLE. BEND THE LONG TUBE UNTIL IT IS PARALLEL WITH THE
ISOLATOR, METHANATOR TWO COLUMN TUBES SHORT TUBE AND THE ENDS ARE AROUND THE SAME HEIGHT.
6 2-4-0700-208 BE-21340 1
3 5. INSTALL THE RTD (ITEM 8) IN THE HOLE IN THE METHANATOR ISOLATOR.
HEATER, 24V, 35W ENSURING THE RTD WIRES HAVE SLACK, ANCHOR THEM TO THE
7 ( 3/8 "X 1.5 "L)
2-4-0700-224 SC37-1.5/35W/24V/SF1-32 1
HEATER WIRE WITH HIGH TEMPERATURE TAPE WITHIN AN INCH OF
THE HEATER. SLIGHTLY FILL BETWEEN HEATER & COLUMN WITH MILK
MAGNESIA TO MAXIMIZE HEAT CONDUCTION.
VIEW B-B 6. CENTER & ALIGN THE BOTTOM INSULATION FROM INSULATION KIT (ITEM 9)
8 2-4-0700-225 RTD, MINCO S72PD20Y36 1 2
INSULATION KIT INSIDE AND TO THE BASE OF METHANATOR CASE (ITEM1)
SWAGELOK UNION 1 8. PLACE TOP INSULATION FROM INSULATION KIT (ITEM9)FROM ABOVE & ON
10 2-4-9500-004 2 THE METHANATOR ASSEMBLY
SS-1F0-6GC
11 2-4-0700-297 HEATER ADAPTER TUBE 1 VIEW A-A 9. PACK INSULATION AROUND THE WIRES AND TUBES, AND CLEAN
TOP INSULATION (2) INSULATION MATERIAL AWAY FROM INSIDE MATING AREA OF THE CASE.
HEATER WIRE INSULATOR HEATER 7
12 2-4-0710-290 1 10. INSTALL THE THREAD BUSHING (ITEM 4) INTO THE HOLE IN THE
BE-22656 CAP (ITEM 2).
TUBE 11 12 HEATER WIRE INSULATOR
11. PUSH THE WIRES AND TUBES THROUGH THE THREAD BUSHING.
CAREFULLY ALIGN THE CAP WITH THE BORE OF THE CASE AND
12 PRESS INTO PLACE.
12. INSTALL THE RETAINING RING (ITEM 3) INTO THE GROOVE IN THE
CASE OPENING.
SLIDE INSULATOR THRU
HEATER WIRE, RTD
TILL FLUSH WITH HEATER 8
6 ISOLATOR
9
5 COLUMN
CENTER INSULATION
VIEW B-B
INSULATION KIT
7 7
THIS DRAWING IN DESIGN AND DETAIL IS OUR PROPERTY AND MUST NOT BE USED EXCEPT IN CONNECTION WITH OUR
WORK. IT SHALL NOT BE REPRODUCED AND SHALL BE RETURNED TO US ON DEMAND. ALL RIGHTS ARE RESERVED.
THIRD ANGLE PROJECTION TITLE
GEOMETRIC TOLERANCES &
VIEW A-A
DIMENSIONS PER
ANSI Y14.5
LATEST REVISION
ASSEMBLY
MATERIAL: C 11-25-10 JDB ECO-XX-5005915 ADS NP METHANATOR
SEE BOM B 09-28 -10 JDB ECO-XX-5005936 ADS NP
UNLESS OTHERWISE NOTED
ALL DIMENSIONS IN INCHES 700 & 700XA GC
X.XX ±.010
FINISH:
A 6-13 -08 HM ECO-XX-5003758 DM BLB X.XXX
ANGULAR
±.005
±0° 30'
FINISH 200 RA MAX
N/A REV DATE DRN MANCHA DATE 03/28/08 DWG NO. REV
DRN DESCRIPTION CHKD APPD
CE-22210
BREAK ALL SHARP CORNERS TO
.003-.015 RADIUS AND REMOVE
CHKD DM DATE 06/13/08 C
PROJ. FILE NO. - NONE FILE NAME: CE22210C1.SLDDRW, DATE: 11-25-10, TIME: 12:40 P.M. ALL BURRS ENG
BLB DATE
06/13/08
SCALE
3:4 P/N
2-3-0710-073 SHT
1 OF 1
WARRANTY CLAIM PROCEDURES
4. When contacting DMS for product service, the Purchaser is asked to provide
information as indicated on the following page entitled “Customer Repair
Report”.
5. For product returns from locations outside the United States, it will be
necessary for you to obtain the import consignment address so that DMS's
customs broker can handle the importation with the U.S. Customs Service.
6. DMS offers both on call and contract maintenance service designed to afford
single source responsibility for all its products.
7. DMS reserves the right to make changes at any time to any product to
improve its design and to insure the best available product.
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CUSTOMER REPAIR REPORT
FOR SERVICE, COMPLETE THIS FORM, AND RETURN IT ALONG WITH THE AFFECTED EQUIPMENT
TO CUSTOMER SERVICE AT THE ADDRESS INDICATED BELOW.
_____________________________________________________________________________________________
_____________________________________________________________________________________________
_____________________________________________________________________________________________
_____________________________________________________________________________________________
DESCRIPTION OF PROBLEM:___________________________________________________________________
_____________________________________________________________________________________________
_____________________________________________________________________________________________
_____________________________________________________________________________________________
_____________________________________________________________________________________________
_____________________________________________________________________________________________
IF YOU REQUIRE TECHNICAL ASSISTANCE, PLEASE FAX OR WRITE THE CUSTOMER SERVICE
DEPARTMENT AT:
FOR FASTEST SERVICE CONTACT DANIEL MEASUREMENT SERVICES VIA OUR WEBSITE:
www.emersonprocess.com/daniel
This page is intentionally left blank.
This page is intentionally left blank.
www.RosemountAnalytical.com
www.Danalyzer.com
The Emerson logo is a trademark and service mark of Emerson Electric Co. Rosemount Analytical and Danalyzer are
marks of one of the Emerson Process Management family of companies. All other marks are the property of their
respective owners.
The contents of this publication are presented for information purposes only, and while effort has been made to
ensure their accuracy, they are not to be construed as warranties or guarantees, express or implied, regarding the
products or services described herein or their use or applicability. All sales are governed by our terms and
conditions, which are available on request. We reserve the right to modify or improve the designs or specifications
of our products at any time without notice.