0% found this document useful (0 votes)
270 views

1.1 CV Analyser - Manual

Uploaded by

GIRI
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
0% found this document useful (0 votes)
270 views

1.1 CV Analyser - Manual

Uploaded by

GIRI
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 346

Revision P

3-9000-521
April 2012

Model 700 Gas Chromatograph


System Reference Manual

Applies to the Rosemount® Analytical Model 700 and


the Danalyzer™ Model 700
NOTICE

ROSEMOUNT ANALYTICAL, INC. AND DANIEL MEASUREMENT AND CONTROL, INC. (COLLECTIVELY,
“SELLER”) SHALL NOT BE LIABLE FOR TECHNICAL OR EDITORIAL ERRORS IN THIS MANUAL OR OMISSIONS
FROM THIS MANUAL. SELLER MAKES NO WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING THE IMPLIED
WARRANTIES OF MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE WITH RESPECT TO THIS
MANUAL AND, IN NO EVENT, SHALL SELLER BE LIABLE FOR ANY SPECIAL OR CONSEQUENTIAL DAMAGES
INCLUDING, BUT NOT LIMITED TO, LOSS OF PRODUCTION, LOSS OF PROFITS, ETC.

PRODUCT NAMES USED HEREIN ARE FOR MANUFACTURER OR SUPPLIER IDENTIFICATION ONLY AND MAY
BE TRADEMARKS/REGISTERED TRADEMARKS OF THESE COMPANIES.

THE CONTENTS OF THIS PUBLICATION ARE PRESENTED FOR INFORMATIONAL PURPOSES ONLY, AND
WHILE EVERY EFFORT HAS BEEN MADE TO ENSURE THEIR ACCURACY, THEY ARE NOT TO BE CONSTRUED
AS WARRANTIES OR GUARANTEES, EXPRESSED OR IMPLIED, REGARDING THE PRODUCTS OR SERVICES
DESCRIBED HEREIN OR THEIR USE OR APPLICABILITY. WE RESERVE THE RIGHT TO MODIFY OR IMPROVE
THE DESIGNS OR SPECIFICATIONS OF SUCH PRODUCTS AT ANY TIME.

SELLER DOES NOT ASSUME RESPONSIBILITY FOR THE SELECTION, USE OR MAINTENANCE OF ANY
PRODUCT. RESPONSIBILITY FOR PROPER SELECTION, USE AND MAINTENANCE OF ANY SELLER PRODUCT
REMAINS SOLELY WITH THE PURCHASER AND END-USER.

DANIEL AND THE DANIEL LOGO ARE REGISTERED TRADEMARKS OF DANIEL MEASUREMENT AND
CONTROL, INC. ROSEMOUNT AND THE ROSEMOUNT ANALYTICAL LOGO ARE REGISTERED TRADEMARKS
OF ROSEMOUNT ANALYTICAL. THE EMERSON LOGO IS A TRADEMARK AND SERVICE MARK OF EMERSON
ELECTRIC CO.

©2012

ROSEMOUNT ANALYTICAL, INC.

DANIEL MEASUREMENT AND CONTROL, INC.

HOUSTON, TX

USA

All rights reserved. No part of this work may be reproduced or copied in any form or by any means–graphic,
electronic, or mechanical–without first receiving the written permission of Rosemount Analytical Inc. or Daniel
Measurement and Control, Inc., Houston, Texas, U.S.A.
WARRANTY

1. LIMITED WARRANTY: Subject to the limitations contained in Section 2 herein and except as otherwise
expressly provided herein, Rosemount Analytical and Daniel Measurement and Control, Inc., (collectively
“Seller”) warrants that the firmware will execute the programming instructions provided by Seller, and that
the Goods manufactured or Services provided by Seller will be free from defects in materials or
workmanship under normal use and care until the expiration of the applicable warranty period. Goods are
warranted for twelve (12) months from the date of initial installation or eighteen (18) months from the
date of shipment by Seller, whichever period expires first. Consumables and Services are warranted for a
period of 90 days from the date of shipment or completion of the Services. Products purchased by Seller
from a third party for resale to Buyer (“Resale Products”) shall carry only the warranty extended by the
original manufacturer. Buyer agrees that Seller has no liability for Resale Products beyond making a
reasonable commercial effort to arrange for procurement and shipping of the Resale Products. If Buyer
discovers any warranty defects and notifies Seller thereof in writing during the applicable warranty period,
Seller shall, at its option, promptly correct any errors that are found by Seller in the firmware or Services, or
repair or replace F.O.B. point of manufacture that portion of the Goods or firmware found by Seller to be
defective, or refund the purchase price of the defective portion of the Goods/Services. All replacements or
repairs necessitated by inadequate maintenance, normal wear and usage, unsuitable power sources,
unsuitable environmental conditions, accident, misuse, improper installation, modification, repair, storage
or handling, or any other cause not the fault of Seller are not covered by this limited warranty, and shall be
at Buyer's expense. Seller shall not be obligated to pay any costs or charges incurred by Buyer or any other
party except as may be agreed upon in writing in advance by an authorized Seller representative. All costs
of dismantling, reinstallation and freight and the time and expenses of Seller's personnel for site travel and
diagnosis under this warranty clause shall be borne by Buyer unless accepted in writing by Seller. Goods
repaired and parts replaced during the warranty period shall be in warranty for the remainder of the
original warranty period or ninety (90) days, whichever is longer. This limited warranty is the only warranty
made by Seller and can be amended only in a writing signed by an authorized representative of Seller.
Except as otherwise expressly provided in the Agreement, THERE ARE NO REPRESENTATIONS OR
WARRANTIES OF ANY KIND, EXPRESSED OR IMPLIED, AS TO MERCHANTABILITY, FITNESS FOR PARTICULAR
PURPOSE, OR ANY OTHER MATTER WITH RESPECT TO ANY OF THE GOODS OR SERVICES. It is understood
that corrosion or erosion of materials is not covered by our guarantee.

2. LIMITATION OF REMEDY AND LIABILITY: SELLER SHALL NOT BE LIABLE FOR DAMAGES CAUSED BY DELAY
IN PERFORMANCE. THE SOLE AND EXCLUSIVE REMEDY FOR BREACH OF WARRANTY HEREUNDER SHALL BE
LIMITED TO REPAIR, CORRECTION, REPLACEMENT OR REFUND OF PURCHASE PRICE UNDER THE LIMITED
WARRANTY CLAUSE IN SECTION 1 HEREIN. IN NO EVENT, REGARDLESS OF THE FORM OF THE CLAIM OR
CAUSE OF ACTION (WHETHER BASED IN CONTRACT, INFRINGEMENT, NEGLIGENCE, STRICT LIABILITY,
OTHER TORT OR OTHERWISE), SHALL SELLER'S LIABILITY TO BUYER AND/OR ITS CUSTOMERS EXCEED THE
PRICE TO BUYER OF THE SPECIFIC GOODS MANUFACTURED OR SERVICES PROVIDED BY SELLER GIVING
RISE TO THE CLAIM OR CAUSE OF ACTION. BUYER AGREES THAT IN NO EVENT SHALL SELLER'S LIABILITY TO
BUYER AND/OR ITS CUSTOMERS EXTEND TO INCLUDE INCIDENTAL, CONSEQUENTIAL OR PUNITIVE
DAMAGES. THE TERM “CONSEQUENTIAL DAMAGES” SHALL INCLUDE, BUT NOT BE LIMITED TO, LOSS OF
ANTICIPATED PROFITS, LOSS OF USE, LOSS OF REVENUE AND COST OF CAPITAL.
IMPORTANT INSTRUCTIONS

• Read all instructions prior to installing, operating, and servicing this product.

• Follow all warnings, cautions, and instructions marked on and supplied with this
product.

• Inspect the equipment packing case and if damage exists, notify your local carrier
for liability.

• Open the packing list and carefully remove equipment and spare or replacement
parts from the case. Inspect all equipment for damage and missing parts.

• If items are damaged or missing, contact the manufacturer at 1-888-801-1452


for instructions about receiving replacement parts.

• Install equipment as specified per the installation instructions and per applicable
local and national codes. All connections shall be made to proper electrical and
pressure sources.

• Ensure that all equipment doors are closed and protective covers are in place,
except when maintenance is being performed by qualified persons, to prevent
personal injury.

• Use of this product for any purpose other than its intended purpose may result in
property damage and/or serious injury or death.

• Before opening the flameproof enclosure in a flammable atmosphere, the


electrical circuits must be interrupted.

• Repairs must be performed using only authorized replacement parts as specified


by the manufacturer. Use of unauthorized parts can affect the product's
performance and place the safe operation of the product at risk.

• When installing or servicing ATEX-certified units, the ATEX approval applies only
to equipment without cable glands. When mounting the flameproof enclosures in
a hazardous area, only flameproof cable glands certified to IEC 60079-1 must be
used.

• Technical assistance is available 24 hours a day, 7 days a week by calling 1-888-


801-1452.
This page is intentionally left blank.
TA B L E O F C O N T E N T S

Section 1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1


Description of manual . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1
System description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1
Analyzer assembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2
Controller assembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-5
Sample conditioning system (SCS) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-8
Functional description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-8
Available functions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-10
Software description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-11
BOS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-12
MON2000 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-12
Theory of operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-13
Thermal conductivity detector (TCD) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-13
Flame ionization detector (FID) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-16
LSIV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-17
Methanator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-18
Data acquisition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-19
Peak detection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-20
Basic analysis computations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-22
Concentration analysis - response factor . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-22
Concentration calculation - mole percentage (without normalization) . . .1-24
Concentration calculation in mole percentage (with normalization) . . . .1-24
Additional Resources . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-25
Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-25

Section 2 Equipment description and specifications . . . . . . . . . . . . 2-1


Equipment description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
Upper enclosure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-2
Lower Enclosure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-7
Flow Panel Assembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-8
Equipment Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-9
Utilities . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-9
Electronic Hardware . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-11
Micro Heat Sink Oven . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-16
Software . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-17

i
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Section 3 Installation and setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3-1


Precautions and warnings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-1
Hazardous environments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-2
Power source wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-3
Card cage removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-4
Signal wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-10
Electrical and signal ground . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-11
Electrical conduit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-13
Sample system requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-14
Preparation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-16
Site selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-16
Unpacking the unit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-17
Model 700 installation arrangements . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-18
Wall mount . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-18
Pole mount . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-18
Floor mount . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-19
Required Tools and Components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-19
Supporting tools and components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-20
Model 700 installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-21
DC power supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-21
Optional AC — DC power converter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-24
Sample and Gas Lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-26
Setting the Com ID . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-30
Inspect or change the Com ID . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-31
Preparing for serial connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-34
FTB connection (RS-232) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-37
PC to GC cable short distance connection (RS-232) . . . . . . . . . . . . . . . . 3-37
Long distance connection (RS-422, RS-485) . . . . . . . . . . . . . . . . . . . . . . 3-45
GC-Printer wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-46
Discrete digital I/O wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-47
Discrete digital inputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-48
Discrete digital outputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-50
Analog input wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-51
Analog output wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-51
Optional boards . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-53
Optional WinSystems Modem . . . . . . . . . . . . . . . . . . . . . . . . . . 3-53
Optional Radicom Modem Settings . . . . . . . . . . . . . . . . . . . . . . 3-54
Leak checks and purging for
first calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-55
Initial leak check . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-55
Carrier gas line leak checks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-55
Calibration line leak check . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-56
Sample lines (streams) leak check . . . . . . . . . . . . . . . . . . . . . . . 3-57
Purging carrier gas lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-57
Purging calibration gas lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-58
System startup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-59

ii
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Section 4 Maintenance and troubleshooting . . . . . . . . . . . . . . . . . . 4-1


Hazardous environments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-1
Troubleshooting and repair concept . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2
Routine maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2
Bimonthly maintenance checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2
Routine maintenance procedures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-4
Contact service . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-4
Access to GC equipment elements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-4
Electrical/electronic components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-4
Detector elements, heater elements, valves and columns . . . . . . . . . . . 4-6
Precautions for handling pc assemblies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-9
General troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-9
Hardware Alarms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-10
Troubleshooting checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-12
Test points dual methods board and FTB . . . . . . . . . . . . . . . . . . . . . . . . .4-17
Preamplifier . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-20
Flow balance check . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-20
Temperature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-20
FID configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-22
Baseline noise . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-23
Leak checks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-26
Field service . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-26
Factory level leak check . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-27
Plugged Lines, Columns, or Valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-29
Required tools . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-30
Chromatograph valve replacement parts . . . . . . . . . . . . . . . . . . . . . . . . .4-31
Valve Assembly and Disassembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-31
Valve Cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-34
TCD Oven System Removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-35
Micro-FID removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-38
Micro-FID maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-40
Micro-FID re-assembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-41
LSIV maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-42
LSIV removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-43
Replacing LSIV seals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-43
LSIV Disassembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-44
Methanator maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-45
Valve overhaul . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-47
Oven system and stream switching system solenoid valve
replacement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-50
Solenoid valve replacement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-50
TCD detector bridge balance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-53
Measure vent flow . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-55
Model 700 electrical components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-56
DC power supply replacement procedures . . . . . . . . . . . . . . . . . . . . . . .4-59
Communications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4-60

iii
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Model 700 GC with the TCD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-60


Model 700 GC with the FID and TCD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-61
Analog inputs and outputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-63
Model 700 analog inputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-64
Analog output adjustment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-64
Model 700 analog outputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-65
Discrete digital inputs and outputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-67
Recommended spare parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-68
Upgrade procedures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-69
Base operating system . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-69
Applications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-70

Appendix A Communications specifications. . . . . . . . . . . . . . . . . . . . . A-1

TCD serial communications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-1


Model 700 with a TCD communications port . . . . . . . . . . . . . . . . . . . . . . A-2
FID serial communications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-5
Connecting serial communications to the GC . . . . . . . . . . . . . . . . . . . . . . A-8
RS-232 ports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-9
RS-422 ports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-10
RS-485 serial specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-10
FTB serial communications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-10
Jumper Settings for Older WinSystems CPU Boards (P/N#2-3-
0700-028) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-14
WinSystems MCM/LPM — Com4A board . . . . . . . . . . . . . . . . . . A-17
Com4A board compatibility settings . . . . . . . . . . . . . . . . . . . . . A-19
WinSystems Ethernet board . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-20
Radicom 56K baud modem board . . . . . . . . . . . . . . . . . . . . . . . A-21
Wiring local RS-232 communications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-21
GC serial port and cable configurations . . . . . . . . . . . . . . . . . . . . . . . . . . A-21
GC DB 9-pin serial port to PC DB 9-pin port . . . . . . . . . . . . . . . . . . . . . . . A-25
GC DB 9-pin serial port to PC DB 25-pin port . . . . . . . . . . . . . . . . . . . . . . A-25
GC Phoenix plug port to PC DB 9-pin port . . . . . . . . . . . . . . . . . . . . . . . . A-26
GC Phoenix plug port to PC DB 25-pin port . . . . . . . . . . . . . . . . . . . . . . . A-27
Wiring remote RS-232 communications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-28
GC DB 9-pin serial port to modem DB 25-pin port . . . . . . . . . . . . . . . . . A-28
GC Phoenix plug to modem DB 25-pin port . . . . . . . . . . . . . . . . . . . . . . . A-29

iv
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Example RS-422 PC-GC connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .A-30


Example RS-485 PC-GC connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .A-32

Appendix B Modem installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-1

Optional internal modem . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-1


Optional Ethernet board . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-3

Appendix C Manifold Carrier for Gas Bottles . . . . . . . . . . . . . . . . . . . . . C-1

Carrier Gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . C-1


Installation and line purging . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . C-2
Replacing a carrier cylinder . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . C-4
Calibration gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . C-4

Appendix D Local operator interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-1

Interface components for displaying and entering data . . . . . . . . . . . . . . . . . . . . .D-1


Light emitting diode indicators . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-2
LCD screen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-2
Keypad . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-2
The command keys . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-3
The arrow keys . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-3
Pressing a key . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-3
Using the local operator interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-4
Start up . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-4
Navigating menus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-5
Navigating the screen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-5
Editing numeric fields . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-7
Editing non-numeric fields . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-9
Editing alphanumeric fields . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-9
Selecting check boxes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-9
Clicking buttons . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-9
Selecting radio buttons . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-10
Selecting an item from a list box . . . . . . . . . . . . . . . . . . . . . . . . D-10
Selecting an item from a combo box . . . . . . . . . . . . . . . . . . . . D-11
Entering a date and time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-11
Setting the time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-12
Screen navigation and interaction tutorial . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-13
The LOI screens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-23
The Chromatogram menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-25
The Hardware menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-33
The Application menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-39
The Logs/Reports menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-45
The Control menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-50
The Manage menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-57

v
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Troubleshooting a blank LOI screen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-60

Appendix E LX-800 CPU Board Retrofit Instructions . . . . . . . . . . . . . . .E-1

Introduction to the LX-800 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-2


Upgrading your 16-bit application to its 32-bit equivalent . . . . . . . . . . . . . . . . . . E-4
Choosing the appropriate 32-bit application . . . . . . . . . . . . . . . . . . . . . . E-4
Upgrading to the 32-bit application . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-6
Installing the new CPU board . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-8

Appendix F Shipping and long-term storage recommendations. . . . F-1

Appendix G Recommended spare parts . . . . . . . . . . . . . . . . . . . . . . . . . G-1

Appendix H Engineering Drawings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . H-1

List of Engineering Drawings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . H-1

vi
LIST OF FIGURES

Figure 1-5. Analyzer assembly with tcd detector bridge ..................................................1-14


Figure 1-6. Detector output during component elution ..................................................1-15
Figure 1-7. Analyzer assembly with Micro-FID detector bridge ........................................1-16
Figure 1-8. Model 700 LSIV assembly ..............................................................................1-17
Figure 1-9. Model 700 Methanator Assembly ..................................................................1-19
Figure 2-1. Model 700 Gas Chromatograph ......................................................................2-1
Figure 2-3. TCD Oven System Assembly ............................................................................2-3
Figure 2-4. Model 700 Micro-FID upper assembly..............................................................2-4
Figure 2-5. Model 700 Methanator Upper Assembly .........................................................2-4
Figure 2-6. LSIV Assembly .................................................................................................2-5
Figure 2-7. SSS Installed ....................................................................................................2-6
Figure 2-8. Upper Electronics with TCD Block Diagram....................................................2-11
Figure 2-10. Lower Electronics TCD Block Diagram ...........................................................2-13
Figure 3-1. Lower enclosure disassembly ..........................................................................3-5
Figure 3-2. Card cage cable disassembly ...........................................................................3-6
Figure 3-3. Card cage assembly screw locations ................................................................3-7
Figure 3-4. Card cage disassembly ....................................................................................3-8
Figure 3-5. Card cage disassembly for power and signal wiring .........................................3-9
Figure 3-7. Stream Inlets (Right side of unit)....................................................................3-15
Figure 3-8. 24 VDC power connection.............................................................................3-22
Figure 3-9. 24 VDC power inlet .......................................................................................3-23
Figure 3-10. AC/DC Power Converter ................................................................................3-24
Figure 3-11. Model 700 Upper Enclosure...........................................................................3-26
Figure 3-12. Carrier gas inlet left-side upper enclosure......................................................3-27
Figure 3-13. Calibration gas stream inlet (right side of unit) ..............................................3-29
Figure 3-14. Sample stream inlets (Right side of unit)........................................................3-30
Figure 3-15. Dip switch .....................................................................................................3-31

ix
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-16. Oven Mounting Bracket.................................................................................3-32


Figure 3-17. Multifunction Board Location ........................................................................3-32
Figure 3-18. Dip Switch .....................................................................................................3-33
Figure 3-19. Serial port jacks .............................................................................................3-35
Figure 3-20. Field termination board .................................................................................3-38
Figure 3-21. Configuration without Com4A Board ............................................................3-39
Figure 3-22. Configuration with Com4A Board..................................................................3-40
Figure 3-23. FTB Com1 and Com2 DB 9-pin Connector .....................................................3-41
Figure 3-24. FTB Com 1 DB 9-pin Phoenix Connector ........................................................3-42
Figure 3-25. FTB Com2 DB 9-pin Phoenix Connector .........................................................3-42
Figure 3-26. FTB Com5 DB 9-pin Phoenix Connector .........................................................3-43
Figure 3-27. FTB Com6 DB 9-pin Phoenix Connector .........................................................3-43
Figure 3-28. FTB Com7 DB 9-pin Phoenix Connector .........................................................3-44
Figure 3-29. Com8 DB 9-pin Phoenix Connector GC Phoenix Plug Port ..............................3-44
Figure 3-30. GC Phoenix Plug Port to External Modem DB 25-pin Port...............................3-45
Figure 3-31. Field termination board .................................................................................3-49
Figure 4-1. Model 700 with TCD/Micro-FID Front View......................................................4-5
Figure 4-2. Upper Explosion-proof Housing.......................................................................4-7
Figure 4-3. Thermal Conductivity Detector .......................................................................4-8
Figure 4-4. Flame Ionization Detector ...............................................................................4-8
Figure 4-5. Test Points Dual Methods Board (Cut View)...................................................4-18
Figure 4-6. Test Points Dual Methods Board ....................................................................4-18
Figure 4-7. Test Points Field Termination Board (Cut View) .............................................4-19
Figure 4-8. Test Points Field Termination Board ..............................................................4-19
Figure 4-9. Temperature Control Dialog..........................................................................4-21
Figure 4-10. FID Configuration window .............................................................................4-22
Figure 4-14. Disassembled valve .......................................................................................4-32
Figure 4-16. Micro-FID Oven System Thermal Cover .........................................................4-36
Figure 4-18. TCD Oven System Disassembly .....................................................................4-38
Figure 4-20. Model 700 with Micro-FID Upper Assembly ...................................................4-40
Figure 4-21. Upper Enclosure Thermal Cover ....................................................................4-42
Figure 4-22. Model 700 with LSIV ......................................................................................4-44

x
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-23. MON2020 Software for Gas Chromatographs Optional Methanator


Assembly.......................................................................................................4-46
Figure 4-24. TCD Valve Tubing and Fittings .......................................................................4-48
Figure 4-25. Side view TCD oven system mounting bracket ..............................................4-51
Figure 4-26. Rotated TCD upper assembly ........................................................................4-52
Figure 4-27. Stream Switching Assembly ..........................................................................4-52
Figure 4-28. Stream Switching System Final Assembly ......................................................4-53
Figure 4-29. Model 700 Micro-FID/TCD Preamplifier .........................................................4-54
Figure 4-30. Model 700 TCD Bridge Balance......................................................................4-54
Figure 4-31. Model 700 Micro-FID Bridge Balance .............................................................4-55
Figure 4-33. Model 700 lower enclosure ...........................................................................4-57
Figure 4-34. Model 700 Lower Assembly ...........................................................................4-58
Figure 4-35. DC Power Supply Lower Enclosure.................................................................4-59
Figure 4-36. Dip Switch .....................................................................................................4-61
Figure 4-37. Multifunction board ......................................................................................4-62
Figure 4-38. Analog Inputs ................................................................................................4-64
Figure 4-40. Analog Outputs .............................................................................................4-66
Figure 4-41. Optional analog board outputs......................................................................4-67
Figure A-1 Standard configuration without Com4A Board or FID ..................................... A-3
Figure A-2 Configuration with Com4A Board................................................................... A-4
Figure A-3 FTB Com1 and Com2 DB9 connector.............................................................. A-5
Figure A-4 Configuration without Com4A board ............................................................. A-7
Figure A-5 Configuration with Com4A board................................................................... A-8
Figure A-6 FTB Com1 DB 9-pin Phoenix Connector ........................................................ A-11
Figure A-7 FTB Com2 DB 9-pin Phoenix Connector ....................................................... A-11
Figure A-8 FTB Com5 DB 9-pin Phoenix Connector ........................................................ A-12
Figure A-9 FTB Com6 DB 9-pin Phoenix Connector ....................................................... A-12
Figure A-10 FTB Com7 DB 9-pin Phoenix Connector ........................................................ A-13
Figure A-11 FTB Com8 DB 9-pin Phoenix Connector ........................................................ A-13
Figure A-12 FTB Serial Connections ................................................................................. A-22
Figure A-14 Phoenix Connector (J5, J6, J10, and J11) Pinout............................................. A-23

xi
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure A-15 DB 9-pin connector (P2 and P3) and pinout for jacks..................................... A-24
Figure A-17 GC DB 9-pin Port to PC DB 25-pin Port .......................................................... A-26
Figure A-18 GC DB 9-pin Port to PC DB 25-pin Port .......................................................... A-27
Figure A-19 GC Phoenix Plug Port to PC DB 25-pin Port ................................................... A-28
Figure A-21 GC Phoenix Plug Port to External Modem DB 25-pin Port.............................. A-30
Figure A-22 Example RS-422 Serial Cable Terminations ................................................... A-31
Figure A-23 Example RS-485 Serial Cable Terminations, Line Driver to GC
Controller Com3 .......................................................................................... A-33
Figure A-24 Example RS-485 Serial Cable Terminations, Line Driver to GC
Controller Com4........................................................................................... A-34
Figure C-1 Manifold for two carrier gas bottles to GC system........................................... C-2
Figure D-2. Selecting a check box ..................................................................................... D-9
Figure D-3. Selecting a list box........................................................................................ D-10
Figure D-4. Selecting a combo box ................................................................................. D-11
Figure D-5. Entering a date and time .............................................................................. D-12
Figure D-6. Navigate to the Application menu ................................................................ D-14
Figure D-7. The System screen ....................................................................................... D-15
Figure D-8. You must log in to the GC before editing a screen ........................................ D-16
Figure D-9. The Enter the data dialog allows you to edit the selected field ...................... D-17
Figure D-10. The field now holds new data ....................................................................... D-18
Figure D-11. The Is Multi User Write Enabled? check box .................................................. D-19
Figure D-12. The Is Multi User Write Enabled? check box, no longer checked.................... D-20
Figure D-13. The GC Mode field ........................................................................................ D-21
Figure D-14. The Select an Item combo box...................................................................... D-22
Figure D-15. The Chromatogram menu............................................................................ D-26
Figure D-16. The Chromatogram Settings screen ............................................................. D-26
Figure D-17. The Live Chromatogram View (Status Mode) screen..................................... D-27
Figure D-18. The Live Chromatogram View (Advanced Mode) screen ............................... D-28
Figure D-19. The Archived Chromatogram (Advanced Mode) screen................................ D-29
Figure D-20. The Live & Archived Chromatogram Viewer Options screen ......................... D-29
Figure D-21. The CGM Scaling screen ............................................................................... D-30

xii
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-22. The Chromatogram CDT Table screen .......................................................... D-31


Figure D-23. The Chromatogram TEV Table screen........................................................... D-32
Figure D-24. The Chromatogram Raw Data Table screen .................................................. D-32
Figure D-25. The Hardware menu..................................................................................... D-33
Figure D-26. The Heaters screen....................................................................................... D-34
Figure D-27. The Valves screen ......................................................................................... D-35
Figure D-28. The EPC screen ............................................................................................. D-36
Figure D-29. The Detectors screen.................................................................................... D-36
Figure D-30. The Discrete Inputs screen ........................................................................... D-37
Figure D-31. The Discrete Outputs screen ........................................................................ D-37
Figure D-32. The Analog Inputs screen ............................................................................. D-38
Figure D-33. The Analog Outputs screen .......................................................................... D-38
Figure D-34. The Installed Hardware screen...................................................................... D-39
Figure D-35. The Application menu .................................................................................. D-40
Figure D-36. The System screen........................................................................................ D-40
Figure D-37. The CDT screen ............................................................................................ D-41
Figure D-38. The TEV - Valve Events screen....................................................................... D-41
Figure D-39. The TEV - Integration Events screen.............................................................. D-42
Figure D-40. The TEV - Spectrum Gain Events screen ........................................................ D-42
Figure D-41. The TEV - Analysis Time screen ..................................................................... D-43
Figure D-42. The Streams screen ...................................................................................... D-43
Figure D-43. The Status screen ......................................................................................... D-44
Figure D-44. The Ethernet Ports screen............................................................................. D-44
Figure D-45. The Logs/Reports menu ............................................................................... D-45
Figure D-46. The Maintenance Log screen ........................................................................ D-46
Figure D-47. The Event Log screen.................................................................................... D-47
Figure D-48. The Alarm Log screen ................................................................................... D-48
Figure D-49. The Unack Alarms screen.............................................................................. D-48
Figure D-50. The Active Alarms screen.............................................................................. D-49
Figure D-51. The Report Display screen ............................................................................ D-50

xiii
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-52. The Control menu ........................................................................................ D-51


Figure D-53. The Auto Sequence screen ........................................................................... D-52
Figure D-54. The Single Stream screen ............................................................................. D-53
Figure D-55. The Halt screen ............................................................................................ D-54
Figure D-56. The Calibration screen.................................................................................. D-55
Figure D-57. The Validation screen ................................................................................... D-56
Figure D-58. The Stop Now screen.................................................................................... D-56
Figure D-59. The Manage menu........................................................................................ D-57
Figure D-60. The LOI Settings screen ................................................................................ D-58
Figure D-61. The Create PIN screen................................................................................... D-59
Figure D-62. The Diagnostic screen .................................................................................. D-60
Figure E-1 Contents of the retrofitting kit ........................................................................ E-1
Figure E-3 CPU board serial number ................................................................................. E-3
Figure E-4. The System window ........................................................................................ E-5

xiv
LIST OF TABLES

Table 3-1. Modbus slave address (COM ID) dip switch settings ......................................3-34
Table 3-2. Switch positions for cold start........................................................................3-34
Table 3-3. FTB discrete digital inputs..............................................................................3-49
Table 3-4. FTB discrete digital outputs ...........................................................................3-50
Table 3-5. FTB analog inputs ..........................................................................................3-51
Table 3-6. FTB analog outputs........................................................................................3-51
Table 3-7. Optional analog outputs................................................................................3-52
Table 3-8. J8 Modem Board Jumper Settings ..................................................................3-53
Table 3-9. J9 Modem Board Jumper Settings ..................................................................3-53
Table 3-10. J10 Modem Board Jumper Settings ................................................................3-54
Table 3-11. J26 Radicom Modem Jumper Settings ...........................................................3-54
Table 3-12. J27Radicom Modem Jumper Settings ............................................................3-54
Table 3-13. J30 Radicom Modem Jumper Settings ...........................................................3-54
Table 3-14. J31 Radicom Modem Jumper Settings ...........................................................3-55
Table 4-1. Basic Hardware Troubleshooting via Alarms ..................................................4-10
Table 4-2. Troubleshooting Checklist.............................................................................4-13
Table 4-3. Temperature Control Dialog..........................................................................4-21
Table A-1 Matrix of possible TCD configurations field termination board ....................... A-1
Table A-2 Matrix of possible FID configurations field termination board ......................... A-6
Table A-3 Communication with WinSystems CPU ........................................................ A-14
Table A-4 Communication with WinSystems CPU ........................................................ A-15
Table A-5 Communication with WinSystems CPU ........................................................ A-15
Table A-6 Communication with WinSystems CPU ........................................................ A-16
Table A-7 Communication with WinSystems
MCM/LPM — Com4A Board (Optional) .......................................................... A-17
Table A-8 J10 Jumper Settings ...................................................................................... A-19
Table A-9 J7 Jumper Settings ........................................................................................ A-19

xiii
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table A-10 J8 Jumper Settings ........................................................................................ A-20


Table A-11 J9 Jumper Settings ........................................................................................ A-20
Table A-12 Ethernet Board Pin Settings .......................................................................... A-20
Table A-13 J26 Radicom Modem Jumper Settings .......................................................... A-21
Table A-14 J27 Radicom Modem Jumper Settings .......................................................... A-21
Table A-15 J30 Radicom Modem Jumper Settings .......................................................... A-21
Table A-16 J31 Radicom Modem Jumper Settings .......................................................... A-21
Table A-17 Serial Ports on Field Termination Board ........................................................ A-23
Table A-18 Switch Settings for LD485A-MP, RS-422 to GC.............................................. A-31
Table A-19 Jumper Settings for LD485A-MP, RS-422 to GC............................................. A-32
Table A-20 Switch settings for LD485A-MP, RS-485 to GC .............................................. A-34
Table A-21 Jumper settings for LD485A-MP, RS-485 to GC ............................................. A-35
Table C-1 Contents of Example Calibration Gas .............................................................. C-5

xiv
Section 1: Introduction
1

This section describes the contents and purpose of the Model 700 Gas
Chromatograph System Reference Manual, a description of the Model 700
system, an explanation of the theory of operation, and a glossary of
chromatograph terminology.

Use this section to get acquainted with the basic engineering of the
Model 700 product.

1.1 Description of manual

The Model 700 Gas Chromatograph System Reference Manual (P/N 3-


9000-521) consists of installation, operations, and maintenance and
troubleshooting procedures. Also included is information about the
Software Name software interface.

1.2 System description

The Model 700 is a high-speed gas chromatograph (GC) system that is


engineered to meet specific field application requirements based on
typical natural gas stream composition and anticipated concentration of
the selected components. In its standard configuration, the Model 700
can handle up to four streams: typically, three for sample and one for
calibration.

The Model 700 system consists of three major parts: the analyzer
assembly, controller assembly, and sample conditioning system (SCS).

Model 700 subsystems are: a Flame Ionization Detector (Micro-FID), a


Liquid Sample Injector (LSIV) and a Methanator.

1-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

1.2.1 Analyzer assembly

The Analyzer Assembly (upper enclosure) includes columns TCD/FID


detectors, Methanator, preamplifier, preamplifier power supply, stream
switching valves, and solenoids. See Figure and Figure 1-5 . Additionally,
the Model 700 may be equipped with a liquid sample inject valve (LSIV)
or a methantor.

1-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 1-1. Block diagram upper enclosure with TCD

1- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 1-2. Block diagram upper enclosure with Micro-FID

PREAMPLIFIER PCB
PREAMPLIFIER P/S PCB
INPUTS:
DC-DC CONVERTERS
1 TCD DETECTOR
24VDC INPUT 1 FID DETECTOR
24VDC POWER
OUTPUTS OUTPUTS:
+20VDC -20VDC COM (1)
100VDC (RS-232 OR RS-485)
5VDC

3.3 VDC

SERIAL I/O

SOLENOID/HEATER
DRIVER PCB

DC-DC CONVERTERS
24 VDC INPUT
OUTPUTS
5VDC
SOLENOID DRIVERS (16)
HEATERS (4 ZONES)

MULTIFUNCTION SERIAL PORT RS-232


MICRO-CONTROLLER PCB

HEATER PWM CONTROLLER


(4 ZONES)

DIGITAL INPUTS.................(5)
COM RS-232......................(1)
RTD INPUTS.......................(4)
ANALOG INPUTS 4-20mA....(4)
DIGITAL OUTPUTS..............(5) SERIAL PERIPHEERAL INTERFAC
SERIAL DAC CONTROL........(SPI)

1-4
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

1.2.2 Controller assembly

The controller assembly (lower enclosure) includes electronics and ports


for signal processing, instrument control, data storage, personal
computer (PC) interface, and telecommunications. This assembly allows
the user to control the GC functions via a PC with MON2000 (see
Section 1.4).

See Figure and Figure 1-4 for lower enclosure block diagrams.

1- 5
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 1-3. Block diagram TCD lower enclosure

1-6
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 1-4. Block diagram Micro-FID lower enclosure

INPUT OPTIONAL
AC POWER AC-DC
POWER SUPPLY

24* VDC (24.5 - 26.5 OPERATING VOLTAGE RANGE)

FIELD TERMINATION PCB OPTIONAL ANALOG


BUILT IN SURGE PROTECTION OUTPUT PCB
FIELD WIRING FOR THE FOLLOWING: 4 ISOLATED OR
8 NON-ISOLATED
COM 1 & 2, 5-8
ANALOG INPUTS 4-20mA.......(4)
ANALOG OUTPUTS 4-20mA....(4)
DIGITAL INPUTS.....................(5)

DIGITAL OUTPUTS (5) RELAYS


2 RELAYS FORM “A” CONTACT
3 SOLID STATE RELAYS
ANALYZER INTERCONNECT
POWER FOR STANDARD BUS
DC-DC CONVERTER SIGNALS - POWER
OUTPUTS STD-BUS
5VDC, +12VDC, -12 VDC
- 3.8VDC

CPU
MULTIFUNCTION COM 3
COM4A PCB
COM 5-8
FID & TCD PREAMPLIFIER COM 4
ETHERNET PCB

INTERNAL MODEM

OPTIONAL PC104

BOARD STACK

1- 7
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

The GC-PC interface provides the user with the greatest capability, ease-
of-use, and flexibility. One PC running MON2000 can connect with up to
32 chromatographs (via RS-485 serial communications links). MON2000
is used to edit applications, monitor operations, calibrate streams, and
display analysis chromatograms and reports, which can then be stored
to files on the PC hard drive or printed from either the PC printer port or
the GC printer port.

1.2.3 Sample conditioning system (SCS)

The sample conditioning system is located between the process stream


and the Analyzer Assembly sample inlet (mounted on the lower portion
of the Analyzer Assembly stand). The standard configuration includes a
Stream Switching System and filters.

The Model 700 electronics and hardware are housed in two explosion-
proof enclosures and meet IEC Class I, Zone 1, Ex d IIB+H2, T4 (NEC Class
1, Division 1, Groups B, C, and D) approval for use in a hazardous
environment.

1.3 Functional description

A sample of the gas to be analyzed is taken from the process stream by a


sample probe installed in the process line. The sample passes through a
sample line to the SCS where it is filtered or otherwise conditioned. After
conditioning, the sample flows to the Analyzer Assembly for separation
and detection of the gas components.

WARNING
Do not use a PC or a printer in a hazardous area. Serial port and Modbus
communications links are provided to connect the unit to the PC and to connect to
other computers and printers in a safe area. Failure to follow this warning may result in
injury or death to personnel or cause damage to the equipment.

The chromatographic separation of the sample gas into its components


is accomplished in the following manner. A precise volume of sample gas
is injected into one of the analytical columns. The column contains a
stationary phase (packing) that is either an active solid or an inert solid

1-8
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

support that is coated with a liquid phase (absorption partitioning). The


sample gas is moved through the column by means of a mobile phase
(carrier gas). The selective retardation of the components takes place in
the column, causing each component to move through the column at a
different rate. This separates the sample into its constituent gases and
vapors.

A detector located at the outlet of the analytical column senses the


elution of components from the column and produces electrical outputs
proportional to the concentration of each component. Outputs from the
detector(s) are amplified in the Analyzer Assembly electronics, then
transmitted to the Controller Assembly for further processing.

Note
For additional information, see "Section 1.5: Theory of operation".

Output from the Controller Assembly is normally displayed on a


remotely located PC or a printer. Connection between the Controller
Assembly and the PC can be accomplished via a direct serial line or via a
Modbus-compatible communication interface.

Several chromatograms may be displayed via MON2000, with separate


color schemes, allowing the user to compare present and past data.

Use of the MON2000 software for configuration and troubleshooting


procedures is essential in most cases. The PC may be remotely
connected via telephone, radio or satellite communications. Once
installed and configured, the Model 700 can operate independently for
long periods of time.

1- 9
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

1.3.1 Available functions

Individual GC functions that can be initiated or controlled by the GC


system and its software, MON2000, include (but are not limited to) the
following:
• valve activations
• timing adjustments
• stream sequences
• calibrations
• baseline runs
• analyses
• halt operation
• stream/detector assignments
• stream/component table assignments
• stream/calculation assignments
• diagnostics
• alarm and event processing
• event sequence changes
• component table adjustments
• calculation adjustments
• alarm parameters adjustments
• analog scale adjustments

1 - 10
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Reports and logs that can be produced, depending upon the GC


application in use, include (but are not limited to) the following:
• Configuration Report
• Parameter List
• Analysis Chromatogram
• Chromatogram Comparison
• Alarm Log (unacknowledged and active alarms)
• Event Log
• Various Analysis Reports

1.4 Software description

The MON2000 uses three distinct types of software. This enables total
flexibility in defining the calculation sequence, printed report content,
format, type and amount of data for viewing, control and/or
transmission to another computer or Controller Assembly. The three
types are:
• Baseline Operating System (BOS)
• Application configuration software
• Maintenance and Operations software (MON2000 version 2.2 or
later)

The BOS and the Application configuration software are installed when
the Model 700 system is shipped. The application configuration is
tailored to the customer’s process and shipped on a floppy disk. Note
that the hardware and software are tested together as a unit before the
equipment leaves the factory. MON2000 communicates with the Model
700 system and allows an initial site system setup (i.e., operational
parameters, application modifications, and maintenance).

1 - 11
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

1.4.1 BOS

The Baseline Operating System (BOS) supervises operation of the Model


700 through its internal microprocessor-based controller; all direct
hardware interface is via this control software. It consists of a multi-
tasking program that controls separate tasks in system operation, as well
as hardware self-testing, user application downloading, start-up, and
communications. Once configured, a Model 700 can operate as a stand
alone unit.

1.4.2 MON2000

MON2000, available as a Windows-based program, provides the human-


machine interface for maintenance, operation, and troubleshooting. It
allows the user to download applications developed for a specific GC
unit. MON2000 provides operator control of the connected Model 700,
monitors analysis results, and inspects and edits various parameters that
affect Model 700 operation. It also controls display and printout of the
chromatograms and reports, and it stops and starts automatic analysis
cycling or calibration runs.

After the equipment/software has been installed and the operation


stabilized, automatic operation can be initiated. The link between the
MON2000 computer and the Model 700 can either be direct, via a local
serial connection or remote, via an ethernet network, modems,
telephone lines and/or radio.

Operation of multiple Model 700 chromatographs (up to 32) with a


single MON2000 computer, via a multi-drop serial link, is also supported.

1 - 12
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

1.5 Theory of operation

The following sections discuss the theory of operation for the Model
700, the engineering principles and concepts used.

Note
See "Section 1.8: Glossary" for definitions of the terminology used in the following
explanations.

1.5.1 Thermal conductivity detector (TCD)

One of the detectors (located on the oven in the Analyzer upper


assembly) is a thermal conductivity detector that consists of a balanced
bridge network with heat sensitive thermistors in each leg of the bridge.
Each thermistor is enclosed in a separate chamber of the detector block.

One thermistor is designated the reference element and the other the
measurement element. See Figure 1-5 for a schematic diagram of the
thermal conductivity detector (TCD).

1 - 13
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 1-5. Analyzer assembly with tcd detector bridge

In the quiescent condition (prior to injecting a sample), both legs of the


bridge are exposed to pure carrier gas. In this condition, the bridge is
balanced and the bridge output is electrically nulled. (The bridge can be
balanced by the fine and coarse adjustment potentiometers located on
the preamplifier circuit board.)

The analysis begins when a fixed volume of sample is injected into the
column by operation of the sample valve. The sample is moved through
the column by the continuous flow of carrier gas. As successive
components elute from the column, the temperature of the
measurement element changes.

The temperature change unbalances the bridge and produces an


electrical output proportional to the component concentration.

The differential signal developed between the two thermistors is


amplified by the preamplifier. Figure illustrates the change in detector
electrical output during elution of a component.

1 - 14
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 1-6. Detector output during component elution

1 2 1

1 detector bridge balanced

component begins to elute from column


2 and is measured by thermistor

3 peak concentration of component

In addition to amplifying the differential signal developed between the


two thermistors, the preamplifier supplies drive current to the detector
bridge. The voltage signal is converted to a 4-20 milliampere (mA)
current loop for transmission to the Controller Assembly.

The signal is proportional to the concentration of a component detected


in the gas sample. The preamplifier provides four different gain channels
as well as compensation for baseline drift.

The signals from the preamplifier are sent to the Controller Assembly for
computation, recording on a printer, or viewing on a PC monitor (via
MON2000).

1 - 15
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

1.5.2 Flame ionization detector (FID)

The other detector (located on the oven in the Analyzer Assembly) is a


Flame Ionization Detector. The FID requires a polarization voltage and its
output is connected to the input to a high impedance amplifier which is
called an Electrometer. The burner uses a mixture of hydrogen and air to
maintain the flame. The sample of gas to be measured is also injected
into the burner. See Figure 1-7 for a schematic diagram of the Flame
Ionization Detector (FID).

Figure 1-7. Analyzer assembly with Micro-FID detector bridge

1 - 16
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

1.5.3 LSIV

The Liquid Sample Inject Valve (LSIV) penetrates the wall of the upper
enclosure and is held in place by a retaining ring. The mounting
arrangement is designed to ensure integrity of the flameproof enclosure.

Figure 1-8. Model 700 LSIV assembly


Retaining Ring Piston Housing

Retraction Actuation
Air Inlet Air Inlet

The outermost end houses an air operated piston. Air at 15 to 45 psi is


directed by a solenoid valve to either advance the stem to inject the
sample or to retract the stem.

The next section houses an auxiliary stem seal assist. A piston driven by
air at 80 to 100 psi keeps adequate load on the stem seal to counteract
wear at the high temperatures and pressures that might be encountered.
There are two ¼npt ports in this section; one port retracts the sample
piston and the other port activates the seal assist.

The innermost section houses the stem seals and the sample chamber.
There are five ¼ npt ports in this section.

1 - 17
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Within the enclosure cavity are the flash chamber components


surrounded with insulating covers. At working temperatures, the
surfaces of these covers become very hot to the touch.

The tip of the LSIV is the port where flashed sample is taken to the oven
system.

The port at right angles to the length of the LSIV is the input for carrier
gas.

The heater block, a cylinder of aluminum, is installed off-center


surrounding the flash chamber, close to the wall of the upper enclosure.
It houses the heater and an RTD and is retained by a jamb nut that should
only be finger tight.

1.5.4 Methanator

After all other components have been separated from the sample,
normally undetectable CO and CO2 are sent through the methanator.
They are combined with hydrogen to make methane in a heat generated
catalytic reaction. The methanator is also known as a methanizer or a
catalytic converter.

1 - 18
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 1-9. Model 700 Methanator Assembly

Methanator
Assembly

1.5.5 Data acquisition

Every second, exactly 40 equi-spaced data samples are taken (i.e., one
data sample every 25 milliseconds) for analysis by the Controller
Assembly. The sampling frequency of 40 Hertz (Hz) was chosen to
reduce normal mode noise (at 60 Hz).

After each point on the chromatograph signal is sampled, the resulting


number is stored for processing in a buffer area of the Controller
Assembly memory. During the analysis, only the last 256 data points are
available for processing.

Because the data analysis is done as the signal is sampled (in real-time),
only a limited number of past data samples is required to analyze any
signal.

1 - 19
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

As a part of the data acquisition process, groups of incoming data


samples are averaged together before the result is stored for processing.
Non-overlapping groups of N samples are averaged and stored, and thus
reduce the effective incoming data rate to 40/N samples per second. For
example, if N = 5, then a total of 40/5 or 8 (averaged) data samples are
stored every second.

The value for the variable N is determined by the selection of a Peak


Width parameter (PW). The relationship is

N = PW

where PW is given in seconds. Allowable values of N are 1 to 63; this


range corresponds to PW values of 2 to 63 seconds.

The variable N is known as the integration factor. This term is used


because N determines how many points are averaged, or integrated, to
form a single value. The integration of data upon input, before storing,
serves two purposes:
• The statistical noise on the input signal is reduced by the square root
of N. In the case of N = 4, a noise reduction of two would be realized.
• The integration factor controls the bandwidth of the chromatograph
signal. It is necessary to match the bandwidth of the input signal to
that of the analysis algorithms in the Controller Assembly. This
prevents small, short-duration perturbations from being recognized
as true peaks by the program. It is therefore important to choose a
Peak Width that corresponds to the narrowest peak in the group
under consideration.

1.5.6 Peak detection

For normal area or peak height concentration evaluation, the


determination of a peak's start point and end point is automatic. The
manual determination of start and end points is used only for area
calculations in the Forced Integration mode. Automatic determination of
peak onset or start is initiated whenever Integrate Inhibit is turned off.
Analysis is started in a region of signal quiescence and stability, such that
the signal level and activity can be considered as baseline values.

1 - 20
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Note
The Controller Assemblysoftware assumes that aregion of signal quiescenceand
stability will exist.

Having initiated a peak search by turning Integrate Inhibit off, the


Controller Assembly performs a point by point examination of the signal
slope. This is achieved by using a digital slope detection filter, a
combination low pass filter and differentiator. The output is continually
compared to a user-defined system constant called Slope Sensitivity. A
default value of 8 is assumed if no entry is made. Lower values make peak
onset detection more sensitive, and higher values make detection less
sensitive. Higher values (20 to 100) would be appropriate for noisy
signals, e.g. high amplifier gain.

Onset is defined where the detector output exceeds the baseline


constant, but peak termination is defined where the detector output is
less than the same constant.

Sequences of fused peaks are also automatically handled. This is done by


testing each termination point to see if the region immediately following
it satisfies the criteria of a baseline. A baseline region must have a slope
detector value less than the magnitude of the baseline constant for a
number of sequential points. When a baseline region is found, this
terminates a sequence of peaks.

A zero reference line for peak height and area determination is


established by extending a line from the point of the onset of the peak
sequence to the point of the termination. The values of these two points
are found by averaging the four integrated points just prior to the onset
point and just after the termination points, respectively.

The zero reference line will, in general, be non-horizontal, and thus


compensates for any linear drift in the system from the time the peak
sequence starts until it ends.

In a single peak situation, peak area is the area of the component peak
between the curve and the zero reference line. The peak height is the
distance from the zero reference line to the maximum point on the
component curve. The value and location of the maximum point is

1 - 21
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

determined from quadratic interpolation through the three highest


points at the peak of the discrete valued curve stored in the Controller
Assembly.

For fused peak sequences, this interpolation technique is used both for
peaks, as well as, valleys (minimum points). In the latter case, lines are
dropped from the interpolated valley points to the zero reference line to
partition the fused peak areas into individual peaks.

The use of quadratic interpolation improves both area and height


calculation accuracy and eliminates the effects of variations in the
integration factor on these calculations.

For calibration, the Controller Assembly may average several analyses of


the calibration stream.

1.6 Basic analysis computations

Two basic analysis algorithms are included in the Controller Assembly:

Note
For additional information about other calculations performed, see the MON2000
Software for Gas Chromatographs User Manual (P/N 3-9000-522).

• Area Analysis — calculates area under component peak


• Peak Height Analysis — measures height of component peak

1.6.1 Concentration analysis - response factor

Concentration calculations require a unique response factor for each


component in an analysis. These response factors may be manually
entered by an operator or determined automatically by the system
through calibration procedures (with a calibration gas mixture that has
known concentrations).

The response factor calculation, using the external standard, is:

1 - 22
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Area n Ht n
ARF n = --------------- or HRF n = -----------
Cal n Cal n

where

ARFn area response factor for component “n” in area per mole percent
Arean area associated with component “n” in calibration gas
Caln amount of component “n” in mole percent in calibration gas
Htn peak height associated with component “n” mole percent in calibration
gas
HRFn peak height response factor for component “n”

Calculated response factors are stored by the Controller Assembly for


use in the concentration calculations, and are printed out in the
configuration and calibration reports.

Average response factor is calculated as follows:


k

 RFi
RFAVG n = i------------------
=1
k

where

RFAVGn area or height average response factor for component “n”


RFi area or height average response factor for component “n” from the
calibration run
k number of calibration runs used to calculate the response factors

The percent deviation of new RF averages from old RF average is


calculated in the following manner:

RF new – RF old
deviation = -----------------------------------  100
RF old

where the absolute value of percent deviation has been previously


entered by the operator.

1 - 23
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

1.6.2 Concentration calculation - mole percentage (without


normalization)

Once response factors have been determined by the Controller


Assembly or entered by the operator, component concentrations are
determined for each analysis by using the following equations:

Area n Ht n
CONC n = --------------- or CONC n = --------------
ARF n HRF n

where

ARFn area response factor for component “n” in area per mole percent
Arean area associated with component “n” in unknown sample
CONCn concentration of component “n” in mole percent
Htn peak height associated with component “n” mole percent in unknown
sample
HRFn peak height response factor for component “n”

Component concentrations may be input through analog inputs 1 to 4 or


may be fixed. If a fixed value is used, the calibration for that component is
the mole percent that will be used for all analyses.

1.6.3 Concentration calculation in mole percentage (with


normalization)

The normalized concentration calculation is:

CONC n
-  100
CONCN n = ---------------------------
k

 CONCi
i=1

1 - 24
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Note
The average concentration of each component will also be calculated when data
averaging is requested.

where
CONCNn normalized concentration of component “n” in percent of total gas
concentration
CONCi non-normalized concentration of component “n” in mole percent for
each “k” component
CONCn non-normalized concentration of component “n” in mole percent
k number of components to be included in the normalization

1.7 Additional Resources

In addition to this manual, Model 700 Gas Chromatograph System


Reference Manual, refer to the MON2000 Software for Gas
Chromatographs User Manual (P/N 3-9000-522). Use this manual for
installing the MON2000 and Modbus Test (WinMB) software programs,
getting started, checking various gas chromatograph (GC) application
settings, and configuring and monitoring your GC system.

1.8 Glossary

Auto Zero

Automatic zeroing of the TCD preamplifier may be configured to take


place at any time during the analysis when either the component is not
eluting or the baseline is steady.

The FID is automatically zeroed at each new analysis run and can be
configured to take place anytime during the analysis when either the
component is not eluting or the baseline is steady. The TCD is only
automatically zeroed at the start of a new analysis.

1 - 25
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Baseline

Signal output when there is only carrier gas going across the detectors.
In a chromatogram you should only see Baseline when running an
analysis without injecting a sample.

Carrier Gas

The gas used to push the sample through the system during an analysis.
In C6+ analysis we use Ultra Pure (zero grade) Carrier Gas for the carrier.
This gas is 99.995 percent pure.

Chromatogram

A permanent record of the detector output. A chromatograph is


obtained from a PC interfaced with the detector output through the
Controller Assembly. A typical chromatogram displays all component
peaks, and gain changes. It may be viewed in color as it is processed on a
PC VGA display. Tick marks recorded on the chromatogram by the
Controller Assembly indicate where timed events take place.

Component

Any one of several different gases that may appear in a sample mixture

For example, natural gas usually contains the following components:


nitrogen, carbon dioxide, methane, ethane, propane, isobutane, normal
butane, isopentane, normal pentane, and hexanes plus.

Condulet

A box with a removable cover providing access to wiring in conduit


(conduit outlet) that is part of an optional cable entry package.

CTS

Clear to send

DCD

Data carrier detect

1 - 26
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

DSR

Data set ready

DTR

Data terminal ready

FID

Flame Ionization Detector - The optional


FID may be used in place of one TCD for the detection of trace
compounds. The
Micro-FID requires a polarization voltage and its output is connected to
the input to a high impedance amplifier, an Electrometer. The sample of
gas to be measured is injected into the burner with a mixture of
hydrogen and air to maintain the flame.

LSIV

Liquid Sample Inject Valve - The optional LSIV is used to convert a liquid
sample to a gas sample by vaporizing the liquid in a heated chamber,
then analyzing the flashed sample.

Methanator

The optional Methanator, a catalytic converter, converts otherwise


undetectable CO2 and/or CO into methane by adding hydrogen and heat
to the sample.

Response Factor

Correction factor for each component as determined by the calibration:

RawArea
RF = ----------------------------------------------------------------------
CalibrationConcentration

1 - 27
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Retention Time

Time (in seconds) that elapses between the start of analysis (0 seconds)
and the sensing of the maximum concentration of each component by
the detector.

RI

Ring indicator

RLSD

Received Line Signal Detect (a digital simulation of a carrier detect).

RTS

Request to send

RxD, RD, or Sin

Receive data, or signal in

TCD

Thermal Conductivity Detectors — Detectors that use thermal


conductivity of the different gas components to produce an unbalanced
signal across the bridge of the preamplifier. The higher the temperature
the lower the resistance on the detectors.

TxD, TD, or Sout

Transmit data, or signal out

1 - 28
Section 2: Equipment description and
2

specifications

Use the following sections to reference the Model 700 equipment


description or specifications.

2.1 Equipment description

The Model 700 consists of two copper-free aluminium explosion-proof


housings, upper and lower, and a front flow panel assembly. The
enclosures are separated by a pipe conduit which routes electrical wiring
from the lower enclosure to the upper enclosure. Designed to be
explosion-proof, this unit is built for installation in hazardous locations.
See Section 3.1 for more information.

Figure 2-1. Model 700 Gas Chromatograph

2-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

2.1.1 Upper enclosure

The Model 700 upper explosion-proof housing contains the electronic


controller (multifunction board), the Oven System, the Stream Switching
System (SSS) and preamplifier assembly.

Note
All circuit boards are connected through a common ground via the enclosure.

Figure 2-2. Upper Enclosure Assembly

Insulating Cover

Preamplifier Assembly

Multifunction Board

Micro-FID Exhaust Line

2-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

A more detailed equipment list includes:


• TCD Oven System (consists of the electronics, up to three
chromatograph valves and the stream switching system):
- column module (i.e., “oven”)
- one or two pairs thermal conductivity detectors (TCDs)
- valve system consisting of:
• three sample-directing valves
• plastic manifold that thermally insulates the Oven System and
connects the actuating part to the solenoid valves attached to
the plastic manifold
- two heater zones: column with one cartridge heater and one
block with three heaters
- two thermal cut-off switches:
(oven temperature switch) opens at 257°F (±5 °) (125 °C)

Figure 2-3. TCD Oven System Assembly

• Micro-FID

2- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 2-4. Model 700 Micro-FID upper assembly

Micro-FID

The optional flame ionization detector may be used in place of one TCD
for the detection of trace levels of compounds.
• Methanator

Figure 2-5. Model 700 Methanator Upper Assembly

Methanator
ssembly

2-4
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

The optional Methanator, a catalytic converter, converts


otherwise undetectable CO2 and/or CO into methane by adding
hydrogen and heat to the sample.

Figure 2-6. LSIV Assembly

The optional liquid sample inject valve (LSIV) is used to convert a liquid
sample to a gas sample for analysis on the Model 700 Gas
Chromatograph.

A measured sample is placed in a heated chamber above the


vaporization point of the liquid and then it is flashed to a gas. Once
vaporized, the sample is pushed by the carrier gas through the heated
tubing into the column train.
• Stream Switching System (SSS) that consists of the following:
- manifold block
- solenoid valves
- valve clamps
- temperature sensor
- oven temperature switch
- tubing
- insulation cover

2- 5
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 2-7. SSS Installed

• TCD Electronics
- Dual Methods Adapter Board
- Driver I/O Board
- Multifunction Board
- Preamplifier Board
- External Locking Device
• FID Electronics
- Solenoid/Heater Driver Board
- Multifunction Board
- Preamplifier Power supply
- Driver I/O Board
- Multifunction Board

2-6
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

2.1.2 Lower Enclosure

The Model 700 lower enclosure consists of the Card cage assembly,
which contains the following:
• CPU board
• Com4A board (optional)
• Analog board
• Additional analog board (optional)
• Digital I/O
• Internal modem (optional)
• Ethernet card (optional)
• Field termination board (FTB)
• Connection for AC/DC power supply
(converter)
• Internal and external ground

Note
The Model 700 CSA-certified unit is equipped with 3/4 inch cross-over adapters.

• External locking device


• DB pin connection for serial communications

WARNING
See power supply label prior to connection. Check the unit power design to determine
if it is equipped for AC or DC power. Applying 110/ 220 VAC to a DC power input unit
will severely damage the unit. Failure to do so may result in injury or death to personnel
or cause damage to the equipment.

2- 7
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

2.1.3 Flow Panel Assembly

The flow panel assembly is attached to the front of the upper enclosure
and consists of the following: (see Figure 2-2):
• Carrier pressure regulator(s) and gauge(s)
• Sample flow meter
• Sample Vent (SV)
• Measure Vent (MV)
• Actuation pressure limiting regulator
• Pressure switch, mounted internally

CAUTION
If the carrier gas pressure drops below a set point, this switch causes the analysis to stop
and activates the analyzer failure alarm.

2-8
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

2.2 Equipment Specifications

2.2.1 Utilities

Use the following table to determine the utility specifications.

Type Specification

unit • basic unit envelope


dimensions w - 15.2” (387 mm)
h - 41.5” (1054 mm) Note: Allow 14” (360 mm) additional clearance for removal
(P/N 20351)
of dome.
d - 19.2” (488 mm)
• wall mount
w - 18.2” (463 mm)
h - 41.5” (1054 mm)
d - 19.2” (488 mm)
• pole mount
w - 18.2” (463 mm)
h - 41.5” (1054 mm)
d - 25.0” (635 mm)
• floor mount
w - 18.2” (463 mm)
h - 58.0” (1470 mm)
d - 19.2” (488 mm)
unit weight • wall mount 130 lbs (59 kg)
• pole mount 135 lbs (61 kg)
• floor mount 150 lbs (68)
materials • 303 and 316 stainless steel
• 316 stainless steel and Kapton in contact with sample
• Swagelock and Valco fittings
mounting • floor mount
• pole mount: 2” (60.3 mm); 3” (89.0 mm); 4” (114.3 mm)
• direct wall mount

2- 9
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Type Specification

power • 24VDC standard (24.5 - 26.5 VDC operating voltage range); 80 watts
• AC optional 90-130/180-264 VAC; 47-63 Hz; 80 watts
80 watts start-up; 33 watts nominal
• 47-63Hz (single phase)
• 75W (Model 700 w/TCD)
• 150W (Model 700 w/Methanator or LSIV)
• 36VDC, Sol/Drv PCB Transorb
Note: Voltage range includes line voltage variations. Ensure the GC receives at
least 24.5 VDC at the terminals. If the power supply is located more than 164 feet
(50 meters) from the GC, a voltage drop may occur across the cable and cause the
solenoids to fail. If your GC installation is more than 164 feet (50 meters) away
from the power supply, use an AC power supply to avoid problems with a voltage
drop across the cable.
instrument not required; optional for valve actuation, minimum pressure of 90 psig
air
environment • -18 to 55 oC (0 to 130 oF)
• 0 to 95% RH (non-condensing)
• indoor/outdoor
• pollution - degree 2 (the unit can withstand some non conductive
environmental pollutants e.g., humidity)
• max altitude 2000m

2 - 10
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Type Specification

approvals

For USA, Class I, Zone 1, AEx d IIB+H2, T4, Enclosure Type 4


Class I, Division 1, Group B, C and D
For Canada, Class I, Zone 1, Ex d IIB+H2, T4, Enclosure Type 4
Class I, Division 1, Group B, C and D
Gas Chromatograph, Model 700, permanently connected, rated 90-130/180-264 V ac,
75W, 50/60 Hz, I phase, or 23-28 V dc, 75W, Operating Temperature Ambient -18oC to
+55oC.

0518
SIRA 04ATEX1055X

II 2 G
Ex d IIC T4 Gb
Tamb = +60oC
IECEx SIR 08.0008X
Ex d IIC T4 Gb
Tamb = 60oC

2 - 11
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

2.2.2 Electronic Hardware

Review the system block diagrams, Upper and Lower Electronics, to


become familiar with the Model 700.

Figure 2-8. Upper Electronics with TCD Block Diagram

2 - 12
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 2-9. Upper Electronics with Micro-FID Block Diagram

PREAMPLIFIER PCB
PREAMPLIFIER P/S PCB
INPUTS:
DC-DC CONVERTERS 1 TCD DETECTOR
24VDC INPUT 1 FID DETECTOR
24VDC POWER
OUTPUTS OUTPUTS:
+20VDC -20VDC COM (1)
100VDC (RS-232 OR RS-485)
5VDC

3.3 VDC

SERIAL I/O

SOLENOID/HEATER
DRIVER PCB

DC-DC CONVERTERS
24 VDC INPUT
OUTPUTS
5VDC
SOLENOID DRIVERS (16)
HEATERS (4 ZONES)

MULTIFUNCTION SERIAL PORT RS-232


MICRO-CONTROLLER PCB

HEATER PWM CONTROLLER


(4 ZONES)

DIGITAL INPUTS.................(5)
COM RS-232......................(1)
RTD INPUTS.......................(4)
ANALOG INPUTS 4-20mA....(4)
DIGITAL OUTPUTS..............(5) SERIAL PERIPHEERAL INTERFACE
SERIAL DAC CONTROL.........(SPI)

2 - 13
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 2-10. Lower Electronics TCD Block Diagram

2 - 14
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 2-11. Lower Electronics Micro-FID Block Diagram

INPUT OPTIONAL
AC POWER AC-DC
POWER SUPPLY

24 VDC

FIELD TERMINATION PCB OPTIONAL ANALOG


BUILT IN SURGE PROTECTION OUTPUT PCB
FIELD WIRING FOR THE FOLLOWING: 4 ISOLATED OR
8 NON-ISOLATED
COM 1 & 2, 5-8
ANALOG INPUTS 4-20mA.......(4)
ANALOG OUTPUTS 4-20mA....(4)
DIGITAL INPUTS.....................(5)

DIGITAL OUTPUTS (5) RELAYS


2 RELAYS FORM “A” CONTACT
3 SOLID STATE RELAYS
ANALYZER INTERCONNECT
POWER FOR STANDARD BUS
DC-DC CONVERTER SIGNALS - POWER
OUTPUTS STD-BUS
5VDC, +12VDC, -12 VDC
- 3.8VDC

CPU
MULTIFUNCTION COM 3
COM4A PCB
COM 5-8
FID & TCD PREAMPLIFIER COM 4
ETHERNET PCB

INTERNAL MODEM

OPTIONAL PC104

BOARD STACK

2 - 15
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Use the following table to determine the electronic hardware


specifications.

Type Specification

Rating Division 1; no purge required


CPU AMD Geode LX800 500MHz
Memory 128 MB System RAM
CompactFlash 128 MB
Communication Ports 6 configurable Modbus ports; support RS-232/422/485 protocols
Optional Modem 56K Baud Telephone
Analog Inputs 4, 12-pin Phoenix on FTB
Standard Analog Outputs 4, 12-pin Phoenix on FTB
Optional Analog Outputs 8, non-isolated outputs 24-pin Phoenix
Located on Optional Analog Board
Or,
4, isolated outputs 12-pin Phoenix connector
Located on Optional Analog Board
Discrete Digital Inputs GC_IN (dedicated to pressure switch); 4 user-defined inputs
Digital Outputs (5) 2 Relays “Form A” contacts
Relay contact rating 24 VDC nominal @ 1 Amp
3 Solid State Relays - Rating of 0.375A @30 VDC on FTB - 10 pin
Phoenix connector
Detector Inputs Optionally 2 micro-volume TCD inputs
1 Flame Ionization Detector (Micro-FID) input
Transient Protection over-voltage category II

2 - 16
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

2.2.3 Micro Heat Sink Oven

Use the following table to determine the oven specifications.


Type Specification

Valves 6-port and 10-port valves; piston-operated diaphragms


with pneumatic actuation
Columns max of 40 feet (12 m) of micro-packed columns; 1/16-
inch
(1.6-mm) outside diameter
Solenoid Actuation • 24 VDC
• max 90 psi
Wetted Parts 316 stainless steel and kapton diaphragm
Temperature Control • 24 VDC heat sink
• 2 zones (1 column, 1 block)
• max operating temperature of 115 °C (239 °F)
Sample System 1 zone, includes Stream Switching System
Sample Streams • standard: max of 3 analytical and 1 auto calibration
• optional: max of 8

2 - 17
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

2.2.4 Software

Use the following table to determine the software specifications.

Note
The Model 700 has its own applications and is not compatible with 2350/2350A
applications.

Type Specification

Software PC-based MON2000; runs 2350 and 2350A applications (v2.4


or later)
Firmware embedded firmware compatible with 2350/2350A
applications (v1.8 or later)
Methods 4 Timed Event Tables and 4 Component Data Tables
assignable to each stream
Peak Integration • fixed time or auto slope and peak identification
• update Retention Time upon
calibration or during analysis

2 - 18
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

This page is intentionally left blank.

2 - 19
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

2 - 20
Section 3: Installation and setup
3-

This section provides instructions for installing and setting up the Model
700 gas chromatograph (GC) system for Zone 1/ Division I
environments.

This procedure involves the following steps:


• Observe precautions and warnings
• Plan site location
• Obtain supplies and tools
• Install GC wiring
• Install GC sample and gas lines
• Perform leak checks
• Purge carrier gas lines
• Purge calibration lines
• Start up GC system

3.1 Precautions and warnings

WARNING
Install and operate all equipment as designed and is compliant with all safety
requirements. The “Seller” does not accept any responsibility for installations of the
Model 700, or any attached equipment, in which the installation or operation thereof
has been performed in a manner that is negligent and/or non-compliant with
applicable safety requirements.

3-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

3.1.1 Hazardous environments

WARNING
Observe all precautionary signs posted on the Model 700 enclosure. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.

WARNING
Observe all precautionary signs posted on the Model 700 enclosure.

WARNING
The Model 700 enclosures are certified by CSA for Class I, Zone 1, Ex d IIB+H2 T4,
Enclosure Type 4 and Class I, Division 1, Groups B,C,D. The Model 700 enclosures are
certified by ATEX for ATEX Ex d IIC T4 and IEC-Ex Ex dIIC T4.

WARNING
ATEX certified units must be installed strictly in compliance with the requirements of
IEC 60079-14.

Special conditions for safe use must be met. The maximum constructional gap (ic) is
less than that required by Table 2 of EN 60079-1:2007.

Before opening the Model 700 enclosure, reduce the risk of igniting hazardous
atmospheres by disconnecting the equipment from all power supplies. Keep the
assembly closed tightly when in operation to reduce the risk of igniting hazardous
atmospheres. Inlet (incoming) wiring must meet local standards (i.e. in conduit with
seal fitting within 18 or via cable glands certified to IEC 60079-1). Upper enclosure
threaded entry is ¾ NPT. Lower enclosure threaded entries are M32-1.5.

Observe all precautionary signs posted on the Model 700 enclosure. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.

Please direct all health, safety and certification related questions to: Emerson Process
Management, Gas Chromatographs, Applications Engineering Group, 713-827-6380 or
1-866-GC Center (1-866-422-3683).

3-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Follow these precautions if installing or operating the Model 700


instrumentation in a hazardous area:

1. Install and operate only the Zone 1/ Division I version of the


Model 700 in a hazardous area.

2. Do not operate any printer or personal computer (PC) that is


connected to a GC which is installed in a hazardous area. To
interface with a GC in a hazardous area, use a PC that is located in
a nonhazardous area and remotely connected to the GC.

3. Ensure that field connections to the analyzer are made through


explosion-proof conduit or flameproof glands.

3.1.2 Power source wiring

Follow these precautions when installing AC power source wiring:

1. All wiring must conform to the CEC or NEC, local state or other
jurisdiction, and company standards and practices.

2. Provide 24 VDC (24.5 - 26.5 VDC range) power or optional single-


phase, 3-wire, power at 115 or 230 VAC, 47-63 Hertz.

3. Locate circuit breaker and optional power disconnect switch in a


safe area.

4. Provide the Model 700 system and any optionally installed


devices with one 15-Amp circuit breaker for protection.

CAUTION
15 amps is the maximum current for 14 AWG (wire).

5. Ensure that the 24 VDC input power is S.E.L.V. compliant by


suitable electrical separation from other circuits.

3- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

6. Use multi-stranded copper conductor wire according to the


following recommendations:
• For power feed distances up to 250 feet (76 meters), use 14
AWG (American Wire Gauge) (18 Metric Wire Gauge),
stranded.
• For power feed distances 250 to 500 feet (76 to 152 meters),
use 12 AWG
(25 Metric Wire Gauge), stranded.
• For power feed distances 500 to 1000 feet (152 to 305
meters), use 10 AWG
(30 Metric Wire Gauge), stranded.
• Cable entries are M32 in accordance with ISO 965.

3.1.3 Card cage removal

The Model 700 card cage assembly is designed to be disconnected and


removed from the lower enclosure to allow space for user power and
signal connections. This may be particularly important for applications
where large numbers of I/O connections are required.

Note
Card cage removal is not necessary for I/O connections.

To disassemble the card cage, do the following:

1. Remove the lower enclosure cover and the front flow panel
assembly or LOI.

3-4
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-1. Lower enclosure disassembly

Cover

LOI

If removing a flow panel assembly, leave the wires attached to it


and allow it to hang outside of the enclosure.

2. Carefully disconnect all of the ribbon cables from the boards in


the card cage assembly (CPU, Analog, Modem, etc.).

Note
Note the location of the ribbon cables for ease of reassembly.

3- 5
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-2. Card cage cable disassembly

Flow Panel

3. Use a Phillips head screw driver and remove the two screws
located at the top of the card cage and one screw on the bottom
left side of the card cage (not visible in the figure).

3-6
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-3. Card cage assembly screw locations

Card Cage
Screws

4. Slide the card cage assembly out of the lower enclosure.

3- 7
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-4. Card cage disassembly

5. User power and signal connections may be made with the card
cage removed from the lower enclosure.

3-8
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-5. Card cage disassembly for power and signal wiring

3- 9
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

3.1.4 Signal wiring

Follow these general precautions for field wiring digital and analog
input/output (I/O) lines:

CAUTION
Observe all precautionary signs posted on the Model 700 enclosure. Applicable to all
digital and analog I/O lines connecting to the GC: Any loop of extra cable left for service
purposes inside the GC housing must not be placed near any AC power lines. If this
precaution is not followed, the data and control signals to and from the GC can be
adversely affected.

• Metal conduit must be used for all process signal wiring (assuming
operation in a Class 1, Division 1 Explosive Area). Metal conduit is not
required for use in general purpose areas.
• Metal conduit or cable (in compliance with EN 60079-14) used for
process signal wiring must be grounded at conduit support points
(intermittent grounding of conduit helps prevent induction of
magnetic loops between the conduit and cable shielding).
• All process signal wiring should be a single, continuous length
between field devices and the GC. If, however, length or conduit runs
require that multiple wiring pulls be made, the individual conductors
must be interconnected with suitable terminal blocks.
• Use suitable lubrication for wire pulls in conduit to prevent wire
stress.
• Use separate conduits for AC voltage and DC voltage circuits.
• Do not place digital or analog I/O lines in same conduit as AC power
circuits.
• Use only shielded cable for digital I/O line connections.
- Ground the shield at only one end.
- Shield-drain wires must not be more than two AWG sizes smaller
than the conductors for the cable.
• When inductive loads (relay coils) are driven by digital output lines,
the inductive transients must be diode-clamped directly at the coil.
• Any auxiliary equipment wired to the GC must have its signal
common isolated from earth/chassis ground.

3 - 10
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3.1.5 Electrical and signal ground

Follow these general precautions for grounding electrical and signal


lines:
• For shielded signal conducting cables, shield-drain wires must not be
more than two AWG sizes smaller than the conductors for the cable.
Shielding is grounded at only one end.
• Metal conduit used for process signal wiring must be grounded at
conduit support points (intermittent grounding of conduit helps
prevent induction of magnetic loops between the conduit and cable
shielding).
• A single-point ground (the outside case ground lug) must be
connected to a copper-clad, 10-foot long, 3/4-inch diameter steel
rod, which is buried, full-length, vertically into the soil as close to the
equipment as is practical (note: the grounding rod is not furnished.)

3 - 11
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-6. Ground Lug Lower Enclosure

Ground Lug Ground Lug


Inside Lower Outside Lower
Enclosure Enclosure

• Resistance between the copper-clad steel ground rod and the earth
ground must not exceed 25 Ohms.
• On ATEX certified units, the external ground lug must be connected
to the customer’s protective ground system via AWG 9 (6mm2)
ground wire. After the connection is made, apply a non-acidic grease
to the surface of the external ground lug to prevent corrosion.
• The equipment-grounding conductors used between the GC and the
copper-clad steel ground rod must be sized according to the
following specifications:
Length Wire

15 ft. (4.6 m) or less 8 AWG


stranded, insulated copper

3 - 12
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Length Wire

15 to 30 ft. (4.6 to 9.1 m) 6 AWG


stranded, insulated copper
30 to 100 ft. (9.1 to 30.5 m) 4 AWG
stranded, insulated copper

• All interior enclosure equipment-grounding conductors must be


protected by metal conduit.
• External equipment, such as data printers, that are connected to the
GC should be powered via isolation transformers to minimize the
ground loops caused by the internally shared safety and chassis
grounds.

3.1.6 Electrical conduit

Follow these general precautions for conduit installation:


• Conduit cutoffs must be square. Cutoffs must be made by a cold
cutting tool, hacksaw, or by some other approved means that does
not deform the conduit ends or leave sharp edges.
• All conduit fitting-threads, including factory-cut threads, must be
coated with a metal-bearing conducting grease, such as Crouse-
Hinds STL or equivalent, prior to assembly.
• Temporarily cap the ends of all conduit runs immediately after
installation to prevent accumulation of water, dirt, or other
contaminants. If necessary, swab out conduits prior to installing the
conductors.
• Install drain fittings at the lowest point in the conduit run; install seals
at the point of entry to the GC explosion-proof housing to prevent
vapor passage and accumulation of moisture.
• Use liquid-tight conduit fittings, such as Myers Scru-tite or similar, for
conduits exposed to moisture.

When conduit is installed in hazardous areas (e.g., areas classified as NEC


Class I, Division 1, Groups B, C, and D), follow these general precautions
for conduit installation:

3 - 13
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

WARNING
Observe all precautionary signs posted on the equipment. Consult your company
policies and procedures and other applicable requirements documents to determine
wiring and installation practices that are appropriate for hazardous areas. Failure to do
so may result in injury or death to personnel or cause damage to the equipment.

• All conduit runs must have a fitting, which contains explosion-proof


sealing (potting) located within 18 inches from the conduit entrance
to the explosion-proof housing.
• The conduit installation must be vapor tight, with threaded hub
fittings, sealed conduit joints and gaskets on covers, or other
approved vapor-tight conduit fittings.

3.1.7 Sample system requirements

Observe the following guidelines for installing GC sample systems:

Line length:

If possible, avoid long sample lines. In case of a long sample line, flow
velocity can be increased by decreasing downstream pressure and using
by-pass flow via a speed loop.

Note
Stream switching requires a sample pressure of 20 psig.

Sample line tubing material:

Note
The calibration gas stream inlet is the last stream inlet following the sample gas.

• Use stainless steel tubing for noncorrosive streams.


• Ensure tubing is clean and free of grease (see Figure 3-7 for details).

3 - 14
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-7. Stream Inlets (Right side of unit)

Stream 1 - 8
Gas Connections

Dryers and filters:

Use small sizes to minimize time lag and prevent back diffusion.

Note
Install the probe/regulator first, immediately followed by the coalescing filter and then
the membrane filter. See Appendix C for a recommended natural gas installation.

• Install a minimum of one filter to remove solid particles. Most


applications require fine-element filters upstream of the GC. The
Model 700 hardware includes a 2-micron filter.
• Do use ceramic or porous metallic type filters. Do not use cork or felt
filters.

3 - 15
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Pressure regulators and flow controllers:

• Do not use types containing cork or felt filters, or absorbent


diaphragms.

Pipe Threads, dressing:

• Do use Teflon tape. Do not use pipe thread compounds (dope).

Valving:

• Install a block valve downstream of sample takeoff point for


maintenance and shutdown.
• Block valve should be needle valve or cock valve type, of proper
material and packing, and rated for process line pressure.

3.2 Preparation

Your Model 700 GC was started and checked out before it left the
factory. Program parameters were installed and documented in the PC
Config Report furnished with your Model 700.

3.2.1 Site selection

Install the GC as close as possible to the sample system but allow for
adequate access space for maintenance tasks and adjustments. Allow a
minimum of 14 inches (36 cm) in front for enclosure opening and access.
• Allow a minimum of 14 inches (36 cm) above the top of the dome
enclosure for dome removal and access.
• Ensure that exposure to radio frequency (RF) interference is minimal.

3 - 16
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3.2.2 Unpacking the unit

See the following checklist for unpacking the unit and inspecting for
damage:

1. Unpack the equipment:


• Model 700 system
• MON2000 CD-ROM

2. Ensure that all documentation and software are included on the


CD-ROM:
• This manual: Model 700 Gas Chromatograph System Reference
Manual (P/N 3-9000-521)
• The software manual: MON2000 Software for Gas
Chromatographs User Manual (P/N 3-9000-522)
• The MON2000 Software for Gas Chromatographs Windows
application, Modbus Test application, and GC applications
(P/N 2-3-2350-400)

3. Remove any packing materials from internal areas of the unit


(particularly in the dome enclosure).

4. If an FID is present, remove the vent plug from the FID outlet. The
vent plug has a tag attached to it that reads “REMOVE VENT
PLUGS PRIOR TO OPERATION”. Failure to remove the cap could
result in a performance failure or in damage to the detector.

Installation and startup should proceed only if all required materials are
on hand and free from obvious defects.

If any parts or assemblies appear to have been damaged in shipment,


first file a claim with the carrier. Next, complete a full report describing
the nature and extent of the damage and forward this report
immediately to Measurement Services for further instructions (see the
Customer Repair Report at the back of this manual). Include complete
model number information. Disposition instructions will be returned
immediately.

3 - 17
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

3.2.3 Model 700 installation arrangements

The Model 700 GC can be ordered for installation in the following


mounting arrangements (see drawing P/N DE-20993):

Note
The wall should be strong enough to support the 200-pound load.

• Wall mount
• Pole mount
• Floor mount

3.2.3.1 Wall mount

The simplest arrangement is wall mount (see drawing P/N DE-20993).


The unit has two mounting ears on each side. The ear-holes are used to
attach the unit to a wall.

The uppermost of the holes should be about 30 inches from the floor for
the most efficient use of the unit.

The space between the enclosures and the wall (1.3 inches) allows
adequate access above and around the unit.

3.2.3.2 Pole mount

The pole mount arrangement uses mounting ears as attachment points


for the plates clamped to a pole (see drawing P/N DE-20993). The plates
accept the recommended u-bolt systems for the 2 inch, 3 inch or 4 inch
nominal pipe sizes. The base attachment of the pole being used must be
able to accommodate the weight of the unit.

3 - 18
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3.2.3.3 Floor mount

The floor mount arrangement includes additional external framing that


creates a free-standing unit (see drawing P/N DE-20993). The mounting
ears, located on the base of the frame, are used to anchor the unit to a
floor or instrument pad. The frame, also provides a means for attaching
sample-conditioning plates or for anchoring
tubing-runs.

3.2.4 Required Tools and Components

You will need these tools and components to install the Model 700:
• Zero grade carrier gas (99.995% pure, with less than 5 ppm water,
and less than 0.5 ppm hydrocarbons)
• High pressure dual-stage regulator for the carrier gas cylinder, high
side up to 3000 pounds per square inch, gauge (psig), low side
capable of controlling pressure up to 150 psig
• Calibration standard gas with correct number of components and
concentrations. See Appendix Table C-1.
• Single-stage regulator for the calibration gas cylinder, low pressure
side capable of controlling pressure up to 30 psig
• Sample probe regulator (fixture for procuring the stream, or sample
gas for chromatographic analysis)
• Coalescing filter
• Membrane filter
• 1/8-inch stainless steel (SS) tubing for connecting calibration
standard to GC, 1/8 inch SS tubing for connecting carrier gas to the
GC, 1/8-inch SS tubing for connecting stream gas to the GC
• Heat tracing (as required) for sample transport and calibration lines
• Miscellaneous Swagelok tube fittings, tubing benders and tubing
cutter
• 14 AWG (18 MWG) or larger electrical wiring and conduit to provide
115 or 230 volts AC, single phase, 50 to 60 Hertz, from an
appropriate circuit breaker and power disconnect switch. See
guidelines in “Power source wiring” on page 3-3.
• Liquid leak detector (Snoop® or equivalent)

3 - 19
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

• Digital volt-ohm meter with probe-type leads


• Flow measuring device
• Open-end wrenches sized 1/4, 5/16, 7/16, 1/2, 1/16 and 5/8-inch

3.2.5 Supporting tools and components

WARNING
Do not use a PC or a printer in a hazardous area. Serial port and Modbus
communications links are provided to connect the unit to the PC and to connect to
other computers and printers in a safe area. Failure to follow this warning may result in
injury or death to personnel or cause damage to the equipment.

Supporting tools and components include:


• Use an IBM-compatible PC and either a direct or remote
communications connection to interface with the Model 700 system.
See Section 2.1 of the MON2000 Software for Gas Chromatographs
User Manual
(P/N 3-9000-522) for more information on specific PC requirements.
• The Model 700 comes with serial Port 2 on the Field Termination
Board (FTB) factory-wired with a DB 9-pin connection. Use the
provided serial cable (P/N 3-2350-068) to hookup to a PC. See Table
A-4 for more information regarding these connections.

Note
You can use the serial cable installed for the Model 700. For straight-through serial
cable installation and fabrication instructions, see Appendix A.

If a different serial cable is used to connect from the PC to the pre-


wired DB 9-pin, follow these specifications:
Terminal Connection

DB 9-pin male Serial Port 2


DB 9-pin male PC serial port
DB 25-pin female

3 - 20
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

• Use items necessary for connecting the GC to a network or other


type of remote data transfer system (an example item might be an
RS-232/RS-485 conversion box for long distance serial transmission),
as applicable.
• Use a printer, connected either at the PC or the GC unit, to record
analysis and other data. See Section 3.4.6 for wiring information.

3.3 Model 700 installation

3.3.1 DC power supply

WARNING
Ensure that the DC power source is switched OFF before connecting the wires. Also,
ensure that the DC power is S.E.L.V. compliant by suitable electrical separation from
other circuits. Failure to follow these warnings may result in injury or death to personnel
or cause damage to the equipment.

CAUTION
Check the unit prior to wiring to determine if it is equipped for DC power. Failure to
observe this precaution may damage equipment.

To connect DC power to the GC:

1. Locate the plug-together termination block inside the lower


enclosure.

3 - 21
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-8. 24 VDC power connection

24 VDC Power Connection

2. Bring the two leads in through the entry on the left side of the
lower enclosure. Connect to the termination plug provided with
the unit. See Appendix H Drawing DE- 20993.

3 - 22
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-9. 24 VDC power inlet

24 VDC Power Inlet

Use the following table for the DC power wiring details:


Attribute Wire Color

+ (positive) red
— (negative) black

3. Each board that connects to the 24 VDC is protected from lead


reversal by the use of blocking diodes. The following boards are
connected to the 24 VDC:
• Field Termination Board
• Isolated Analog Output Option Board
• Solenoid/Heater Driver board

Note
A new version of the Solenoid/Heater Driver Board that includes the Diode protection
will soon be released.

• FID/TCD Preamplifier Board


If the Red (+) and Black (-) leads are inadvertently reversed, no
damage will occur, however, the system will not have power.

3 - 23
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4. Connect the DC power leads to the power disconnect switch that


is properly fused. The recommended fuse size is 10 Amps.

3.3.2 Optional AC — DC power converter

To connect 115 or 230 VAC power to the GC:

WARNING
Check the unit prior to wiring to determine if it is equipped for optional AC power.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.

1. Locate the plug-together termination block inside the lower


enclosure (located on the lower left side behind the power
supply).

Figure 3-10. AC/DC Power Converter

AC / DC Power
Converter

3 - 24
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

WARNING
Do not connect AC power leads without first ensuring that AC power source is switched
OFF. Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.

CAUTION
Do not apply electrical power to the GC until all interconnections and external signal
connections have been verified, and proper grounds have been made. Failure to
observe this precaution may cause damage to equipment.

AC wiring is usually colored as:


Attribute Wire Color

hot brown or black


neutral blue or white
ground green or green

2. Bring the power leads in through the left entry on the bottom of
the enclosure.

3. If necessary, connect the GC chassis ground to an external copper


ground rod (at remote locations). See Section 3.1.5 regarding
electrical and signal grounding.

3 - 25
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

3.3.3 Sample and Gas Lines

To install GC sample and gas lines:

Note
Use SS tubing. Keep tubing clean and dry internally to avoid contamination. Before
connecting the sample and gas lines, flow clean air or gas through them. Blow out
internal moisture, dust, or other contaminants.

1. Remove the plug from the Sample Vent (SV) line (1/16-inch
tubing marked “SV” located on the Flow Panel Assembly).
• If desired, connect the SV line to an external (ambient
pressure) vent. If the vent line is terminated in an area exposed
to wind, protect the exposed vent with a metal shield.
• Use 1/4-inch or 3/8-inch tubing for vent lines longer than 10
feet.

Figure 3-11. Model 700 Upper Enclosure

SV

MV

Sample Vent and


Measure Vent Lines

Note that, at this stage in the installation, the GC Measure Vent


(MV) line (marked “MV”) remains plugged until leak checks are
completed. For regular operation, however, the MV line must be
unplugged, or open.
Do not discard the vent line plugs. They are useful at any time
when leak-checking the GC and its sample or gas line
connections.

3 - 26
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

2. Connect carrier gas to the GC. (The carrier gas inlet is a 1/8-inch
tee fitting located on the left side of the upper enclosure.)

CAUTION
Do not turn on gas until you have completed leak checking the carrier and sample lines
(see Step 5). Failure to follow this precaution may cause injury to personnel or damage
equipment.

Figure 3-12. Carrier gas inlet left-side upper enclosure

Carrier Gas
Inlet

• Use 1/8-inch or 1/4-inch stainless steel tubing to conduct


carrier gas.
• Use a dual-stage regulator with high-side capacity of 3000
psig and low-side capacity of 150 psig.

3 - 27
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

• See Appendix C for a description of a dual-cylinder carrier gas


manifold (P/N 3-5000-050) with these features:

Note
The first stream is the calibration gas stream.

- Carrier gas is fed from two bottles.


- When one bottle is nearly empty (100 psig), the other
bottle becomes the primary supply.
- Each bottle can be disconnected for refilling without
interrupting GC operation.

3. Connect calibration standard gas to the GC

Note
When installing the calibration standard gas line, ensure that the correct
tubing connection is made.

• Use 1/8-inch stainless steel tubing to conduct calibration


standard gas.
• Use a single-stage regulator with low-side capacity of up to 30
psig.
• The calibration gas inlet is the last inlet following the sample
gas.

3 - 28
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-13. Calibration gas stream inlet (right side of unit)

Calibration
Gas Inlet

4. Connect sample gas stream(s) to the GC (see Figure 3-11 Model


700 Upper Enclosure panel).
• Use 1/8-inch or 1/4-inch stainless steel tubing to conduct
calibration standard gas.
• Ensure that pressure of sample line is regulated to maintain 15
to 30 psig (±10%).
• Gas stream inlet(s) are identified (see Figure 3-14) for details.

3 - 29
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-14. Sample stream inlets (Right side of unit)

Streams 1 - 7 Calibration
Gas Inlets Gas Inlet

5. After all lines have been installed, proceed with leak checking the
carrier and sample lines. See Section 3.5.1; note that it requires
the AC power to be turned on at the GC.

3.4 Setting the Com ID


The Model 700 Com ID is determined by dual inline package (DIP) switch
settings.

Note
Follow the steps in this section only if you wish to change the Com ID setting or visually
inspect and verify the DIP switch settings.

3 - 30
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-15. Dip switch

In most cases, the Com ID configuration made at the factory will not
need to be changed. The factory DIP switch settings produce a Com ID of
1.

3.4.1 Inspect or change the Com ID

To visually inspect and verify the DIP switch settings or to change the
Com ID settings on the multifunction board,

1. Remove the dome from the upper enclosure.

CAUTION
Use caution when accessing an enclosure. A voltage of 115 to 230 VAC, along with
various DC voltages, are present. Failure to follow this precaution may cause injury to
personnel or damage equipment.

2. Loosen the thumb screws on the oven system mounting plate.

Note
Note that MON2000 Com I.D. settings will override the hardware settings. To
use the hardware Com I.D. configuration, enter a zero in the MON2000 Com
I.D. settings. For details, refer to MON2000 Software for Gas Chromatographs
User Manual (P/N 3-9000-522).

3. Carefully lift up the assembly and rotate so that the enclosure


opening is accessible.

3 - 31
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-16. Oven Mounting Bracket

Mounting Bracket
Thumb Screw

4. Locate the multifunction board. It is mounted on a bracket


towards the center of the upper enclosure.

Figure 3-17. Multifunction Board Location

Multifunction
Board

3 - 32
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

5. On the multifunction board, locate the Modbus slave address


(Com ID) DIP switch. It is labeled “S1” and mounted on the lower
right corner of the board.

Figure 3-18. Dip Switch

6. Inspect or change the DIP switch as necessary, using the wiring


diagram as a guide. See Table 3-1.
• Make settings on switch S1 located on the multifunction
board.
• Switches “1” through “5” form a 5-bit binary number for
setting the Modbus slave address (also known as Com ID or
Device ID).
• Switch number “1” is the least significant bit, and switch
number “5” is the most significant bit. Set these switches
either ON or OFF.
• Switch “6” and “7” are spares and switch “8” is used to cold
start the processor. See Table 3-2.

3 - 33
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Use the GC maintenance records to document any changes made to the


switch settings.

Table 3-1. Modbus slave address (COM ID) dip switch settings

Com ID 1 2 3 4 5

1 ON OFF OFF OFF OFF


2 OFF ON OFF OFF OFF
3 ON ON OFF OFF OFF
4 OFF OFF ON OFF OFF
5 ON OFF ON OFF OFF
6 SPARE
7 SPARE
8 COLD START

Table 3-2. Switch positions for cold start

Normal (Run) OFF


Cold Start ON

3.4.2 Preparing for serial connections

The method for operating a Model 700 system is from a connected


personal computer (PC). The PC must be:
• Running MON2000 software (version 2.2 or later). See the MON2000
User Manual (P/N 3-9000-522) for more information.
• Connected to the Model 700 via a serial link.

This section addresses the basic ways to wire a serial connection


between a PC and the GC system.

Before connecting a PC to the Model 700, determine the following:

3 - 34
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

1. What serial ports are available at the PC?


When you select one, consider these points:
• Standard PC serial ports are type
RS-232.
• Usually there are two external serial port jacks on a PC,
located on the rear panel. Most often, they are either DB-9 or
DB-25 male (see below).

Note
Model 700 software upgrades can be installed via any available
communications port.

Figure 3-19. Serial port jacks

• PC serial ports can be used by other peripheral equipment


attached to the PC, such as a printer, mouse, or modem, etc.
To determine which PC serial ports are already being used by
other equipment and which port can be used for connecting
to the GC, note existing serial connections, refer to your PC
user manual, and use diagnostic software (such as Norton
Utilities).

2. What serial ports are available at the GC?


The Model 700 without the FID comes equipped with three serial
ports (standard), unless the customer needs a LOI Interface
connection, then only two com ports are standard. The
installation of the optional Com4A board (with or without a LOI)
brings the total number of available serial ports to six.

3 - 35
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

When you select a serial port, consider these points:


• Com1 and Com2 from the WinSystems CPU board (J1) and
Com4 from the WinSystems CPU board (J6) to Field
Termination board (J5 and J7) (standard configuration)
• Com3 from WinSystems CPU board (J6) to the multifunction
board
• Com4 is reserved for the LOI (Local Operator Interface), if
installed.
The Model 700 with the FID comes equipped with two serial ports
(standard). The installation of the optional Com4A board bring
the total number of available serial ports to six.

When you select a serial port, consider these points:


• Com1 and Com2 from the WinSystems CPU board (J1) to
Field Termination board (J5 and J7) standard configuration
• Com3 from WinSystems CPU board (J6) to the multifunction
board (J4)
• Com4 from the WinSystems board (J6) is connected to the
FID/TCD Preamplifier board (J4)
For additional serial ports, the:
• Optional Com4A board may be installed at the factory. Com5
through Com8 are fully available to the user and are factory-
configured to RS-232 protocol. See Appendix A for additional
options (RS-422/485).
• With the optional Com4A board installed, six Com ports are
available to the user.

3. Is the connection to be made in a …


• Short distance between the PC and GC?
• With temporary or permanent cable connection?
See Section 3.4.3, FTB connection (RS-232).

4. Is the connection to be made with a …


• Short distance between the PC and GC?
• Permanent cable connection (see Section 3.4.4).

3 - 36
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

5. Is the connection to be made with a …


• Long distance between the PC and GC?
• Permanent cable connection (see Section 3.4.5).

3.4.3 FTB connection (RS-232)

The easiest way to connect a PC to the GC is with an off-the-shelf,


straight-through serial cable connected to the GC serial port DB 9-pin
connector pre-wired on the FTB.

1. Obtain a straight-through serial cable with these specifications:

Note
You can buy this cable from most computer supply retailers. If, however, it is
necessary to custom-wire a cable because of circumstances, see guidelines
provided in Appendix B.

• 50 feet long (or less)


• DB 9-pin or DB 25-pin female plug at one end (for PC
connection)
• DB 9-pin male plug at the other end (for GC connection)

2. Connect the serial cable plugs to the appropriate serial port jacks
at the PC and GC. Use the MON2000 software to monitor and
operate the GC as needed.

3.4.4 PC to GC cable short distance connection (RS-232)

The PC-GC connection is made with straight-through serial cable


connected to one of the GC internal serial ports on the FTB.

Note
For detailed information concerning serial communications, refer to Appendix A.

3 - 37
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

If the length of cable can be 50 feet or less, connect the serial cable to
one of the GC serial ports configured for RS-232. (Recall that output
from a standard PC serial port follows RS-232 serial definition.) Cable
that is longer than 50 feet, when used for RS-232 serial transmission, can
result in spurious loss or corruption of data.

To connect your PC to one of the Model 700 serial port jacks:

1. Access the GC’s field termination board, located on the right wall
of the lower enclosure.

Figure 3-20. Field termination board

FTB

2. Choose an available serial port on the FTB (see P/N CE-21157 in


Appendix H) that is configured for RS-232 protocol.

Note
Model 700, standard configuration, has three communications ports available
on the FTB: Com1, Com2 and Com5.

Unless specified by the customer, serial ports are configured for


RS-232.

3 - 38
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Note
Com 4 is dedicated to the Micro-FID/TCD Preamplifier.

For further details, see Figure 3-21 and Figure 3-22.

Figure 3-21. Configuration without Com4A Board

Multifunction FID/TCD
Board Preamplifier Board
Com3 (1) Com4

CPU Field Termination


Board
Com1 Com1
Com2 Com2
Com3 (2)
Com4
Com5
Com6
(1) optional Com7
Com8
(2) standard

3 - 39
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-22. Configuration with Com4A Board


Multifunction FID/TCD
Board Preamplifier Board
Com3 (1) Com4

CPU Field Termination


Board
Com1 Com1
Com2 Com2
Com3
Com4

Com4A

Com5 Com5
Com6 Com6
Com7 Com7
Com8 Com8

(1) optional

Note
Model 700, with the Com 4A board installed, has six communications ports
available on the FTB; Com1 and Com2, and Com5, Com6, Com7, and Com8.

Note
Com 4 is dedicated to the Micro-FID/TCD Preamplifier.

3. Connect the appropriate serial cable.

Note
See Appendix A for instructions on fabricating a direct serial cable.

If using a direct 6 conductor serial cable, connect the exposed


cable leads to the FTB serial port. A pinout of a female DB 9-pin
socket is shown in Figure 3-23.

3 - 40
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-23. FTB Com1 and Com2 DB 9-pin Connector


Com1
P2

5
RI 1 9
DSR 1 4
RTS 1 8
RXD 1 3
CTS 1 7
TXD 1 2
DTR 1 6
DCD 1 1

GND Com2
P3

5
RI 2 9
DSR 2 4
RTS 2 8
RXD 2 3
CTS 2 7
TXD 2 2
DTR 2 6
DCD 2 1

4. Field Termination Board serial communications settings are


shown in Figure 3-24 through Figure 3-28.

3 - 41
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-24. FTB Com 1 DB 9-pin Phoenix Connector


Com1

RS-232 RS-485 RS-422 J5


DCD 1
1
RXD 1 TX/RX+ TX+
2
TXD 1 TX/RX- TX- 3
DTR 1
4
5
DSR 1 RX+
6
RTS 1 RX-
7
CTS 1 8
RI 1 9

Figure 3-25. FTB Com2 DB 9-pin Phoenix Connector

Com2

RS-232 RS-485 RS-422 J7


DCD 2
1
RXD 2 TX/RX+ TX+
2
TXD 2 TX/RX- TX- 3
DTR 2
4
5
DSR 2 RX+
6
RTS 2 RX-
7
CTS 2 8
RI 2 9

3 - 42
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-26. FTB Com5 DB 9-pin Phoenix Connector


Com5

RS-232 RS-485 RS-422 J9


RLSD 5
1
RXD 5 TX/RX+ TX+
2
TXD 5 TX/RX- TX- 3
DTR 5
4
5
DSR 5 RX+
6
RTS 5 RX-
7
CTS 5 8
RI 5 9

Figure 3-27. FTB Com6 DB 9-pin Phoenix Connector


Com6

RS-232 RS-485 RS-422


J13
RLSD 6
1
RXD 6 TX/RX+ TX+
2
TXD 6 TX/RX- TX- 3
DTR 6
4
5
DSR 6 RX+
6
RTS 6 RX-
7
CTS 6 8
RI 6 9

3 - 43
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 3-28. FTB Com7 DB 9-pin Phoenix Connector

Com7

RS-232 RS-485 RS-422 J17


RLSD 7
1
RXD 7 TX/RX+ TX+
2
TXD 7 TX/RX- TX- 3
DTR 7 4
5
DSR 7 RX+
6
RTS 7 RX-
7
CTS 7 8
RI 7 9

Figure 3-29. Com8 DB 9-pin Phoenix Connector GC Phoenix Plug Port


Com8

RS-232 RS-485 RS-422 J18


RLSD 8
1
RXD 8 TX/RX+ TX+
2
TXD 8 TX/RX- TX- 3
DTR 8
4
5
DSR 8 RX+
6
RTS 8 RX-
7
CTS 8 8
RI 8 9

To make an RS-232 serial connection between one of the Phoenix Plug


serial ports of the GC, and an external modem with DB 25-pin serial port,
you will need to manufacture the cable and its DB 25-pin, male plug
cable end as illustrated below. See Figure 3-30.

3 - 44
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-30. GC Phoenix Plug Port to External Modem DB 25-pin Port

3.4.5 Long distance connection (RS-422, RS-485)

RS-422 and RS-485 serial protocols are recommended for longer


distance serial connections between the PC and GC System (i.e.,
distances greater than the 50 feet).

To connect your PC to one of the internal Model 700 RS-422/RS-485


serial port jacks:

1. Obtain the following equipment:


• An asynchronous line driver (or interface device) with RS-232
input and RS-422/RS-485 output. See Appendix A for example
brand and model.
• Shielded, computer-grade, twisted pair cable (to connect the
asynchronous line driver device to the GC).
• A straight-through serial cable (to connect the PC to the line
driver).

2. Connect the straight-through serial cable from the PC serial port


to the RS-232 serial port of the line driver device. Then connect

3 - 45
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

the twisted pair cable to the RS-422/RS-485 serial port of the line
driver.

3. Configure the line driver for data communications equipment


(DCE) operation. See Appendix A for an example configuration.

4. Access the GC FTB (see Figure 3-20 in "Section 3.4.2: Preparing for
serial connections").

5. Choose an available serial port on FTB that is configured for RS-


422 or RS-485 serial protocol, and connect the twisted pair cable
from the line driver. See Appendix A for example connection. Also
see Figure 3-24 through see Figure 3-28 for a list of ports and
terminals assigned for serial communications.

Note
Serial ports Com1 through Com3 are configured by default for RS-232. For
further details or instructions on how to configure these ports to RS- 422/485,
see Appendix A.

3.4.6 GC-Printer wiring

A printer can be connected directly to the GC the field termination board


(FTB) at one of the serial ports. The type and scheduling of reports
produced at the GC printer are determined by settings made in
MON2000 (from the Reports menu, select GC Report Request and/or GC
Printer Control; see the MON2000 Software for Gas Chromatographs User
Manual (P/N 3-9000-522) for more information).

Note
The GC uses only a generic printer driver. The PC printer allows more control and better
quality output.

To connect a printer to the GC serial port:

1. Access the GC FTB (see Figure 3-20 in "Section 3.4.2: Preparing for
serial connections").

3 - 46
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

2. Choose an available serial port on the FTB that is configured for


RS-232 serial protocol.

Note
See Appendix A for a complete listing of the serial ports and corresponding
pinouts to fabricate a serial printer cable.

3. After the wiring connections have been completed, use


MON2000 to configure the GC serial port.
(a.) From the Application menu, select Serial Ports. The Serial
Ports window appears.
(b.) Select the appropriate Port row and set Usage to “Report”,
Protocol to “ASCII” and RW to “W”.
(c.) Ensure that the Com ID setting is correct.
(d.) Leave all other settings at the default values (see the
MON2000 User Manual for more information).

3.4.7 Discrete digital I/O wiring

The Field Termination Board (P/N 3-0700-010) has five discrete outputs
and four discrete inputs. Refer to the MON2000 Software for Gas
Chromatographs Manual (P/N 3-9000-522) and use the Application>User
Defined>Selection menu to to configure the Digital Outputs.

3 - 47
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Note
Configure the Digital Output using the MON2000 Software, from the Application >
User Defined>Selections, set the enable the Common Alarm either Normally Open or
Normally Closed.

3.4.7.1 Discrete digital inputs

To connect digital signal input/output lines to the GC (P/N 3-0700-010):

1. Access the FTB (see Figure 3-31)


(P/N 3-0700-010).

3 - 48
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 3-31. Field termination board

J14

J10

The FTB has five discrete outputs and four discrete inputs. The
discrete input, DIG_IN4, is dedicated to a pressure switch. The
discrete inputs are located on J10 (10 pin Phoenix connector).

2. Route digital I/O lines appropriately, especially in the case of the


explosion-proof enclosure.
There are connections for four digital inputs and five digital
output lines (Phoenix 10-pin connector), as follows:

Table 3-3. FTB discrete digital inputs

J10 Function Description

Pin 1 DIG_IN1
Pin 2 GND
Pin 3 DIG_IN2
Pin 4 GND
Pin 5 DIG_IN3 to customer
Pin 6 GND

3 - 49
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table 3-3. FTB discrete digital inputs

J10 Function Description

Pin 7 DIG_IN4 dedicated to a pressure switch


Pin 8 GND dedicated to a pressure switch
Pin 9 DIG_IN5
Pin 10 GND

3.4.7.2 Discrete digital outputs

The discrete outputs are located on J14 (P/N 3-0700-010) (Phoenix 10-
pin connector) have two “Form A” relays on the FTB. Outputs 3-5 are
Solid State switches with a rating of .375A @30 VDC. The relays, with
sealed enclosures, have a contact current rating of 1.0 Amperes each.

For discrete digital outputs, see Table 3-4.


Table 3-4. FTB discrete digital outputs

J14 Function

Pin 1 DIG_OUT
Pin 2 DIG_OUT
Pin 3 DIG_OUT
Pin 4 DIG_OUT
Pin 5 DIG_OUT_ 3+
Pin 6 DIG_OUT_ 3-
Pin 7 DIG_OUT_ 4+
Pin 8 DIG_OUT_ 4-
Pin 9 DIG_OUT_ 5+
Pin 10 DIG_OUT_ 5-

3 - 50
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3.4.8 Analog input wiring

There are four analog inputs on the Field Termination Board (P/N 3-0700-
010 and drawing CE-21157) located at J4 (12-pin Phoenix connector).
Table 3-5. FTB analog inputs

J4 Function

Pin 1 VIN+_1
Pin 2 VIN-_1
Pin 3 Shield
Pin 4 VIN+_2
Pin 5 VIN-_1
Pin 6 Shield
Pin 7 VIN+_3
Pin 8 VIN-_1
Pin 9 Shield
Pin 10 VIN+_4
Pin 11 VIN-_1
Pin 12 Shield

3.4.9 Analog output wiring

There are four standard analog outputs on the standard FTB (P/N 3-
0700-010 and drawing CE-21157); located at J8 (12-pin Phoenix
connector). Additionally, if installed, the optional analog board has eight
analog outputs
Table 3-6. FTB analog outputs

J8 Function

Pin 1 IOUT+_1
Pin 2 IOUT-_1
Pin 3 Shield
Pin 4 IOUT+_2
Pin 5 IOUT-_2

3 - 51
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table 3-6. FTB analog outputs

J8 Function

Pin 6 Shield
Pin 7 IOUT+_3
Pin 8 IOUT-_3
Pin 9 Shield
Pin 10 IOUT+_4
Pin 11 IOUT-_4
Pin 12 Shield

There are eight analog outputs on the optional analog output board (P/N
2-3-0580-037 and drawing CE-21157); located at J3 (24-pin Phoenix
connector):
Table 3-7. Optional analog outputs

J3 Function

Pin 1 IOUT+_5
Pin 13 IOUT-_5
Pin 2 Shield
Pin 14 IOUT+_6
Pin 3 IOUT-_6
Pin 15 Shield
Pin 4 IOUT+_7
Pin 16 IOUT-_7
Pin 5 Shield
Pin 17 IOUT+_8
Pin 6 IOUT-_8
Pin 18 Shield
Pin 7 IOUT+_9
Pin 19 IOUT-_9
Pin 8 Shield
Pin 20 IOUT+_10
Pin 9 IOUT-_10

3 - 52
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Table 3-7. Optional analog outputs

J3 Function

Pin 21 Shield
Pin 10 IOUT+_11
Pin 22 IOUT-_11
Pin 11 Shield
Pin 23 IOUT+_12
Pin 12 IOUT+_12
Pin 24 Shield

3.4.10 Optional boards

Optional modem boards are available for the Model 700 GC.

The jumper settings and pinouts for each board is shown below.

3.4.10.1 Optional WinSystems Modem

Table 3-8. J8 Modem Board Jumper Settings

Pin(s) Position

1 and 2 In
3 and 4 In
5 and 6 In
7 and 8 In

Table 3-9. J9 Modem Board Jumper Settings

Pin(s) Position

1 and 2 In

5 and 6 In

3 - 53
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table 3-10. J10 Modem Board Jumper Settings

Pin(s) Position

1 and 2 In

3 and 4 In

5 and 6 In

9 and 10 In

15 and 16 In

3.4.10.2 Optional Radicom Modem Settings

Table 3-11. J26 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table 3-12. J27Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table 3-13. J30 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

3 - 54
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Table 3-14. J31 Radicom Modem Jumper Settings

Pin(s) Position

2 and 3 In

3.5 Leak checks and purging for


first calibration
Apply AC power to the unit after verifying all electrical connections are
correct and safe. Ensure that all interconnections and external signal
connections have been verified and proper grounds have been made
before turning on the power.

3.5.1 Initial leak check

The focus of this section is for field connections to the analyzer, during
the installation process. See “Leak checks” on page 4-26 for an in depth
discussion of analyzer leak checks.

3.5.1.1 Carrier gas line leak checks

1. Plug the Measure Vent (labeled “MV”) to block the free flow of
Carrier Gas through the GC.

Note
The GC does not have an inline Block Valve to shut off the Carrier Gas flow.

2. Slowly pressurize the “GC side” of the Carrier Gas to 110 psig (±2
percent) with the dual-stage regulator at the Carrier Gas cylinder.

3 - 55
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

3. After two minutes, shut off the Carrier Gas bottle valve by turning
it clockwise. Then, observe the high-side regulator gauge on the
Carrier Gas bottle.
• The gauge should not bleed down more than 200 psig in 10
minutes.
• If Carrier Gas is lost at a faster rate, then all tube fittings
between the Carrier Gas bottle and the GC (including the
dual-stage regulator) must be checked for leaks and
tightened if necessary.
Most leaks at this stage (Installation and Setup) are usually
found between the Carrier Gas bottle and the GC.
The dual-stage regulator fitting connecting to the Carrier
bottle, may not seat properly with some Carrier Gas bottles
and allow a leak. If this occurs, carefully wrap a small length of
Teflon tape around the tip of the inlet tube on the dual-stage
regulator (which sits against the Carrier Gas bottle valve seat).

4. Once the GC passes the “Initial leak check”, reopen the Carrier
Gas bottle valve and remove the Measurement Vent (MV) plug.

3.5.1.2 Calibration line leak check

1. Slowly pressurize the Calibration line (up to 20 psig).

2. Block-in the line by turning the “Cal Stream” blocking valve


clockwise until seated.

3. Shut off the Calibration gas at the gas bottle by turning the valve
clockwise.

4. Observe the high-side of the Calibration gas dual-stage regulator


making sure the pressure holds. The pressure should not
decrease for a period of two to three minutes.

5. When the GC passes the “Initial Calibration Gas leak check”, re-
open the Calibration gas bottle valve and the in-line “Cal Stream”
block valve.

3 - 56
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3.5.1.3 Sample lines (streams) leak check

1. Slowly pressurize the Sample line (up to 20 psig).

2. Block-in the line.

3. Observe the regulator, making sure the pressure holds. The


pressure should not decrease for a period of two to three
minutes.

4. When the GC passes the “Initial Sample Gas leak check”, re-open
the Sample Gas lines.

3.5.2 Purging carrier gas lines

Purging carrier and calibration gas lines requires AC power. Use Helium
that is 99.995% pure and that has less than 5ppm water and less than
0.5ppm hydrocarbons.

Note
Tubing should be clean and dry internally. During installation, the tubing should have
been blown free of internal moisture, dust, or other contaminants.

To purge the carrier gas lines,

1. Ensure that the MV vent line plug has been removed, and the vent
line is open.

2. Ensure that the carrier gas bottle valve is open.

3. Set the carrier gas line pressure at 110 psig. Use the dual stage
regulator at the carrier gas bottle to adjust pressure.

Note
Do not use the “Carrier Pressure Adjust” regulator adjustment (on the Flow Panel
Assembly) to adjust carrier gas line pressure. This pressure is factory-set and should not
be adjusted.

3 - 57
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4. Turn ON the AC power to the GC.

5. Establish communications with the GC via the MON2000


software. (Use the File > Quick Connect menu path; see Section
2.7.2 in the MON2000 Software for Gas Chromatographs User
Manual (P/N 3-9000-522) for more information.)

6. Use the Applications>Temperature Control menu path to access this


function. The readouts of the block, column and SSS heater
controllers should indicate that the unit is warming up. Also, the
yellow and red status indicators on the FTB4 should be on.

7. Allow the GC system temperature to stabilize and the Carrier Gas


lines to become fully purged with Carrier Gas.

8. Select the Auto Sequence Function. Use the Control > Auto
Sequence menu path described in Section 4 of the MON2000
Software for Gas Chromatographs User Manual (P/N 3-9000-522).

Note
A period of 4 to 8 hours (or overnight) is recommended, during which all of the
settings described in Steps 1 through 7 are maintained. No other settings
should be made.

3.5.3 Purging calibration gas lines

To purge the calibration gas lines, as preparation for first calibration:

1. Ensure that the Carrier Gas lines have been fully purged, as
described in the previous section, and that the SV plug has been
removed.

2. Close the calibration gas bottle valve.

3. Fully open the block valve associated with calibration gas feed
(the block valve should be located on lower right-hand corner of
the front panel).
See Section 5.8 in the MON2000 Software for Gas Chromatographs
User Manual (P/N 3-9000-522) for instructions on selecting
streams.

3 - 58
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

4. Open the calibration gas bottle valve.

5. At the calibration gas bottle regulator, increase outlet pressure to


20 psig, ±5%.

6. Close the calibration gas bottle valve.

7. Let both gauges on the calibration gas bottle valve bleed down to
0 (zero) psig.

8. Repeat Steps 4 through 7, five times.

9. Open the calibration gas bottle valve.

3.6 System startup

To perform system start-up,

1. For system startup, run an analysis of the calibration gas.


If equipped with an optional stream switching board, ensure that
the stream switch for the calibration stream is set to AUTO.
Otherwise, ensure that the calibration gas supply is turned on and
set to the correct pressure (25 to 30 PSIG).
Using the MON2000 software, run a single stream analysis on the
calibration stream. Once proper operation of the GC is verified,
halt the analysis.
Use the Control > Calibration and Control > Halt menu
paths; see Sections 4.3 and 4.4 in the MON2000 Software for Gas
Chromatographs User Manual (P/N 3-9000-522) for more
information.

2. Start Auto Sequence of the line gas stream(s).


Use the Control > Auto Sequence menu path; see Section 4.1 in
the MON2000 Software for Gas Chromatographs User Manual (P/N
3-9000-522) for more information. The GC will begin the Auto
Sequence analysis mode.

3 - 59
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

This page is intentionally left blank.

3 - 60
Section 4: Maintenance and troubleshooting
4--

4.1 Hazardous environments

WARNING
Observe all precautionary signs posted on the Model 700 enclosure. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.

WARNING
ATEX certified units must be installed strictly in compliance with the requirements of
IEC 60079-14.

Special conditions for safe use must be met. The maximum constructional gap (ic) is
less than that required by Table 2 of EN 60079-1:2007.

Before opening the Model 700 enclosure, reduce the risk of igniting hazardous
atmospheres by disconnecting the equipment from all power supplies. Keep the
assembly closed tightly when in operation to reduce the risk of igniting hazardous
atmospheres. Inlet (incoming) wiring must meet local standards (i.e. in conduit with
seal fitting within 18 or via cable glands certified to IEC 60079-1). Upper enclosure
threaded entry is ¾ NPT. Lower enclosure threaded entries are M32-1.5.

Observe all precautionary signs posted on the Model 700 enclosure. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.

Please direct all health, safety and certification related questions to: Emerson Process
Management, Gas Chromatographs, Applications Engineering Group, 713-827-6380 or
1-866-GC Center (1-866-422-3683).

4-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4.2 Troubleshooting and repair concept

The most efficient method for maintaining and repairing the Model 700
GC system is a component-replacement concept that allows you to
return the system to operation as quickly as possible. Sources of trouble,
such as printed-circuit assemblies, valves, etc., are identified during
troubleshooting test procedures and are replaced at the lowest level
practical with units in known working order. The defective components
are then either repaired in the field or returned to Measurement Services
for repair or replacement.

4.3 Routine maintenance

The Model 700 GC system will perform accurately for long periods with
very little attention (except for maintaining the Carrier Gas cylinders). A
bimonthly record of certain parameters will assist greatly in assuring that
your Model 700 is operating to specifications. The maintenance checklist
should be filled out bimonthly, dated, and kept on file for access by
maintenance technicians as necessary.This gives you a historical record
of the operation of your Model 700, enables a maintenance technician to
schedule replacement of gas cylinders at a convenient time, and allows
quick troubleshooting and repair when it becomes necessary.

A chromatogram, a Configuration Report, and a Raw Data Report should


also be made and filed with the checklist, furnishing a positive dated
record of the Model 700. The chromatogram and reports can also be
compared to the chromatograms and reports run during the
troubleshooting process.

4.3.1 Bimonthly maintenance checklist

Copy the sample maintenance checklist as necessary for your files. If you
have a problem, please complete the checklist and reports, and have the
results available when calling Measurement Services with a problem.
Also have the Sales Order number. The Sales Order number can be found
on the nameplate located on the left side wall of the upper housing of
the Model 700. The chromatograms and reports archived when your
Model 700 left the factory are filed by this number.

4-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

MAINTENANCE CHECKLIST

Date Performed: _______________ Sales Order Number: _______________

System Parameters As Found As Left

Carrier Gas Cylinder


Cylinder Pressure Reading (High) _____ psig _____ psig
Cylinder Pressure Outlet Reading _____ psig _____ psig
Cylinder Pressure Panel Regulator _____ psig _____ psig

Sample System
Sample Line Pressure(s) (1)_____ psig _____ psig
(2)_____ psig _____ psig
(3)_____ psig _____ psig
(4)_____ psig _____ psig
(5)_____ psig _____ psig

Sample Flows (1)___ cc/min ___ cc/min


Sample Vent 1 (SV1) (2)___ cc/min ___ cc/min
Sample Vent 2 (SV2) (3)___ cc/min ___ cc/min
(4)___ cc/min ___ cc/min
(5)___ cc/min ___ cc/min

Calibration Gas
High Pressure Reading _____ psig _____ psig
Outlet Pressure Reading _____ psig _____ psig
Flow ___ cc/min ___ cc/min

4- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4.3.2 Routine maintenance procedures

• Complete the maintenance checklist bi-monthly. Place the sales


order number, date, and time on the form and file it. This gives you a
basis for comparison in the future if you need it.
• Save a Chromatogram of the operating Model 700 on the PC with the
MON2000 software. Print Configuration, Calibration, and Raw Data
reports and file them with the MON2000.
• Check the printer paper (if used) to ensure that a sufficient supply of
paper remains. Check carrier and calibration gas supplies.

4.3.3 Contact service

Measurement Services offers maintenance service programs that are


tailored to fit specific requirements. Contracts for service and repair can
be arranged by contacting Measurement Services at the address or
telephone number on the Customer Repair Report at the back of this
manual.

4.4 Access to GC equipment elements

4.4.1 Electrical/electronic components

WARNING
The explosion-proof housing should not be opened when the unit is exposed to an
explosive environment. If access to the explosion-proof housing is required,
precautions must be taken to ensure that an explosive environment is not present.
Failure to do so may result in injury or death to personnel or cause damage to the
equipment.

The Model 700 electrical/electronic components are located in the


upper and lower explosion-proof housings. All of the electrical/electronic
components are fully accessible from the front and top of the Model 700.

4-4
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-1. Model 700 with TCD/Micro-FID Front View

Model 700 with TCD Upper Enclosure

• Multifunction Board
• Dual Methods Adapter Board
• Dual Methods Preamplifier Board
• Solenoid Heater/Driver Board

Model 700 with TCD Lower Enclosure

• WinSystems CPU Board


• Analog Board
• Analog Board (optional)
• Com4A Board (optional)
• Radicom Modem board (optional)
• DC/DC Field Termination Board

4- 5
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Model 700 with Micro-FID/TCD Upper Enclosure

• Multifunction Board
• Solenoid/Heater Driver Board
• FID/TCD Preamplifier Board
• FID/TCD Preamplifier Power Supply Board
• FID Connector Board

Model 700 with Micro-FID/TCD Lower Enclosure

• Field Termination Board


- Backplane Board
- Interconnect Board
- WinSystems CPU (with PC104 interface)
- Com4A PC/104 Board (optional)
- Radicom Modem Board (optional)

Note
The optional Radicom Modem is always mounted on top of the PC/104 card
stack.

- Eight Channel Analog (non-isolated


4-20mA) Output Board (optional)
- Four Channel Analog (isolated 4-20mA) Output Board (optional)
- Front Panel Analytical and Stream Switch Panel
- Dual Methods Adapter Board

4.4.2 Detector elements, heater elements, valves and


columns

The detector elements, heater elements, valves and columns are located
in the upper explosion-proof housing of the Danalyzer Pro GC.

Remove the thermal cover and insulating shield to gain access to these
components.

4-6
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-2. Upper Explosion-proof Housing

Thermal
Cover

The detector elements, including the FID, are located in the block (TCD)
and on the FID Base attached to the valve block.

4- 7
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-3. Thermal Conductivity Detector

Thermal
Conductivity
Detectors

Figure 4-4. Flame Ionization Detector

FID

FID Block

There are five heater elements: three valve block heaters, the column
heater, and the stream switching system heater.

4-8
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

The stream switching heater is a cartridge heater inserted into the


stream switch block (manifold).

The column heater is a cartridge heater located in the middle of the


column mandrel.

The block heaters are cartridge heaters located in the corners of the
block. Column and block heaters are identical and are installed from the
underside of the manifold (plastic base) of the oven.

4.5 Precautions for handling pc assemblies

Printed circuit assemblies contain CMOS integrated circuits, which can


be damaged if the assemblies are not properly handled. The following
precautions must be observed when working with the assemblies:
• Do not install or remove the Model 700 printed circuit assemblies
while power is applied to the units.
• Keep electrical components and assemblies in their protective
(conductive) carriers or wrapping until ready for use.
• Use the protective carrier as a glove when installing or removing
printed circuit assemblies.
• Maintain contact with a grounded surface to prevent static discharge
when installing or removing printed circuit assemblies.

4.6 General troubleshooting


This section contains general troubleshooting information for the Model
700. The information is arranged as appropriate either by major
subsystems or by major functions of the instrument. See Table 4-1 for
frequent possible causes of the hardware alarms.

Note
Correct ALL alarms before re-calibration.

4- 9
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4.6.1 Hardware Alarms

Use the following table to identify the alarm and possible cause to
remedy the problem.
Table 4-1. Basic Hardware Troubleshooting via Alarms

Alarm Possible Cause

Application Checksum Failure DiskOnChip

ROM Checksum Failure DiskOnChip

RAM Diagnostics Failure bad RAM

Micro-FID/TCD Preamplifier
Alarms
extinguished flame
Micro-FID Temperature High
Micro-FID Comm. Failure

Analog Output 1 High Measured value program for Analog Output 1 is


greater than user-defined full scale range.

Analog Output 2 High same as Analog Output 1 High


Analog Output 3 High same as Analog Output 1 High
Analog Output 4 High same as Analog Output 1 High
Analog Output 5 High same as Analog Output 1 High
Analog Output 6 High same as Analog Output 1 High
Analog Output 7 High same as Analog Output 1 High
Analog Output 8 High same as Analog Output 1 High
Analog Output 9 High same as Analog Output 1 High
Analog Output 10 High same as Analog Output 1 High
Analog Output 11 High same as Analog Output 1 High
Analog Output 12 High same as Analog Output 1 High

Analog Output 1 Low Measured value program for Analog Output 1 is


lower than user-defined zero range.

4 - 10
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Table 4-1. Basic Hardware Troubleshooting via Alarms (Continued)

Alarm Possible Cause

Analog Output 2 Low same as Analog Output 1 Low


Analog Output 3 Low same as Analog Output 1 Low
Analog Output 4 Low same as Analog Output 1 Low
Analog Output 5 Low same as Analog Output 1 Low
Analog Output 6 Low same as Analog Output 1 Low
Analog Output 7 Low same as Analog Output 1 Low
Analog Output 8 Low same as Analog Output 1 Low
Analog Output 9 Low same as Analog Output 1 Low
Analog Output 10 Low same as Analog Output 1 Low
Analog Output 11 Low same as Analog Output 1 Low
Analog Output 12 Low same as Analog Output 1 Low

Analog Input High 1 Measured value program for Analog Input 1 is


greater than the user-defined full scale range.

Analog Input High 2 Same as Analog Input 1 High


Analog Input High 3 Same as Analog Input 1 High
Analog Input High 4 Same as Analog Input 1 High

Analog Input Low 1 Measured value program for Analog Input 1 is


lower than the user-defined full scale range.

Analog Input Low 2 Same as Analog Input 1 Low


Analog Input Low 3 Same as Analog Input 2 Low
Analog Input Low 4 Same as Analog Input 3 Low

Preamp Input 1 Out of Range Indicates either Carrier Gas gone; air not purged
from carrier lines; power failure; bad
thermistors; preamp out of balance or failed;
analyzer temperature low; interconnection
wiring.

Preamp Input 2 Out of Range same as Preamp Input 1 Out of Range

Preamp Input 3 Out of Range same as Preamp Input 1 Out of Range

4 - 11
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table 4-1. Basic Hardware Troubleshooting via Alarms (Continued)

Alarm Possible Cause

Preamp Input 4 Out of Range same as Preamp Input 1 Out of Range

Preamp Failure same as Preamp Input 1 Out of Range

Analyzer Failure Indicates either the Carrier Gas is low (below 90


psig at Carrier Gas bottle) or gone; a bad
solenoid; a Carrier Gas leak in system.

Power Failure GC Controller has experienced a re-start since


alarms were last cleared, caused by power
failure. Automatically starts in RUN mode and
runs calibration gas until it identifies all retention
times or for a maximum of two hours before
switching to line gas.

TCD
Fused Peak Overflow - Noisy Air not purged from carrier lines; bad
Baseline thermistors; shields.

RF% Deviation Calibration gas low or out; valve timing error;


faulty auto-calibration solenoid.

Warm Start Calibration Failure same as RF% deviation

Valve Timing Failure same as RF% deviation

4.6.2 Troubleshooting checklist

An online gas chromatograph can operate properly only if flows are


balanced and constant, the temperature is constant, no leaks are
present, and the GC Controller is correctly timed. Before going through
the troubleshooting procedures, perform the routines of the Basic
Hardware Troubleshooting via Alarms. Checklist records performed
regularly may indicate problems and prevent any sudden breakdown.

Use the MON2000 software in the offline mode and select Logs >
Parameter List from the drop-down menu and open a saved *.par file.
Do not adjust any values if they are within the nominal tolerance values
on the Checklist. Compare the values with those obtained in preceding
weeks. This may pinpoint your problem immediately.

4 - 12
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

The following is a guide for troubleshooting if a problem with sample


analysis occurs. See Table 4-1 for diagnostic data. This data will be useful
if it becomes necessary to call Measurement Services for assistance.
Table 4-2. Troubleshooting Checklist

Description As Found As Left Notes

Analyzer

Leak check with Snoop from


Carrier Gas bottle to Analyzer
regulator.

Leak check with Snoop from


calibration standard to auto-
calibration solenoid.

Pre-amp balance voltage

___________mV _________mV 0 (±0.5 mV)


Sample System

Leak check with Snoop from


sample probe to sample solenoid

4 - 13
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table 4-2. Troubleshooting Checklist

Description As Found As Left Notes

Controller Inputs

GRI (CH.1) 0.0 - 0.0


GRI (CH.2) 0.8 - 1.2
GRI (CH.3) 0.8 - 1.2
GRI (CH.4) 0.8 - 1.2
____________ ___________ 4800 to 6400
Value (12-bit AD) ____________ ___________ 4800 to 6400
PAZ1 ____________ ___________ 4800 to 6400
PAZ2 ____________ ___________ 9200 to 12000
PAZ3
PAZ4
____________ ____________ -32767 to 32767
Value (16-bit AD) ____________ ____________ -32767 to 32767
GC 1 ____________ ____________ -32767 to 32767
GC2
____________ ____________ -32767 to 32767
GC3
GC4

4 - 14
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Table 4-2. Troubleshooting Checklist

Description As Found As Left Notes

Power Supply (DC — DC) Note: See Figure 4-5


through Figure 4-8 for test
Input Voltage Ranges: point locations.
(24.5V - 26.5VDC)
FTB:
+ 12V @ 0.25A (± 0.6)
+ 5V @ 3A (± 0.25V)
- 3.8V @ 0.1A (± 0.2V)
- 12 V @ 0.25A (C 0.6V)
Dual Methods Adapter:
+ 20V @ 0.35A (± 1V)
- 20V @ 0.35A (± 1V)
+ 5VDC (± 0.25V)
Note: The Dual Methods
Board is used on Model 700
GCs with 2350A
Controllers.
SOL/HTR Driver:
Power Supply (AC — DC)
N/A
Input Voltage Range:
Output Voltage/Current:
(90—130/180-264 VAC)
(Auto-ranging) 24.0VDC
Output Power:
Continuous load demand
power, measured at the
Output Terminals of the
Power Supply, shall not
exceed 140 Watts.

4 - 15
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table 4-2. Troubleshooting Checklist

Description As Found As Left Notes

Chromatogram

Check baseline

Check component values on


report

Number of peaks

Retention times

Date and file


Temperature

Column Module Temperature ____ °C ____°C 79.80 - 80.20 °C


____ °F ____°F 175.64 - 176.36 °F

Valve Block Temperature ____°C ____ °C 79.80 - 80.20 °C


____°F ____ °F 175.64 - 176.36 °F

Stream Switching System ____ °C ____ °C 64.0 - 66.0 °C


____ °F ____ °F 147.2 - 150.8 °F

Sample System Temperature ____ °C ____ °C **

4 - 16
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Table 4-2. Troubleshooting Checklist

Description As Found As Left Notes

Measure Vent Flow

Valve 3 ON ___ cc/min ____ cc/min Flow should be as specified


on the Parameter List for
Valve 3 OFF ___ cc/min ____ cc/min
the particular GC (from
MON2000 use
Logs>Parameter List menu
path to access the list).
Check the flow using a
portable electronic flow
meter or a mechanical flow
meter like a Set-a-Flo. If a
RotameterTM is
permanently installed it will
cause baseline noise.

Note
Refer to System Operational Parameters.

4.6.3 Test points dual methods board and FTB

This section applies to Model 700 GCs with the TCD and 2350A
Controllers. If your Model 700 GC is equipped with an FID or LSIV this
section does not apply.

Use the test points in Figure 4-5 through Figure 4-8 to ensure that the
voltage meets specifications on the dual methods adapter board and the
field termination board. See Table 4-2 for voltage specifications.

4 - 17
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-5. Test Points Dual Methods Board (Cut View)

Test Points

Figure 4-6. Test Points Dual Methods Board

Dual Methods Bd. Test Points

4 - 18
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-7. Test Points Field Termination Board (Cut View)


FTB Test Points

Figure 4-8. Test Points Field Termination Board


Test Points

4 - 19
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4.6.4 Preamplifier

The preamplifier (P/N 3-0580-002) has no parts that may be serviced in


the field. If the unit fails, return it to Measurement Services for repair or
replacement.

4.6.5 Flow balance check

Ensure that the flow panel gauge is properly set. Refer to the Model 700
Troubleshooting Checklist for values. Do not adjust; check with
Measurement Services if your reading is abnormal.

Check the flow at the measure vent and sample vent.

4.6.6 Temperature

Use the Temperature Control function for monitoring the Temperature


of the Oven (Detector/s and Columns) and the Stream Switching block
to determine when the MON2020 Software for Gas Chromatographs is
thermally stable. The bottom row labeled Temperature (C) displays the
current temperatures.

The settings and values shown in Figure 4-9 and described in Table 4-3
are preset at the factory and are based on the specific customer
application. These values should not be changed unless recommended
by Application Engineering or Customer Service Personnel, or it is a
factory application requirement.

When connected via MON2000, use the Application>Temperature


Control menu path to access this function.

The Temperature Control dialog displays.

4 - 20
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-9. Temperature Control Dialog

Use the pull down menu to select the appropriate mode setting (e.g.
AUTOMATIC, MANUAL, or OUT OF SERVICE). Ensure that the
temperature is constant for the Oven (i.e. Multivalve System block and
column module kit) and the SSS.

Columns 1 through 3 (Zones 1-3) have a temperature range of 20 oC to


100 oC (68 oF to 212 oF). Column 4 (Zone 4) has a temperature range of
20 oC to 450 oC (68 oF to 842 oF).
Table 4-3. Temperature Control Dialog

Zone Function Typical Setting

1 Detector/s or Block Temperature 80 oC (176.0 oF)

2 Column Temperature 80 oC (176.0 oF)

3 Sample Stream Block or ValcoTM Valve 40 oC (104 oF)


60 oC (140 oF)

4 - 21
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table 4-3. Temperature Control Dialog

Zone Function Typical Setting

4 Spare N/A
Or, Methanator 300 oC (572 oF)
150 oC (302 oF)
Or, LSIV

4.6.7 FID configuration

When connected to the GC via MON2000, use the Application>FID


Configuration menu to access the FID Configuration dialog. Refer to the
MON2000 Software for Gas Chromatographs User Manual (P/N 3-9000-
522) for additional configuration details.

Figure 4-10. FID Configuration window

Configure the following fields from the FID Configuration dialog:


• FID Ignition - Manual or Automatic
• Number of Ignition attempts
• Wait time between attempts

4 - 22
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

• Igniter ON duration
• Flame ON sense temperature Degrees C
• Flame OUT sense temperature Degrees C
• Electrometer (TCD) gain

4.6.8 Baseline noise

Baseline noise is any perturbation on the detector output that is not


related to an eluted solute. It is a fundamental property of the detecting
system and determines its maximum sensitivity. Baseline noise can be
divided into the following three types:
• Short term noise
• Long term noise
• Drift

Short term noise results from baseline upsets that have frequencies
significantly higher than those of an eluted peak. Short term noise is not
a serious problem as it is easily removed by appropriate noise filters
without significantly affecting the profiles of the peaks. Its source usually
originates from either the detector sensor system or the preamplifier.

4 - 23
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-11. An example of baseline noise

Long term noise results from baseline upsets that have frequencies similar
to those of an eluted peak. This type of noise is the most damaging
because it can not be differentiated from very small peaks. Long term
noise cannot be removed by electronic filtering without affecting the
profiles of the eluted peaks. Long term noise usually arises from
temperature, pressure or flow rate changes in the sensing cell. It is this
noise that ultimately limits the sensitivity of the detector.

A noisy baseline can be caused by carrier leaks, an electronic failure in


the preamplifier, a faulty power supply, imbalance of carrier flow or
defective thermistors in the detector.

4 - 24
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Baseline drift results from baseline upsets that have frequencies that are
significantly larger than those of the eluted peak. Drift is almost always
due to either changes in ambient temperature, changes in mobile flow
rate, detector cell pressure or column bleed in the GC. Drift is easily
controlled by choosing operating parameters that are within detector
and column specifications.

Figure 4-12. An example of baseline drift

Ensure that no evidence of component elutions is present when sample


is not being injected.

4 - 25
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

To ensure that the baseline is not drifting, compare the baseline upsets
caused by valve actuations with those of the spectrum chromatogram
provided with the Operational Parameters Sheet.

If differences exist between the two spectrum chromatograms, the


problem may be due to one or more of the following:
• Programming of events.
• Leaks in the carrier system.
• Column deterioration due to liquid contamination from a sample.

A noisy baseline can be caused by carrier leaks, an electronic failure in


the preamplifier, a faulty power supply, or defective thermistors in the
detector. If the baseline is still noisy after correcting for leaks, perform
the Detector Bridge Balance procedure on page 53 before replacing the
detector thermistors or the preamplifier board.

4.7 Leak checks

4.7.1 Field service

To perform a field-service leak check of the Model 700,

1. Plug all Model 700 vents.

2. Make sure the setting of the carrier cylinder regulator is 115 psig
(pounds per square inch, gauge).

3. Check all fittings at the pressure regulator flow panel and at the
carrier cylinder regulator with a leak detector. Correct any leaks
detected by a bubble indication.

4. Turn the Carrier Gas shut-off valve clockwise to close. Observe the
carrier pressure for ten minutes to check for a drop in carrier
pressure.
The drop should be less than 200 psig on the high side of
the regulator/gauge. If the carrier pressure remains
constant, no leaks are present.

4 - 26
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

5. Use MON2000 to manually actuate the valves ON and OFF and


observe the pressure with the valves in different positions.

Note
When the valves are switched, some pressure change is normal because of
carrier loss. Momentarily open the cylinder valve to restore pressure if
necessary.

6. If the pressure does not hold constant, check all valve fittings for
tightness.

7. Repeat Step 5. If leaks persist, check the valve ports with a


commercial gas leak detector.

Note
Do not use a liquid leak detector on the valve or components within the MVS
insulated cover.

4.7.2 Factory level leak check

This section describes how to perform a factory-level leak check. Before


performing the leak check, plug the Measure Vent (labeled “MV”) vent
line if it is open. The Sample Vent (labeled “SV”) line should be left open,
or unplugged.

The following steps are performed to leak-check the Model 700 at the
factory when the unit is quality-checked prior to release. This procedure
is more thorough and is designed to isolate specific zones where a leak
may occur.

Leak check the Carrier Gas line first, according to the steps that follow.

1. Purge the valves with Carrier Gas:


(a.) Open the Carrier Gas bottle valve and slowly increase the
Carrier Gas feed line pressure to 110 psig, ±2%, with a
dual-stage regulator at the Carrier Gas bottle.

4 - 27
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Note
Do not use the “Carrier Pressure Adjust” valve (on the Flow Panel of the Model
700 GC) to adjust Carrier Gas line pressure. The valve is factory-set and should
not be adjusted.

(b.) Using MON2000, manually actuate the valves ON and OFF


about four to five times.

2. Pressurize and check the Carrier Gas feed line:


(a.) Set all Model 700 valves to ON.
(b.) Open the Carrier Gas bottle valve, and ensure that the
Carrier Gas feed line pressure is 110 psig, ±2%.
(c.) Shut the Carrier Gas bottle valve.
(d.) Observe the pressure on the high-side regulator gauge of
the Carrier Gas bottle. Because the MV vent line is
plugged, the pressure should not decrease in 2 to 3
minutes.
(e.) Set all valves to OFF position.
(f.) Repeat Steps (b) through (d).
(g.) Via MON2000, set all valves to AUTO for regular operation.

Next, leak check the calibration gas feed line, per the following steps:

Note
Calibration gas line pressure of 50 psig is for leak check and test purposes only. For
normal operation, the calibration gas line pressure is maintained at 20-30 psig.

1. Plug the SV vent line.

2. Pressurize the calibration gas line to


50 psig.
(a.) Shut the calibration gas bottle valve.
(b.) Observe the pressure on the high-side regulator gauge of
the calibration gas bottle. Because the SV vent line is
plugged, the pressure should not decrease in a period of 2
to 3 minutes.

4 - 28
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Next, leak check the sample gas lines, per the following steps:

1. Ensure that the Sample valve (SV) vent line is plugged.


(a.) Pressurize the sample gas line to 50 psig or a known
pressure.

Note
Calibration gas line pressure of 50 psig is for leak check and test purposes only.
For normal operation, the calibration gas line pressure is maintained at 20-30
psig.

(b.) Shut off the sample gas.


(c.) Observe the pressure on any gauge that indicates pressure
between the closed sample gas block valve and the
plugged SV vent line. Because the line is plugged, the
pressure should not decrease during a period of 2 to 3
minutes.

2. Leak test all other sample stream lines by connecting gas to each
of the sample streams and repeating Step 1(a) through 1(b).

Finish the test and set up the Model 700 for normal operation, as follows:

1. Using MON2000, ensure that all valves are set to AUTO.

2. Unplug, or open, the MV and SV vent lines.

3. If the calibration gas bottle was used to leak check the sample
stream lines, reconnect the calibration gas bottle to the
calibration gas line on the flow panel assembly. Reconnect the
sample stream lines.

4.7.3 Plugged Lines, Columns, or Valves

To ensure that lines, columns, and valves are not plugged, check the gas
flow at valve ports. For a reference, use the flow diagram in the drawing
package, and remember these points about flow diagrams:
• Port-to-port flow paths are indicated by solid or dashed lines.

4 - 29
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

• A dashed line indicates flow direction when the valve is ON, that is,
energized.
• A solid line indicates flow direction when the valve is OFF, i.e., not
energized.
• A combination of solid and dashed lines indicates a constant flow
path regardless of the ON/OFF state of the valve.

Figure 4-13. Chromatograph valve assemblies

6-port Valve 10-port Valve

Only minimal repair and maintenance is required by the customer (e.g.,


replacing the diaphragms). Measurement Services recommends
returning the Oven Assembly for major repairs to maintain the validity of
the warranty.

4.7.4 Required tools

The tools required for performing repair and general maintenance on the
valve assemblies are:
• Torque wrench, scaled in foot-pounds
• 1/2” socket
• 1/4” open-end wrench

4 - 30
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

• #1 flat screwdriver

4.7.5 Chromatograph valve replacement parts

Note
If an existing unit has a teflon gasket between the lower actuation diaphragms and the
kiosk block, install gasket P/N 2-4-0700-064 (for 6-port valves) and P/N 2-4-0700-160
(for 10-port valves). Otherwise, the teflon gasket is not required.

Replacement parts required for each of the chromatograph valves on the


Oven Assembly consists of the following parts:
• Diaphragm Kit 6-port Valve (P/N 2-4-0700-187)
• Diaphragm Kit 10-port Valve (P/N 2-4-0700-171)

4.7.6 Valve Assembly and Disassembly

Perform valve maintenance in a clean and dry area. Assembly and


disassembly procedures are the same for 6-port and 10-port valves.

To disassemble a valve, unscrew the torque bolt and then flip the valve
over so that the bolt is pointed toward the floor.

4 - 31
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-14. Disassembled valve

torque bolt

The dismantled valve contains the following parts:


• Three plates
• Three short pistons
• Three long pistons
• Four types of diaphragms
- One sealing diaphragm
- One cushion diaphragm
- Two upper actuator diaphragms
- Two lower actuator diaphragms
• One torque bolt and washer

4 - 32
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-15. Valve parts

Blow clean and dry valve parts with nitrogen before reassembling.

To reassemble a valve, do the following:

1. Inspect the primary plate (Item #9, refer to Figure 4-15) to insure
that the tubing parts are clean and that the sealing surface has no
scratches or pits.

2. Insert guide pins (#2 and #3) in the locating holes in the primary
plate (#9).

3. Place the sealing diaphragm over the guide pins and onto the
primary plate.

4 - 33
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4. Place the cushion diaphragm over the guide pins and onto the
sealing diaphragm and the primary plate.

5. Slide the upper piston plate (#5) over the guide pins.

6. Set the three short pistons (#6) into their respect places in the
upper piston plate.

7. Place the two upper actuator diaphragms over the guide pins and
onto the upper piston plate, covering the short pistons.

8. Slide the lower piston plate (#1) over the guide pins and onto the
upper actuator diaphragms.

9. Set the three long pistons (#4) into their respect places in the
lower piston plate.

10. Place the two lower actuator diaphragms over the guide pins and
onto the lower piston plate, covering the long pistons.

11. Install the torque bolt and washer (#8 and #7) up through the
primary plate and tighten the bolt to 30 ft. lbs.

12. Holding the bolthead and retainer with one hand, install the
plastic retainer disk and cap to hold the assembly together until
the valve is installed onto the GC.

4.7.7 Valve Cleaning

Note
Do not use an oil-based cleaner on the valve.

For cleaning the valve, isopropyl alcohol (P/N 9-9960-111) should be


used.

4 - 34
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

4.7.8 TCD Oven System Removal

Use the following procedure for removing the Oven System from the
Model 700 unit:

Note
The Oven System may be removed and repaired at a bench. However, it is not necessary
to remove the oven.

WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.

1. Disconnect all power to the unit.

2. Remove the explosion proof dome and the thermal cover.

4 - 35
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-16. Micro-FID Oven System Thermal Cover

Thermal
Cover

3. Loosen the screw on the mounting bracket that secures the Oven
Plate to the support post (see Figure 4-17).

4. Lift up slightly and rotate the oven forward one quarter turn so
that the components are accessible.

4 - 36
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-17. TCD upper assembly components

Oven System

Wiring Plug

Connector
Blocks

5. Unplug the solenoid wiring from the driver board end.

6. Unplug the heat control wiring from the driver board side.

7. Unplug the heater wiring from the driver board end.

8. Loosen the screws on the connector blocks.

4 - 37
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-18. TCD Oven System Disassembly

9. Disconnect the three Preamplifier wires and the solenoid wire


plug (see Figure 4-18).

10. Lift the oven assembly from the unit for bench maintenance and
repairs.

11. Reinstall in reverse order of Steps 1-9.

4.7.9 Micro-FID removal

Use the following procedure for removing the FID from the Model 700
unit.

WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.

1. Disconnect all power to the unit.

2. After powering down the Danalyzer Pro, allow at least 10 minutes


for the components to cool-down.

4 - 38
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3. Remove the explosion proof dome and the thermal cover.

CAUTION
This unit operates at high temperature. Allow a cool-down period of at least 10 minutes
after shutdown and handle the unit carefully. Failure to follow this precaution may
result in injury to personnel.

Figure 4-19. Micro-FID upper assembly components

FID

Oven System

Connector Blocks

4. Grasp the edges of the Connector Board on top of the unit and
pull and wiggle to remove the six socket tubes that extend onto
the pins in the cap (see Figure 4-20).

5. Remove the exhaust tube from the side by pulling the 'U' shaped
retainer from the top of the exhaust body and moving the
exhaust tube away from the FID. Take care not to lose the clip.

4 - 39
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-20. Model 700 with Micro-FID Upper Assembly


Connector Board 'U' shaped retainer

FID Shield FID Exhaust Tube

6. Loosen the two screws in the top of the FID.

7. Grasp the shielded section and lift it over the burner. Pull the cap
out of the shield. Remove the body from the shield, if necessary.

4.7.10 Micro-FID maintenance

The FID cap has no replaceable parts. Damage like a broken RTD or
broken igniter coil requires a replacement cap.

The burner tip can be removed for cleaning.

1. Loosen the isolating nut one turn.

4 - 40
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

2. Gently lift out the burner tip tube. Use short needle nose pliers if
it is stubborn, taking care not to bend the tube. The alternative is
to unscrew the assembly and clean as an assembly.

4.7.11 Micro-FID re-assembly

1. Insert burner tip tube into the isolating nut. Be certain it is fully
seated. There should be about .350 of tube visible.

2. Tighten the isolating nut in small increments until the tube ceases
to pull free. Slight additional tightening will ensure proper
sealing.

3. Place the cap onto the end of the body with the deep cavity.
Once the alignment pin is in its mating hole, gently press the two
parts together and ensure the o-ring is seated properly.

4. Slide the FID shield onto the body from the bottom. Align the
notch with the exhaust fitting and insert the two screws.

5. Lower the FID body assembly onto the base, placing the
alignment pin in its hole. Press the body into place, seating the o-
ring. Tighten the screws slightly more than 'finger tight.'

6. Re-connect the ground lead.

7. Press the FID exhaust tube onto the fitting and anchor with the
‘U’ shaped clip. (1/16 tubing makes an adequate clip.)

8. Plug the connector board onto the cap.

9. Replace the thermal cover on the upper enclosure.

4 - 41
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-21. Upper Enclosure Thermal Cover

Thermal
Cover

10. Replace the explosion-proof cover on the assembly, then apply


power to the unit.

4.7.12 LSIV maintenance

The LSIV can be maintained while attached to the enclosure. However,


the user may find it easier to perform maintenance with the LSIV
removed from the MON2020 Software for Gas Chromatographs upper
enclosure.

CAUTION
This unit operates at high temperature. Allow a cool-down period of at least 10 minutes
after shut-down and handle the unit carefully. Failure to follow this precaution may
result in injury or death to personnel.

4 - 42
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

4.7.13 LSIV removal

Inside the MON2020 Software for Gas Chromatographs upper enclosure


there are two insulation covers (which open like clam shells that slide off
of the end of the LSIV) to be removed.

1. Disconnect the carrier and sample tubing from the LSIV.

2. Remove the heater and RTD from the heater block.

3. Disconnect sample and air tubing from the outer portions of the
LSIV.

4. Unscrew the retaining ring, using a pin spanner wrench or other


tool. With the retaining ring loose, the LSIV assembly is free to be
pulled out of the upper enclosure.

4.7.13.1 Replacing LSIV seals

CAUTION
Use of wrenches other than a strap wrench to disassemble the LSIV can damage the
valve beyond repair. Failure to follow this precaution may damage equipment.

Tools Required for Disassembly:


• 2 each - 1 inch strap wrenches
• 1 each - assembly tool for seal nuts

1. Using two strap wrenches, if needed, unscrew the seal assist


housing from the LSIV body. Once the threads are free, pull the
pieces apart taking care to avoid bending the stem.

2. There are two seals with a central packing gland between them to
be removed, either from the stem or the bore in the body. Use
care to avoid scratching the stem or bore surfaces.

3. Replace the two seals with the central packing gland between
them onto the stem. Carefully align the two assemblies and insert
the seals into the bore.

4 - 43
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4. Screw the assemblies together hand-tight.

4.7.13.2 LSIV Disassembly

Use the following procedure to disassemble the LSIV and refer to Figure
4-22.

Figure 4-22. Model 700 with LSIV

1. Use the one (1) inch strap wrenches and unscrew the piston
housing (counter-clockwise) from the seal assist housing (use one
strap wrench on the piston housing and one strap wrench on the
seal assist housing).

CAUTION
Use care when disassembling the LSIV to prevent bending the valve stem. Failure to
follow this precaution may cause damage to the equipment.

2. When the threads disengage, slowly continue to pull apart the


LSIV assembly. Be careful not to bend the valve stem and pull until
the valve stem is free of the seal assist housing or the piston is free
of the piston housing.

4 - 44
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3. Separate the piston and valve stem assembly from the piston
housing or seal assist housing by carefully pulling it straight out.

4. Unscrew (counter-clockwise) the seal assist housing from the


lower body.

5. Unscrew (counter-clockwise) the retaining ring from the body.

6. Pull the piston/packing gland out of the lower body.

7. Push out the football seals and the central packing gland from the
body.

8. Unscrew (counter-clockwise) the stem lock nut from the piston.

9. Remove the valve stem from the piston.

10. Unscrew the seal nut from the upper piston packing gland.

11. Remove the o-rings and the collar.

4.7.14 Methanator maintenance

The optional Methanator, a catalytic converter, converts otherwise


undetectable CO2 and/or CO into methane by adding hydrogen and heat
to the sample. The Methanator requires little maintenance.

4 - 45
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-23. MON2020 Software for Gas Chromatographs Optional Methanator


Assembly

A. Case
B. Insulation
C. Tube
D. Catalytic Column
E. Heater
F. RTD (temperature detector)
G. Two #6-20 x 1/2 stainless steel screws

The RTD can be replaced , if necessary. If it is replaced, care must be


taken to anchor the RTD cable to the tubing to prevent loosening over
time.

A catalytic column needing replacement should be replaced with a full


heater/column assembly that includes the tube, column, heater and
RTD.

4 - 46
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

To replace the catalytic column,

1. Disconnect the tubing and wiring, then lift the Methanator from
the enclosure.

2. Remove the two screws and open the box (enclosure). The
catalytic column assembly is housed inside this insulation-filled
box.

3. Exchange the catalytic assembly and re-fill the enclosure with


insulation.

4. Reverse this procedure to reassemble the Methanator.

4.7.15 Valve overhaul

The chromatograph valves are designed to withstand millions of


actuation cycles without leakage or failure. If service is required, the
valve can be overhauled using replacement parts available from
Measurement Services.

Note
Replacement factory-built valves are available. We recommend returning and replacing
the 6-port valve for extensive repairs or complete replacement.

Use the following procedure for overhauling a 6-Port Valve:

1. Shut off carrier and sample gas streams entering the unit.

2. Remove the insulating cover from the Oven System.

3. If the faulty valve is not easily accessible, loosen the thumb screw
and rotate the oven forward (see Figure 4-17 and Figure 4-18).

4 - 47
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Note
The Oven System may be removed and repaired at a bench. However, it is not
necessary to remove the oven.

4. Disconnect tubing and fittings that attach to the valve from other
locations.

Figure 4-24. TCD Valve Tubing and Fittings

Valve
Attaching
Bolt

Fitting
Tubing

5. Loosen the attaching bolt on the valve to be replaced or serviced


(see Figure 4-24).

6. Holding the lower piston plate, pull the valve straight off the
block. The alignment pins may stick slightly.

4 - 48
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Note
Ensure that the primary seal diaphragm is correctly installed on the primary
plate.

7. Remove and discard the old valve diaphragms and gaskets.


Replace, in the same order, with the new ones supplied.

8. Reinstall the valve using the following steps:

Note
Do not scratch the primary plate surface.

(a.) Clean the sealing surface as required using Chemwipes


with alcohol.
Blow the sealing surface with clean, dry instrument air or
Carrier Gas. Dirt including dust and lint can cause
troublesome leakage.

Note
Do not use an oil base cleaner on the valve.

(b.) Align the pins with holes in the block and push the valve
assembly into place.
(c.) Tighten the valve “attaching bolt” to 30 lbs./ft. (40 N-m)
(d.) Reconnect all fittings and tubing
(see Figure 4-24).

4 - 49
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4.7.16 Oven system and stream switching system solenoid


valve replacement

Both the oven system and the stream switching system use the same
solenoid valves. The solenoids are replaced in both systems using the
same procedure.

WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.

4.7.17 Solenoid valve replacement

Replace the oven system and stream switching system (SSS) solenoids
using the following steps.

Note
Carrier Gas leaks may be caused by the SSS solenoids See “Leak checks” on page 4-26
for leak check procedures.

1. Remove the dome from the upper enclosure.

2. Loosen the mounting bracket thumb screw that secures the oven
to the chassis, see Figure 4-25.

4 - 50
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-25. Side view TCD oven system mounting bracket

Thumb Screw

3. Holding the left side of the oven mounting plate, gently lift up the
assembly and rotate it so that the enclosure opening is accessible.

4 - 51
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-26. Rotated TCD upper assembly

4. Loosen the thumb screws holding the valve in place.

Figure 4-27. Stream Switching Assembly

4 - 52
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

5. Lift the solenoid off of the alignment pins (approximately 1/8”).

6. Slide out the solenoid block.

7. Disconnect the wire leads and remove the gasket from the
bottom of the solenoid block.

8. Replace the old leads at the connector plug or splice the wires
from the new solenoid to the old leads.

Note
The solenoids are not polarity sensitive.

9. Reassemble the SSS and Oven System in reverse order of Steps 1


through 7.

Figure 4-28. Stream Switching System Final Assembly

4.8 TCD detector bridge balance

The following procedure should be performed if the Model 700 does not
produce a chromatogram.

To balance the detector bridge, do thee following:

1. Remove the cover of the upper explosion- proof housing and the
thermal cover on the Model 700 for access the preamplifier.

4 - 53
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-29. Model 700 Micro-FID/TCD Preamplifier

2. Attach the negative lead of a digital voltmeter to the black test


point (-BRIDGE BALANCE). Attach the positive lead of the digital
voltmeter to the red test point (+BRIDGE BALANCE).

Figure 4-30. Model 700 TCD Bridge Balance

Detector 1 Detector 2

4 - 54
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-31. Model 700 Micro-FID Bridge Balance

Detector 1

3. Check the detector bridge voltage. The voltage should read 0


millivolts (mV), ±0.5 mV. Adjust the coarse and fine
potentiometers which are located immediately to the left of each
of the (red) test points to obtain the specified reading.

4.9 Measure vent flow

You will need an accurate flow meter for this measurement.

To measure the MV vent flow, proceed as follows:

1. Attach a flow meter to the vent output on the right side of the
Model 700 “MV1”(marked on the tag).

The flow should measure 12-18 cc/min.

2. Attach a flow meter to the vent “MV2” marked on the tag.

The flow should measure 12-18 cc/min.

4 - 55
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-32. Measure flow vents

MV1

(Marked on tags)

MV2

4.10 Model 700 electrical components

The Model 700 GC is designed to operate for long periods of time


without need for preventive or regularly scheduled maintenance. The
Model 700 is designed using explosion-proof enclosures. The enclosure
is dust-proof, water-proof, and flame-proof.

WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.

Should there be a need to open the explosion-proof enclosure, first


disconnect all electrical power to the unit, and ensure the area is free of
explosive gases. Prior to opening the Model 700, check the operating
parameters of the application with a PC using MON2000 and attempt to
isolate or fix any incorrect parameters.

4 - 56
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

To access the GC electrical components,

1. Ensure electrical power is disconnected from the unit and the


environment is safe.

2. Remove the lower enclosure cover and access the card cage
assembly holding the circuit boards.

Figure 4-33. Model 700 lower enclosure

Explosion-proof Cover

3. Note the location and direction of any board removed. Remove


only one end of any cable necessary to obtain access to the
desired board. Remember or make note of the cable installation
so that the cables can be replaced in the same order. Release the
catch(es) and remove/replace the circuit board(s) as necessary.

4 - 57
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Note
After removing the cable(s), any board may be replaced without removing the
card cage assembly.

Figure 4-34. Model 700 Lower Assembly

Card Cage Assembly

4 - 58
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

4.10.1 DC power supply replacement procedures

The DC/DC power supply is mounted on the left wall of the lower
enclosure (see Figure 4-35) and is accessible by removing the threaded
cover plate from the housing.

WARNING
Disconnect all electrical power to the unit and ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or death to personnel or cause
damage to the equipment.

Figure 4-35. DC Power Supply Lower Enclosure

DC Power
Supply

Tools required to remove and replace the DC Power Supply:


• Cross point #2 Phillips screw driver (long shank is helpful).
• Head lamp (flashlight)

To remove and replace a faulty DC Power supply:

Note
Needle nose pliers may be used to turn rear thumbscrews.

4 - 59
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

1. Disconnect the cables from the CPU, the Com4A board (if
installed), and the modem board.

2. Unscrew the card cage thumb screws and remove the card cage
assembly.

3. Unscrew the two thumb screws on the power supply bracket.

4. Remove the assembly from the unit.

5. Disconnect, label and bundle all leads.

6. Attach all leads to the new DC Power Supply.

7. Align the power supply bracket and tighten the two thumb
screws.

8. Reinstall the card cage assembly, tighten the thumb screws and
reconnect all cables.

9. Replace the threaded cover plate on the lower enclosure housing.

4.11 Communications

4.11.1 Model 700 GC with the TCD

The Model 700 with the TCD has up to six communications channels
available; up to three communications ports from the WinSystems CPU
board and four communications ports from the Com4A board.

Note
See Appendix A for a list of the ports and terminals (pins) assigned to serial communica-
tions.

4 - 60
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

4.11.2 Model 700 GC with the FID and TCD

The MON2020 Software for Gas Chromatographs GC with an FID has


two communications channels available without the Com4A board
installed. With the Com4A board installed, the GC has six
communications ports available on the FTB; Com1 and Com2, and
Com5, Com6, Com7, and Com8.

Com4 is dedicated to the FID/TCD Preamplifier.

The communication protocols are selected inside the Model 700 GC with
jumpers. The protocols are normally specified by the customer and then
set at the factory.

If it becomes necessary to change the communications settings at the


site, access to the boards inside the enclosure is required to make
changes. See Section 3.4.2 if a communications change becomes
necessary.

WARNING
The enclosure should not be opened when hazardous gases are present. Failure to do so
may result in injury or death to personnel or cause damage to the equipment.

The jumpers to be changed are located on the CPU board and the
Com4A board.

When the desired GC address (Com ID) is known, it will be set before the
unit leaves the factory. If the address (Com ID) needs to be changed in
the field, it will be necessary to change the arrangement of an 8-position
DIP switch on the multifunction board.

Figure 4-36. Dip Switch

4 - 61
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

This board is mounted on a bracket towards the center of the upper


enclosure.

Figure 4-37. Multifunction board


Multifunction Board

Ensure the cables are replaced in the exact order and positions.

Note
See “Inspect or change the Com ID” on page 3-31 for an explanation of DIP switch
settings and their determination of the GC Controller Modbus slave address (Com ID).

4 - 62
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

1. For example MON2020 Software for Gas Chromatographs GCs


with a TCD,
• Switches 1 through 5 form a 5-bit binary number for setting
the Modbus slave address (also known as Com ID or Device
ID.)
• Switch number “1” is the least significant bit, and switch
number “5” is the most significant bit. Set these switches
either ON or OFF.
• Switch 6 is a spare for future use. Switches 7 and 8 are set as
needed for the presence of an optional LOI (Local Operator
Interface) connected via COM8 (when the COM4A board is
installed). If the COM4A board is not installed, the LOI is
connected via COM4. This address should display via
MON2000.

2. For example MON2020 Software for Gas Chromatographs GCs


with an FID,
• Switch number “1” is the least significant bit, and switch
number “5” is the most significant bit. Set these switches
either ON or OFF.
• Switch “6” and “7” are spares and switch “8” is used to cold
start the processor. See Table 3-2.

4.12 Analog inputs and outputs

The analog outputs can be calibrated and or adjusted via the MON2000
software. However, these outputs should be measured with a good
digital meter upon initial installation at zero scale and full scale. Then the
span can be set with MON2000 software so that it represents values
from zero to 100 percent of the user-defined units in use.

Nominally, calibration is made within a range of 4-20 milliamperes (mA)


output from each analog channel. However, zero scale calibrations can
be set with 0 mA output, and full scale calibration can be set with up to
22.5 mA output. If there is reason to suspect that the span on any
particular channel might be off after a period of time and heavy use, then
the analog output for that channel should be recalibrated.

4 - 63
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4.12.1 Model 700 analog inputs

There are four analog inputs available on the Field Termination Board (J4
- 12-pin Phoenix connector).

The Model 700 analog inputs are configured as follows:

Figure 4-38. Analog Inputs


J4
VIN +_1
1
AGND 2
Shield
3
VIN + _2
4
AGND 5
Shield
6
VIN + _3
7
AGND 8
Shield 9
VIN + _4
10
AGND 11
Shield
12

4.12.2 Analog output adjustment

The initial analog output adjustment will be set at the factory, before
shipment, at standard values (4-20 mA). It may be necessary to check
and/or adjust these values depending on output cabling/impedance.
The adjustment may require two persons if the units are some distance
apart. It will require a good digital meter to check the zero and full scale
values at the receiving end. The scale or span value can be adjusted by a
PC with the Model 700 when the values are known at the receiving end.

It is possible to calibrate the analog outputs using different engineering


units, volts and percentages. For examples and detailed instructions,
refer to the MON2000 Software for Gas Chromatographs Users Manual
(P/N 3-9000-522).

4 - 64
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

4.12.3 Model 700 analog outputs

The Model 700 has four standard analog outputs (J8 - 12-pin Phoenix
connector) on the Field Termination board (P/N 3-0700-010).

Figure 4-39. FTB Board Analog Outputs


Analog
Inputs

J4

J8

Analog
Outputs

The Model 700 analog outputs are configured as follows:

4 - 65
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure 4-40. Analog Outputs


J8
IOut +_1
1
IOut - _1
2
Shield
3
IOut +_2
4
IOut -_2
5
Shield
6
IOut +_3
7
IOut -_3
8
Shield 9
IOut +_4 10
IOut -_4
11
Shield
12

The analog outputs for the optional analog board (P/N 2-3-0580-037)
are configured as follows:

4 - 66
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure 4-41. Optional analog board outputs


J3
IOut +_5
1
IOut - _5
13
Shield
2
IOut +_6
14
IOut - _6
3
Shield
15
IOut +_7
4
IOut - _7
16
Shield
5
IOut +_8 17
IOut - _8
6
Shield
18
IOut +_9 7
IOut - _9 19
Shield 8
IOut +_10
20
IOut - _10 9
Shield
21
IOut +_11
10
IOut - _11
22
Shield
11
IOut +_12 23
IOut - _12 12
Shield 24

4.13 Discrete digital inputs and outputs

For instructions on connecting digital inputs and outputs to the GC Field


Termination Boards, see Section 3.4.7 for more details.

An external loopback test circuit can be built for troubleshooting the


Model 700 digital input/output operation.

4 - 67
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4.14 Recommended spare parts

The quantities listed in the following table represent the number of


spares needed to cover most contingencies at facilities where GC
systems are in operation, for a period of less than two years, or a period
of two years or more.

Measurement Services offers service and repair service contracts that


make maintaining most spares for the GC system unnecessary. Details
regarding service contracts may be obtained by contacting
Measurement Services at the address or telephone number on the
“Customer Repair Report” provided at the back of this manual.
Quantity for Quantity
Part Number Item Name Less than 2 for 2 years
years or more

2-3-0500-391 Teflon Thermistor Seals (Set of 10) 1 1


2-3-0520-101 Col Set BTU 4 Minute M/121705 1 1
2-3-0580-002 Preamplifier board 1 1
2-3-580-037 PCA Analog I/O - 8 additional 4-20 mA channels non- optional optional
isolated
2-3-0700-004 Multifunction board 1 1
2-3-0700-005 Driver IO board 1 1
2-3-0700-007 PCA Analog I/O - 4 additional 4-20 mA channels optional optional
isolated
2-3-0700-010 Field Termination Board 1 1
2-3-0700-011 Dual Methods Adapter Board Application Application
dependent dependent
2-3-0700-029 Modem board PC104 (If replacing faulty modem 1 1
board; if a new kit is needed, purchase 2-3-2350-
142)
2-3-0700-034 PCA Analog I/O - for use with 2-3-0700-036 CPU 1 1
board
2-3-0700-036 PCA CPU with 4 RS-232 & 700 BOS (Confirm that this 1 1
part number matches that on the existing board.)
2-3-0700-110 AC Power Supply Optional Optional
2-3-0700-136 Fuses, Assortment (5 each of 1, 2, and 6 A) 1 2

4 - 68
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Quantity for Quantity


Part Number Item Name Less than 2 for 2 years
years or more

2-3-2350-098 Ethernet PCA (If replacing faulty Ethernet board; if a Optional Optional
new kit is needed, purchase 2-3-2350-143)
2-4-0700-152 Solenoid valve, Srs 3 3
2-4-0700-171 Repair Kit, 10-Port Valve (For use on Model 700 GCs Application Application
only) dependent dependent
2-4-0700-187 Repair Kit, 6-Port Valve 3 6
2-4-5000-113 Filter Element 2 Micron, Swagelok SS-2F-K4-2 1/stream 2/stream
2-4-5000-938 Membrane Kit, Genie® Model 120 Filter/Bypass/LSO 1/stream 2/stream

2-4-9500-084 Regulator, carrier gas, 60-110 PSIG, Masoneilan 1 1


(Baked)
2-6-1611-083 Kit, 9K Thermistors (Not for use with Hydrogen ½ ½
Carrier)
2-3-0500-521 Kit, 9K Thermistors, double-dipped (For use with Application Application
Hydrogen Carrier) dependent dependent

4.15 Upgrade procedures

4.15.1 Base operating system

The Base Operating System (BOS) performs functions similar to


operating systems such as DOS or Windows® or Linux®.

Note
Refer to the MON2000 Software for Gas Chromatographs User Manual (P/N 3-9000-522)
for BOS upgrade procedures.

BOS provides the basic resources and interfaces to run the user's tasks.
Unlike DOS or Windows or Linux, since BOS is an embedded real-time
multi-tasking preemptive operating system, there is no direct user level
interface to it. If a BOS upgrade is required to your system, refer to the
MON2000 Software for Gas Chromatographs User Manual (P/N 3-9000-
522) for additional BOS information.

4 - 69
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

4.15.2 Applications

The GC application, which runs under BOS, utilizes the tools provided by
BOS to perform the desired gas chromatograph functions for the user.
There are different applications to provide for different gas
chromatographic needs. To load a new application or to upgrade an
existing application refer to the MON2000 Software for Gas
Chromatographs User Manual (P/N 3-9000-522) for details.

4 - 70
Appendix A: Communications specifications
A

A.1 TCD serial communications

The MON2020 Software for Gas Chromatographs with a TCD has three
standard CPU serial communications ports: Com1, Com2, and Com4;
and four optional Com4A board serial ports: Com5 Com6, Com7, Com8
and Com9 for the optional internal modem. Per the matrix below,
jumper settings can be configured for either RS-232, RS-422, or
RS-485 serial signal definitions.

Note
Com3 is reserved for the multifunction board.

Table A-1 Matrix of possible TCD configurations field termination board

Logical Address Operation Comments

Com1 and Com2 (WinSys CPU RS-232, RS-422 or RS-485 PC, Flow Computer, Modem
Board) J1 to FTB (external)
Com3 (WinSys CPU Board) J6 to RS-232 Reserved for Multifunction Board
Multifunction Board
Com4 (WinSys CPU Board) RS-232, RS-422 or RS-485
J6 to FTB
Com5 (WinSys Com4A Board) RS-232, RS-422 or RS-485 Modem (External)
J9 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com6 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J13 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com7 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J17 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)

A-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table A-1 Matrix of possible TCD configurations field termination board

Logical Address Operation Comments

Com8 (WinSys Com4A Board) RS-232, RS-422 or RS-485


J18 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com9 Reserved for internal modem

A.1.1 Model 700 with a TCD communications port

The CPU board has three communications ports that can be used for the
PC or the Flow Computer, as the customer desires.

Note
A telephone modem can be connected to any of the GC serial ports configured for RS-
232. If an internal modem (WinSystems P/N 3-0580-042) or (P/N 3- 0700-029
Radicom) is installed, it is assigned to serial port Com9. If the Com4A board is installed,
the modem is assigned to Com9. With or without the Com4A board, the internal
modem is assigned to Com9.

The optional 4-channel Com4A board can be installed for applications


requiring more than three communications ports. Each channel can be
configured for RS-232, RS-422, or RS-485 (for ports Com5, Com6,
Com7, and Com8).

Each channel can be configured using MON2000. For more information,


see the “Serial Ports” section of the MON2000 Software for Gas
Chromatographs manual.

If a modem and a serial controller are both required, an external modem


will be assigned to either Com1 or to Com5.

Serial ports configured for RS-232 are most commonly used for direct
serial communication between the GC and a PC or modem.

Serial ports configured for RS-422 or RS-485 are most commonly used
for long distance serial communications systems, such as a DCS or a
network. For these systems, the GC can communicate as a Modbus slave
device.

A-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Note
In any Modbus host-slave DCS or network, there must only be one host to which any
one of the GC serial ports can respond as a Modbus slave. To use MON2000 to configure
the GC for Modbus communication, see the MON2000 Software for Gas Chromatographs
User Manual (P/N 3-9000- 522).

For further details, see Figure A-1 through Figure A-3.

Note
The Model 700, standard configuration, has three ports available on the FTB: Com 1,
Com 2, and Com 5.

Figure A-1 Standard configuration without Com4A Board or FID

Multifunction
Board
Com3
CPU
Field Termination
Com1
Board
Com2
Com1
Com3 Com2
Com4
Com5
Com6
Com7
Com8

Note
The Model 700 with the Com4A board installed has six communications ports available
on the FTB: Com1 and Com2, and Com5, Com6, Com7, and Com8.

A- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure A-2 Configuration with Com4A Board


Multifunction
Board
Com3
CPU

Com1
Field Termination
Com2 Board
Com3
Com1
Com4 Not
Connected Com2

Com5
Com 4A Com6
Com7
Com5
Com8
Com6
Com7
Com8

If using a direct 6-conductor serial cable, connect the exposed cable


leads to the FTB serial port. A pinout of a female DB 9-pin socket is shown
in Figure A-3.

A-4
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure A-3 FTB Com1 and Com2 DB9 connector

Com1
P2

5
RI 1 9
DSR 1 4
RTS 1 8
RXD 1 3
CTS 1 7
TXD 1 2
DTR 1 6
DCD 1 1

GND Com2
P3

5
RI 2 9
DSR 2 4
RTS 2 8
RXD 2 3
CTS 2 7
TXD 2 2
DTR 2 6
DCD 2 1

A.2 FID serial communications


The MON2020 Software for Gas Chromatographs with a FID and a TCD
has two standard CPU board serial communications ports–Com1 and
Com2–that can be used for the PC or the flow computer, as the
customer desires.

Note
Com3 is reserved for Multifunction board. Com4 is reserved for the FID/TCD board.

A- 5
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

The optional 4-channel Com4A board can be installed for applications


requiring more than two communications ports. Each channel can be
configured for RS_232, RS-422 or RS-485 (for ports Com5 Com6, Com7,
Com8).
Table A-2 Matrix of possible FID configurations field termination board

Logical Address Operation Comments

Com1 and Com2 (WinSys CPU Board) J1 RS-232, RS-422 or RS-485 PC, Flow Computer, Modem
to FTB (external)
Com3 (WinSys CPU Board) J6 to RS-232 Reserved for Multifunction
Multifunction Board PCB
Com4 (WinSys CPU Board) RS-232 Reserved for FID/TCD
J6 to FID/TCD Preamplifier Preamplifier PCB
Com5 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J9 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com6 (WinSys CPU Board) RS-232, RS-422 or RS-485
J13 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com7 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J17 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com8 (WinSys Com4A Board) RS-232, RS-422 or RS-485
J18 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)
Com9 Reserved for internal modem

Each channel can be configured using MON2000. For more information,


see the “Serial Ports” section of the MON2000 Software for Gas
Chromatographs manual.

Note
In any Modbus host-slave DCS or network, there must only be one host to which any
one of the GC serial ports can respond as a Modbus slave. To use MON2000 to configure
the GC for Modbus communication, see the MON2000 Software for Gas Chromatographs
User Manual (P/N 3-9000- 522).

A-6
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

If a modem and a serial controller are both required, an external modem


will be assigned to either Com1 or to Com5.

Serial ports configured for RS-232 are most commonly used for direct
serial communication between the GC and a PC or modem.

Serial ports configured for RS-422 or RS-485 are most commonly used
for long distance serial communications systems, such as a DCS or a
network. For these systems, the GC can communicate as a Modbus slave
device.

For further details, see Figure A-4 and Figure A-5.

Note
The Model 700, standard configuration, has two communications ports available on
the FTB: Com1 and Com2.

Figure A-4 Configuration without Com4A board

Multifunction FID/TCD
Board Preamplifier Board
Com3 Com4

CPU Field Termination


Board
Com1 Com1
Com2 Com2
Com3
Com4
Com5
Com6
Com7
Com8

Note
Com4 is dedicated to the FID/TCD Preamplifier. When the LOI becomes available, it will
use a video board instead of a serial port connection.

A- 7
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure A-5 Configuration with Com4A board


Multifunction FID/TCD
Board Preamplifier Board
Com3 Com4

CPU Field Termination


Board
Com1 Com1
Com2 Com2
Com3
Com4

Com4A

Com5 Com5
Com6 Com6
Com7 Com7
Com8 Com8

Note
The Model 700, with the Com 4A board installed, has six communications ports
available on the FTB: Com1 and Com2, Com5, Com6, Com7, and Com8.

Note
Com4 is dedicated to the Micro-FID/TCD Preamplifier. When the LOI becomes available,
it will use a video board instead of a serial port connection.

A.2.1 Connecting serial communications to the GC

To connect serial communications lines to the GC,

A-8
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Note
Serial communications for FTB (Com1- Com4) is standard. Com3 reserved for the
Multifunction board. Serial communications with optional Com4A board are available
on ports Com5 - Com8.

1. Access the FTB in the lower enclosure.

2. Route serial communications lines appropriately.

3. Make serial communications line connections to the FTB. See


Section A.1.1 for port numbers and pinouts.
Each of the various combinations available for GC serial
communications ports (i.e., RS-232, RS-422, or RS-485) require
specific jumper settings on the WinSystems CPU board or the
optional Com4A board.
In most instances, installation of these jumper settings requires no
modification. Configurations have been performed at the factory
prior to shipment of the MON2020 Software for Gas Chromato-
graphs, according to customer specifications for serial communi-
cations.

Note
If you are changing or adding serial communications to the GC, ensure that the
correct jumpers are set.

A.2.1.1 RS-232 ports

See Appendix A.2.2 for RS-232 port connections


Voltage: ±5 volts or ±12 volts, depending on jumper settings
Recommended Maximum Cable Length: 50 feet (15 meters)
Pinouts: See Appendix A.2.2

A- 9
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

A.2.1.2 RS-422 ports

See Appendix A.2.2 for RS-422 port connections.


Voltage: line drivers meet Electronics Industries Association (EIA)
specifications for RS-422.
Recommended Maximum Cable Length: 4000 feet (1219 meters)
Pinouts: See Appendix A.2.2

A.2.1.3 RS-485 serial specifications

See Appendix A.2.2 for RS-485 port connections.


Voltage: line drivers meet Electronics Industries Association (EIA)
specifications for RS-485
Recommended Maximum Cable Length: 4000 feet (1219 meters)
Pinouts: See Appendix A.2.2

A.2.2 FTB serial communications

The settings are shown in Figure A-6 through Figure A-11.

A - 10
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure A-6 FTB Com1 DB 9-pin Phoenix Connector


Com1

RS-232 RS-485 RS-422 J5


DCD 1
1
RXD 1 TX/RX+ TX+
2
TXD 1 TX/RX- TX- 3
DTR 1
4
5
DSR 1 RX+
6
RTS 1 RX-
7
CTS 1 8
RI 1 9

Figure A-7 FTB Com2 DB 9-pin Phoenix Connector

Com2

RS-232 RS-485 RS-422 J7


DCD 2
1
RXD 2 TX/RX+ TX+
2
TXD 2 TX/RX- TX- 3
DTR 2
4
5
DSR 2 RX+
6
RTS 2 RX-
7
CTS 2 8
RI 2 9

A - 11
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure A-8 FTB Com5 DB 9-pin Phoenix Connector


Com5

RS-232 RS-485 RS-422 J9


RLSD 5
1
RXD 5 TX/RX+ TX+
2
TXD 5 TX/RX- TX- 3
DTR 5
4
5
DSR 5 RX+
6
RTS 5 RX-
7
CTS 5 8
RI 5 9

Figure A-9 FTB Com6 DB 9-pin Phoenix Connector


Com6

RS-232 RS-485 RS-422


J13
RLSD 6
1
RXD 6 TX/RX+ TX+
2
TXD 6 TX/RX- TX- 3
DTR 6
4
5
DSR 6 RX+
6
RTS 6 RX-
7
CTS 6 8
RI 6 9

A - 12
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure A-10 FTB Com7 DB 9-pin Phoenix Connector

Com7

RS-232 RS-485 RS-422 J17


RLSD 7
1
RXD 7 TX/RX+ TX+
2
TXD 7 TX/RX- TX- 3
DTR 7
4
5
DSR 7 RX+
6
RTS 7 RX-
7
CTS 7 8
RI 7 9

Figure A-11 FTB Com8 DB 9-pin Phoenix Connector

Com8

RS-232 RS-485 RS-422 J18


RLSD 8
1
RXD 8 TX/RX+ TX+
2
TXD 8 TX/RX- TX- 3
DTR 8
4
5
DSR 8 RX+
6
RTS 8 RX-
7
CTS 8 8
RI 8 9

A - 13
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

A.2.2.1 Jumper Settings for Older WinSystems CPU Boards (P/N#2-


3-0700-028)

This section applies only to GCs not installed with the WinSystems LX-
800 CPU board (P/N #2-3-0700-036).

Jumper settings and pinouts for the COM1 - COM4 serial


communications ports are defined in the following tables.

Table A-3 Communication with WinSystems CPU

Com1

RS-232 Mode
J8 — Jumpers Pins 1 and 2
J13 — No jumpers
U2 — Installed (Standard)
U5 — Removed
U6 — Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J8 — Jumper Pins 1 and 2


J13 — No jumpers
U2 — Removed
U5 — Installed
U6 — Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J8 — Jumper Pins 1 and 2


J13 — Jumper Pins 2 and 3
U2 — Removed
U5 — Removed
U6 — Installed

A - 14
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Table A-4 Communication with WinSystems CPU

Com2

RS-232 Mode
J9 — Jumpers Pins 1 and 2
J16 — No jumpers
U9 — Installed (Standard)
U11 — Removed
U12 — Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J9 — Jumper Pins 1 and 2


J16 — No jumpers
U9 — Removed
U11 — Installed
U12 — Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J9 — Jumper Pins 1 and 2


J16 — Jumper pin 2 and 3
U9 — Removed
U11 — Removed
U12 — Installed

Table A-5 Communication with WinSystems CPU

Com3 Reserved for Multifunction Board

RS-232 Mode
J12 — Jumpers Pins 1 and 2
J14 — No jumpers
U4 — Installed (Standard)
U7 — Removed
U8 — Removed

A - 15
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table A-6 Communication with WinSystems CPU

Com4 (Reserved for FID/TCD Preamplifier Board)

RS-232 Mode
J15 — Jumpers Pins 1 and 2
J17 — No jumpers
U10 — Installed (Standard)
U13 — Removed
U14 — Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J15 — Jumpers Pins 1 and 2


J17 — No jumpers
U10 — Removed
U13 — Installed
U14 — Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J15 — Jumpers Pins 1 and 2


J17 — Jumpers Pins 2 and 3
U10 — Removed
U13 — Removed
U14 — Installed

A - 16
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

A.2.2.2 WinSystems MCM/LPM — Com4A board

Jumper settings and pinouts for the four serial communications ports
(COM5 - COM8) on the optional WinSystems Com4A board are defined
in the following tables.
Table A-7 Communication with WinSystems
MCM/LPM — Com4A Board (Optional)

Com5

RS-232 Mode
J2 — No jumpers
U6 — Installed (Standard)
U3 — Removed
U4 — Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J2 — No jumpers
U6 — Removed
U3 — Installed
U4 — Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J2 — Jumper Pins 2 and 3


U6 — Removed
U3 — Removed
U4 — Installed

Com6

RS-232 Mode
J5 — No jumpers
U13 — Installed (Standard)
U10 — Removed
U14 — Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J5 — No jumpers

A - 17
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Com6

U13 — Removed
U10 — Installed
U14 — Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J5 — Jumper pins 2 and 3


U13 — Removed
U10 — Removed
U14 — Installed

Com7

RS-232 Mode
J4 — No jumper
U11 — Installed (Standard)
U9 — Removed
U12 — Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J4 — No jumpers
U11 — Removed
U9 — Installed
U12 — Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J4 — Jumper pins 2 and 3


U11 — Removed
U9— Removed
U12 — Installed

Com8

RS-232 Mode

J1 — No jumpers
U5 — Installed (Standard)

A - 18
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Com8

U1 — Removed
U2 — Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J1 — No jumpers
U5 — Removed
U1 — Installed
U2 — Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J1 — Jumper pins 2 and 3


U5 — Removed
U1 — Removed
U2 — Installed

A.2.2.3 Com4A board compatibility settings

Table A-8 J10 Jumper Settings

Pin(s) Position

1 and 2 In
3 and 4 In
7 and 8 In
9 and 10 In

Table A-9 J7 Jumper Settings

Pin(s) Position

1 and 2 Open
3 and 4 Open
5 and 6 Open

A - 19
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table A-10 J8 Jumper Settings

Pin(s) Position

1 and 2 In
3 and 4 In
5 and 6 In
7 and 8 In

Table A-11 J9 Jumper Settings

Pin(s) Position

1 and 2 In
5 and 6 In

A.2.2.4 WinSystems Ethernet board

The PCM-NE2000-16 PC-104 can be configured by using the on-board


jumper block .

Jumper settings and pinouts used on the MON2020 Software for Gas
Chromatographs for the PCM-NE-2000-16 PC-104 Ethernet board
(optional) are defined in the following table:
Table A-12 Ethernet Board Pin Settings

Jumper Pin Position “In”

J1 13 and 14
15 and 16
17 and 18
23 and 24
27 and 28
J2 1 and 2
J3 1 and 2

A - 20
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

A.2.2.5 Radicom 56K baud modem board

The jumper settings and pinouts for the Radicom Modem (P/N 3-0700-
029) are shown below:
Table A-13 J26 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table A-14 J27 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table A-15 J30 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table A-16 J31 Radicom Modem Jumper Settings

Pin(s) Position

2 and 3 In

A.3 Wiring local RS-232 communications

A.3.1 GC serial port and cable configurations

This section provides more detailed information about local serial port
connections for the Model 700. It identifies serial port pin assignments
and diagrams for designing
RS-232 serial cables.

A - 21
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

GC serial ports are found on the Field Termination Board and the
connection points for external devices are as follows:

Figure A-12 FTB Serial Connections

Figure A-13. FTB Serial Connections

A - 22
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Table A-17 Serial Ports on Field Termination Board

Phoenix Plug
Port Comments (bare-wire)
connection

Serial Port 1 (Com1) P2 DB 9-pin Connection J5


Serial Port 2 (Com2) P3 DB 9-pin Connection J7
Serial Port 3 (Com3) Reserved for Multifunction Board N/A
Serial Port 4 (Com4) Reserved for FID/TCD Preamplifier N/A
Board (FID/TCD units)
Serial Port 5 (Com5) J9
Serial Port 6 (Com6) J13
Serial Port 7 (Com7) J17
Serial Port 8 (Com8) J18

Phoenix plug (bare-wire) connections are available to all four serial ports.
Pin-outs are identical for all four serial port Phoenix plugs and jacks. Each
Phoenix plug/jack (male) combination allows a bare-wire connection and
uses 9-Pins as illustrated:

Figure A-14 Phoenix Connector (J5, J6, J10, and J11) Pinout

Null modem connections (DB 9-pin) are available for Serial Ports 1 and 2
only, as noted in Table A-17.

A - 23
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Note
PC-to-GC connections, direct serial: The GC serial ports were wired to appear as DCE, so
a straight-through serial cable is used for a direct serial connection between the GC and
the PC. (The PC is Data Terminal Equipment, or DTE.) See “GC DB 9-pin serial port to PC
DB 9-pin port” on page A-25.

External modem-to-GC connections, serial: a null modem cable and gender changes
may be purchased from any computer products store, for the GC to external modem
connection. However, a custom serial cable may be built to emulate a null-modem
cable for a connection between the GC Controller and an external modem. (The
modem is Data Communications Equipment, or DCE.) See “Wiring remote RS-232
communications” on page A-28.

Both of the GC DB 9-pin jacks are female and have identical pin
assignments. Note that a DB 9-pin male numbering scheme is also
illustrated, but for reference purposes only as follows.

Figure A-15 DB 9-pin connector (P2 and P3) and pinout for jacks

A - 24
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

A.3.2 GC DB 9-pin serial port to PC DB 9-pin port

To make an RS-232 serial connection between one of the DB 9-pin serial


ports of the GC, and a PC with DB 9-pin serial port, use a straight-through
serial cable, terminated as DB 9-pin male / DB 9-pin female. This will work
if the PC has a male DB 9-pin serial port, and its pin assignments are
identical to those found on a typical DB 9-pin serial port of an IBM PC.

The straight-through serial cable can be obtained from most computer


products suppliers, so custom-building a cable normally is not necessary.
Wiring and signal paths are illustrated as follows.

Figure A-16. GC DB 9-pin Port to PC DB 9-pin Port

Female DB-9 Male DB-9 Female DB-9


connector on GC cable end to GC cable end to PC
5 1 1 5 5 1

9 6 6 9 6
9

9 RI 9 RI 9 RI
8 RTS 8 CTS 8 CTS
7 CTS 7 RTS 7 RTS
6 DTR 6 DSR 6 DSR
5 GND 5 GND 5 GND
4 DSR 4 DTR 4 DTR
3 RxD 3 TxD 3 TxD
2 TxD 2 RxD 2 RxD
1 RLSD 1RLSD 1RLSD
(DCD) (DCD) Straight-through serial cable(DCD)

A.3.3 GC DB 9-pin serial port to PC DB 25-pin port

To make an RS-232 serial connection between one of the DB 9-pin serial


ports of the GC, and a PC with DB 25-pin serial port, you may be able to
use a straight-through serial cable, terminated as DB 9-pin male / DB 25-
pin female. This will work if the PC has a male DB 25-pin serial port, and
its pin assignments are identical to those found on an IBM PC.

A - 25
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

The necessary straight-through serial cable can be obtained from most


computer products suppliers, so custom-building a cable normally is not
necessary. Wiring and signal path are illustrated as follows.

Figure A-17 GC DB 9-pin Port to PC DB 25-pin Port

A.3.4 GC Phoenix plug port to PC DB 9-pin port

To make an RS-232 serial connection between one of the Phoenix Plug


serial ports of the GC, and a PC with DB 9-pin serial port, you will need to
manufacture the cable and its DB 9-pin, female plug cable end as
illustrated below (see Figure A-18).

Note
The cable for this application is also available(P/N 3-2350-068) in a customer-specified
length with six exposed leads and a female DB 9-pin connector.

A - 26
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure A-18 GC DB 9-pin Port to PC DB 25-pin Port

A.3.5 GC Phoenix plug port to PC DB 25-pin port

To make an RS-232 serial connection between one of the Phoenix Plug


serial ports of the GC, and a PC with DB 25-pin serial port, you will need
to manufacture the cable and its DB 25-pin, female plug cable end as
illustrated below.

A - 27
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure A-19 GC Phoenix Plug Port to PC DB 25-pin Port

A.4 Wiring remote RS-232 communications

A.4.1 GC DB 9-pin serial port to modem DB 25-pin port

To make an RS-232 serial connection between one of the DB 9-pin serial


ports of the GC, and an external modem with a DB 25-pin serial port, you
may use gender changes and a null modem cable purchased from any
computer products supplier, or you may manufacture a cable. The
manufactured null modem cable will need a male DB 9-pin connector
and a male DB 25-pin connector. Wire the cable ends as illustrated
below.

A - 28
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Note
Data Communications Equipment (DCE). Use a custom nullmodem type cable to make
the connection between the GC and an external modem. GC serial ports were wired to
appear as DCE so that a straight-through serial cable could be used for a direct serial
connection between the GC Controller and the PC, which is Data Terminal Equipment
[DTE].

Figure A-20. GC DB 9-pin Port to External Modem DB 25-pin Port


Female DB-9 Serial Male DB-9 cable end Male DB-25 cable end
connector on GC to GC Serial Port to External Modem DCE

5 1 1 5 1 13

9 6 6 9 14 25

9 RI 9 RI 22 RI
8 RTS 8 CTS 4 RTS
7 CTS 7 RTS 5 CTS
6 DTR 6 DSR 20 DTR
5 GND 5 GND 7 GND
4 DSR 4 DTR 6 DSR
3 RxD 3 TxD 3 RxD
2 TxD 2 RxD 2 TxD
1 RLSD 1 DCD 8 DCD
(DCD) Null Modem cable

A.4.2 GC Phoenix plug to modem DB 25-pin port

To make an RS-232 serial connection between one of the Phoenix Plug


serial ports of the GC, and an external modem with DB 25-pin serial port,
you will need to manufacture the cable and its DB 25-pin, male plug
cable end as illustrated below.

A - 29
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure A-21 GC Phoenix Plug Port to External Modem DB 25-pin Port

A.5 Example RS-422 PC-GC connection

This section demonstrates an example RS-422 connection from a PC to


GC that is accomplished through use of an asynchronous line driver/
interface device. The line driver device serves as an interface between
the RS-232 output of the PC and the RS-422 protocol needed for long
distance serial input to the GC. Specifics of the line driver are as follows:

Note
See “Setting the Com ID” on page 3-30 for additional details about serial
communication setups.

• Black Box brand


• Model LD485A-MP RS-232/RS-485 Multipoint Line Driver
• RS-232 input (to connect to the PC)

A - 30
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

• RS-422 or RS-485 output (to connect to the GC)

Note
For this example, a straightthrough RS-232 serial cable is used to connect between the
PC and the line driver.

RS-422 line terminations are illustrated in Figure A-22, below, and


jumper and switch settings to configure the line driver device are listed in
Table A-18 and Table A-19.

Figure A-22 Example RS-422 Serial Cable Terminations

Table A-18 Switch Settings for LD485A-MP, RS-422 to GC

Switch Type Label Position Purpose

Front Panel Switch NORMAL / DLB NORMAL Uses normal operation, instead of
loopback testing.
DIP Switch Bank XW1A DCE / XW1A DCE Sets line driver to operate as data
communications equipment (DCE).
XW1B DTE
DIP Switch Bank S2 UNTERM Eliminates need for resistor network
termination to connect one PC directly
to one GC.

A - 31
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Table A-19 Jumper Settings for LD485A-MP, RS-422 to GC

Jumper Position Purpose

W8 HALF half duplex operation


W9 ON no delay, clear to send (CTS) always true
W15 A-B RS-485 driver enabled by request to send (RTS)
W16 A-B half duplex turnaround delay at 5 ms
W17 B 100 ms disable timeout delay by 100 ms
W18 B-C RS-485 driver enabled by RTS

A.6 Example RS-485 PC-GC connection

This section demonstrates an example RS-485 connection from a PC to


GC that is accomplished through use of an asynchronous line driver/
interface device. The line driver device serves as an interface between
the RS-232 output of the PC and the RS-485 protocol needed for long
distance serial input to the GC. specifics of the line driver are as follows:

Note
See “Setting the Com ID” on page 3-30 for additional details about serial
communication setups.

• Black Box brand


• Model LD485A-MP RS-232/RS-485 Multipoint Line Driver
• RS-232 input (to connect to the PC)
• RS-422 or RS-485 output (to connect to the GC)

Refer to Figure A-23 and Figure A-24 for RS-485 line terminations,
jumpers and switch settings to configure the line driver device (also
listed in Table A-19).

A - 32
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Note
For this example, a straightthrough RS-232 serial cable is used to connect between the
PC and the line driver.

Figure A-23 Example RS-485 Serial Cable Terminations, Line Driver to GC


Controller Com3

A - 33
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure A-24 Example RS-485 Serial Cable Terminations, Line Driver to GC


Controller Com4

Table A-20 Switch settings for LD485A-MP, RS-485 to GC

Switch Type Label Position Purpose

Front Panel NORMAL / DLB NORMAL Normal operation used, instead of loopback
Switch testing.
DIP Switch Banks XW1A DCE / XW1A DCE Sets line driver to operate as data
communications equipment (DCE).
XW1B DTE
DIP Switch Banks S2 UNTERM Eliminates need for resistor network
termination to connect one PC directly to
one GC.

A - 34
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Table A-21 Jumper settings for LD485A-MP, RS-485 to GC

Jumper Position Purpose

W8 HALF half duplex operation


W9 0 ms 0 milliseconds delay from time request to send (RTS) received as
true until clear to send (CTS) asserted as true
W15 A-B RS-485 driver enabled by RTS
W16 A-B half duplex turnaround delay at 5 ms
W17 B 100 ms disable timeout delay by 100 ms
W18 B-C RS-485 driver enabled by RTS

A - 35
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

This page is intentionally left blank.

A - 36
Appendix B: Modem installation
B

This appendix provides information for installing the optional internal


modem for the Model 700 (P/N 3-0700-029). The modem
communications is established via COM4 and the MON2000 version 2.2
software, which then redirects modem communications through to
Com9.

Note
Revision C of the Internal Modem requires MON2000 software, version 2.2 or later.

B.1 Optional internal modem

WARNING
Before removing the cover from the GC, ensure that the power supply switch is OFF and
the AC power cord is disconnected. Failure to follow this warning may result in injury or
death to personnel or cause damage to the equipment.

To install the internal modem, do the following:

1. Halt any ongoing analysis runs.

2. Disconnect the power from the unit.

3. Remove the explosion-proof dome and the Oven System


protective cover.

4. Disconnect the Analog cable from J6 of the System Interface


board, then disconnect all CPU cables from the System Interface
board.

5. Remove the CPU assembly and install the modem, with


associated hardware into J19 and J20 PC/104 Bus connector on
the CPU assembly. The modem must be the top board in the
assembly.

B-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure B-25. Radicom 56K baud modem installation

6. Set communication port jumper settings on the modem board


(P/N 3-0700-029) as follows:
Jumper Pin

J26 1-2
J27 1-2
J30 1-2
J31 2-3

7. Plug one end of the modem extension cable (P/N 3-2350-075)


into RJ11 of the modem assembly. The in-line jack on the
remaining end of the modem extension cable attaches to the
lower left inside wall of the card cage shield (after the CPU
assembly is reinstalled and all cables reconnected to the System
Interface board). No software setup is required for this board.

8. Insert the phone line into the modem extension assembly.

B-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

B.2 Optional Ethernet board

To add an Ethernet assembly, do the following:

1. Disconnect the Analog cable from J6 of the FTB, then disconnect


all CPU and optional board cables and lines.

2. Remove the CPU assembly and install the Ethernet assembly with
associated hardware into J19 and J20 PC/104 Bus connector on
the CPU assembly. If an option board is already plugged into the
PC/104 Bus on the CPU, install the Ethernet assembly and
mounting hardware into the PC/104 Bus connector on the option
board.

3. Plug one end of the Ethernet extension cable (P/N 3-2350-088)


into J5 of the Ethernet assembly. The in-line jack on the remaining
end of the Ethernet extension cable attaches to the lower left
inside wall of the card cage shield, after the CPU assembly is
reinstalled and all cables and lines reconnected. No software
setup is required for this board.

4. Run the Ethernet line through the conduit into the lower
enclosure and connect it to the Ethernet extension cable.

B- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

This page is intentionally left blank.

B-4
Appendix C: Manifold Carrier for Gas Bottles
C

C.1 Carrier Gas

This appendix provides a description of the carrier manifold (P/N 3-5000-


050) that permits connection of two carrier gas bottles, or cylinders, to a
gas chromatograph (GC) system. The benefits of this manifold are as
follows:

Note
The illustration and information in this appendix are adapted from drawing #AE-10098.

• When one bottle is nearly empty (i.e., 100 psig remaining), the other
bottle becomes the primary supply.
• Each bottle can be disconnected for refilling without interrupting GC
operation.

C-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure C-1 Manifold for two carrier gas bottles to GC system

C.2 Installation and line purging

To install and purge the dual-bottle carrier gas manifold, proceed as


follows:

1. Install manifold as shown in Figure C-1. Close all valves and


tighten all fittings. Run tubing to the Analyzer, but do not
connect.

2. Back off pressure regulator (counter clockwise) fully.

C-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3. Open cylinder valve for Carrier Cylinder 1. The pressure indicator


will read the cylinder pressure.

4. Open the shut-off valve attached to the carrier regulator.

5. Regulate pressure out of the cylinder to 20 psig, then close the


cylinder valve.

6. Open V-1 (bleed valve) and let the carrier gas bleed to
atmosphere until both gauges read 0 psig, then close V-1.

7. Repeat Steps 4 and 5 two more times to purge the line to V-2.

8. Purge the line to V-3 by repeating Steps 2 through 6; but this


time, use bleed valve V-4 and Carrier Cylinder 2.

9. With valves 1-4 closed, open both cylinder valves and regulate
both carriers to approximately 10 psig.

10. Open V-2 and V-3 simultaneously, then turn both cylinder valves
off and let the carrier gasses bleed through the line to the
Analyzer until all gauges read 0 psig.

11. Repeat steps (8) and (9) two more times to purge line to Analyzer.

12. Close V-3, leave V-2 open.

13. Open cylinder valve of Carrier Cylinder 1 and, with carrier gas
flowing at 10 psig or below, connect carrier line to Analyzer.

14. Slowly regulate Carrier Cylinder 1 to 110 psig.

15. Open V-3 and slowly regulate Carrier Cylinder 2 to 100 psig. (By
doing this, all but 100 pounds of Carrier Cylinder 1 will be used
before any of Carrier Cylinder 2 is used. When Carrier Cylinder 1
gets to 100 pounds, replace the cylinder). Leak-check all of the
fittings carefully.

16. Let the Analyzer run overnight before calibrating.

C- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

C.3 Replacing a carrier cylinder

To replace one carrier cylinder without interrupting GC operation,


proceed as follows:

1. Turn cylinder valve off.

2. Back off on cylinder pressure regulator until handle turns freely.


Remove cylinder.

3. Attach new cylinder to regulator and repeat Steps 3 through 7 of


Installation Instructions, "Section C.2: Installation and line
purging", using appropriate bleed valve to purge line. Leak-check
the fitting.

4. Open the appropriate block valve to the Analyzer (V-2 or V-3) and
regulate outlet pressure to appropriate level. (See Steps 14 and
15 of Installation Instructions, "Section C.2: Installation and line
purging".)

C.4 Calibration gas

The calibration gas used for BTU analysis should be blended of gases
specified as Primary Standards. Primary Standard gases are blended
using weights that are traceable to the National Institute of Standards
and Technology (N.I.S.T). For other applications, the calibration gas
should be blended to the specifications detailed in the analyzer’s
Application Data Sheets.

The calibration gas should not have any component that could drop out
at the coldest temperature to which the gas will be subjected. A typical
blend for a temperature of zero degrees Fahrenheit is listed in Table C-1.
No dropout will occur in this calibration gas if it is blended at a pressure
below 250 psig.

C-4
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Table C-1 Contents of Example Calibration Gas

Mole
Gas
Percent

Nitrogen 2.5
Carbon Dioxide 0.5
Methane Balance
Propane 1.0
Isobutane 0.3
N-butane 0.3
Neopentane 0.1
Isopentane 0.1
N-pentane 0.1
N-hexane 0.03

The sampling system should be carefully planned for the best


chromatographic analyses.

C- 5
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

This page is intentionally left blank.

C-6
Appendix D: Local operator interface

D.1 Interface components for displaying and


entering data

The local operator interface (LOI) has multiple components that you can
use to interact with the unit.

Figure D-1. The LOI

A. LCD screen
B. Keypads
C. LED indicators

D-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

D.1.1 Light emitting diode indicators

There are three light emitting diode (LED) status indicators on the LOI
that show the overall status of the gas chromatograph. These LEDs are
positioned to the right of the display screen. Each LED, when lit, indicates
a specific condition.

The GC is currently running an analysis.

The GC has at least one unacknowledged alarm.

The GC has an out-of-tolerance or alarm condition that requires an


operator action.

D.1.2 LCD screen

The LCD screen measures 111.4mm by 83.5 mm and is capable of 640 by


4800 VGA pixel resolution, supporting both text and full graphics. The
backlighting, boost, and brightness are all under software control. The
boost and brightness levels are user-adjustable.

D.1.3 Keypad

The keypad consists of eight infrared keys. See “Navigating the screen”
on page D-5 for more information.

D-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

D.1.3.1 The command keys

The four keys located above the LCD screen are “command” keys.

D.1.3.2 The arrow keys

The four keys below the LCD screen are arrow keys that allow you to
navigate within the screen by scrolling or moving the cursor from field to
field. These keys function in the same way as a computer keyboard’s
arrow keys.

D.1.3.3 Pressing a key

A key is “pressed” by placing a finger on the glass over the associated key
hole and then removing the finger. Holding a finger over the key hole will
cause that key to repeat until the finger is removed.

D- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

D.2 Using the local operator interface

D.2.1 Start up

Upon starting the GC, the LOI automatically runs in Status Display
mode, in which it scrolls through a predefined series of screens,
displaying each screen for approximately 30 seconds.

Status Displays information about the operational state of the analyzer, including a
scrolling list of up to 25 user-selectable parameters that can be defined or
modified using the MON 2000 application.
NOTE: There may be more than one Status screen, depending upon the GC’s
mode of operation.
Live Chromatogram Displays the chromatogram for the current analysis in real time.
NOTE: There may be more than one Live Chromatogram screen, depending
upon the GC’s mode of operation.
NOTE: This screen does not display if the GC is not currently analyzing a
sample.
Active Alarms Lists active alarms, if any.
Heater Displays information about the PID temperature control loops.
Valves Displays the settings and states of the stream and analyzer valves.

In Status Display mode, you can manually scroll to the next screen
using the RIGHT arrow key, or to the previous screen using the LEFT
arrow key. You can pause automatic scrolling at any time by pressing the
EXIT key, and you can resume automatic scrolling by pressing either the
LEFT or the RIGHT arrow key. Automatic scrolling resumes after ten
minutes of keypad inactivity.

Pressing F1 when “MOVE” is displayed in the green box below it takes the
focus inside the screen so that you can navigate through the controls of
the screen using the LEFT, RIGHT, UP and DOWN keys. Pressing EXIT
returns the focus to the top level–that is, outside of the screen. Pressing
LEFT or RIGHT at the top level resumes automatic scrolling in addition
to moving to the previous or next screen.

At any time while in Status Display mode, you can press ENTER or F2 to
enter the Main Menu. Use the EXIT key to leave the Main Menu and

D-4
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

return the LOI to Status Display mode. If you log onto the GC from the
Main Menu to perform operations or edit data, when you exit the menu
you will automatically be logged off the LOI.

D.2.2 Navigating menus

At any time while in Status Display mode, you can press ENTER or F2 to
enter the Main Menu.

Use the UP and DOWN arrow keys to navigate between fields or controls
within each drop down menu. Pressing the DOWN arrow key while focus
is on the last field of a drop down menu moves the focus to the first field
on a screen. Alternatively, pressing the UP arrow key while focus is on the
first field of the drop down menu causes the focus to move to the last
field.

Use the ENTER key from the Main Menu to activate submenus and
individual menu items.

Press EXIT to leave the Main Menu and return the LOI to Status
Display mode, if no menu is dropped down. If a menu is dropped down
then pressing EXIT closes that menu.

If you log onto the GC from the Main Menu to perform operations or
edit data, when you exit the menu you will automatically be logged off
the LOI.

The Main Menu allows you access to all of the available LOI screens.;
however, you must be logged on to make changes. If you are not logged
on and you attempt to edit a field, the Login screen will appear first.

After a period of fifteen minutes of inactivity, you will be automatically


logged off.

D.2.3 Navigating the screen

LOI screens have several functions. They can display data for review; they
can display data for editing; and they can be used to initiate activities.

D- 5
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Within any given screen, the function of the ENTER key depends upon
the context. It can be used to validate and save changes or to initiate an
action.

If a validation error is found after pressing ENTER, an “Invalid Entry”


message displays. Press ENTER again to close the message and then re-
enter your data.

Pressing EXIT closes the currently open screen. If you have made
changes to the screen, the LOI will display a confirmation message asking
if you want to save your changes. Use the arrow keys to select the
appropriate button and press ENTER. If you select No, your changes will
be discarded and the Main Menu will display; if you select Cancel, the
message window will close and you will be returned to the current
screen; if you select Yes, your changes will be validated and saved and
then you will be returned to the Main Menu.

The F1 and F2 keys are context dependent. A one-word description of the


function of each of these keys displays in a green prompt box directly
under the key in the title bar of the top-level full-sized screen.

In some cases, F1 acts as a toggle between scrolling either a line or a


page at a time. When this is true, the currently selected option (LN or PG)
displays with a green background and black text, while the non-selected
option displays with a black background and green text. The table below
lists the possible functions of the F1 key:
Press F1 to move the cursor around within the boundary of
the screen.

Press F1 to open the edit dialog for the field that contains the
cursor. The type of dialog that displays depends upon the
type of field to be edited. See “Editing numeric fields” on
page D-7 and “Editing non-numeric fields” on page D-9 for
more information.
Press F1 to select the field to be edited.

Press F1 to delete the character to the left of the cursor.

D-6
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Press F1 to scroll line by line within a screen.

Press F1 to scroll page by page within a screen.

Note
Throughout this appendix, when referring to the F1 key, the key’s current valid
function will be indicated in parenthesis–for instance, F1 (MOVE) or F1 (SELECT).

The F2 key, when “MAIN” is displayed in the prompt box, closes all
screens and goes back to the Main Menu.

There is a navigation icon in the upper right corner of the screen that
indicates which navigation keys are active for the currently displayed
screen.

None Left Up Right

Down Left/Right Up/Down All

When you press a key, a green square will flash in the upper left corner if
the key is valid; if the key is not valid, a red box will flash in the upper left
corder.

D.2.4 Editing numeric fields

When the focus is on an editable field, pressing F1 (EDIT) will display the
Edit Dialog containing the field’s original text.

Use the LEFT and RIGHT arrow keys to move through the individual
characters within the field and to select the character to be changed. Use

D- 7
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

the UP and DOWN arrows keys to select the value of each digit. The
possible values are 1, 2, 3, 4, 5, 6, 7, 8, 9, 0, “-” (minus), “.” (period), and
“E”.

The “-” value is available for signed numbers.

The “.” and the “E” values are available for floating-point numbers,
except for retention times and timed event values.

The following rules apply when entering a floating-point value:


• More than one “E” is not allowed.
• More than one “.” is not allowed.
• If the previous position is an “E” then a “.” and a 0 is not allowed.
• A “” is allowed only after an “E” or at the first position only.
• If the previous position is “.” then an “E” is not allowed.
• If the first character is a “-” and the current index is 1 then a “.” is not
allowed.
• If the previous position is a “-” then a 0 is not allowed.
• If the next character is an “E” then a “.” is not allowed at the previous
location.

The DOWN arrow key moves backward in the list from the current value
of the selected digit.

The UP arrow key moves forward in the list from the current value of the
selected digit.

The F1 (BACKSP) key acts as a backspace and deletes the digit


immediately to the left of the current position.

The ENTER key validates and saves the entry, then closes the Edit
Dialog. The new entry will display in the field.

The EXIT key cancels any changes that were entered and closes the Edit
Dialog, restoring the previous value to the field.

D-8
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

D.2.5 Editing non-numeric fields

The function of the keys when editing non-numeric data is context-


dependant.

D.2.5.1 Editing alphanumeric fields

Alphanumeric fields take numbers (0 - 9) and letters (a - z, A - Z).

D.2.5.2 Selecting check boxes

Press F1 (SELECT) to select or clear a check box.

Figure D-2. Selecting a check box

D.2.5.3 Clicking buttons

Press F1 (EXECUTE) to click the button and execute the command.

D- 9
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

D.2.5.4 Selecting radio buttons

1. Press F1 (SELECT) to select a group of radio buttons.

2. Use the UP and DOWN arrow keys to move through the various
radio buttons within the group.

3. Press ENTER to accept the current selection or press EXIT to


abort any changes and to restore the previous selection.

D.2.5.5 Selecting an item from a list box

1. Press F1 (SELECT) while focused on the list box to switch it to edit


mode.

Figure D-3. Selecting a list box

2. Use the UP and DOWN arrows keys to move between the values
within the list box.

D - 10
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3. Press ENTER to accept the current selection or press EXIT to


abort the new selection and the list box will revert to the previous
selection.

D.2.5.6 Selecting an item from a combo box

1. Press F1 (SELECT) while focused on the combo field and a Combo


Dialog opens and displays a list of available selections.

Figure D-4. Selecting a combo box

2. Use the UP and DOWN arrow keys to move between the


selections.

3. Press ENTER to select the desired value or press EXIT to restore


the combo box’s initial value.

D.2.5.7 Entering a date and time

1. Press F1 (SELECT) while focused on the Date and Time field and
the Enter the Date and Time dialog displays. By default, the
focus is set on the “Month” unit.

D - 11
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-5. Entering a date and time

2. Use the UP and DOWN arrow keys to change the value of the
unit–that is, to go from January to February, or from 1 to 2.

3. Use the LEFT and RIGHT arrow keys to change units–that is, to
go from months to years or hours to minutes.

Note
If the focus is on the left most section, the LEFT arrow key will be inactive and
similarly if the focus is on the right most section, the RIGHT arrow key will be
inactive.

4. Press ENTER to save the change or press EXIT to discard the


change and restore the original value.

D.2.5.8 Setting the time

1. Press F1 (SELECT) while focused on the Time field and the Enter
the Time dialog displays. By default, the focus is set on the “Hour”
unit.

D - 12
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

2. Use the UP and DOWN arrow keys to change the value of the unit.

3. Use the LEFT and RIGHT arrow keys to change units–to go from
hours to minutes, for example.

Note
If the focus is on the left most section, the LEFT arrow key will be inactive and
similarly if the focus is on the right most section, the RIGHT arrow key will be
inactive.

4. Press ENTER to save the change or press EXIT to discard the


change and restore the original value.

D.3 Screen navigation and interaction tutorial

This tutorial, which guides you through the procedure for editing data on
a screen, will incorporate all of the preceding information to
demonstrate the typical method of navigating and interacting with the
LOI. You will learn how to perform the following actions:
• Opening and closing screens
• Navigating through tables
• Selecting fields for editing
• Saving data

1. From the Main Menu, click the RIGHT arrow key enough times
to navigate to the Application menu. The System submenu, since
it is the first item in the list, is already selected.

D - 13
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Note
In this instance, the term “click” means to tap the glass on the spot directly
above the arrow’s keyhole.

Figure D-6. Navigate to the Application menu

Note
Notice the navigation icon in the upper right corner, which indicates that all
four arrow keys are active. This allows you to navigate to all of the menu items
and sub menu items.

Note
Notice that the green prompt boxes are empty. This means that the F1 and F2
keys are inactive from the Main Menu.

2. Click ENTER. The System screen displays.

D - 14
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-7. The System screen

Note
Notice the navigation icon in the upper right corner, which indicates that no
arrow keys are active.

3. Notice that the green prompt boxes now display function


keywords. “MAIN” means that if you click the F2 key, the LOI will
close the current screen and return you to the Main Menu.
“MOVE” means that if you click the F1 key, you will be allow to use
the arrow keys to navigate within the System screen. Click F1.
The LOI switches to Edit mode.

4. Notice that the navigation icon in the upper right corner of the
screen indicates that the down arrow is active. Click the down
arrow once. Now the navigation icon indicates that both the up
and down arrows are active. Click the up arrow once to return to
the previous cell. The navigation icon again indicates that only the
down arrow is active.

5. Notice that the green F1 prompt box reads “EDIT”. Click F1.

D - 15
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

6. You must be logged in to the GC to make a change to any screen.


If you try to edit a field before logging in–as you just did–the LOI
displays the Login dialog to prompt you to log in.

Figure D-8. You must log in to the GC before editing a screen

Note
Notice that there is also a navigation icon on the Login dialog.

7. Click F1 (SELECT) and navigate up or down the list to highlight


your user name.

Note
For the remainder of this tutorial, when referring to the F1 key, the key’s
current valid function will be indicated in parenthesis–for instance, F1
(MOVE) or F1 (SELECT).

8. Click ENTER.

9. Navigate to the Pin field, press F1 (EDIT), and enter your


password.

D - 16
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

10. Click ENTER twice.

11. Now that your are logged in, you can edit the fields on the screen.
Click F1 (EDIT). The Enter the data dialog displays.

Figure D-9. The Enter the data dialog allows you to edit the selected field

12. To delete a character, press F1 (BACKSP). To enter new data, use


the UP and DOWN arrows to cycle through the available
characters, and use the RIGHT arrow key to add a new character
to the field.

13. When you are finished entering data, press ENTER to validate and
save the new information. To discard the information, press EXIT.

D - 17
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-10. The field now holds new data

Note
If a validation error is found after pressing ENTER, an “Invalid Entry” message
displays. Press ENTER to close the message and then re-enter your data.

14. Use the down arrow to move to the Is Multi User Write
Enabled? check box.

D - 18
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-11. The Is Multi User Write Enabled? check box

15. Press F1 (SELECT). This clears the check box.

D - 19
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-12. The Is Multi User Write Enabled? check box, no longer checked

16. Click F1 (SELECT) again to re-select the check box.

17. Navigate to the GC Mode field.

D - 20
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-13. The GC Mode field

18. Press F1 (SELECT). The Select an Item combo box displays.

D - 21
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-14. The Select an Item combo box

19. Use the DOWN arrow to scroll down to the last item in the combo
box. Press ENTER.

20. Press ENTER a second time to save all the changes that were
made to the table.

Note
If you neglect to press ENTER at this point, all of your changes will be lost.

21. Press F2 (MAIN) to return to the Main Menu.

This concludes the tutorial.

D - 22
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

D.4 The LOI screens

The Main Menu has six top-level submenus: Chromatogram,


Hardware, Applications, Control, Logs/Reports, and Manage.

The table below lists the submenus and commands that are available
from the Main Menu.
Submenu Command Subcommands Reference

Chromatogram
View
Chromatogram Settings page 26
Live Chromatogram View Screen page 27
(Status Mode)
Live Chromatogram Screen (Advanced page 28
Mode)
Archived Chromatogram Screen page 29
(Advanced Mode)
Live & Archived Chromatogram Viewer page 29
Options Menu
CGM Scaling Screen page 30
Chromatogram CDT Table page 31
Chromatogram TEV Table page 32
Chromatogram Raw Data Table page 32
Hardware
Heaters page 34
Valves page 35
Electronic Pressure Ctrl page 36
Detectors page 36
Discrete Inputs page 37
Discrete Outputs page 37
Analog Inputs page 38
Analog Outputs page 38
Installed Hardware page 39

D - 23
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Submenu Command Subcommands Reference

Application
System page 40
Component Data page 41
CDT 1
CDT 2
CDT 3
CDT 4
Timed Events page 41
TEV 1
TEV 2
TEV 3
TEV 4
Streams page 43
Status page 44
DET1
DET2
Ethernet Ports page 44
Logs/Reports
Maintenance Log page 46
Event Log page 47
Alarm Log page 48
Unack Alarms page 48
Active Alarms page 49
Report Display page 50
Control
Auto Sequence page 52
Single Stream page 53
Halt page 54
Calibration page 55
Validation page 56

D - 24
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Submenu Command Subcommands Reference

Stop Now page 56


Manage
LOI Settings page 58
Change PIN page 59
Diagnostics page 60
Log out no screen

Refer to the MON2020 Software for Gas Chromatographs User Manual for
detailed information regarding the commands listed in The table above.

D.4.1 The Chromatogram menu

The Chromatogram menu enables you to view live and archived


chromatograms and their associated CDT and TEV tables, as well as to
edit the display properties if the chromatogram screens.

Refer to the “Using the chromatograph functions” section of the


MON2020 Software for Gas Chromatographs User Manual for detailed
information regarding the Chromatogram menu screens.

D - 25
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-15. The Chromatogram menu

Figure D-16. The Chromatogram Settings screen

D - 26
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-17. The Live Chromatogram View (Status Mode) screen

Note
The blue box displays the current analysis time.

D - 27
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-18. The Live Chromatogram View (Advanced Mode) screen

Note
The blue box displays the current analysis time.

D - 28
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-19. The Archived Chromatogram (Advanced Mode) screen

Figure D-20. The Live & Archived Chromatogram Viewer Options screen

D - 29
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Note
The blue box displays the cursor’s x- (analysis time) and y- (amplitude) coordinates.

Figure D-21. The CGM Scaling screen

D - 30
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-22. The Chromatogram CDT Table screen

D - 31
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-23. The Chromatogram TEV Table screen

Figure D-24. The Chromatogram Raw Data Table screen

D - 32
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

D.4.2 The Hardware menu

The Hardware menu enables you to view and manage the GC’s
hardware components.

Refer to the “Using the hardware functions” section of the MON2020


Software for Gas Chromatographs User Manual for detailed information
regarding the Hardware menu screens.

Figure D-25. The Hardware menu

D - 33
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-26. The Heaters screen

D - 34
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-27. The Valves screen

Note
The usage (Sample/BF1, Dual Column), mode (Auto, Off), and state (green = on, black =
off, red = error) of each valve is displayed. See the “Configuring the valves” section of
the MON2020 Software for Gas Chromatographs User Manual for more information.

D - 35
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-28. The EPC screen

Figure D-29. The Detectors screen

D - 36
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-30. The Discrete Inputs screen

Figure D-31. The Discrete Outputs screen

D - 37
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-32. The Analog Inputs screen

Figure D-33. The Analog Outputs screen

D - 38
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-34. The Installed Hardware screen

D.4.3 The Application menu

The Application menu allows you to view the CDT, TEV and streams
tables for the GC. The System, Status, and Ethernet Ports screens are
also accessible from this menu.

Refer to the “Using the application functions” section of the MON2020


Software for Gas Chromatographs User Manual for detailed information
regarding the Application menu screens.

D - 39
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-35. The Application menu

Figure D-36. The System screen

D - 40
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-37. The CDT screen

Figure D-38. The TEV - Valve Events screen

D - 41
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-39. The TEV - Integration Events screen

Figure D-40. The TEV - Spectrum Gain Events screen

D - 42
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-41. The TEV - Analysis Time screen

Figure D-42. The Streams screen

D - 43
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-43. The Status screen

Figure D-44. The Ethernet Ports screen

D - 44
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

D.4.4 The Logs/Reports menu

The Logs/Reports menu enables you to view the various reports that
are available from the GC.

Refer to the “Logs/Reports” section of the MON2020 Software for Gas


Chromatographs User Manual for detailed information regarding the
Logs/Reports menu screens.

Figure D-45. The Logs/Reports menu

D - 45
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-46. The Maintenance Log screen

D - 46
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-47. The Event Log screen

D - 47
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-48. The Alarm Log screen

Figure D-49. The Unack Alarms screen

D - 48
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-50. The Active Alarms screen

D - 49
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-51. The Report Display screen

D.4.5 The Control menu

The Control menu enables you to stop, calibrate, or place on automatic


control a sample stream from the analyzer.

Refer to the “Control menu” section of the MON2020 Software for Gas
Chromatographs User Manual for detailed information regarding the
Control menu screens.

D - 50
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-52. The Control menu

D - 51
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-53. The Auto Sequence screen

D - 52
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-54. The Single Stream screen

D - 53
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-55. The Halt screen

D - 54
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-56. The Calibration screen

D - 55
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-57. The Validation screen

Figure D-58. The Stop Now screen

D - 56
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

D.4.6 The Manage menu

The Manage menu enables you to change the LOI’s settings, change a
user’s password, and log off of the GC to which you are connected.

Refer to the “Manage menu” section of the MON2020 Software for Gas
Chromatographs User Manual for detailed information regarding the
Manage menu screens.

Figure D-59. The Manage menu

D - 57
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-60. The LOI Settings screen

D - 58
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-61. The Create PIN screen

D - 59
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Figure D-62. The Diagnostic screen

D.5 Troubleshooting a blank LOI screen

If the LOI is powered up but the LCD screen is blank, do the following:

1. Unscrew and remove the LOI from the GC.

2. Flip the LOI over to expose its motherboard and associated


electronics.

D - 60
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Figure D-63. Jumpers at J105 on LOI motherboard

3. Check the jumpers located at J105 on the motherboard. These


jumpers control the screen’s power. To function properly, jumper
pins 3 and 4 must be set; if they are not, set them.

If the screen is still blank, contact Customer Service at 1-713-827-6380


for assistance.

D - 61
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

This page is intentionally left blank.

D - 62
Appendix E: LX-800 CPU Board Retrofit Instructions

This section describes a procedure for retrofitting a Model 700 gas


chromatograph with a WinSystems® LX-800 CPU board (P/N #2-3-2350-
190). The new CPU board is supplied with a retrofitting kit.

Figure E-1 Contents of the retrofitting kit

In addition to the new CPU board, the kit contains the following items:
• MON2000 Gas Chromatograph Software for Windows (P/N #2-3-2350-
400). This CD-ROM also contains the software’s user manual (P/N #3-
9000-522).
• Six replacement cables
- P/N #2-3-2350-083
- P/N #2-3-2350-077
- P/N #2-3-2350-087
- P/N #2-3-2350-084
- P/N #2-3-2350-080
- P/N #2-3-2350-081
• A extra fuse (P/N #2-5-4203-130)
• Two replacement card guides (P/N #2-4-5001-078)

E-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Due to the addition of the Flash Memory connector on the back of the
new CPU board, a new Analog board (P/N #2-3-0700-034) also must be
installed to prevent interference with the back of the CPU board when
inserted into the card cage. The new analog board is included with the
retrofit kit.

E.1 Introduction to the LX-800

The LX-800 CPU assembly has been designed to include all digital I/O and
COM1 through COM4 serial ports.

Figure E-2. LX-800 CPU board

In addition, the Unified Baseline Operating System (UniBOS) is now


resident on a 128 MB CompactFlash card instead of the slower 16 MB
DiskOnChip module. The CompactFlash card provides additional
memory for archiving data.

The UniBOS file on the CompactFlash card can be upgraded in the field
with MON2000. Refer to the MON2000 Software for Gas Chromatographs
user manual, which is located on the MON2000 CD-ROM, for
information about downloading 2350A applications and UniBOS
upgrades.

E-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

CAUTION
UniBOS is preloaded on this CPU board. Do not attempt to install BOS or an earlier
version of UniBOS. Doing so will irreversibly corrupt the firmware and will require the
purchase of a new CPU board. To learn the version level of the UniBOS loaded onto your
CPU board, refer to the label on the board’s back.

Figure E-3 CPU board serial number

The protocol setup for serial ports COM1 through COM4 can now be
configured through MON2000 version 2.58 or later. Each serial port can
be set to RS-232, RS-422 or RS-485. Protocol changes to the serial ports
on the COM4A board still require different jumper settings and IC chip
changes.

Other relevant facts about the LX-800 CPU board include:


• Up to three optional boards can be plugged directly into the PC104
bus (connectors J29 and J27) on the CPU board assembly.
• An optional COM4A board provides four additional serial ports:
COM5 through COM8.
• A video driver board for the LOI and modem board and/or Ethernet
board can also be plugged directly into the PC104 bus for additional
communications capabilities.
• If more that one PC104 board is installed and a modem is included,
the modem must always be installed on top of the stack.

E- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

• A new video card cable (PN #2-3-0700-098) is required because the


PC104 connectors on the new CPU noard have been moved to the
end of the board next to the edge connectors; this places the LOI
Video card 'Panel Out' connector about 3.5 inches further away from
the front panel.

E.2 Upgrading your 16-bit application to its


32-bit equivalent

Before replacing a 16-bit CPU board with the new 32-bit version, you
must first upgrade the 16-bit application to its 32-bit equivalent.

Note
This procedure applies to MON2000 version 4.04 or later.

E.2.1 Choosing the appropriate 32-bit application

Before performing the upgrade, you need to know the file names of the
16-bit application and its 32-bit equivalent.

If you don’t know the filename of the 16-bit application that you intend
upgrade, you can call Customer Support at 1-713-827-6314 to learn it.
Be prepared to supply a sales order number or a GC serial number.

Once you know the filename of the appropriate 16-bit application, do


the following to learn its Application Base Name, which will aid you in
learning the file name of the 16-bit application’s 32-bit equivalent:

1. Select File  Offline Edit  File Selection.... The Open GC


Application File dialog displays.

2. Locate the appropriate 16-bit application file and select it. Click
Open.

E-4
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

3. Select System from the Application menu. The System window


displays.

Figure E-4. The System window

4. The Application Base Name is located at the bottom of the window.


Make note of it.

5. Click OK to close the window.

E- 5
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

6. When you know the Application Base Name of the 16-bit


application, consult the following table to learn the file name of
its 32-bit equivalent:
16-bit Application Base Name 32-bit Application File Name

USASTD1A Energy Measurement C6+ 4 min (700_Mode0_v4XX).APP


USADUAL1 Energy Measurement C9+ 5 min (700_Mode1_4XX).APP
ISOSNGLSTD1 ISO Energy Measurement C6+ 4 min (700_2350ISO1_v4XX).APP
ISODULSTD1 ISO Energy Measurement C9+ 5 min (700_2360ISO1_v4XX).APP
USADUALM2 Energy Measurement C9+ 5 min (700_Mode2_v4XX).App
700Dew2US Energy Measurement C9+ 5 min (700_2360Dew2US_v4XX).APP
700DewUS Energy Measurement C9+ 5 min (700_2360DewUS_v4XX).app
USSTDFILE01 Energy Measurement C6+ 4 min (700_2350EXMB_v4XX).APP
700EXMBHCD Energy Measurement C9+ 5 min (700_EXMBHCDP_v4XX).APP
USASTD1A15 Energy Measurement C6+ 4 min (700_Mode0_15s_v4XX).App

E.2.2 Upgrading to the 32-bit application

The end result of this procedure will be a 32-bit version of the 16-bit
application using a 32-bit application template file.

1. Select File  Offline Edit  Upgrade Application. The Select


model application for the upgrade dialog displays.

2. Navigate to the appropriate 32-bit application template file and


select it.

E-6
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Note
The latest versions of these application template files were installed with
MON2000 and are typically located at C:\GC\APP\.

Note
If the application template file selected is not newer than the currently
installed application, or if it is not the same type of application, MON2000
displays the following error message:
The selected application is not a compatible upgrade

3. Click Open. The Save upgraded application as... dialog displays.

4. Type a new name for the upgraded application into the File name
field.

Note
It is recommended that you give the 32-bit application a name similar to the
name of the 16-bit application it will replace.

Note
It is recommended that you do not give the 32-bit application the same name
as the application template file on which it is based. Doing so will over-write
the application template file.

5. Click Save. MON2000 will create a 32-bit version of the 16-bit


application. When the process completes, the Application
upgrade complete message displays.

6. Click OK.

You can now install the 32-bit CPU board.

E- 7
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

E.3 Installing the new CPU board

To install the new CPU board, do the following:

1. Remove the front panel or the LOI and disconnect the cables
going to the card cage assembly.

2. Remove the CPU board from the card cage.

3. Unplug all PC104 boards from the CPU board and set them aside.

4. Make note of the analog board’s slot number in the card cage and
then eject the analog board from the card cage.

5. Install the new analog board (P/N #3-0700-034) and insert it in


the same slot of the card cage as the previous board.

6. Re-install the PC104 option boards on the new CPU board.

7. If there is a video driver board for an LOI in the stack, replace the
'Panel Out' cable with the new cable (P/N #3-0700-098) that is
supplied with the kit.

8. Insert the CPU board into the slot above the analog board and
connect the remaining cables. If necessary, refer to “Internal
Cable Wiring” (DE-20991), which is located in the drawings
section at the back of the manual.

9. If there is an Ethernet card in the stack, replace the Ethernet


extension cable with the longer cable that is supplied in the kit.

10. If there is a COM4A board in the stack that is not installed at the
top position, it may be necessary to remove the cable clamp on
the connector that plugs into the board to avoid interference with
the board above it. The clamp is not required and can be
discarded.

11. Reconnect all cables to the switch panel or LOI and the analog
card.

E-8
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

12. Power up the analyzer and download the desired application to


the system.

13. Start MON2000. The four CPU serial ports, COM1 - COM4, can be
configured through MON2000.

Note
Make sure that MON2000 version 2.58 or later is installed.

14. Select Serial Ports... from the Application menu. The Serial Ports
window displays.

15. Use the Mode column to select the protocol for each serial port.

Figure E-5. Serial ports window

E- 9
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

This page is intentionally left blank.

E - 10
Appendix F: Shipping and long-term storage
recommendations

The following recommendations should be followed:


• For shipping purposes the gas chromatograph should be secured to a
wooden pallet, maintained in a vertical position and enclosed in a
wood framework with a cardboard skin.
• Auxiliary equipment such as sample probes may be stored in the
packaging in which it was shipped. If this packaging material is no
longer available, secure the equipment to prevent excessive shaking
and protect the accessories in a water proof enclosure.
• The gas chromatograph should be stored in a sheltered environment
that is temperature controlled between -30oC (-22oF) and 70oC
(158oF) to keep the gas chromatograph’s protective coatings from
deteriorating from exposure to rain or caustic or corrosive
environments. Humidity in the sheltered environment should be
non-condensing.
• The program stored in the remote or integral controller memory may
be retained through battery back-up for at least two years. If lost for
some reason, a custom program for downloading the appropriate GC
application is included on the CD shipped with the system
documentation.
• If the gas chromatograph has been in operation, the system should
be purged with carrier gas before powering the gas chromatograph
down. Allowing the gas chromatograph to perform a couple of
analysis cycles without sample gas is an acceptable method of
purging the system. Monitor the results and remove power after
component values fall to “0” or after peaks are significantly reduced
in size.
• After removing power from the GC, remove the purge gas and
immediately cap all inlets and vents, including the carrier drier. These
vents and inlets should be capped with the fittings that were in place
when the GC shipped from the factory or with Swagelok caps (not
provided). This will protect the columns and filters and should result
in a trouble-free start up when the unit is returned to service.

F-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

• The sample conditioning system vents and inlets should also be


capped with the fittings that were in place when the system shipped
from the factory. Additionally, all vents should be closed.
• Any remaining openings–such as conduit entries–should also have
appropriate plugs installed to prevent foreign material such as dust or
water from entering the system.

F-2
Appendix G: Recommended spare parts

The following tables list the recommended spare parts that would allow
you to maintain a single GC gas chromatograph for one year.

Quantity Single or Dual TCD GCs

5+ GCs or
1-5 GCs Critical Description Part No.
Installations

0 1 PCA, CPU 32-bit w/ (4) RS-232 & BOS - Requires 32-bit 2-3-0700-232
application file
0 1 PCA Analog I/O (8 in / 4 out) 2-3-2350-041
0 1 Preamplifier Board 2-3-0580-002
0 1 Field Termination Board 2-3-0700-010
1 2 Fuses, Assortment (5 each 1A, 3A and 6A) 2-3-0700-136
0 1 Dual Methods Adapter Board 2-3-0700-011
0 1 Driver I/O Board 2-3-0700-005
0 1 Multifunction Board 2-3-0700-004
0 Note 1 Modem Bd. PC104 - Board Only, Upgrade Kit is part 2- 2-3-0700-029
3-2350-142
0 Note 1 PCA, 4 Isolated Analog Outputs Board 2-3-0700-007

0 Note 1 PCA - Board with 8 Non-Isolated Analog Outputs for 2-3-0580-037


use with the Model 700/1000A only
0 Note 2 Power Supply 24 VDC 2-3-0700-117

0 Note 3 Assembly, Power Supply 115/230 VAC - Model 700 and 2-3-0700-110
Model 1000A only
2 2 Solenoid Valve, Srs 2-4-0700-152
1/Valve 1/Valve Repair Kit, 6-port Valve - For use on Model 700 only 2-4-0700-187
1/Valve 1/Valve Repair Kit, 10-port Valve - For use on Model 700 only 2-4-0700-171
1 1 Column Set Note 4
0 1/Detector Kit, Thermistors (TCD) Note 4
1 1 Teflon Thermistor Seals (Set Of 10) 2-3-0500-391

G-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Quantity Single or Dual TCD GCs

5+ GCs or
1-5 GCs Critical Description Part No.
Installations

1/Stream 1/Stream Filter Element 2-micron,Swagelok SS-2F-K4-2 2-4-5000-113


1/Stream 1/Stream Membrane Kit, Genie® Model 120 Filter/Bypass/LSO 2-4-5000-938

1 1 recommended if this option is installed on the Model 700.


2
1 recommended if Model 700 is powered with 24 VDC line.
3 1 recommended if Model 700 is powered with AC line.
4
Application dependent. Please contact customer service at 1-888-801-1452 and provide
sales order number for recommended part number and description.

Quantity FID/TCD GCs

5+ GCs or
1-5 GCs Critical Description Part No.
Installations

0 1 PCA, CPU 32-bit w/ (4) RS-232 & BOS - Requires 32-bit 2-3-0700-232
application file
0 1 PCA Analog I/O (8 in / 4 out) 2-3-2350-041
0 1 Preamplifier Board 2-3-0580-002
0 1 PCA ADC Main Board Modified for FID/FPD 2-3-0700-032
0 1 Field Termination Board 2-3-0700-010
1 2 Fuses, Assortment (5 each 1A, 3A and 6A) 2-3-0700-136
0 1 Dual Methods Adapter Board 2-3-0700-011
0 1 Driver I/O Board 2-3-0700-005
0 1 Multifunction Board 2-3-0700-004
0 Note1 Modem Bd. PC104 - Board Only, Upgrade Kit is part 2-3- 2-3-0700-029
2350-142
0 Note1 PCA, 4 Isolated Analog Outputs Board 2-3-0700-007

0 Note1 PCA - Board with 8 Non-Isolated Analog Outputs for use 2-3-0580-037
with the Model 700/1000A only
0 Note2 Power Supply 24 VDC 2-3-0700-117

0 Note3 Assembly, Power Supply 115/230 VAC - Model 700 and 2-3-0700-110
Model 1000A only

G-2
Model 700 Gas Chromatograph System Reference Manual
APRIL 2012 3-9000-521

Quantity FID/TCD GCs

5+ GCs or
1-5 GCs Critical Description Part No.
Installations

2 2 Solenoid Valve, Srs 2-4-0700-152


1/Valve 1/Valve Repair Kit, 6-port Valve - For use on Model 700 only 2-4-0700-187
1/Valve 1/Valve Repair Kit, 10-port Valve - For use on Model 700 only 2-4-0700-171
1 1 Column Set Note4
0 1 Methanator Convertor Assembly Note4
0 1 Assembly, Micro-FID Detector and Connector Board 2-3-0700-148
complete, Model(s) 700 and 1000A
0 1/Detector Kit, Thermistors (TCD) Note4
1 1 Teflon Thermistor Seals (Set Of 10) 2-3-0500-391
1/Stream 1/Stream Filter Element 2-micron,Swagelok SS-2F-K4-2 2-4-5000-113
1/Stream 1/Stream Membrane Kit, Genie® Model 120 Filter/Bypass/LSO 2-4-5000-938

1
1 recommended if this option is installed on the Model 700.
2 1 recommended if Model 700 is powered with 24 VDC line.
3
1 recommended if Model 700 is powered with AC line.
4 Application dependent. Please contact customer service at 1-888-801-1452 and provide
sales order number for recommended part number and description.

Quantity FID GCs

5+ GCs or
1-5 GCs Critical Description Part No.
Installations

0 1 PCA, CPU 32-bit w/ (4) RS-232 & BOS - Requires 32-bit 2-3-0700-232
application file
0 1 PCA Analog I/O (8 in / 4 out) 2-3-2350-041
0 1 Preamplifier Board 2-3-0580-002
0 1 PCA ADC Main Board Modified for FID/FPD 2-3-0700-032
0 1 Field Termination Board 2-3-0700-010
1 2 Fuses, Assortment (5 each 1A, 3A and 6A) 2-3-0700-136
0 1 Dual Methods Adapter Board 2-3-0700-011

G- 3
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

Quantity FID GCs

5+ GCs or
1-5 GCs Critical Description Part No.
Installations

0 1 Driver I/O Board 2-3-0700-005


0 1 Multifunction Board 2-3-0700-004
0 Note1 Modem Bd. PC104 - Board Only, Upgrade Kit is part 2- 2-3-0700-029
3-2350-142
0 Note1 PCA, 4 Isolated Analog Outputs Board 2-3-0700-007

0 Note1 PCA - Board with 8 Non-Isolated Analog Outputs for 2-3-0580-037


use with the Model 700/1000A only
0 Note2 Power Supply 24 VDC 2-3-0700-117

0 Note3 Assembly, Power Supply 115/230 VAC - Model 700 and 2-3-0700-110
Model 1000A only
2 2 Solenoid Valve, Srs 2-4-0700-152
1/Valve 1/Valve Repair Kit, 6-port Valve - For use on Model 700 only 2-4-0700-187
1/Valve 1/Valve Repair Kit, 10-port Valve - For use on Model 700 only 2-4-0700-171
1 1 Column Set Note4
0 1 Methanator Convertor Assembly Note4
0 1 Assembly, Micro-FID Detector and Connector Board 2-3-0700-148
complete, Model(s) 700 and 1000A
1/Stream 1/Stream Filter Element 2-micron,Swagelok SS-2F-K4-2 2-4-5000-113
1/Stream 1/Stream Membrane Kit, Genie® Model 120 Filter/Bypass/LSO 2-4-5000-938

1 1 recommended if this option is installed on the Model 700.


2
1 recommended if Model 700 is powered with 24 VDC line.
3 1 recommended if Model 700 is powered with AC line.
4
Application dependent. Please contact customer service at 1-888-801-1452 and provide
sales order number for recommended part number and description.

G-4
Appendix H: Engineering Drawings
H

H.1 List of Engineering Drawings

This addendum contains the following engineering drawings:


Drawing # Title

BE-21154 Assembly Modem Board Model 700 GC


CE-21744 Assembly CPU Board Model 700
CE-20931 Assembly Radial 6-port Valve, Kiosk Oven Model 700 GC
CE-20958 Assembly 10-port Valve Model 700 GC
CE-21276 Assembly Micro-FID Model 700 GC
CE-22210 Methanator Assembly
CE-25002 C9+ Flow Config. Det. 1 B/F to Meas.D/C Det. 2 to Meas.
CE-25003 C6+ Flow Config. Det. 1 B/F to Meas.D/C Det. 2 to Meas.
CE-25004 C6+ Flow Config. Det. 1 B/F to Meas.to Meas.
CE-25006 C6+ and O2 Flow Config. Det. 1 B/F to Meas.D/C, DC
CE-25007 Flow ConfigurationDet. 1 B/F to Meas. (Helium)Det. 2 B/F to Meas.
(Argon)
DE-20991 Internal Cable Wiring Model 700 Analyzer (Sheets 1 & 2)
DE-20992 Field Wiring Field Termination Board Model 700 GC
DE-20993 Outline and Dimensional Pole, Wall & Floor Mounting Units Model
700 GC
DE-21405 Internal Wiring Micro-FID

H-1
System Reference Manual Model 700 Gas Chromatograph
3-9000-521 APRIL 2012

This page is intentionally left blank.

H-2
(2) NOTES:
LOWER ACTUATOR PLASTIC RETAINER DISK 13. 6 PORT VALVE ASSEMBLY INSTRUCTIONS
DIAPHRAGMS 10
THIS PROCEDURE TO BE PERFORMED IN A CLEAN AND DRY
LARGE AREA. ALL PARTS TO BE BLOWN CLEAN AND DRY WITH
GUIDE NITROGEN BEFORE ASSEMBLY.
3
PIN 1. ASSEMBLY IS ACCOMPLISHED IN THE UPSIDE DOWN POSITION.
10 VITON GASKET
(3) 2. PLACE ITEM 9, PRIMARY PLATE INTO SHOP ASSEMBLY FIXTURE AND
LONG INSTALL ITEM 3, LARGE DOWEL PIN AND ITEM 2, SMALL DOWEL PIN.
PISTON 4
3. PLACE ITEM 10, AMBER SEALING DIAPHRAGM ( HAVING NO ACTUATOR
2 SMALL GUIDE PIN HOLES) ALIGN LARGE AND SMALL DOWEL PIN HOLES.

(2) 4. PLACE ITEM 10, WHITE NOMEX CUSHION DIAPHAGM (HAVING NO


LOWER ACUATOR HOLES) ALIGN LARGE AND SMALL DOWEL PIN HOLES.
PISTON 1 10 UPPER ACTUATOR DIAPHRAGMS
PLATE 5. PLACE ITEM 5, UPPER PISTON PLATE OVER DOWEL PINS.

(3) 10 NOMEX CUSHION DIAPHRAGM 6. PLACE ITEM 6, SHORT PISTONS IN PISTON PLATE 3 PLACES.
SHORT PISTON SHAFT MUST FALL THROUGH HOLES. DO NOT FORCE.
6
PISTONS
7. PLACE ITEM 10, AMBER UPPER ACTUATOR DIAPHRAGMS WITH
10 LARGE ACTUATOR HOLES OVER DOWEL PINS 2 PLACES. ALIGN
SEALING DIAPHRAGM WITH LARGE AND SMALL DOWEL PINS.
UPPER
PISTON 5 8. PLACE ITEM 1, LOWER PISTON PLATE OVER DOWEL PINS.
PLATE 9 PRIMARY PLATE
9. PLACE ITEM 4, LONG PISTONS IN PISTON PLATE 3 PLACES.
PISTON SHAFT MUST FALL FREELY THROUGH HOLES.
DO NOT FORCE.
7 FLAT WASHER
13. 10. PLACE ITEM 10, AMBER LOWER ACTUATOR DIAPHRAGMS WITH
SMALL ACTUATOR HOLES OVER DOWEL PINS 2 PLACES. ALIGN
WITH LARGE AND SMALL DOWEL PINS.
8 TORQUE BOLT
11. PLACE ITEM 10, BLACK VITON GASKET, OVER DOWEL PINS. ALIGN WITH
LARGE AND SMALL DOWEL PINS.
12. INSTALL ITEM 8, BOLT AND ITEM 7, FLAT WASHER UP THRU
PRIMARY PLATE. REMOVE FROM FIXTURE AND INSTALL INTO UNIT.

13. IF THE ASSEMBLED VALVE IS TO BE SHIPPED AS A SPARE OR


REPLACEMENT VALVE, INSTALL PLASTIC RETAINER DISK (2-4-700-191).

14. TORQUE THE BOLT (ITEM 8) TO 30 FT. LBS. WHEN THE VALVE IS
INSTALLLED ON THE ANALYZER.

SI METRIC G 08/13/10 CC ECO-XX-5005838 EM HS THIS DRAWING IN DESIGN AND DETAIL IS OUR PROPERTY AND MUST NOT BE USED EXCEPT IN CONNECTION WITH OUR
WORK. IT SHALL NOT BE REPRODUCED AND SHALL BE RETURNED TO US ON DEMAND. ALL RIGHTS ARE RESERVED.
THIRD ANGLE PROJECTION F 7-6-06 HM ECO-XX-5001969 EM NP TITLE
GEOMETRIC TOLERANCES &
E 4-2-06 HM ECO-XX-5001716 EM NP DIMENSIONS PER
ANSI Y14.5
D 2-25-05 HM ECO-XX-5000518 EM BLB LATEST REVISION ASSEMBLY
MATERIAL: C 8-3-04 HM ECO-XX-212474 EM HS RADIAL 6 PORT VALVE, KIOSK OVEN
B 6-29-04
UNLESS OTHERWISE NOTED MODEL 700 G.C.
SEE ORDER DLT ECO-XX-209763 EM DLT ALL DIMENSIONS IN INCHES
X.XX ±.015

A 10-17-03 HM REL'D ECO 189137 DLT BLB X.XXX


ANGULAR
±.005
±0° 30'
FINISH:
FINISH 200 RA MAX
DRN DATE DWG NO. REV
REV DATE DRN DESCRIPTION CHKD APPD HM 8-19-02
BLOCK N/A
BREAK ALL SHARP CORNERS TO CHKD DLT DATE
10-17-03
CE-20931 G
.003-.015 RADIUS AND REMOVE
PROJ. FILE NO. G-00001 FILE NAME: CE20931G1.SLDDRW, DATE: 08/13/10, TIME: 8:45 A.M. BLB DATE
10-17-03 SCALE
1:1 P/N SHT
ALL BURRS APPD 2-3-0700-107 1 OF 1
NOTES:
PLASTIC RETAINER DISK THIS PROCEDURE TO BE PERFORMED IN A CLEAN AND DRY
AREA. ALL PARTS TO BE BLOWN CLEAN AND DRY WITH
14. 7 VITON GASKET NITROGEN BEFORE ASSEMBLY.
10 PORT VALVE ASSEMBLY INSTRUCTIONS

(2)
7 LOWER ACTUATOR DIAPHRAGMS

(5)
5 LONG PISTON

LOWER
PISTON 3 .156 DIA.
PLATE 6 GUIDE PIN

14.
(2)
.093 DIA. 10
GUIDE PIN 7 UPPER ACTUATOR DIAPHRAGMS

(5)
SHORT
PISTONS 4

2 UPPER PISTON PLATE

(2)
CUSHION 7
DIAPHRAGM

14.

SEALING 7 15.
DIAPHRAGM

1 PRIMARY PLATE

9 FLAT WASHER

8 TORQUE BOLT

SI METRIC H 08/13/10 CC ECO-XX-5005838 EM HS THIS DRAWING IN DESIGN AND DETAIL IS OUR PROPERTY AND MUST NOT BE USED EXCEPT IN CONNECTION WITH OUR
WORK. IT SHALL NOT BE REPRODUCED AND SHALL BE RETURNED TO US ON DEMAND. ALL RIGHTS ARE RESERVED.
THIRD ANGLE PROJECTION G 7-6-06 HM ECO-XX-5001969 EM NP TITLE
GEOMETRIC TOLERANCES &
F 4-2-06 HM ECO-XX-5001716 EM NP DIMENSIONS PER

E 2-25-05 HM ECO-XX-5000518 EM BLB


ANSI Y14.5
LATEST REVISION ASSEMBLY
8-3-04 HM ECO-XX-212474 EM HS
10 PORT VALVE
MATERIAL: D
UNLESS OTHERWISE NOTED MODEL 700 G.C.
SEE ORDER C 6-29-04 HM ECO-XX-209763 EM DLT ALL DIMENSIONS IN INCHES
X.XX ±.015

FINISH:
B 11-11-03 HM ECO-XX-190965 EM BLB X.XXX
ANGULAR
±.005
±0° 30'
FINISH 200 RA MAX
REV DATE
DRN HM DATE 10/1/03 DWG NO. REV
BLOCK N/A DRN DESCRIPTION CHKD APPD
CE-20958
BREAK ALL SHARP CORNERS TO
.003-.015 RADIUS AND REMOVE
CHKD DLT DATE 10-17-03 H
PROJ. FILE NO. G-00001 FILE NAME: CE20958H1.SLDDRW, DATE: 08/13/10, TIME: 8:15 A.M. ALL BURRS APPD BLB DATE 10-17-03 SCALE
1:1 P/N 2-3-0700-118 SHT
1OF1
ITEM PART DESCRIPTION QTY. METHANATOR ASSEMBLY:
NO. NUMBER
1. INSERT & ALIGN HEATER (ITEM 7) INSIDE HEATER ADAPTER TUBE
1 2-4-0710-181 METHANATOR CASE 1 (ITEM 11).
BE-22201
METHANATOR CAP 2. CENTER & ALIGN THE HEATER ADAPTER TUBE (ITEM11) IN THE
2 2-4-0710-180 BE-22200 1 COLUMN (ITEM 5) WITH THE HEATER WIRES AT THE SHORT END
OF THE COLUMN.
3 2-4-9214-016 RETAINING RING 1
WH_275 (2) 3. SLIDE INSULATOR (ITEM12) THRU THE HEATER WIRES TO FLUSH WITH HEATER
AS SHOWN IN VIEW A-A
4 2-4-9326-911 BUSHING, 1 10
NIAGARA SB437-5 4. CENTER & ALIGN HEATER (ITEM 7) & INSULATOR (ITEM12), FROM ABOVE
ALONG WITH HEATER ADAPTER TUBE (ITEM11) & COLUMN ASSEMBLY (ITEM
5 2-4-0700-207 COLUMN, METH 1 5)IN THE ISOLATOR METHANATOR WITH THE HEATER WIRES AT THE END
BE-21339 WITH THE RTD HOLE. BEND THE LONG TUBE UNTIL IT IS PARALLEL WITH THE
ISOLATOR, METHANATOR TWO COLUMN TUBES SHORT TUBE AND THE ENDS ARE AROUND THE SAME HEIGHT.
6 2-4-0700-208 BE-21340 1
3 5. INSTALL THE RTD (ITEM 8) IN THE HOLE IN THE METHANATOR ISOLATOR.
HEATER, 24V, 35W ENSURING THE RTD WIRES HAVE SLACK, ANCHOR THEM TO THE
7 ( 3/8 "X 1.5 "L)
2-4-0700-224 SC37-1.5/35W/24V/SF1-32 1
HEATER WIRE WITH HIGH TEMPERATURE TAPE WITHIN AN INCH OF
THE HEATER. SLIGHTLY FILL BETWEEN HEATER & COLUMN WITH MILK
MAGNESIA TO MAXIMIZE HEAT CONDUCTION.
VIEW B-B 6. CENTER & ALIGN THE BOTTOM INSULATION FROM INSULATION KIT (ITEM 9)
8 2-4-0700-225 RTD, MINCO S72PD20Y36 1 2
INSULATION KIT INSIDE AND TO THE BASE OF METHANATOR CASE (ITEM1)

7. WRAP CENTER INSULATION FROM INSULATION KIT(ITEM9) AROUND


METHANATOR ASSEMBLY & PLACE THE METHANATOR ASSEMBLY INSIDE
9 2-4-0710-289 INSULATION KIT 1 4 THE CASE(ITEM1)

SWAGELOK UNION 1 8. PLACE TOP INSULATION FROM INSULATION KIT (ITEM9)FROM ABOVE & ON
10 2-4-9500-004 2 THE METHANATOR ASSEMBLY
SS-1F0-6GC
11 2-4-0700-297 HEATER ADAPTER TUBE 1 VIEW A-A 9. PACK INSULATION AROUND THE WIRES AND TUBES, AND CLEAN
TOP INSULATION (2) INSULATION MATERIAL AWAY FROM INSIDE MATING AREA OF THE CASE.
HEATER WIRE INSULATOR HEATER 7
12 2-4-0710-290 1 10. INSTALL THE THREAD BUSHING (ITEM 4) INTO THE HOLE IN THE
BE-22656 CAP (ITEM 2).
TUBE 11 12 HEATER WIRE INSULATOR
11. PUSH THE WIRES AND TUBES THROUGH THE THREAD BUSHING.
CAREFULLY ALIGN THE CAP WITH THE BORE OF THE CASE AND
12 PRESS INTO PLACE.

12. INSTALL THE RETAINING RING (ITEM 3) INTO THE GROOVE IN THE
CASE OPENING.
SLIDE INSULATOR THRU
HEATER WIRE, RTD
TILL FLUSH WITH HEATER 8

6 ISOLATOR
9

5 COLUMN

CENTER INSULATION

BOTTOM INSULATION (2)


12

VIEW B-B
INSULATION KIT

7 7

THIS DRAWING IN DESIGN AND DETAIL IS OUR PROPERTY AND MUST NOT BE USED EXCEPT IN CONNECTION WITH OUR
WORK. IT SHALL NOT BE REPRODUCED AND SHALL BE RETURNED TO US ON DEMAND. ALL RIGHTS ARE RESERVED.
THIRD ANGLE PROJECTION TITLE
GEOMETRIC TOLERANCES &

VIEW A-A
DIMENSIONS PER
ANSI Y14.5
LATEST REVISION
ASSEMBLY
MATERIAL: C 11-25-10 JDB ECO-XX-5005915 ADS NP METHANATOR
SEE BOM B 09-28 -10 JDB ECO-XX-5005936 ADS NP
UNLESS OTHERWISE NOTED
ALL DIMENSIONS IN INCHES 700 & 700XA GC
X.XX ±.010

FINISH:
A 6-13 -08 HM ECO-XX-5003758 DM BLB X.XXX
ANGULAR
±.005
±0° 30'
FINISH 200 RA MAX
N/A REV DATE DRN MANCHA DATE 03/28/08 DWG NO. REV
DRN DESCRIPTION CHKD APPD
CE-22210
BREAK ALL SHARP CORNERS TO
.003-.015 RADIUS AND REMOVE
CHKD DM DATE 06/13/08 C
PROJ. FILE NO. - NONE FILE NAME: CE22210C1.SLDDRW, DATE: 11-25-10, TIME: 12:40 P.M. ALL BURRS ENG
BLB DATE
06/13/08
SCALE
3:4 P/N
2-3-0710-073 SHT
1 OF 1
WARRANTY CLAIM PROCEDURES

To make a warranty claim, you, the Purchaser, must:

1. Provide Rosemount Analytical, Inc. or Daniel Measurement and Control, Inc.


with proof of the Date of Purchase and proof of the Date of Shipment of the
product in question.
2. Return the product to Daniel Measurement Services (DMS) within 12 months
of the date of original shipment of the product, or within 18 months of the
date of original shipment of the product to destinations outside of the
United States. The Purchaser must prepay any shipping charges. In addition,
the Purchaser is responsible for insuring any product shipped for return, and
assumes the risk of loss of the product during shipment.
3. To obtain warranty service or to locate the nearest DMS office, sales office, or
service center, call 1-888-801-1452, fax a request to (713) 827-6312, or
write to:
Daniel Measurement Services
11100 Brittmore Park Drive
Houston, Texas 77041

You can also contact DMS via www.emersonprocess.com/daniel.

4. When contacting DMS for product service, the Purchaser is asked to provide
information as indicated on the following page entitled “Customer Repair
Report”.
5. For product returns from locations outside the United States, it will be
necessary for you to obtain the import consignment address so that DMS's
customs broker can handle the importation with the U.S. Customs Service.
6. DMS offers both on call and contract maintenance service designed to afford
single source responsibility for all its products.
7. DMS reserves the right to make changes at any time to any product to
improve its design and to insure the best available product.
This page is intentionally left blank.
CUSTOMER REPAIR REPORT

FOR SERVICE, COMPLETE THIS FORM, AND RETURN IT ALONG WITH THE AFFECTED EQUIPMENT
TO CUSTOMER SERVICE AT THE ADDRESS INDICATED BELOW.

COMPANY NAME: ____________________________________________________________________________

TECHNICAL CONTACT:_____________________________________ PHONE: __________________________

REPAIR P. O. #:________________________ IF WARRANTY, UNIT S/N: ________________________________

INVOICE ADDRESS: ___________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

SHIPPING ADDRESS: __________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

RETURN SHIPPING METHOD: __________________________________________________________________

EQUIPMENT MODEL #:____________________ S/N:__________________FAILURE DATE: _______________

DESCRIPTION OF PROBLEM:___________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

WHAT WAS HAPPENING AT TIME OF FAILURE?__________________________________________________

_____________________________________________________________________________________________

ADDITIONAL COMMENTS: ____________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

REPORT PREPARED BY:__________________________________ TITLE: ______________________________

IF YOU REQUIRE TECHNICAL ASSISTANCE, PLEASE FAX OR WRITE THE CUSTOMER SERVICE
DEPARTMENT AT:

DANIEL MEASUREMENT SERVICES


DIVISION OF EMERSON PROCESS MANAGEMENT PHONE: 1-888-801-1452
ATTN: CUSTOMER SERVICE FAX: 1-713-827-6312
11100 BRITTMOORE PARK DRIVE
HOUSTON, TEXAS 77041

FOR FASTEST SERVICE CONTACT DANIEL MEASUREMENT SERVICES VIA OUR WEBSITE:
www.emersonprocess.com/daniel
This page is intentionally left blank.
This page is intentionally left blank.
www.RosemountAnalytical.com

www.Danalyzer.com

AMERICAS MIDDLE EAST AND AFRICA


Emerson Process Management Emerson Process Management
Rosemount Analytical Gas Chromatograph Center Emerson FZE
of Excellence Jebel Ali Free Zone
10241 West Little York, Suite 200 Dubai, United Arab Emirates, P.O. Box 17033
Houston, TX 77040 USA T +971 4 811 8100
Toll Free 866 422 3683 F +971 4 886 5465
T +1 713 396 8880 (North America) [email protected]
T +1 713 396 8759 (Latin America)
F +1 713 466 8175 ASIA-PACIFIC
[email protected] Emerson Process Management
Asia Pacific Pivate Limited
EUROPE 1 Pandan Crescent
Emerson Process Management Singapore 128461
Bond Street, Dumyat Business Park Republic of Singapore
Tullibody FK10 2PB UK T +65 6 777 8211
T +44 1259 727220 F +65 6 777 0947
F +44 1259 727727 [email protected]
[email protected]

©2012 Emerson Process Management. All rights reserved.

The Emerson logo is a trademark and service mark of Emerson Electric Co. Rosemount Analytical and Danalyzer are
marks of one of the Emerson Process Management family of companies. All other marks are the property of their
respective owners.

The contents of this publication are presented for information purposes only, and while effort has been made to
ensure their accuracy, they are not to be construed as warranties or guarantees, express or implied, regarding the
products or services described herein or their use or applicability. All sales are governed by our terms and
conditions, which are available on request. We reserve the right to modify or improve the designs or specifications
of our products at any time without notice.

You might also like