K19400, K19410

High Temperature Dropping Point

Apparatus

Operation and Instruction Manual

REV B

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA
Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815
http://www.koehlerinstrument.com • e-mail: [email protected]
Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing
 K194XX High Temperature Dropping Point Apparatus
Operation and Instruction Manual

CERTIFICATE OF CONFORMANCE

High Temperature Dropping Point Apparatus

K194XX

This certificate verifies that part number K194XX, High Temperature Dropping
Point Apparatus, was manufactured in conformance with the applicable
standards set forth in this certification.

Specifications: ASTM D2265

ASTM D4950

This unit is tested before it leaves the factory, to ensure total functionality and
compliance to the above specifications and ASTM standards. Test and inspection
records are on file for verification.

Jesse Kelly
Application Engineer
Koehler Instrument Company

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WEEE Directive Compliance Statement

Background
The goal of the WEEE Directive is to encourage design of environment-friendly products that increase reuse,
recycling and other forms of recovery to reduce waste streams and applies to listed Electronic and Electrical
Equipment (EEE) and Koehler's equipment falls broadly into Appendix 1A; Section 9 Monitoring and Control
Equipment: Measuring, weighing or adjusting appliances for household or as laboratory equipment.

Any associated non-embedded equipment such as Lighting (Saybolt Color) and PCs/Printers also fall under
WEEE. If provided with an order these ancillary items must be WEEE compliant. For these and other reasons
(printer cartridges are regionalized) the equipment must be supplied through a third party supplier in Europe.

The WEEE Directive applies to electrical and electronic equipment falling under the categories set out in Annex
IA provided that the equipment concerned is not part of another type of equipment that does not fall within the
scope of this Directive. Annex IB contains a list of products which fall under the categories set out in Annex IA.

http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2003:037:0024:0038:en:PDF

We do not qualify for any of the 10 exemption categories.

http://www.dpa-system.dk/en/WEEE/Products/Exemptions

Professional use
For equipment defined for ’professional use’ local authorities have no role to play. Producers and importers are
basically responsible for collection of WEEE recyclables from the professional user and for subsequent
management. A separate statement is given cataloging the items that require separation from the equipment
along with basic information on subsequent processing or recycling prior to disposal of the equipment.
http://www.dpa-system.dk/en/WEEE/Products/Private-or-professional-use

Responsibility for Registration and Annual Reporting:

Koehler will not sell directly to end users in the EU and so has no responsibility to register within each EU state
and to make annual reports. Koehler declares that this responsibility is born by the importer who is the first
level of the distribution chain and is subject to producer responsibility. We will communicate this in writing to
our distributor/importers in the EU stating they are responsible to satisfy WEEE registration and reporting
requirements in the EU states where they conduct sales activities.

It is illegal to market electrical and electronic equipment covered by producer responsibility without being
registered.

http://www.dpa-system.dk/en/WEEE/Producers/Whoissubjecttoproducerresponsibility

Product Design
Koehler's designs allow for complete disassembly to a modular level which usually allows for standard
recycling. A qualified refrigeration system technician must be consulted when disassembling and de-
commissioning any equipment with refrigeration systems.

Koehler's scientific testing equipment is robustly designed to function over a long service life and are typically
repaired many times over the course of years rather than being replaced. We believe that re-use and
refurbishment is the very best form of re-cycling.

All batteries must be readily removable not soldered in place.

Recycling instructions
In the event that replacement becomes necessary, we will include instructions, particularized to each
instrument that informs the customer of their recycling responsibilities and giving them guidance in doing this.
All Koehler equipment has been placed on the market since 13th August 2005 and so Koehler is defined as a
"new WEEE producer". As such we must provide information on refurbishment, treatment, and re-use.

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Our instrument manual will include this compliance statement and indicate that any collection of materials will
be handled by their authorized distributor. In the event that the distributor is unreachable or is no longer a
distributor for Koehler Instrument, Co., other arrangements may be made including accepting the materials
directly.

Recycling is free of charge. Shipping is the responsibility of the end users. Whether shipping to a distributor or
to Koehler directly, safe, properly declared, and labeled packaging and shipping expenses are the sole
responsibility of the end user.

WEEE Marking

Since Koehler products are subject to the WEEE Directive we must display the WEEE symbol shown above in
accordance with European Standard EN 50419 on the equipment. It must be indelible, at least 5mm in height,
and clearly legible. If the equipment is too small the mark must be in the product literature, guarantee
certificate, or on the packaging. Rules on marking are established in section 49 of the WEEE Order.

Koehler Instrument Company, Inc.

c/o RECYCLING
1595 Sycamore, Ave.
Bohemia, NY 11716

As a minimum the following substances, preparations and components have to be removed from any
separately collected WEEE:
- Mercury containing components, such as switches or backlighting lamps (compact fluorescent lamps, CFL),
- Batteries
- Printed circuit boards if the surface of the printed circuit board is greater than 10 square centimeters (about 4
sq in.),
- Toner cartridges, liquid and pasty, as well as color toner,
- Chlorofluorocarbons (CFC), hydrochlorofluorocarbons (HCFC) or hydrofluorocarbons (HFC), hydrocarbons
(HC)
- Liquid crystal displays (together with their casing where appropriate) of a surface greater than 100 square
centimeters and all those back-lighted with gas discharge lamps,
- External electric cables
- Components containing refractory ceramic fibers as described in Commission Directive 97/69/EC of 5
December 1997 adapting to technical progress Council Directive 67/548/EEC relating to the classification,
packaging and labeling of dangerous substances (2),
- Electrolyte capacitors containing substances of concern (height > 25 mm, diameter > 25 mm or
proportionately similar volume)

2. The following components of WEEE that is separately collected have to be treated as indicated:
- Equipment containing gases that are ozone depleting or have a global warming potential (GWP) above 15,
such as those contained in foams and refrigeration circuits: the gases must be properly extracted and properly
treated. Ozone-depleting gases must be treated in accordance with Regulation (EC) No 2037/2000 of the
European Parliament and of the Council of 29 June 2000 on substances that deplete the ozone layer (4).

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Table of Contents

1 Introduction ............................................................................................................ 10
1.1 Koehler’s Commitment to Our Customers ..................................................................................... 10
1.2 Recommended Publications .......................................................................................................... 10
1.3 Instrument Specifications ............................................................................................................... 10
2 Safety Information and Warnings ......................................................................... 10
3 Getting Started ....................................................................................................... 11
3.1 Packing List .................................................................................................................................... 11
3.2 Unpacking ...................................................................................................................................... 11
4 Descriptions ........................................................................................................... 12
4.1 Test Tube Assembly ...................................................................................................................... 12
4.2 Temperature Controller Operation ................................................................................................. 12
5 Operation ................................................................................................................ 12
6 Service .................................................................................................................... 14
7 Replacement Parts................................................................................................. 14
8 Storage ................................................................................................................... 14
9 Warranty ................................................................................................................. 14
10 Returned Goods Policy ......................................................................................... 14
11 Wiring Diagrams .................................................................................................... 16
Notes ............................................................................................................................ 17
Notes ............................................................................................................................ 18
Notes ...................................................................................Error! Bookmark not defined.

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1 Introduction
ASTM Publication:
The Koehler Model K19400/K19410 High  ASTM D2265: Standard Test Method for
Temperature Dropping Point Apparatus is used Dropping Point of Lubricating Grease
for identification and quality control applications, Over Wide Temperature
and as an indication of the highest temperature  ASTM D4950: Standard Classification
a grease can undergo without complete and Specification for Automotive Service
liquefaction or oil separation. This unit performs Greases
dropping point determinations on lubricating
greases of up to 752°F (400°C). 1.3 Instrument Specifications
This manual provides operating instructions
for the K194XX High Temperature Dropping Models: K19400
Point Apparatus, and should be used in K19410
conjunction with applicable standard test
methods. Electrical 115V, 60Hz 6.5A
Requirements: 220-240V
1.1 Koehler’s Commitment to Our 50/60Hz 3.4A
Customers
Maximum Temperature: 400°C (752°F)
Providing quality testing instrumentation and
technical support services for research and Control Stability: ±0.5°C (±1°F)
testing laboratories has been our specialty for
more than 50 years. At Koehler, the primary Dimensions: 11½x9x14
focus of our business is providing you with the LxWxH, in. (cm) 29x33x36
full support of your laboratory testing needs. Our
products are backed by our staff of technically Net Weight: 24½ lbs (11.1kg)
knowledgeable, trained specialists who are
experienced in both petroleum products testing
and instrument service to better understand your
requirements and provide you with the best
2 Safety Information and Warnings
solutions. You can depend on Koehler for a full Safety Considerations. The use of this
range of accurate and reliable instrumentation equipment may involve hazardous materials and
as well as support for your laboratory testing operations. This manual does not purport to
programs. Please do not hesitate to contact us address all of the safety problems associated
at any time with your inquiries about equipment, with the use of this equipment. It is the
tests, or technical support. responsibility of any user of this equipment to
investigate, research, and establish appropriate
Toll Free: 1-800-878-9070 (US only) safety and health practices and determine the
Tel: +1 631 589 3800 applicability of regulatory limitations prior to use.
Fax: +1 631 589 3815
Equipment Modifications and Replacement
Email: [email protected] Parts. Any modification or alteration of this
http://www.koehlerinstrument.com equipment from that of factory specifications is
not recommended and voids the manufacturer
1.2 Recommended Publications warranty, product safety, performance
specifications, and/or certifications whether
1. American Society for Testing and Materials specified or implied, and may result in personal
(ASTM) injury and/or property loss. Replacement parts
100 Barr Harbor Drive must be O.E.M. exact replacement equipment.
West Conshohocken, Pennsylvania 19428-
2959, USA Over Temperature Protection. This unit is
Tel: +1 610 832 9500 equipped with Over Temperature Protection
Fax: +1 610 832 9555 (OTP) circuitry to prevent overheating. The unit
http://www.astm.org will automatically interrupt power whether
email: [email protected] equipment malfunction or operator error causes
the temperature to exceed either 20 °C above

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the set point or the maximum recommended  (1) Thermometer Depth Gauge (K194E5)
temperature range. The power can only then be  (1) Polished Metal Rod (K194E6)
restored by identifying and correcting the
problem, allowing the unit to return to normal Accessories (purchased separately):
operating temperatures, and resetting the power
to the unit.  (1) Cup Plug Gauge (K194E7)
 (1) ASTM 3F Thermometer (250-000-03F)
Unit Design. This equipment is specifically Range: 20 to 760°F
designed for use in accordance with the  (1) ASTM 3C Thermometer (250-000-03C)
applicable standard test methods listed in Range: -5 to +400°C
section 1.2 of this manual. The use of this
equipment in accordance with any other test 3.2 Unpacking
procedures, or for any other purpose, is not
recommended and may be extremely Remove the bath from the crate and place on a
hazardous. firm, level table.

Chemical Reagents Information. Chemicals

and reagents used in performing the test may WARNING: Be sure two or more
exhibit potential hazards. Any user must be individuals are available for extracting and lifting
familiarized with the possible dangers before instrument from box to cart and from cart to
use. We also recommend consulting the bench. Individuals must lift in accordance to
Material Data and Safety Sheet (MSDS) on each proper technique. See Figure below.
chemical reagent for additional information.
MSDS information can be easily located on the
internet at http://siri.uvm.edu or
http://www.sigma-aldrich.com.

Mineral Spirits:

WARNING: Flammable. Vapors harmful

if inhaled.
 Keep away from heat, sparks, open
flames, and any other sources of Environmental Conditions: The instrument
ignition. environment must comply with the following
 Keep container closed. Use with conditions for proper setup:
adequate ventilation.  No / Low Dust
 Avoid prolonged breathing of vapor or
spray mist.  No direct sunlight
 Avoid contact with eyes, skin, or  Not near heating or AC ventilation ducts
clothing.
 Wash thoroughly after each use.  No Vibrations
 Clearance from other instruments
3 Getting Started
 Temperature Range: 5 to 40°C
3.1 Packing List  Elevation to 2000 meters
 (1) High Temperature Dropping Point  Relative Humidity: < 80%
Apparatus (K19400 or K19410)
 (6) Grease Cup (K194EA) Power. Connect the line cord to a properly fused
 (6) Test Tube, 13 x 100 mm (K194EB) and grounded receptacle with the correct
 (6) Cup Support (K194EC) voltage as stated in the Instrument
 (6) Thermometer Clamp (K194E1) Specifications section of this manual. To double
 (6) Upper Bushing (K194E2) check the voltage requirements, refer to the
 (6) Lower Bushing (K194E3) information plate on the side of the unit. Before
 (6) Bushing Support Ring (K194E4) plugging in this unit, be sure all switches are off.

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4 Descriptions
2. Set Point Temperature Display. The
4.1 Test Tube Assembly lower green LED display shows the set
point temperature of the controller.

3. Programming Key. Permits scrolling

through controller menu parameters.
One Level Forward

4. Down Key. Used to decrease the set

point temperature and to decrease or
change parameter values when
programming the temperature controller.

5. Up Key. Used to increase the set point

temperature and to increase or change
parameter values when programming
the temperature controller.

6. Exit / Function Key. This key is used to

exit or leave a level. One level backward

IMPORTANT NOTE: The digital

temperature controller for the unit
comes pre-programmed from the
Koehler factory. Please do NOT attempt
to re-program the digital temperature
controller as this will void the product
4.2 Temperature Controller Operation warranty. If assistance is required,
please do not hesitate to contact the
Koehler technical service department.

Setting the Temperature. Set the desired

operating temperature by adjusting the set
point with the up and down keys. The set
point will be displayed in the lower green Set
Point LED display and the actual
temperature will be displayed in the upper
red Process LED display. Please allow the
instrument to fully equilibrate before
proceeding with any testing.

Temperature Calibration. This routine allows

the digital temperature controller to be
calibrated to a certified thermometer.

a. Use a certified calibrated measuring

device to acquire the temperature.
Calculate the difference between the
Figure 4. Temperature Controller measuring device and the Process
value displayed on the controller.
b. Press the program key two times until
1. Process Temperature Display. The
PCt is displayed in the lower green LED
upper red LED display shows the
display. Press the DOWN key. CAL will
process temperature as read from the
display on the lower green display. If
RTD probe.
there is a value observed in the upper

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red LED display, add it to the calculated 3. Turn the Light switch to ON. The switch is
difference obtained in the previous step. located on the bottom left-hand corner of the
This is the offset value. unit.

c. Press the Program Key. The lower 4. Insert a calibrated thermometer into the
green display will flash. Use the up or aluminum block thermometer-well.
down keys to adjust to the new
calibration offset value on the upper red 5. Observe the display panel of the digital
display calculated in the previous step. temperature control. Upon power
When the value has been entered, the initialization all LED’s will momentarily be
controller will automatically store the illuminated. After five seconds, the control
value. The lower green display will stop will reset and display the current block
flashing. If further adjustments are temperature on top as PV or process (or
necessary, press the Program Key actual) value. The bottom display is the
again. Resume regular operations by setpoint value or SV.
pressing the Exit / Function key two
times. Verify if the new calibration is The temperature control is programmed for
correct by observing the upper red a maximum operating temperature of 400°C.
display and comparing the value with In the unlikely event of a malfunction, this
the calibrated reference device. unit is equipped with an overtemperature
safety cutoff which will activate if the
temperature exceeds 405°C.
Auto Tune. This routine allows the digital
temperature control to learn the heating Do not alter any of the parameters. This
parameters needed for any particular set instrument has been factory programmed
point temperature. This operation should be and malfunctions could occur if the
done when installing a new unit, after parameters are tampered with.
replacing or changing the bath medium type,
or utilizing a different temperature set point 6. When the process value and the setpoint
20% different from the previously used set value are equilibrated, place the prepared
point temperature. and assembled test tubes into the top holes.

a. Set the operating temperature to the 7. Heat the samples as described in the test
desired setting. method until the dropping point occurs.

b. Press the up and down arrow buttons 8. After the dropping point occurs, continue
simultaneously for about 5 seconds. testing with new samples or shut the unit
When Auto Tune is active, the lower OFF.
green LED display will blink TUNE. Auto
Tune will automatically toggle off when
the set point temperature is reached.
WARNING: For personal safety,
Auto tune can be terminated by pressing
exercise extreme caution when using high
the up & down buttons simultaneously
voltage electrical instruments to avoid the
again.
possibility of electrical shock.
5 Operation
1. Be sure to read the safety and hazard WARNING: For personal safety, this
warnings and any of the standard test unit can reach very high temperatures which
methods mentioned in the Introduction could cause severe burns. Use protective
before operating this instrument. gear when adding and removing test tubes
to and from the unit.
2. Turn the Line switch ON. This switch is
located on the bottom right-hand corner on
the unit.

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6 Service This equipment was shipped from the factory

in a corrugated cardboard container. If long term
Under normal operating conditions and with storage is anticipated, re-packing the instrument
routine maintenance, the K194XX High in a water-resistant container is recommended
Temperature Dropping Point Apparatus should to ensure equipment safety and longevity.
not require service. Any service problem can be
quickly resolved by contacting Koehler’s 9 Warranty
technical service department either by letter,
phone, fax, or email. In order to assure the We, at Koehler, would like to thank you for
fastest possible service, please provide us with your equipment purchase, which is protected by
the following information. the following warranty. If within one (1) year from
the date of receipt, but no longer than fifteen
Model Number: (15) months from the date of shipment, Koehler
equipment fails to perform properly because of
Serial Number:
defects in materials or workmanship, Koehler
Date of Shipment: Instrument Company, Inc. will repair or, at its
sole
discretion, replace the equipment without charge
7 Replacement Parts F.O.B. its plant, provided the equipment has
been properly installed, operated, and
Part Number Replacement Part maintained. Koehler Instrument Company must
K194-0-2 Top Plate be advised in writing of the malfunction and
authorize the return of the product to the factory.
K194E1 Thermometer Clamp The sole responsibility of Koehler Instrument
K194E2 Upper Bushing Company and the purchaser’s exclusive remedy
for any claim arising out of the purchase of any
K194E3 Lower Bushing product is the repair or replacement of the
product. In no event shall the cost of the
K194E4 Bushing Support Ring
purchaser’s remedy exceed the purchase price,
K194E5 Thermometer Depth Gauge nor shall Koehler Instrument Company be liable
for any special, indirect, incidental,
K194E6 Polished Metal Rod consequential, or exemplary damages.
K194EA Grease Cup KOEHLER INSTRUMENT COMPANY, INC.
DISCLAIMS ALL OTHER WARRANTIES,
K194EB Test Tube 13 x 100mm EXPRESSED OR IMPLIED, INCLUDING ANY
K194EC Cup Support IMPLIED WARRANTIES OF FITNESS FOR A
PARTICULAR PURPOSE. Please save the
220-120-001 Heater Cartridge, 115V shipping carton in the event the equipment
needs to be returned to the factory for warranty
220-240-001 Heater Cartridge, 230V
repair. If the carton is discarded, it will be the
279-115-002 Fluorescence Lamp purchaser’s responsibility to provide an
appropriate shipping carton.
265-203-001 Temperature Probe, Type K
275-103-044 Digital Temperature Controller

10 Returned Goods Policy

To return products for credit or replacement,
8 Storage please contact Koehler Customer Service with
your purchase order number, our packing
This laboratory test instrument is equipped list/invoice number, the item(s) to be returned
with electrical components. Storage facilities and the reason for the return. You will be issued
should be consistent with an indoor laboratory a Returned Authorization (RA) number, which
environment. This testing equipment should not must be prominently displayed on the shipping
be subjected to extremes of temperature and/or container when you return the material to our
moisture. plant. Shipping containers without an RA

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number prominently displayed with will be

returned to the sender. Goods must be returned
freight prepaid. Returns will be subject to a
restocking charge, the application of which will
depend upon the circumstances necessitating
the return. Some returns cannot be authorized,
including certain products purchased from
outside vendors for the convenience of the
customer, products manufactured on special
order, products shipped from the factory past
ninety (90) days, and products which have been
used or modified in such a way that they cannot
be returned to stock for future sale.

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11 Wiring Diagrams

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Notes

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Notes

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