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International Standard: Oil of Rose (Rosa

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International Standard: Oil of Rose (Rosa

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INTERNATIONAL ISO
STANDARD 9842

Second edition
2003-09-01

Oil of rose (Rosa × damascena Miller)


Huile essentielle de rose (Rosa × damascena Miller)

Reference number
ISO 9842:2003(E)

© ISO 2003
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ISO 9842:2003(E)

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ISO 9842:2003(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the
International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.

International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.

The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.

Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.

ISO 9842 was prepared by Technical Committee ISO/TC 54, Essential oils.

This second edition cancels and replaces the first edition (ISO 9842:1991), which has been technically revised.

© ISO 2003 — All rights reserved iii


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INTERNATIONAL STANDARD ISO 9842:2003(E)

Oil of rose (Rosa × damascena Miller)

1 Scope 3 Terms and definitions


This International Standard specifies certain For the purposes of this document, the following
characteristics of the oil of rose (Rosa ¥ damascena terms and definitions apply.
Miller) cultivated in Turkey, Morocco and Bulgaria,
of the Rosaceae family, in order to facilitate 3.1
assessment of its quality. oil of rose
essential oil obtained by steam distillation of the
flowers of Rosa × damascena Miller, of the
Rosaceae family, cultivated in Turkey, Morocco and
2 Normative references Bulgaria

The following referenced documents are NOTE For information on the CAS number, see
indispensable for the application of this document. ISO/TR 21092.
For dated references, only the edition cited applies.
For undated references, the latest edition of the
referenced document (including any amendments)
applies. 4 Requirements (all origins)
ISO/TR 210, Essential oils — General rules for
packaging, conditioning and storage 4.1 Appearance

ISO/TR 211, Essential oils — General rules for Liquid or more or less crystallized.
labelling and marking of containers

ISO 212, Essential oils — Sampling 4.2 Colour

ISO 279, Essential oils — Determination of relative Light yellow.


density at 20 °C — Reference method

ISO 280, Essential oils — Determination of 4.3 Odour


refractive index
Floral, rose.
ISO 592, Essential oils — Determination of optical
rotation 20
4.4 Relative density at 20 °C, d 20
ISO 709, Essential oils — Determination of ester
value Minimum: 0,848
Maximum: 0,880
ISO 1041, Essential oils — Determination of
freezing point
4.5 Refractive index at 20 °C
ISO 11024-1, Essential oils — General guidance on
chromatographic profiles — Part 1: Preparation of Minimum: 1,452 0
chromatographic profiles for presentation in Maximum: 1,470 0
standards

ISO 11024-2, Essential oils — General guidance on 4.6 Optical rotation at 20 °C


chromatographic profiles — Part 2: Utilization of
chromatographic profiles of samples of essential oils Between −5° and −1,8°.

© ISO 2003 — All rights reserved 1


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ISO 9842:2003(E)

4.7 Freezing point 6 Test methods


Between +16 °C and +23,5 °C. 6.1 20
Relative density at 20 °C, d 20
4.8 Ester value See ISO 279.
Minimum: 7 6.2 Refractive index at 20 °C
Maximum: 24
See ISO 280.
4.9 Chromatographic profile
6.3 Optical rotation at 20 °C
Analysis of the essential oil shall be carried out by
gas chromatography. In the chromatogram obtained, See ISO 592.
the representative and characteristic components
shown in Table 1 shall be identified. The proportions 6.4 Freezing point
of these components, indicated by the integrator,
shall be as shown in Table 1. This constitutes the See ISO 1041.
chromatographic profile of the essential oil.
6.5 Ester value
4.10 Flashpoint
See ISO 709.
Information on the flashpoint is given in Annex B.
Time of saponification: 1 h

5 Sampling 6.6 Chromatographic profile

See ISO 212. See ISO 11024-1 and ISO 11024-2.

Minimum volume of test sample: 25 ml


7 Packaging, labelling, marking and
NOTE This volume allows each of the tests specified storage
in this International Standard to be carried out at least
once. See ISO/TR 210 and ISO/TR 211.

Table 1 — Chromatographic profile


Values in percent

Turkey
Bulgaria Turkey Morocco
Component (“peasant” type)
min. max. min. max. min. max. min. max.

Ethanol — 2,0 — 7 — 3 — 2,0


Citronellol 20,0 34,0 34,0 49,0 30,0 47,0 26 40,0
Nerol 5,0 12,0 3,0 11,0 3,0 11,0 6,0 12,0
Geraniol 15,0 22,0 8,0 20,0 6,0 23,0 12,0 29,0
β-Phenylethanol — 3,5 — 3,0 — 3,0 — 3,0
Heptadecane (Paraffin C17) 1,0 2,5 0,8 3,0 0,6 4,0 0,7 3,0

Nonadecane (Paraffin C19) 8,0 15,0 6,0 13,0 7,0 16,0 6,0 8,5

Heneicosane (Paraffin C21) 3,0 5,5 2,0 4,0 2,0 5,5 1,5 4,0

NOTE The chromatographic profile is normative, contrary to typical chromatograms given for information in Annex A.

2 © ISO 2003 — All rights reserved

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