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Calibration Procedureoxsas

1. The document outlines the calibration procedure for an XRF instrument in 5 steps: setting up the method, creating calibration standards, analyzing and batching samples, calibrating using the standards, and running sample analyses. 2. Key steps include naming the method, selecting elements, setting counting time and power, creating samples from the method, measuring calibration standards, batching samples and standards, and checking calibration curves to ensure points are within range. 3. After calibration is complete and curves are validated, sample batches can be run for analysis.

Uploaded by

Satyendra Kumar
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© © All Rights Reserved
Available Formats
Download as DOC, PDF, TXT or read online on Scribd
212 views

Calibration Procedureoxsas

1. The document outlines the calibration procedure for an XRF instrument in 5 steps: setting up the method, creating calibration standards, analyzing and batching samples, calibrating using the standards, and running sample analyses. 2. Key steps include naming the method, selecting elements, setting counting time and power, creating samples from the method, measuring calibration standards, batching samples and standards, and checking calibration curves to ensure points are within range. 3. After calibration is complete and curves are validated, sample batches can be run for analysis.

Uploaded by

Satyendra Kumar
Copyright
© © All Rights Reserved
Available Formats
Download as DOC, PDF, TXT or read online on Scribd
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1

CALIBRATION PROCEDURE

OPERATION SETUP
↓
METHODS
↓
NEW
↓
CHANGE THE NEW METHOD NAME (EXP. RAWMEAL)
↓

SELECT CATEGARY TO USER


↓

PERIODIC TABLE
IN PERIODIC TABLE SELECT MORE THEN 10% HAS MAJOR ELEMENT, 0.5 TO
10% MINOR AND LESS THEN 0.5 HAS TRACES.
↓

CLICK ADD ELEMENT


Select the monochromator element which is available in your instrument has _m (exp.
Ca_m) . then select other element in goniometer.
Change the Kv/mA has 30Kv 70mA. Change the counting time 20. Then click ok.

METHOD HEADER
↓

Select OXIDE
↓

COMPONENTS
Change the display name for all the elements.
↓

PSEUDOS(FORMULA) enter the name and formula


↓

SETTING UP SAMPLES
In this save and keep the windows open and again go to
↓

OPERATION SETUP
↓

1
SETTING UP SAMPLES
↓

2
CREATE FROM METHOD
↓

CREATE FROM METHODE


↓

In method select your method (exp. RAWMEAL)

Change the template name to samples name (exp.RM1)

Category to user
Position no to 1 and validity period to 48
Chick UPD ALWAYS chick DO FULL UPDATE
Again click DUPLICATE
Enter the second sample name and position No. do the same upto your samples to be
completed.
↓

SAVE THEN CANCEL.


↓

In open method windows at setting up samples box, select your TOP AND BOTTOM in
all element. SAVE AND CLOSED THE BOX.

2nd STEP

OPERATION SETUP
↓

CALIBRATION MVR
↓

In right side box directly come to down and select calibration STANDARD
Click right batten in mouse
NEW MATRIX
↓

CLICK NEW MATRIX


Enter the method name (exp. RAWMENAL)
↓

2
RIGHT CLICK METHOD
↓

3
NEW SET OF CALIBRATION STANDARDS
Enter same method name
Right click EDITFROM METHOD select your methodOK
Enter all the samples name and chemical values-SAVEOK

Again go to top of the same windows and select your method


Double click the your method measure standards right click
Measure calibration standards select your mrthodOK
BATCHCREATE BATCH
Its shows batch has been successfully created and note the batch name.

IIIrd STEP

ANALYSIS AND DATA


↓

MANAGE SCT SAMPLES(F12)


In select itemselect your method(exp RAWMEAL)
↓

BATCH ALL SAMPLESCREATE BATCH


Shows batch has been successfully createdclick OK

Then keep the samples in position and click GREEN ANALYSIS BOTTEN
After completing the SUS batch select calibration batch and run all calibration samples.

IVth STEP

OPERATION SETUP
↓

CALIBRATION –MVR
↓

METHODselect your methodselect ANALYTES—CLICK select the element and


see the curve, if any point out from the curve uncheck the same and compute. Then save.
Same to be repute all the element.

Vth step.

ANALYSIS AND DATA

3
↓
MANAGE SCT SAMPLES
4
↓

SELECT ITEM(YOUR METHOD)


↓

BATCH-ALL SAMPLESCREATE BATCH


Run the samples and after completed the analysis do your regular analysis.

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