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Boiling Up Rate For Batch Distillation

This document summarizes the design of a batch multicomponent distillation column. It includes details of the batch reactor such as its capacity, dimensions, temperatures and heat transfer rates. It then calculates the steam requirements to distill the reactor contents within a 23.8 hour cycle. The minimum and maximum vapor rates from the reactor to the distillation column are determined to be 510 kg/hr and 6900 kg/hr respectively. The total and peak steam requirements to complete the batch are calculated to be 24.2 tons and 1.4 tons/hr.

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Kanhaiyalal Patil
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954 views4 pages

Boiling Up Rate For Batch Distillation

This document summarizes the design of a batch multicomponent distillation column. It includes details of the batch reactor such as its capacity, dimensions, temperatures and heat transfer rates. It then calculates the steam requirements to distill the reactor contents within a 23.8 hour cycle. The minimum and maximum vapor rates from the reactor to the distillation column are determined to be 510 kg/hr and 6900 kg/hr respectively. The total and peak steam requirements to complete the batch are calculated to be 24.2 tons and 1.4 tons/hr.

Uploaded by

Kanhaiyalal Patil
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Batch Multicomponant System Distillation Column Vapor rate:

Sr.
Description Units Quantity
No.
Batch Reactor Details

1 Tag No. 01-V-XXX

2 Batch Reactor Capacity KL 125.0

3 Reactor Diameter m 3.50

4 Reactor Length m 5.25

5 Reactor Surface area for Jacket m2 42.9


Heat Transfer Area (Surface) -
6 m2 42.9
(Jacket or Limpet of reactor)
7 Reactor content Density kg/m3 970.0

8 Reactor Mass kg 41646.4

9 Reactor Content m3 106.3

10 Temp - In Steam - MPS *C 165

11 Temp - Out Cond. *C 100

12 Reactor fluid Initial Temp *C 40

13 Reactor fluid final Temp *C 150

14 q1 *C 15

15 q2 *C 60

16 LMTD *C 32.5

17 Heat Transfer Co-Efficient kcal/hrm2*k 250

18 Latent Heat kcal/kg 112.0

19 Heat Evolved kcal/hr 348419

20 Boil - Up Rate Kg/hr 3110.9

21 Boil-Up Rate -Selected kg/hr 1750

Steam Line Loop Line Sizing Calculation:

22 Mass to be distilled out kg 41646.4


23 Time Cycle hr 23.8

24 Heat Required Kcal/ hr 196000

25 Steam Enthalpy kCal/kg 659.9

26 Steam Required kg/ hr 363.0

27 Density of Steam kg/ m3 1.8

28 Steam Flow Rate Required m3/ hr 201.6

29 Steam Flow Rate Required m3/ s 0.06

30 Velocity of Steam m/s 60

31 Area of Pipe m2 0.001

32 Diameter of Pipe m 0.03

33 Diameter of Pipe NB 34.5

34 Selected Pipe Size - Steam NB 40

Conclusion:

1 Minimum Vapor rate from reactor to column = 510 kg/hr

2 Maximum Vapor rate from reactor to column = 6900 kg/hr

3 Total Steam requirement to completed batch = 24.2 Tons

4 Peak Steam requirement to complete batch= 1.4 Tons/hr


Chem-1 Chem-2 Chem-3 Remarks

Mid volatile High volatile Low volatile

- - -

- - -

68.4% occupied 85% occupied 30.1% occupied

30.1 42.9 18.9

30.1 42.9 18.9

960.0 970.0 954.0

28851.9 41646.4 18022.1

37.2 21.3 47.8 Chem-1 + Chem-2 + Chem-3

165 - -

100 - -

80 40 90

90 80 100 Boiling point of respective chemicals

75 85 65

20 60 10

41.6 71.8 29.4

220 250 190 From Lab

160.0 112.0 210.0 for Respective chemicals

275130 770413 105466 U*A*DTLM

1719.6 6878.7 502.2

1725 6900 510 For Design

28851.9 41646.4 18022.1


16.7 6.0 35.3

276000 772800 107100

659.9 659.9 659.9 @165°C from steam table

511.1 1431.1 198.3

1.8 1.8 1.8

284.0 795.1 110.2

0.08 0.22 0.03

60 60 60 As per limits in pipe

0.001 0.004 0.001

0.04 0.07 0.03

40.9 68.5 25.5

80 80 80 Header Size selection

kg/hr

kg/hr

Tons

Tons/hr

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