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Dr. Laurie S. Starkey, Organic Chemistry Lab CHM 318L

13 C-NMR introduction

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Sankar Adhikari
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21 views

Dr. Laurie S. Starkey, Organic Chemistry Lab CHM 318L

13 C-NMR introduction

Uploaded by

Sankar Adhikari
Copyright
© © All Rights Reserved
Available Formats
Download as PDF, TXT or read online on Scribd
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California State Polytechnic University, Pomona

Dr. Laurie S. Starkey, Organic Chemistry Lab CHM 318L


Introduction to 13C NMR

- 13C ("carbon-13") NMR spectra show one signal for each unique carbon
- chemical shifts ~0-220 ppm
- signals are all singlets (called proton-decoupled spectra)
- peak size is not quantitative, but C's without attached hydrogens are often small peaks
- # of hydrogens attached to each carbon can be determined by a DEPT experiment
(DEPT differentiates between signals arising from C, CH, CH2, and CH3 carbons)
- C isotope is only ~1% of carbons so 13C NMR requires more sample and/or more scans
13

O
O
OH

OH
O

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