Fann 35 Manual
Fann 35 Manual
Instruction Manual
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copied in any form or by any means -- graphic, electronic, or mechanical
without first receiving the written permission of Fann Instrument Company,
Houston, Texas, U.S.A.
Printed in U.S.A.
NOTE
Fann reserves the right to make improvements in design, construction
and appearance of our products without prior notice.
®
FANN is a registered trademark of Fann Instrument Company.
Section Page
9 Specifications...... ..................................................................................................21
Tables Page
3 Dial Deflection for Calibration Weights and Torsion Spring Assemblies ........................13
Figures Page
The FANN® Model 35 viscometer are direct reading instruments which are available in six speed and 12
speed designs for use on either 50 Hz or 60 Hz electrical power. The standard power source is 115 volts
but all of the models may be fitted with a transformer which makes operation with 220/230 volts possible.
These are true Couette coaxial cylinder rotational viscometer since the test fluid is contained in the annular
space (shear gap) between an outer cylinder and the bob. Viscosity measurements are made when the
outer cylinder, rotating at a known velocity, causes a viscous drag to be exerted by the fluid. This drag
creates a torque on the bob, which is transmitted to a precision spring where its deflection is measured and
then compared with the test conditions and the instrument's constants. This system permits the true
simulation of many of the significant flow process conditions encountered in industrial processing.
Viscosity as measured by a Couette type viscometer such as the Model 35 is a measure of the shear
stress caused by a given shear rate. This relationship is a linear function for Newtonian Fluids, i.e. a plot of
shear stress vs. shear rate is a straight line. In many instances, while the fluid of interest may not be
Newtonian, its rheology is near enough to Newtonian that this viscometer can be used and the viscosity
calculated as though it were Newtonian. It should be noted that the recommended calibration of the Model
35 is a linear or Newtonian calibration. This means that if the sample fluid characteristics are extremely
Non-Newtonian the linear method of calculating the viscosity cannot be used. In this case the Model 35 dial
reading and speed along with the dimensional data on the rotor and bob used will have to be calculated
using an appropriate formula for a non-linear shear stress / shear rate relationship that closely fits the
characteristics of the fluid.
These instruments have been designed so that viscosity in centipoise (or milli-Pascal seconds) of a
Newtonian fluid is indicated on the dial with the standard rotor, bob, and torsion spring operating at 300 rpm.
Viscosities at other test speeds may be measured by using multipliers of the dial reading. A simple
method of close approximation of viscosity in a plastic fluid, such as a drilling fluid is described in Section
6B.
The range of shear rates may be changed by selecting rotor speed and using various rotor-bob
combinations. A variety of torsion springs are available and designed to be easily interchanged in order to
broaden shear stress ranges and allow the measuring of viscosity in a wide variety of fluids.
2
Fig. 1
Model 35 Viscometer
3
SECTION 2
SAFETY CONSIDERATIONS
A. SAFE OPERATION
The safe operation of the FANN Model 35 Series Viscometer requires that the laboratory technician
be familiar with the proper operating procedures and potential hazards associated with the instrument.
This instrument is driven by 115 volt or 230 volt electrical power. Keep hands, clothes and other
objects away from the rotating parts of the machine
The optional heated sample cups and recirculating sample cups are electrically heated. Make sure
the power cord and other wiring associated with these cups is no good condition and properly
grounded.
Make sure the viscometer is turned off and unplugged from the source before cleaning or other repair
or maintenance. Do not allow the Viscometer Base to get wet. If samples have been spilled or
splattered, wipe clean with a damp cloth. Do not allow water to run into the base, as excessive water
could cause damage to the electrical components.
B. STANDARD B1 BOB
The standard B1 Bob normally furnished with the Model 35 Series Viscometer is a hollow Bob and
must not be to test samples hotter than 200°F (93°C). Solid Bobs are available for this type testing.
Precautions should be taken when testing heated samples using the optional heated sample cups to
avoid possible burns from spilled hot sample, or from touching the hot sample cup.
When heated sample cups are being used, do not exceed 200°F
4
SECTION 3
VISCOSITY TEST
The stainless steel sample cup provided has a line at the proper 350 ml test fluid level. Fill the cup to that
line with recently stirred test fluid. A scribed line on the rotor indicates proper immersion depth. Refer to
Fig. 1. Damage to the bob shaft bearings may occur if this immersion depth is exceeded. If other sample
holders are used, the space between the bottom of the rotor and the bottom of the sample holder should be
one-half inch (1.27cm) or greater.
WARNING
The Model 35A and 35SA viscometer are instruments with the ability to test at six different speeds.
Their range is from 3 rpm up to 600 rpm with the speed being determined by a combination of speed
switch setting and viscometer gear knob placement. To select the desired speed, set the speed
switch located on the right side of the base to the high or low speed position as desired. Then turn
the motor on and move the viscometer gear shift knob located in the center of the top of the
instrument to its desired position.
Table 1 lists the proper positions for the viscometer switch and the gear knob combinations to obtain
the desired speed. The viscometer gear shift knob may be engaged while the motor is running.
Read the dial for shear stress values.
TABLE 1
200 High Up
100 Low Up
6 High Center
3 Low Center
5
B. SR-12 Model 35A/SR12 and 35SA/SR12
The Model 35A/SR12 and 35SA/SR-12 have twelve speed testing capabilities. To achieve this
broader testing range (from 0.9 rpm up to 600 rpm) an additional gear box shift lever is used and it is
located on the right side of the gear box. Refer to Fig. 2. Position this lever to the Left or Right as
determined from Table 2.
CAUTION
Only the viscometer gear shift knob on the top of the instrument can be changed while the motor is
running.
After preparing the instrument for 12-speed testing by setting the gear box shift lever, select the
proper speed range with the speed shift switch on the right side of the base, then turn on the motor
and set the viscometer gear knob on the top of the instrument. Refer to Table 2 for the correct
combination of gear box shift lever setting; speed switch selection; and viscometer gear knob
placement. The stress values will appear on the dial.
6
Fig. 2
Gear Box Lever
TABLE 2
TWELVE-SPEED TESTING COMBINATIONS
MODEL 35A/SR12 AND MODEL 35SA/SR12
60 Right High Up
30 Right Low Up
C. GEL STRENGTH
Gel strengths are measured by first stirring the sample thoroughly at 600 rpm. Set gears to the
neutral position and turn motor off. After desired wait period, turn gel knob, located below gear shift
knob, refer to Fig. 1, slowly counterclockwise and read the dial at instant of the gel break (Peak Dial
Reading). Gel reading is in lbs/100 ft 2.
7
Fig. 3
Rotor Removal / Installation
8
Fig. 4
Torsion Spring Removal and Replacement
9
SECTION 4
CHANGING ROTORS, BOBS, AND TORSION SPRING
The R1-B1-F1 rotor-bob-torsion spring combination is standard for all FANN viscometer. Other rotor-bob
combinations may be used, provided shear rates are calculated for the fluid being tested. Use of rotor-bob
combinations which result in large gap sizes can lead to shear stress dial readings not consistent with
readings from a smaller gap.
The rotor can be removed from its socket by twisting counterclockwise, when viewed from above,
while gently pulling straight down. Refer to Fig. 3. The rotor may be replaced by aligning the rotor
slot and groove with the lock pin in the main shaft socket. Push the rotor upward and lock it into
position by turning it clockwise.
The bob shaft end that fits into the Bob is tapered and fits into a matching tapered hole in the bob. To
remove the bob twist the bob clockwise while pulling downward. To install the bob, twist it clockwise
while pushing upward.
2. Loosen set screws [C] and [D] about 1/2 turn. The spring can now be lifted out. Be careful not
to stretch the spring.
3. Insert the new spring, making sure the bottom mandrel is properly oriented and seated. Set
screw [D] should line up with the point at which the spring leaves the bottom mandrel. A notch
cut into the upper end of the bottom mandrel will help locate this point. Tighten set screw [D],
so that it presses against the split ring to hold the bottom mandrel of the spring.
NOTE: Before tightening set screw [C] be positive that the top of the
adjustable mandrel is flush with the top of clamp [E]. It may be
necessary to slightly compress or stretch the spring to accomplish
this.
4. Tighten set screw [C]. The slot in the top of the adjustable mandrel should line up with
clamping set screw [C].
5. Loosen set screw [F] to zero dial under index, then rotate knob [G] as required for alignment,
then adjust knob [G] vertically to allow the spring to be clamped in a "free" position, neither
stretched or compressed.
6. Tighten set screw [F] and replace the dust cap [A].
10
Fig. 1
Dead Weight Calibration
DW-3 Calibration Fixture
SECTION 5
11
INSTRUMENT CALIBRATION
Periodically the Model 35 Series Viscometer should be checked for proper calibration and if found in error
the viscometer should be calibrated or repaired. Continued accuracy of measurements requires the
instrument be properly calibrated. The calibration is checked by applying know torques to the bob shaft.
For any applied torque, within the torque range of the spring, there should be a specific dial reading plus or
minus a small tolerance. Two methods of calibration are described.
The Dead Weight Calibration is easier to perform and if the spring requires adjustment, the proper setting
can easily be verified. The Standard Fluid Calibration check verifies the complete instrument is operating
properly. It will determine problems of bent bob shaft, rotor eccentricity, and/or runout of the rotor or bob
more effectively than the Dead Weight method. Refer to Section 5-B.
A. Dead Weight Calibration Check Using Model DW3 Calibration Kit. Refer to Fig. 5.
1. Remove rotor and bob. Refer to Section 3-A and 3-B. Be sure that the tapered end of the bob
shaft is clean, then install the calibrating spool.
2. Install the DW-3 calibrating fixture by clamping it onto the upper portion of the viscometer
support legs.
3. Select a weight according to Table 3. Insert the bead at the end of the thread into the recess in
the top of the calibrating spool. Wrap the thread a little more than once around the spool and
then drape the thread over the pulley.
4. Hang the selected weight on the thread and adjust the calibrating fixture up or down until the
thread from the spool to the pulley is horizontal. Compare the dial reading with the reading on
Table 3.
5. If necessary, adjust the torsion spring. Refer to Section 5-C, "Adjusting Torsion Spring".
Factory tolerances for F1 spring only are 127 ± 1/2° for 50 g and 254 ± 1/2° for 100 g. A movement of
± 1/2° is permissible when the main shaft is turning. This movement will generally be dampened out
when a fluid is being tested. Check the linearity of the dial reading with at least three weights. If the
spring appears to be non-linear it is usually a sign that the bob shaft is bent. An instrument with
these characteristics needs additional service and/or repair.
TABLE 3
Dial Deflection For Calibration Weights And Torsion Spring Assemblies
Torsion Spring Assembly Torsion Spring Constant, K1 Weight in Grams
(with R1-B1 combination) Dynes/cm/° def
10 20 50 100 200
Dial Reading
F-0.2 77.2 127.0 254.0 - - -
F-0.5 193.0 50.8 101.6 254.0 - -
F-1 386.0 25.4 50.8 127.0 254.0 -
F-2 772.0 - 25.4 63.5 127.0 254.0
F-3 1158.0 - - 43.0 84.7 169.4
F-4 1544.0 - - - 63.5 127.0
F-5 1930.0 - - - 50.8 101.6
F-10 3860.0 - - - - 50.8
12
B. Fluid Calibration Check
This procedure is to be used for calibration using only Newtonian certified calibration fluids. Fann
Calibration Fluids are available in nominal 20, 50, 100, 200, and 500 cP. All are traceable to ASTM
standards and each bottle of fluid is furnished with a viscosity temperature chart certifying that batch
of fluid.
1. The instrument being checked must be clean before immersing the rotor and bob into the
calibration fluid. If necessary, remove the rotor and thoroughly clean the bob, bobshaft, and
rotor. Make sure the bob shaft and rotor are straight and have not been damaged.
CAUTION
2. Fill the sample cup to the scribed line with calibration fluid and place it on the instrument stage.
Elevate the stage so that the rotor is immersed to the proper immersion depth. Refer to Fig.
1.
3. Place a thermometer into the sample until the bulb touches the bottom and then secure it to
the side of the viscometer to prevent breakage.
4. Operate the instrument at 300 rpm for three (3) minutes. This will equalize the temperature of
the bob, rotor and the fluid.
5. Read the dial at 300 rpm and 600 rpm. Record these numbers, and the temperature from the
thermometer to the nearest 0.1° C,(0.15° F).
The viscosity from the temperature chart at the recorded temperature should be within ±2 cP of the 300 rpm
reading. Twice the cP viscosity from the chart should be within ± 3 of the 600 rpm reading. Plot the 300
rpm reading and the 600 rpm reading then draw a straight line from zero through these two points. If zero,
300 and 600 points do not fall in a straight line, probably either the rotor, bob or bobshaft is bent or other
eccentricity exists. Points at 100 rpm and 200 rpm can be plotted if verification is needed. Readings
outside the specified limits are indications that the instrument should be either calibrated or repaired. Refer
to Section 5-C for procedure to calibrate the spring. After completion of the calibration check, carefully
wipe clean the rotor inner and outer surfaces, the bob, the thermometer, the sample cup, and work area.
NOTE: Make sure the bob shaft is not bent before attempting to adjust the torsion spring,
1 Remove dust cap [A], then loosen set screw [C] about 1/2 turn.
2. Insert the calibration tool into the spring and rotate the adjustable mandrel (inside the spring)
slightly. Turn the mandrel counterclockwise if the dial reading is too low or turn the mandrel
clockwise if the dial reading is too high.
NOTE: Before tightening set screw [C] check the top of the upper threaded mandrel and be
positive that it is flush with the top of the clamp [E]. To accomplish this, it may be
necessary to adjust the spring by slightly compressing or stretching the spring.
3. Tighten set screw [C]. The slot in the top of the adjustable mandrel should line up with
clamping set screw [C].
4. Loosen set screw [F] to zero dial under index, then rotate knob [G] as required for alignment,
then adjust knob [G] vertically to allow the spring to be clamped in a "free" position, neither
stretched or compressed.
5. Tighten set screw [F] and replace the dust cap [A].
13
SECTION 6
DATA REDUCTION
A. Newtonian Viscosity Calculations
Newtonian Viscosity in centipoise may be read directly from the dial when viscometer is run at 300
rpm with R1-B1-F1 combination. Other springs may be used providing the dial reading is multiplied by
the "f" factor (spring constant).
To rapidly determine Newtonian viscosities in cP with FANN viscometer, use the following formula:
?N = S x ? x f x C
where,
Example: Using an R2-B1 combination at a speed of 600 rpm with an F5.0 spring, and a dial
deflects to 189.
NOTE: Combinations with the larger gaps are likely to give results that differ from these figures.
For best accuracy, calibrate with a standard fluid having a viscosity near the range of
interest and using the R-B-F combination to be used in the test.
TABLE 4 TABLE 5
Calculated C values from rotor-bob dimensions Speed Factor S base 300 rpm = 1
14
B. Approximation of Plastic Viscosity and Yield Point
Using R1-B1-F1 components, test a sample running the viscometer at 600 rpm and note the dial
reading. Change the speed to 300 rpm and note the dial reading. Determine the PV and YP using
the following equations. PV represents the slope of a straight line between the two dial readings. YP
represents the theoretical point at which the straight line, when projected, will intercept the vertical
axis.
CAUTION
A spring other than F1 may be used if the dial readings are multiplied by the proper
"f" factor, but the other rotor-bob combinations can not be used for this rapid, two
point method.
Grg
K1 =
?
Where K1 = spring constant - dynes/cm/degree deflection
G = Load in grams
r = Radius arm = 1 cm
Example: The required setting for the F1 spring is 386 dynes/cm/degree deflection with the R1-B1
combination. Using the 50 gm weight supplied with the fixture, the formula is:
50 x 981 x 1
K1 = = 127?
386
15
SECTION 7
MEASURING RANGE
TABLE 6
Measuring Range for FANN Direct Indicating Viscometer
ROTOR-BOB R1 B1 R2 B1 R3 B1 R1 B2 R1 B3 R1 B4
BASIC DATA
Rotor Radius, R0,cm 1.8415 1.7588 2.5866 1.8415 1.8415 1.8415
Bob Radius. R1, cm 1.7245 1.7245 1.7245 1.2276 0.8622 0.8622
Bob height, L, cm 3.800 3.800 3.800 3.800 3.800 1.900
Shear Gap in Annulus, cm 0.1170 0.0343 0.8621 0.6139 0.9793 0.9793
Radii Ratio, R1/R0 0.936 .09805 0.667 0.666 0.468 0.468
Maximum Use Temperature, °C (°F) 93(200) 93(200) 93(200) 993(200 93(200) 93(200)
Minimum Use Temperature, °C (°F) 0(32) 0(32) 0(32) 0(32) 0(32) 0(32)
Overall Instrument Constant, K 300.0 94.18 1355 2672 7620 15,200
Standard F1 Torsion Spring ? = Kfq/N
16
VISCOSITY RANGE IN CENTIPOISE(1)
Minimum Viscosity (2)
All models, 600 rpm maximum 0.5(3) 0.5(3) 2.3 4.5 12.7 25
Maximum Viscosity (4)
For Model 34A & HC34A, 300 rpm minimum 300 94 1,350 2,700 7,620 15,000
For Model 35A & 35SA, 3 rpm minimum 30,000 9,400 135,000 270,000 762,000 1,500,000
For Model 35A/SR12 & 35SA/SR12,0.9 rpm
minimum 100,000 31,400 400,000 890,000 2,550,000 5,000,000
Notes:
(1) Computed for standard Torsion Spring (f = 1.) For other torsion
springs multiply viscosity range by f factor.
(2) Minimum viscosity is computed for minimum shear stress and
maximum shear rate.
(3) For practical purposes the minimum viscosity is limited to 0.5 cP
because of Taylor Vortices.
(4) Maximum viscosity is computed for maximum shear stress and
minimum shear rate.
17
18
SECTION 8
TROUBLE SHOOTING AND MAINTENANCE
A. Troubleshooting
Symptoms Causes
B. Maintenance
The bob and rotor should be cleaned after each test and examined periodically for dents, abrasion or other
damage. Oiling or greasing of the viscometer is not required in normal service. Always remove the bob from
the bob shaft when transporting instrument to avoid bending bob shaft.
Periodically test the bob shaft bearings. Operate the instrument at 3 or 6 rpm with no sample around the
rotor and bob. Observe movement of the dial. It should not move more that +/- 1 division. Rough bob shaft
bearings should be replaced.
Instrument should be serviced by qualified personnel only. If factory service is required, contact Fann for
return authorization.
19
SECTION 9
SPECIFICATIONS
H W D LB KG
30164 35A 3, 6, 100, 200 115 Volts, 60 In. 15.2 6 10.5 15 6.8
300 and 600 Hz, Cm. 39 1 27
.075 Amps 5
30165 35SA 3, 6, 100, 200 115 Volts, 50 In. 15.2 6 10.5 15 6.8
300 and 600 Hz,
0.75 Amps
30166 35A/SR-12 .09, 1.8, 3, 6, 115 Volts, 60 In. 15.2 6 10.5 17 7.7
30, Hz, Cm. 39 1 27
60, 90, 100, 0.75 Amps 5
180,
200, 300 and
600
30167 34SA/SR- 0.9, 1.8, 3, 6, 115 Volts, 50 In. 15.2 6 10.5 17 7.7
12 30, Hz, Cm. 39 1 27
60, 90, 100, 0.60 Amps 5
180,
200, 300 and
600
TABLE 7
Rotor-Bob Dimensions
20
SECTION 10
ACCESSORIES
Torsion Springs
Part No. F. Constant Max Shear Stress Color Code
31068 F0.2 77.2 307 Green
31069 F0.5 193 766 Yellow
30752 F1 386 1,533 Blue
31070 F2 772 3,066 Red
31071 F3 1,158 4,600 Purple
31072 F4 1,544 6,132 White
31073 F5 1,930 7,665 Black
31074 F10 3,860 15,330 Orange
Rotors
30847 R1, Chrome-plated Brass
30849 R2, Chrome-plated Brass
30851 R3, Chrome-plated Brass
31716 R1, 303 Stainless Steel
31718 R2, 303 Stainless Steel
31720 R3, 303 Stainless Steel
35617 R1, Closed-end, Stainless Steel
35619 R2, Closed-end, Stainless Steel
Bobs
30844 B1, 303 Stainless Steel, Hollow
30843 B2, 303 Stainless Steel, Solid
30842 B3, 303 Stainless Steel, Solid
30841 B4, 303 Stainless Stell, Solid
Sample Cups
31203 Thermocup, 115 Volts, 50/60 Hz, 2 amps
31204 Thermocup, 230 Volts, 50/60 Hz, 1 amp
31759 Double-Wall Circulating Cup
35283 Insulated Sample Cup
30929 Stainless Steel Sample Cup
Circulators
35293 Heat-only Circulator, 90°- 212°F, four-liter cap., 115 Volts, 60 Hz, 1,000 Watt
35294 Refrigerated Circulator, 0°- 210°F, five-liter cap., 115 Volts, 60 Hz. Heater Capacity 1,000 Watt
Calibration
31517 DW3 Dead Weight Calibration Fixture
28696 Calibration Reference Fluid, 10 cP, 16 oz (475 ml)
28691 Calibration Reference Fluid, 20 cP, 16 oz (475 ml)
28692 Calibration Reference Fluid, 50 cP, 16 oz (475 ml)
28693 Calibration Reference Fluid, 100 cP, 16 oz (475 ml)
28694 Calibration Reference Fluid, 200 cP, 16 oz (475 ml)
28695 Calibration Reference Fluid, 500 cP, 16 oz (475 ml)
21
Fig. 6
35A & 35SA
22
SECTION 11
PARTS LIST
Please refer to the accompanying warranty statement enclosed with your product.
Return of Items
For your protection, items being returned must be carefully packed to prevent damage in shipment and
insured against possible damage or loss. Fann will not be responsible for damage resulting from careless or
insufficient packing.
Before returning items for any reason, authorization must be obtained from Fann Instrument Company.
When applying for authorization, please include information regarding the reason the items are to be
returned.