International University, Vietnam National University - HCMC 1

GENERAL CHEMISTRY LABORATORY

DATA SHEET
EXPERIMENT 1: CHEMICAL REACTIONS

Group: ______________ Section: _____1________Date: ______________

Group members: _______________________________

_______________________________

_______________________________

_______________________________

Instructor’s/TA’s signature and comments:

Expt. 1 Expt. 6

Expt. 2 Expt. 7

Expt. 3 Expt. 8

Expt. 4 Expt. 9

Expt. 5 Approval
 International University, Vietnam National University - HCMC 2
GENERAL CHEMISTRY LABORATORY

1. Reactions of Cu2+

Reaction Observation
0.5M CuSO4

+ 2M NaOH

0.5M CuSO4

+ 2M NH4OH

2. Reactions of silver halides

Reaction Observation
0.5M KCl

+ 0.1M AgNO3

0.5M KCl

+ 0.1M AgNO3

+ 2M NH4OH

0.5M KBr

+ 0.1M AgNO3

0.5M KBr

+ 0.1M AgNO3

+ 2M NH4OH

0.5M KI

+ 0.1M AgNO3

0.5M KI

+ 0.1M AgNO3

+ 2M NH4OH
 International University, Vietnam National University - HCMC 3
GENERAL CHEMISTRY LABORATORY

3. Reactions of H2O2

Reaction Observation
0.1M KMnO4

+ 2M H2SO4

+ H2O2

0.1M KI

+ 2M H2SO4

+ H2O2

H2O2

+ MnO2

4. Reactions of Nitrate

Reaction Observation
1M NaNO3

+ FeSO4

+ concentrated

H2SO4

1M NaNO2

+ FeSO4

+ concentrated

H2SO4

1M NaNO3

+ FeSO4

+ concentrated

CH3COOH
 International University, Vietnam National University - HCMC 4
GENERAL CHEMISTRY LABORATORY

5. Reactions of KMnO4
Reaction Observation
0.5M Na2SO3

+ 2M H2SO4

+ 0.1M KMnO4

0.5M Na2SO3

+ 6N NaOH

+ 0.1M KMnO4

0.5M Na2SO3

+ H2O

+ 0.1M KMnO4

6. Reaction of Potassium Dichromate (K2Cr2O7)

Reaction Observation
2M K2Cr2O7

+ 6M H2SO4

+ C2H5OH

7. A. Reactions of Fe3+
Reaction Observation
0.5M FeCl3

+ 2M KOH

0.5M FeCl3

+ 2M NH4OH
7. B. Reactions of Fe2+

Reaction Observation
0.5M FeSO4
+ 2M KOH
0.5M FeSO4
+ 2M NH4OH
 International University, Vietnam National University - HCMC 5
GENERAL CHEMISTRY LABORATORY

8. Reactions of Al3+

Reaction Observation
0.5M Al2(SO4)3

+ 2M NaOH

0.5M Al2(SO4)3

+ 2N NaOH

+ 2M HCl

0.5M Al2(SO4)3

+ 2M NaOH

+ 2M NaOH

9. Flame test
Solution Dominant flame color
LiCl

NaCl

KCl

CaCl2

BaCl2
 International University, Vietnam National University - HCMC 6
GENERAL CHEMISTRY LABORATORY

DATA SHEET
EXPERIMENT 2: pH AND BUFFERS

Group: ______________ Section: _____2________Date: ______________

Group members: _______________________________

_______________________________

_______________________________

_______________________________

Instructor’s/TA’s signature and comments:

Expt. 1 Expt. 4

Expt. 2 Expt. 5

Expt. 3 Approval
 International University, Vietnam National University - HCMC 7
GENERAL CHEMISTRY LABORATORY

1. pH OF DEIONIZED WATER

Observed pH
Time
(second) 1st (your group) 2nd (other group in the class)
(Group___) (Group___)
0
20
40
60
80
100
120
140
160

2. pH OF STRONG ACID

Measured pH
Solution Theoretical pH
1st 2nd
(Group___) (Group____)

10 mL of 0.1M HCl

Add 90 mL of distilled
water
Add 10 mL of
0.1M NaOH
Add 90 mL of
0.01M NaOH

3. pH OF WEAK ACID
Measured pH
Solution st
1 2nd Averaged Ka
(Group___) (Group____)

0.1M acetic acid

0.01M acetic acid

0.001M acetic acid

 International University, Vietnam National University - HCMC 8
GENERAL CHEMISTRY LABORATORY

4. pH OF SALTS
Measured pH
Solution Predicted pH 1st 2nd
(Group____) (Group____)

0.1M NaCl

0.1M CH3COONa

0.1M NH4Cl

5. pH OF BUFFERS

Volume (mL) Volume (mL) Measured pH

Calculated
Buffer 0.1M 0.1M Acid Base
pH 1st 2nd
CH3COOH CH3COONa
(Group__) (Group__)

A 10.0 40.0

B 40.0 10.0

C 25.0 25.0

 Part I: Addition of 10 drops 0.1 M HCl

pH after adding 10 Total volume HCl (drops) to change
Buffer pH from the start, pHo
drops HCl pH by one unit (pHo-1)

 Part II: Addition of 10 drops 0.1 M NaOH

pH after adding 10 Total volume NaOH (drops) to
Buffer pH from the start, pHo
drops NaOH change pH by one unit (pHo+1)

C
 International University, Vietnam National University - HCMC 9
GENERAL CHEMISTRY LABORATORY

DATA SHEET
EXPERIMENT 3: REDOX TITRATION

Group: _____________ Section: _____3_________ Date: ____________

Group members: _______________________________

_______________________________

_______________________________

_______________________________

Instructor’s/TA’s signature and comments:

Expt. 1 Expt. 3

Expt. 2 Expt. 4

Approval
 International University, Vietnam National University - HCMC 10
GENERAL CHEMISTRY LABORATORY

1. TITRATION OF KMnO4 SOLUTION WITH STANDARD H2C2O4 SOLUTION

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of KMnO4 (N)

1 -

2 -

Average Normality of KMnO4 = ____________ (N)

2. TITRATION OF UNKNOWN CONCENTRATION H2C2O4 SOLUTION WITH STANDARD

KMnO4 SOLUTION

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of H2C2O4 (N)

1 -

2 -

Average Normality of H2C2O4 =_______ (N)

3. TITRATION OF UNKNOWN CONCENTRATION FeSO4 SOLUTION WITH STANDARD

KMnO4 SOLUTION

Trial # Burette reading(mL) Volume of KMnO4 (mL) Normality of FeSO4(N)

1 -

2 -

Average Normality of FeSO4 =_______ (N)

 International University, Vietnam National University - HCMC 11
GENERAL CHEMISTRY LABORATORY

DATA SHEET
EXPERIMENT 4: CHEMICAL EQUILIBRIUM

Group: _____________ Section: ______4________ Date: ____________

Group members: _______________________________

_______________________________

_______________________________

_______________________________

Instructor’s/TA’s signature and comments:

Expt. 1 Expt. 4

Expt. 2 Expt. 5

Expt. 3 Approval
 International University, Vietnam National University - HCMC 12
GENERAL CHEMISTRY LABORATORY

1. ACID/BASE EQUILIBRIA

Equilibrium System: 2CrO42(aq) + 2H+(aq) ⇌ Cr2O72(aq) + H2O(l)

Description of Predicted outcome Observation

conditions

Initial solution

+ Conc. HCl

+ 6 N NaOH

2. EQUILIBRIA OF ACID/BASE INDICATORS

Equilibrium System: H(MV)(aq) + H2O(l) ⇌ H3O+(aq) + MV(aq)

Addition Predicted outcome Observation

None (control)

6 M HCl

6 M NaOH

6 M HCl
 International University, Vietnam National University - HCMC 13
GENERAL CHEMISTRY LABORATORY

3. COMPLEX ION FORMATION

Equilibrium System: Fe3+(aq) + SCN (aq) ⇌ [Fe(SCN)]2+(aq)

Addition Predicted outcome Observation

None

(control)

0.01M FeCl3

0.01 M KSCN

6M NaOH

Cold

Hot

0.1M AgNO3
 International University, Vietnam National University - HCMC 14
GENERAL CHEMISTRY LABORATORY

4. EQUILIBRIA OF PRECIPITATION REACTIONS

Equilibrium System: Ca2+(aq) + C2O42(aq) ⇌ CaC2O4(s)

Addition Predicted outcome Observation

Test tube 1:

0.1 M Na2C2O4

Test tube 2:

+ 0.1 M
H2C2O4

Test tube 2:

+ 6 M HCl

Test tube 2:

+ 6 M NH4OH

5. TEMPERATURE EFFECTS ON EQUILIBRIA

Equilibrium System: Co(H2O)62+(aq) + 4Cl(aq) ⇌ CoCl42(aq) + 6H2O(l)

Description of
Predicted outcome Observation
conditions

Nothing
changed

(control)

Hot water bath

Ice-water bath
 International University, Vietnam National University - HCMC 15
GENERAL CHEMISTRY LABORATORY

DATA SHEET
EXPERIMENT 5: FACTORS AFFECTING
REACTION RATE

Group: _____________ Section: _____5_________ Date: _____________

Group members: _______________________________

_______________________________

_______________________________

_______________________________

Instructor’s/TA’s signature and comments:

Expt. 1 Expt. 3

Expt. 2 Approval
 International University, Vietnam National University - HCMC 16
GENERAL CHEMISTRY LABORATORY

1. EFFECT OF CONCENTRATION ON REACTION TIME

Reaction 1:
__________________________________________________

Reaction 2:

__________________________________________________

Calculate the initial concentrations of I- and S2O82- ions:

Mixture # 5:

[I-] =

[S2O82-] =

Mixture Iodide ion Peroxydisulfate Time in seconds

Mixture Iodide ion Peroxydisulfate Time in seconds

10

11
 International University, Vietnam National University - HCMC 17
GENERAL CHEMISTRY LABORATORY

2. EFFECT OF TEMPERATURE ON THE REACTION RATE

Reaction System:

Description of Predicted outcome Observation Reaction time

conditions

Room
temperature

500C

900C

3. EFFECT OF A CATALYST ON THE REACTION RATE (30 pts)

Reaction System:

Trial Description of Predicted outcome Observation (Reaction rate)

conditions

1 + MnCl2

2 + MnO2

3 + NaCl

4 + CaCl2

5 + Zn

6 + KNO3

7 + Fe(NO3)3