1well Logging Methods - Unconventional Gas Characterisation
1well Logging Methods - Unconventional Gas Characterisation
Abstract: This paper provides an overview of the well-logging methods currently used in
the evaluation of shale gas formations. The combination of natural gamma-ray spectrosco-
py, density, neutron, sonic and resistivity logging allows in-situ identification of unconven-
tional reservoirs and the calculation of their total organic matter content. We improve the
regression relation between the total organic content and parameter d estimated by the
Zhao’s method. The level of maturity as a key parameter should be a priori known, and is
treated as an arbitrarily chosen constant during the procedure. We suggest estimating the
optimal value of the maturity constant by reducing the misfit between the observed well
logs and theoretical logs calculated by the Passey’s model in an automated procedure. We
compare the results of the improved well-log-analysis methods with core measurements.
We recommend the use of multivariate statistical and inversion methods to explore the
lithologic and petrophysical characteristics from independent sources, which may help in
resolving the ambiguity frequently encountered with the interpretation of unconventional
formations.
Keywords: well logging, unconventional reservoir, shale gas, total organic content, level of
maturity.
1. INTRODUCTION
The world’s petroleum consumption has been growing steadily since the 1950s.
The continuous rise in living standards and demand entailed increased oil and gas
production, which helped the oil industry to take a leading role in the energy sector.
However, the Earth's hydrocarbon reserves are declining globally. To reach more
resources, significant technological progress is going on today, which allows the
exploitation of complex reservoirs previously thought unattainable. Conventional
hydrocarbon formations such as sediments with high porosity and permeability can
be easily and cheaply produced, but they are relatively small in number and contain
just a small percentage of the Earth’s stored hydrocarbons. The production of ex-
tra-low permeability reservoirs is more expensive and technically challenging;
however, the price of hydrocarbons and the continuous rise of new technologies
have enabled their efficient operation. Unconventional reservoirs are of great im-
Unconventional Shale Characterization Using Improved Well Logging Methods 33
Figure 1.
Petrophysical models used for the interpretation of unconventional reservoirs:
rock models (a)–(c) (PASSEY et al. [5]) and (d)–(e) (ZHAO et al. [6])
rite is also a common building block in organic-rich layers, the amount of which
must be considered. A linear relation was observed between the amount of organic
material and pyrite concentration [12]. The clay volume in shale reservoirs may reach
30–40 v/v. If the salinity of pore fluid is low and the matrix does not contain conduc-
tive minerals, the clay conductivity should be added to the rock conductivity.
The three most commonly used porosity measurements are acoustic, compen-
sated density, and compensated neutron logs. All three methods respond to the
presence of organic matter because of its physical properties. Depending on its
composition, the organic material has an average density of 1 g/cm3, sonic transit-
time of 180 μs/ft, and hydrogen index of 0.67 [13]. The organic matter in mature
reservoirs is indicated by high porosities. The presence of organic matter, due to its
low P-wave velocity, gives high acoustic-interval times [14], which is also affected
by the mineral composition, porosity, and type of pore-filling fluid. The bulk densi-
ty of shale gas formations is normally low, which is due to the low density of the
organic matter. The neutron-porosity response is mostly influenced by the hydro-
gen content of organic matter, pore water, and hydrocarbons and the clay volume.
Other advanced logging technologies can also be used for lithology identification
(e.g. spectral GR and photoelectric absorption index logs), improved estimation of
porosity and permeability (e.g. nuclear magnetic resonance log), and mechanical
characterization (e.g. full waveform sonic log).
R 1
log R log 10 t tbase , (1)
base 50
R
where Rb and tb denote the resistivity reading and acoustic traveltime observed at
the baseline, respectively. In fine-grained organic-matter-free (water saturated)
shaly formations, both curves run along the baseline, while they are separated from
each other in organic matter-rich shale reservoirs [5]. The separation between the
two curves is directly proportional to the TOC. The method assumes a nearly linear
connection between quantities logR and TOC. This connection holds only when
the constant value of Level of Organic Maturity (LOM) is known; LOM is normal-
ly measured in the laboratory. An estimate can be given to the value of TOC by
using
where the default values of regression constants are a = 2.297 and b= 0.1688 [5].
The TOC is estimated in weight percent, which must be corrected for the original
organic carbon content of the shale (it is 0.8%). If the sonic log is not available,
the following empirical formulae can be used analogously to Equation (1)
R
log RN log 10 4ΦN ΦN ,base , (3)
Rbase
R
log RD log 10 2.5 b b,base , (4)
Rb
where ΔlogRN and ΔlogRD are the logarithmic deviation of the density and neutron
log from the resistivity log, respectively, ΦN is the neutron porosity, ΦN,base is the
38 István Bibor–Norbert Péter Szabó
baseline value of neutron porosity, ρb is the bulk density and ρb,base is the bulk den-
sity observed at the baseline. The crossover between the properly scaled well logs
in Equations. (3)–(4) is proportional to the quantity of organic matter [2].
Several authors have proposed modification of the logR method. SONDER-
GELD et al. [11] observed that the traditional method tends to overestimate the val-
ue of TOC in over-matured reservoirs. They introduced an empirical correction
factor, which was used to multiply the right side of Equation (2). WANG et al. [21]
pointed out that the mineral composition of shale reservoirs may vary between
wide limits, which may result in erroneous conclusions in the evaluation of reser-
voirs with complex lithology. PASSEY et al. [5] modified Equation (2) by incorpo-
rating the acoustic traveltime of the rock matrix and cementation factor. Instead of
using LOM in the Passey model, in some cases, the maximum temperature of hy-
drocarbon generation (Tmax) is recommended. Further improvements can be made
by incorporating natural gamma-ray intensity readings, too [21]. RENCHUN et al.
[17] changed the original equation of the Passey model to comprise simultaneously
the differences of resistivity, density, and acoustic logs.
where ΦN,a (v/v) and ΦD,a (v/v) are the apparent neutron and density porosity, re-
spectively. The GR and Icl logs are plotted on the same track. In a formation with
low organic content, the two logs overlap, while in organic-rich intervals they are
separated from each other. The degree of separation is measured by the following
derived parameter
GR GRmin I I
d cl cl ,min , (6)
GRmax GRmin I cl ,max I cl ,min
where GRmin and GRmax are the extreme values of the gamma-ray log, Imin and Imax
are those of the clay indicator. According to ZHAO et al. [6], the parameter d de-
Unconventional Shale Characterization Using Improved Well Logging Methods 39
fined in Equation (6) is linearly proportional to TOC, where the regression coeffi-
cients must be estimated for the given measurement area.
model the response of the resistivity tools and to solve the related inverse problem
more accurately [32], [33], [34].
Cluster analysis may also help in the identification and classification of shale
reservoirs. SZABÓ et al. [35] developed a hierarchical cluster analysis assisted
global inversion technique to estimate the layer thicknesses and zone parameters in
conventional hydrocarbon reservoirs. The rock matrix of unconventional reservoirs
is generally made up of several minerals, the relative amounts of which should be
estimated as accurately as possible. The models illustrated in Figure 1 include sev-
eral other parameters to be determined, too. Local (depth-by-depth) inversion tech-
niques traditionally used in well-log analysis can give an estimate for fewer petro-
physical parameters than data measured in the point. In case of complex reservoirs,
there are many more petrophysical and zone parameters than data, which leads to
an ambiguous (underdetermined) inverse problem. To increase the data-to-
unknowns ratio and stability, we suggest the use of the interval inversion method,
which inverts a data set of a longer depth interval jointly. By using a series expan-
sion-based discretization approach, the inverse problem is solved for a far lower
number of inversion unknowns than data to reduce the estimation error of the mod-
el parameters. An application to multimineral hydrocarbon formations was pub-
lished by DOBRÓKA et al. [36].
5. CASE STUDIES
5.1 Estimation of total organic content
We improve the d method and test it on the same well-logging data set originally
used by ZHAO et al. [6], which was collected in the Sichuan Basin, South-West
China. The investigated formation is mainly made up of calcareous shale with a
thickness varying between 20–120 m. We analyze the natural gamma-ray intensity
(GR), compensated density (DEN) and neutron-porosity (CEN) logs for estimating
the TOC, which is approximately 1–3% according to core measurements. After
calculating the apparent density- and neutron-porosities, we calculate the values of
d along the well. For this, we use the following zone parameters: GRmin = 108,
GRmax = 550, Icl,min = –0.22, Icl,max = 0.8. We study the relation between the TOC
measured on core samples and parameter d estimated by Equation (6). By plot-
ting the TOC and Δd values, Figure 2 shows that the relation is much more nonlin-
ear than linear, as originally suggested by [6]. For a more accurate interpretation,
especially in the domain of large d values, we suggest the use of the regression
model
TOC 1 e d ,
(7)
by the minimization of the misfit between the observed TOC values and those cal-
culated by Equation (7). We use the Marquardt algorithm for solving the least
squares inverse problem [37]. For the Sichuan Basin, we obtain the following re-
gression coefficients: = 4.29, = 0.85, = 55, = 3.
Figure 2.
Nonlinear regression relation between total organic matter content and parameter
d estimated by Equation (6) in the Sichuan Basin
The result of well log analysis is illustrated in Figure 3. The separation between the
GR and Icl curves is directly proportional to the amount of organic matter in the
shales. A potential shale gas zone is indicated by the well logs between 710 and
805 m. The highest values of TOC are around 790–800 m, where it increases up to
5%. The reservoir is also confirmed by high GR, low DEN and CN values.
the data distance as the root mean square error between the measured TOC values
and the calculated ones
1/ 2
1 N 2
RMS TOCimeas TOCicalc 100 (%) . (8)
N i 1
where N is the number of core data. The RMS versus LOM relation for Barnett
shale is given in Figure 5.
Figure 3.
Total organic matter content estimation by the improved d method
in the Sichuan Basin
Unconventional Shale Characterization Using Improved Well Logging Methods 43
Figure 4.
Application of the logR method on well logs measured in the Barnett Shale
The optimal value of LOM is given at the minimum of the RMS curve, which
should be used in Equation (2) to estimate the TOC. By reading the baseline values
on the sonic (80 µs/ft) and resistivity (6 ohmm) logs (Figure 4), we calculate the
well log of parameter ΔlogR using Equation (1). The TOC is calculated at different
values of LOM (Figure 6). The figure confirms that the best fit between the meas-
44 István Bibor–Norbert Péter Szabó
ured and calculated TOC is given by LOM = 8.4. The result agrees well with data
in the literature, e.g. CRAIN [39] suggests a LOM 8.5 for shale gas reservoirs.
Figure 5.
Determination of maturation level by the minimization of data prediction error
Figure 6.
Observed and calculated
organic matter content at
different
maturity levels
in the Barnett Shale
Unconventional Shale Characterization Using Improved Well Logging Methods 45
6. CONCLUSIONS
In this paper, an overview is given on the evaluation of shale gas reservoirs using
well-logging methods. We suggest two improved methods for a more accurate
estimation of total organic matter content. A nonlinear regression model is assumed
between the organic matter content and parameter d suggested previously by
ZHAO et al. [6]. The level of maturity should be optimized for a better estimation of
organic content. We suggest reducing the misfit between the TOC values calibrated
by lab measurement and predicted TOC by the Passey model. We recommend the
use of multivariate statistical and inversion methods to explore the lithologic and
petrophysical characteristics from independent sources, which may help in resolv-
ing the ambiguity frequently encountered with the interpretation of unconventional
formations. A robust form of cluster and factor analysis may help in the identifica-
tion and reserve calculations. Factor analysis explores the connections between the
well-logging data set and the petrophysical properties of shale gas formations. By
the interval inversion of well logs, it becomes possible to an estimate for the petro-
physical parameters of unconventional reservoirs. The added advantage of the in-
version approach is that it can give an estimate also for the layer thicknesses and
zone parameters, including their estimation errors.
ACKNOWLEDGEMENTS
This research was supported by the GINOP-2.3.2-15-2016-00010 “Development of
enhanced engineering methods with the aim at utilization of subterranean energy
resources” project in the framework of the Széchenyi 2020 Plan, funded by the
European Union, cofinanced by the European Structural and Investment Funds.
Special thanks for providing the data set go to Mr. Peiqiang Zhao (Sichuan Basin)
and Mr. Michael Holmes (Barnett Shale).
LIST OF SYMBOLS
Symbol Description Unit
a Regression constant
AC Acoustic traveltime data s/ft
b Regression constant
CEN Neutron-porosity data v/v
DEN Compensated density data g/cm3
GR Natural gamma-ray intensity data API
GRmin Minimal values of the gamma-ray log API
GRmax Maximal values of the gamma-ray log API
Icl Clay indicator v/v
Icl,min Minimal values of the clay indicator v/v
Icl,max Maximal values of the clay indicator v/v
46 István Bibor–Norbert Péter Szabó
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