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Pyrojector II Solid Sample Kit 0048-E

The document describes a solid sampling kit for quantitative analysis of solid samples using pyrolysis gas chromatography. The kit allows weighing samples before and after pyrolysis to determine the exact amount analyzed. It consists of quartz sample tubes that hold weighed samples and a tubular cutter to extract sections from sheet materials like films or paper for analysis. Samples are inserted into the pyrolysis unit to be heated and analyzed, providing either qualitative or quantitative results about the sample's composition.

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Lauro Araripe
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54 views2 pages

Pyrojector II Solid Sample Kit 0048-E

The document describes a solid sampling kit for quantitative analysis of solid samples using pyrolysis gas chromatography. The kit allows weighing samples before and after pyrolysis to determine the exact amount analyzed. It consists of quartz sample tubes that hold weighed samples and a tubular cutter to extract sections from sheet materials like films or paper for analysis. Samples are inserted into the pyrolysis unit to be heated and analyzed, providing either qualitative or quantitative results about the sample's composition.

Uploaded by

Lauro Araripe
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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www.sge.

com SOLID SAMPLING KIT FOR THE SGE PYROJECTOR II

Quantitative In these last three areas, while


qualitative analysis gives a lot of
analysis is complete, the probe,
sample tube and any residue is
very useful information, removed from the furnace. The
Analysis of Solid quantitative analysis is really tube, after cooling, can be
required. It is for this type of reweighed to determine the residue
Samples by analysis that the solid sampling kit
was devised.
if desired.

II. The other method utilised by


Pyrolysis DESCRIPTION this device, takes advantage of the
fact that sheet materials such as
• Solid sampling kit The Kit consists of a sampling polymeric film, tissue, leather
• Known sample size head which is screwed onto the top paper etc can be cut quite easily
• Easily retrofitted to existing of the Pyrojector furnace. Carrier with a "wad" punch or "cork
PRODUCT DATA

• SGE Pyrojectors gas is connected into it. Samples borer", (fig. 2).
• Silica sampling tubes may be presented in one of two
• Simple and reproducible ways. The Kit provides a stainless steel
tubular cutter which incorporates a
I. In the quantitative mode, plunger with a gas tight seal.
INTRODUCTION Using the cutter as you would a
samples are placed inside a
disposable quartz tube 50 x 0.53 cork borer, a section is cut from
Pyrolysis GC has matured
mm ID in size, which is weighed the sample and conveyed within
sufficiently now as an analytical
before and after on an analytical the tube to the pyrolyser inlet
technique, that it finds application
balance, to determine the weight of where it is transferred into the
in may fields.
the sample. furnace by depressing the plunger,
(fig. 3).
Forensic
• Characterisation of paint flakes The tube containing the sample
is attached to the solids sampling The information obtained in this
• Characterisation of tyre tread
probe by means of a spring hook, way is "qualitative" but may just as
rubbers
(fig. 1). The probe is inserted in easily be quantified since the bulk
• Characterisation of fibres etc.
the injection head and the sample sample may be weighed before and
analysed as per the pyrolysis after, to determine how much has
Polymers
temperature selected. When the been taken.
• Identification of Plastics
• Identification of Pigments

Brewing & Foods


• Characterisation of yeasts and
bacteria

Building Products
• Determination of concrete
additives

Geology
• Determination and
characterisation of the organic
content in shale

Paper Industry
• Determination of fillers in paper
• Determination of lignins in Figure 1.
Fitting sample tube to solids sampling probe
paper
SOLID SAMPLING KIT FOR THE SGE PYROJECTOR II

Figure 2. Figure 3.
Using the tubular cutter accessory to cut a section from a piece of film The tubular cutter containing the sample has been transferred to the
material. Weigh the sample before and after to ascertain how much Pyrojector and installed in the sampling head. The sample is injected
has been taken. by depressing the plunger.

Sample Material

ORDERING INFORMATION PYROJECTOR II

Part No. Code Description

095001 PIU - 2 Pyrojector II (110 or 240V - 50/60 Mz)


09500xx* PIU adaptor Instrument and Injector specific adaptor*
0950204 PIU Solid Sample Accessory Kit
0950095 PIU-QST Sample Tubes, Quartz, pack of 50

* Nominate make and model of GC and Injector type.


Specifications are subject to change without notice.
Fused silica columns are manufactured under license granted by the Hewlett Packard Company.
Pyrojector II is a trademark of SGE International.

www.sge.com
Publication No. PD-0048-E Rev:01 03/02

SGE International Pty. Ltd. SGE Incorporated (USA) SGE (France) Sarl SGE Deutschland GmbH SGE Japan Inc.
Tel: +61 (0) 3 9837 4200 Toll Free: 800 945 6154 Tel: +33 (0) 1 6929 8090 Tel: +49 (0) 6151 860486 Tel: +81 (45) 222 2885
Fax: +61 (0) 3 9874 5672 Fax: +1 512 836 9159 Fax: +33 (0) 1 6929 0925 Fax: +49 (0) 6151 860489 Fax: +81 (45) 222 2887
email: [email protected] email: [email protected] email: [email protected] email: [email protected] email: [email protected]

SGE Australia Pty. Ltd. SGE Europe Ltd. (UK) SGE (Italia) Srl. SGE China Service Centre SGE India
Toll Free:1800 800 167 Tel: +44 (0) 1908 568 844 Tel: +39 06 4429 0206 Tel: +86 (10) 6588 8666 Tel: +91 (022) 471 5896
Fax: (03) 9874 5672 Fax: +44 (0) 1908 566 790 Fax: +39 06 4429 0724 Fax: +86 (10) 6588 6577 Fax: +91 (022) 471 6592
email: [email protected] email: [email protected] email: [email protected] email: [email protected] email: [email protected]

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