Synthesis and Organization of Nano Materials
Synthesis and Organization of Nano Materials
Subject:
Dpto./ Faculty:
Department of Inorganic chemistry and Department of Pharmacology and Therapeutical Chemistry UB Department of Molecular Nanoscience and organic materials Instituto de Ciencia de Materiales de Barcelona CSIC
Objectives: General objectives and skills that the student should obtain at the end of the course. General Objectives: Give a general vision of the different procedures for preparation of nanometric materials: bottom up and top down. Deeper in the knowledge of multiple techniques to obtain nanomaterials following the bottom up approximation Relate the material typology with its synthesis method. Know the importance of the synthesis method in the material properties. Give a knowledge of the bibliographical references in this area. Understand and differentiate synthesis strategies in the nanomaterials preparation. Know the fundamental concepts for designing a synthesis procedure. Get the ability in managing the bibliographical sources.
Competencies:
Topics:
Adress: Facultad de Fsica, c/ Marti Franques 1, 08028 Barcelona Espaa Master Community: http://campusvirtual.ub.edu/course/view.php?id=427 Website: http://www.ub.edu/nanotec/ E-mail: [email protected]
Introduction: Nanomateials: concept and typology. Metodological approximations to the nanomaterials: synthesis (Bottom up) and fabrication (top down). Classification of synthesis methods. Importance of the supramolecular chemistry and phases separations as synthesis tools. Zero dimension Nanostructures: Nanoparticles. Homogeneous Nucleation: Growth factors. Heterogeneous nucleation: Sputtering, Thermal oxidation, kinetic controlled synthesis: micelles, spray pyrolisis, Template leaded methods. Covalent synthesis: iterative and self-assembled. Complementary methods: Sonochemistry, microwaves, Compressed fluids.. Nanostructures of one dimension: nanowires, nanorodos and nanotubes. Crystalline growth. Synthesis based template effect: electrochemical and electrophoretic deposition. Covalent synthesis and self-assembled derivation Nanostructures of two dimensions: Thin Films. Physical vapour deposition (PVD). Chemical Vapor Deposition (CVD), Atomic Layer Deposition (ATD), Layer by layer deposition. Langmuir-Blodgett Films. Electrochemical deposition. Sol-gel Films. Synthesis based in templates. Self-assembled monolayer. Application of the synthesis and organization methods for obtaining nanomaterials. Polimers, Zeolites, Nano- Micro and Mesoporous. Nanocompounds, nanocrystalline materials, soft matter. Plan: Lectures: Independent work: Study: Bibliography Nanochemistry: A Chemical Approach to Nanomaterials G. Ozin, A Arsenault ISBN 0 85404 664 X Royal Society of Chemistry, Cambridge, UK, 2005 Nanostructures & Nanomaterials: Synthesis, Properties & Applications Guozhong Cao ISBN 1-86094-480-9 (paperback) Imperial College Press, 2004. Nanochemistry G.B. Sergeev ISBN: 0-444-51956-4 Elsevier, 2006 Grimsdale AC, Mullen K The chemistry of organic nanomaterials ANGEWANDTE CHEMIE-INTERNATIONAL EDITION 44 (35): 5592-5629 2005 22 hours (20 Lectures + 2 exam) 8 hours 39 hours
Adress: Facultad de Fsica, c/ Marti Franques 1, 08028 Barcelona Espaa Master Community: http://campusvirtual.ub.edu/course/view.php?id=427 Website: http://www.ub.edu/nanotec/ E-mail: [email protected]
Toward 'smart' nano-objects by self-assembly of block copolymers in solution Rodriguez-Hernandez J, Checot F, Gnanou Y, Lecommandoux S PROGRESS IN POLYMER SCIENCE 30 (7): 691-724 JUL 2005 New approaches to the synthesis of anisotropic, core-shell and hollow metal nanostructures Sastry M, Swami A, Mandal S, Selvakannan PR JOURNAL OF MATERIALS CHEMISTRY 15 (31): 3161-3174 2005 Nanotechnology with soft materials Hamley IW ANGEWANDTE CHEMIE-INTERNATIONAL EDITION 42 (2005) 1692-1712 Controlled synthesis of high quality semiconductor nanocrystals Peng XG, Thessing J STRUCTURE AND BONDING 118: 79-119 2005 Nanomaterials and supercritical fluids Reverchon E, Adami R JOURNAL OF SUPERCRITICAL FLUIDS 37 (1): 1-22 2006 Polymer sol-gel synthesis of hybrid nanocomposites Pomogailo AD COLLOID JOURNAL 67 (6): 658-677 2005 Dupuis AC The catalyst in the CCVD of carbon nanotubes - a review PROGRESS IN MATERIALS SCIENCE 50 (8): 929-961 2005 Synthesis of materials within reverse micelles Uskokovic V, Drofenik M SURFACE REVIEW AND LETTERS 12 (2): 239-277 APR 2005 Tailor-made nanoparticles via gas-phase synthesis Gutsch A, Muhlenweg H, Kramer M SMALL 1 (1): 30-46 JAN 2005
Adress: Facultad de Fsica, c/ Marti Franques 1, 08028 Barcelona Espaa Master Community: http://campusvirtual.ub.edu/course/view.php?id=427 Website: http://www.ub.edu/nanotec/ E-mail: [email protected]