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Siflon Drugs: Sy. No. 25/4, Rachanapalli (V)

The document summarizes an automatic potentiometric titration experiment. The experiment involved titrating a sample of closantel sodium against a 0.1M perchloric acid solution to determine its concentration. The titration reached the endpoint of 6.79 mL at 2585 mV. Analysis of the results found the closantel sodium sample had an assay of 94.1559% and 99.16% on an anhydrous basis.

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bharath kumar
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48 views

Siflon Drugs: Sy. No. 25/4, Rachanapalli (V)

The document summarizes an automatic potentiometric titration experiment. The experiment involved titrating a sample of closantel sodium against a 0.1M perchloric acid solution to determine its concentration. The titration reached the endpoint of 6.79 mL at 2585 mV. Analysis of the results found the closantel sodium sample had an assay of 94.1559% and 99.16% on an anhydrous basis.

Uploaded by

bharath kumar
Copyright
© © All Rights Reserved
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 4

VEEGO

AUTOMATIC POTENTIOMETRIC
TITRATION APPARATUS

SIFLONDRUGS
Sy. No. 25/4, Rachanapalli (V).
Anantapur 515004. Andhra Pradesh

MODEL: AUTOPOT-KF SERIAL NO.: 20/1218


TIME: 14:57.27 DATE: 28/02/2022

FILE NAME : CLOSANTEL SODBP


SAMPLE NAME CLOSANTELSODIUM
SAMPLE D : CLOSANTEL SODIUM
BATCH NO : CLS0620222
TITRATION NO :2
TITRANT :0.1M PERCHLORICDTHE TI.. AN
ELECTRODES : GLASS
: CALOMEL
OPERATOR NAME : V. SREEKANTH REDDY
TITRATION MODE SINGLE END POINT
TITRATION METHOD STEP VOL DOSING
SENSITIVITY 25
END mV 900

SETTINGs Direet Vol: 5.00 ml Dosing Vol 0.10 ml


End Vol: 20.00 ml Dosing Int: 10 sec

Vol(ml) mV
Difference
0.00 2075
1.00 2133 0
2.00 2186 0
3.00 2234 0
4.00 2283 0
5.00 2340 0
5.00 2348
5.110 2359 11
5.20 2367 8
5.30 2375
5.40 2380
5.50 2392 12
5.60 2406 14
5.70 2417 11
5.80 2419
5.90 2430
6.00 2442 12
6..10 2463 2
6.20 2469
.30 2476 1
40 2491 15
50 2509 18
6.60 2522 13
6.70 2549 27
6.80 2588 39
6.90 2626 38
7.00 2707 81

Page 1 of 4
EndPoint @ 6.7900 ml and 2585 mV

Peak Magnitude: 81 mV

REMARK : TITRATION OVER

Page 2 of 4
VEEGO
AUTOMATIC POTENTIOMETRIC
TITRATION APPARATUS

SIFLON DRUGS
Sy. No. 25/4, Rachanapalli (V).
Anantapur - 515004, Andhra Pradesh

MODEL: AUTO/POT-KF SERIAL NO.: 20/1218


TIME 14:57:27 DATE: 28/02/2022

FILE NAME : CLOSANTEL SODBP


SAMPLENAME :CLOSANTELSODIUM
SAMPLE ID CLOSANTEL SODIUM
BATCH N0 :CLSO620222
TITRATION NO :2
TITRANT :0.IM PERCHLORICDTHE TI.. AN
ELECTRODES :GLASS
CALOMEL
OPERATOR NAME V. SREEKANTH REDDY
TITRATION MODE SINGLE END POINT
TITRATION METHOD STEP VOL DOSING
SENSITIVITY 25
END mV :900

SETTINGS Dire:ct Vol 5.00 ml Dosing Vol: 0.10 ml


End Vol: 20.00 ml Dosing Int: 10 sec

PARAMETER VALUE REMARK

READING 6.7923 ml
BLANK READING 0.0290 ml

SAMPLEQUANTITY 0.50240 g
MOLARITY . 0.10186 M

STANDARD MOLARITY 0.1000 M

STANDARD FACTOR 0.068500 g

WATER CONTENT. 5.05 %

ASSAY AS IS 94.1559 %

ASSAY ANHYDROUS BASIS 99.16 %

AnalyzedBy: Checked By: Approved By:


28 lo22 022

COMMENT:
pwl Comphie pen Apec

Page 3 of 4
GRAPHI DETAILS
TIME: 14:57:27 DATE: 28/02/2022

SAMPLE ID: CLOSANTEL SODIUM BATCH NO. : CLS0620222

SAMPLE NAME: CLOSANTELSODIUM TITRATION NO. : 2

2800

28 00

E 2400

2200

2000

Vonme

100

40

VolumB

80

20

olumE

40

20

AMA

Valu me

Page 4 of 4

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