Operation and Instruction Manual
Operation and Instruction Manual
REV K-A
Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
CERTIFICATE OF CONFORMANCE
Portable Heated Oil Test Centrifuge
K60094, K60005, K60095, K60006, K60096
K60094-FT, K60005-FT, K60095-FT, K60006-FT, K60096-FT
K60094PT, K60005-PT, K60095-PT, K60006-PT, K60096-PT
This certificate verifies that part numbers listed above, Portable Heated Oil Test Centrifuge, was manufactured in
conformance with the applicable standards set forth in this certification.
This unit is tested before it leaves the factory, to ensure total functionality and compliance to the above specifications
and ASTM standards. Test and inspection records are on file for verification.
Vincent Colantuoni
Product Manager
Date: ________________________________
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
WEEE Directive
Background
The goal of the WEEE Directive is to encourage design of environment-friendly products that increase reuse, recycling and other forms
of recovery to reduce waste streams and applies to listed Electronic and Electrical Equipment (EEE) and Koehler's equipment falls broadly
into Appendix 1A; Section 9 Monitoring and Control Equipment: Measuring, weighing or adjusting appliances for household or as
laboratory equipment.
Any associated non-embedded equipment such as Lighting (Saybolt Color) and PCs/Printers also fall under WEEE. If provided with an
order these ancillary items must be WEEE compliant. For these and other reasons (printer cartridges are regionalized) the equipment
must be supplied through a third party supplier in Europe.
The WEEE Directive applies to electrical and electronic equipment falling under the categories set out in Annex IA provided that the
equipment concerned is not part of another type of equipment that does not fall within the scope of this Directive. Annex IB contains a list
of products which fall under the categories set out in Annex IA.
http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2003:037:0024:0038:en:PDF
Professional use
For equipment defined for ’professional use’ local authorities have no role to play. Producers and importers are basically responsible for
collection of WEEE recyclables from the professional user and for subsequent management. A separate statement is given cataloging
the items that require separation from the equipment along with basic information on subsequent processing or recycling prior to disposal
of the equipment.
http://www.dpa-system.dk/en/WEEE/Products/Private-or-professional-use
It is illegal to market electrical and electronic equipment covered by producer responsibility without being registered.
http://www.dpa-system.dk/en/WEEE/Producers/Whoissubjecttoproducerresponsibility
Product Design
Koehler's designs allow for complete disassembly to a modular level which usually allows for standard recycling. A qualified refrigeration
system technician must be consulted when disassembling and de-commissioning any equipment with refrigeration systems.
Koehler's scientific testing equipment is robustly designed to function over a long service life and are typically repaired many times over
the course of years rather than being replaced. We believe that re-use and refurbishment is the very best form of re-cycling.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
Recycling instructions
In the event that replacement becomes necessary, we will include instructions, particularized to each instrument that informs the customer
of their recycling responsibilities and giving them guidance in doing this. All Koehler equipment has been placed on the market since 13th
August 2005 and so Koehler is defined as a "new WEEE producer". As such we must provide information on refurbishment, treatment,
and re-use.
Our instrument manual will include this compliance statement and indicate that any collection of materials will be handled by their
authorized distributor. In the event that the distributor is unreachable or is no longer a distributor for Koehler Instrument, Co., other
arrangements may be made including accepting the materials directly.
Recycling is free of charge. Shipping is the responsibility of the end users. Whether shipping to a distributor or to Koehler directly, safe,
properly declared, and labeled packaging and shipping expenses are the sole responsibility of the end user.
WEEE Marking
Since Koehler products are subject to the WEEE Directive we must display the WEEE symbol shown above in accordance with European
Standard EN 50419 on the equipment. It must be indelible, at least 5mm in height, and clearly legible. If the equipment is too small the
mark must be in the product literature, guarantee certificate, or on the packaging. Rules on marking are established in section 49 of the
WEEE Order.
As a minimum the following substances, preparations and components have to be removed from any separately collected WEEE:
- Mercury containing components, such as switches or backlighting lamps (compact fluorescent lamps, CFL),
- Batteries
- Printed circuit boards if the surface of the printed circuit board is greater than 10 square centimeters (about 4 sq in.),
- Toner cartridges, liquid and pasty, as well as color toner,
- Chlorofluorocarbons (CFC), hydrochlorofluorocarbons (HCFC) or hydrofluorocarbons (HFC), hydrocarbons (HC)
- Liquid crystal displays (together with their casing where appropriate) of a surface greater than 100 square centimeters and all those
back-lighted with gas discharge lamps,
- External electric cables
- Components containing refractory ceramic fibers as described in Commission Directive 97/69/EC of 5 December 1997 adapting to
technical progress Council Directive 67/548/EEC relating to the classification, packaging and labeling of dangerous substances (2),
- Electrolyte capacitors containing substances of concern (height > 25 mm, diameter > 25 mm or proportionately similar volume)
2. The following components of WEEE that is separately collected have to be treated as indicated:
- Equipment containing gases that are ozone depleting or have a global warming potential (GWP) above 15, such as those contained in
foams and refrigeration circuits: the gases must be properly extracted and properly treated. Ozone-depleting gases must be treated in
accordance with Regulation (EC) No 2037/2000 of the European Parliament and of the Council of 29 June 2000 on substances that
deplete the ozone layer (4).
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
Table of Contents
1. Introduction 2
1.1. Koehler’s Commitment to Our Customers 2
1.2. Recommended Resources and Publications 2
1.3. Instrument Specifications 3
2. Safety Information and Warnings 3
3. Getting Started 4
3.1. Packing List 4
3.2. Unpacking 4
3.3. Setup 4
3.4. Accessories for Running Tests 5
4. Descriptions 5
4.1. Instrument Description 5
4.2. Control Panel 6
4.3. Temperature Controller 7
5. Operation 8
5.1. Power Connection 8
5.2. Test Procedure 8
6. Maintenance 9
6.1. Routine Maintenance 9
6.2. Replacement Parts 10
7. Wiring Diagram 11
8. Troubleshooting 12
8.1. The test will not start 12
8.2. The motor stalls or will not come up to speed properly 12
8.3. The unit does not heat up 12
9. Service 12
10. Storage 12
11. Warranty 12
12. Returned Goods Policy 13
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
1. Introduction
The Portable Heated Oil Test Centrifuge is designed expressly for the determination of water and sediment of crude oil. This
unit accommodates four centrifuge tubes of ASTM conical type 6". The molded PTFE supports provide for maximum
protection and easy positioning of the tubes. Includes an integrated tube holder and pre-heater (4) for ease of sample
handling and pre-conditioning.
• Analog Speed Control
• Integrated Tube Holder and Pre-Heater (4)
• Independent Digital Temperature Displays for both the Bowl and Pre-heater temperature
• Switchable Temperature Display between °C and °F
• Substantial Insulation for Reduced Heat Loss
• 115V 60Hz or 220-240V 50/60Hz Power Requirement for laboratory use
• 12V DC Power Requirement for field use
• Opening in Top Lid for Speed Calibration by Portable Laser Tachometer
This manual provides important information regarding safety, technical reference, installation requirements, operating condition
specifications, user facility resource requirements, and operating instructions for the Portable Oil Test Centrifuge. This manual
should also be used in conjunction with applicable published laboratory procedures. Information on these procedures is given in
section 1.2.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
WARNING: Keep the bowl lid closed while the samples are spinning!!!
• Be sure there are no foreign objects in the centrifuge bowl.
• NEVER try to slow the carousel arm down with your hands or place your
hands or any object inside the bowl while the carousel arm is spinning.
Allow the carousel arm to come to a complete stop before removing your
sample. Allow the automatic brake to stop the carousel arm.
• NEVER leave the centrifuge unattended while the samples are spinning.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
• DO NOT leave oily rags or any type of combustible material in or around your centrifuge.
• STAY ALERT! Do not operate this unit while under the influence of medication, alcohol, or drugs.
Equipment Modifications and Replacement Parts: Any modification or alteration of this equipment from that of factory
specifications is not recommended and voids the manufacturer warranty, product safety, performance specifications, and/or
certifications whether specified or implied, and may result in personal injury and/or property loss. Replacement parts must be
O.E.M. exact replacement equipment.
Unit Design: This equipment is specifically designed for use in accordance with the applicable standard test methods listed in
section 1.2 of this manual. The use of this equipment in accordance with any other test procedures, or for any other purpose, is
not recommended and may be extremely hazardous.
Over Temperature Protection: This unit is equipped with Over Temperature Protection (OTP) circuitry to prevent overheating.
The unit will automatically interrupt power to the heater if equipment malfunction or operator error causes the temperature to
exceed 220°F. The power can only then be restored by identifying and correcting the problem and allowing the unit to return to
normal operating temperatures.
Chemical Reagents Information: Chemicals and reagents used in performing the test may exhibit potential hazards. Any user
must be familiarized with the possible dangers before use. We also recommend consulting the Material Data and Safety Sheet
(MSDS) on each chemical reagent for additional information. MSDS information can be easily located on the internet at
http://siri.uvm.edu or http://www.sigma-aldrich.com.
3. Getting Started
3.1. Packing List
• Heated Oil Test Centrifuge
• Short Cone or Finger Centrifuge Tube Holder (4)
• Short Cone or Finger Centrifuge Tube Cushions (4)
• Support Bracket (2)
• Oil Test Centrifuge Operation Manual
3.2. Unpacking
Carefully unpack and place the instrument and accessories in a secure location. Inspect the unit for damage. If any damage is
found, keep all packing materials and immediately report the damage to the carrier. We will assist you with your claim, if requested.
When submitting a claim for shipping damage, request that the carrier inspect the shipping container and equipment. Do not return
goods to Koehler without written authorization.
3.3. Setup
Equipment Placement: Place the instrument on a firm, level table in a secure area.
It is recommended to secure the centrifuge to a bench top prior to operation. Z-brackets are included with the instrument
for this purpose.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
4. Descriptions
4.1. Instrument Description
1. Control Panel. Provides for means to power on/off and adjustment of the speed and temperature of the centrifuge. Refer to
Section 4.2 for detailed description of the control panel.
2. Top Opening Lid. Sliding Aluminum Lid provides access to centrifuge bowl and rotor assembly for loading samples and
cleaning, if necessary.
WARNING: Never try to slow the carousel arm down with your hands or place your hands or any object inside the bowl while
the carousel arm is spinning. Allow the carousel arm to come to a complete stop before removing your sample.
3. Integrated Tube Holder and Pre-Heater. For holding and heating of four centrifuge tubes to test temperature prior to placing
in rotor assembly of centrifuge for testing.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
1. Motor Power. Controls power to the centrifuge motor. Press switch upward to power on. Press switch downward to power
off.
NOTE: Motor is cooled by direct forced air for enhanced temperature maintenance during the test.
2. Motor Speed Dial. Motor dial should be set to the minimum value (turn counter-clockwise) while motor power switch is off.
After motor switch is turned on, slowly turn the dial clockwise to desired speed setting.
NOTE: Indicator markings surrounding the dial are arbitrary and do not represent a specific set speed. Speed readings must
be made and confirmed using a portable tachometer that can read the rotor speed through the small opening in the Centrifuge
Lid.
3. Bowl Heater Power. Controls power to the main chamber or bowl of the centrifuge. Press switch to the right to power on.
Press switch to the left to power off.
4. Bowl Temperature Control. For adjusting the set point temperature of the main chamber or bowl of the centrifuge. Refer to
section 4.3 for detailed description of the Temperature Controller.
5. Pre-heater Power. Controls power to the two preheating chambers. These chambers are the two right most chambers of the
integrated four place tube holder assembly. Press switch to the right to power on. Press switch to the left to power off.
6. Pre-heater Temperature Control. For adjusting the set point temperature of the two integrated centrifuge tube preheating
chambers. Refer to section 4.3 for detailed description of the Temperature Controller.
7. Timer Dial (models with timer only). Turning timer dial to maximum value (clockwise) will set the centrifuge to spin for a
maximum of 60 minutes.
NOTE: Indicator markings surrounding the dial are arbitrary and do not represent a specific time. Time settings must be
determined and confirmed prior to testing. Maximum marking (30 minutes) and minimum marking (0 Minutes) are the only
absolute values.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
1. Temperature Display. The red LED display shows the actual temperature as read from the K Type Thermocouple.
Temperature set point ranges from ambient to 160°F (71.1°C).
2. Display Message. Shows condition of temperature controller. Refer to display messages below.
3. Set Key. Acts as a multi-functional action, advance or enter key. The Set Key is used in conjunction with the up and down
arrow keys to adjust parameter values, programming, restoring factory default settings, etc.
4. Down Arrow. Used to decrease the set point temperature and to decrease or change parameters when programming
temperature controller.
5. Up Arrow. Used to increase the set point temperature and to increase or change parameters when programming
temperature controller.
WARNING: The digital temperature controller for the unit comes pre-programmed from the Koehler factory. Please do
NOT attempt to re-program the digital temperature controller as this will void the product warranty. If assistance is
required, please do not hesitate to contact the Koehler technical service department.
Adjusting the Set Point Temperature. This routine allows the user to adjust the pre-programmed set point temperature of the
digital temperature controller.
a. Press Set
b. Use UP ARROW or DOWN ARROW to adjust value of the temperature parameter to the required value
c. Press Set again to store the value, this will be the new set point.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
5. Operation
5.1. Power Connection
Plug the provided line cord into the power receptacle located at the back of the instrument then connect to properly fused
and grounded receptacle with the correct voltage as indicated in section 1.3 or on the back of the unit.
WARNING: For safety, disconnect the power when performing any maintenance and/or cleaning.
2. Fill each of the centrifuge tubes to exactly the 50-mL (100-part) mark with the test sample.
3. Fill each tube with solvent to exactly the 100-mL (200-part) mark.
NOTE: Read the top of the meniscus at both the 50-mL and 100-mL (100-part and 200-part) marks
NOTE: If experience indicates that a demulsifier is required and one has not already been added to the solvent, add to
each tube quantity of demulsifier solvent stock solution that has previously been determined to be satisfactory for the
crude oil under test. Stopper each tube tightly and invert the tubes a minimum of 10 times to ensure that the oil and
solvent are uniformly mixed.
WARNING: In general, the vapor pressures of hydrocarbons at 60°C (140°F) are approximately double those at 40°C
(104°F). Consequently, tubes should always be inverted at a position below eye level.
NOTE: Where the crude oil is very viscous and mixing of the solvent with the oil is difficult, the solvent may be added
to the centrifuge tube prior to the oil to facilitate mixing. In this case, extreme care must be taken to fill the centrifuge
tube to exactly the 50-mL (100-part) mark with solvent and then to exactly the 100-mL (200-part) mark with the sample.
4. Place stoppers loosely on the centrifuge tubes to prevent pressure buildup during heating.
5. Place centrifuge tubes into the preheated centrifuge tube holders and heat contents of the tubes to 60°C ± 3°C (140°F
± 5°F).
6. Once the sample temperature reaches and is stabilized at the desired test temperature, secure the stoppers and invert
the tubes ten (10) times to ensure uniform mixing of the oil and solvent.
7. Open the lid and load filled tubes into the tube holders.
Make sure there are cushions at the bottom of the tube holders and there is no oil residue or build-up. Always check for
and remove any foreign objects within the bowl.
NOTE: Always balance the rotor by assuring that equal samples are used. Never load unequal samples.
8. Ensure all tubes are properly placed within their holders and close the lid.
9. Check that the Motor dial is set to the minimum value (turn counter-clockwise) before switching on the motor power.
10. If equipped with the timer option, set the timer to the desired setting.
11. Press the Motor Power switch upward to activate the centrifuge motor.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
12. After motor switch is turned on, slowly turn the motor speed dial clockwise to a speed setting that produces a RCF of
500. Please refer to the equation below from ASTM D96 and the rotor diameter referenced in section 1.3 of this
document to determine the appropriate RPM value.
where:
rpm = rotational speed, in revolutions per minute
rcf = relative centrifugal force
d = diameter of swing, in mm (eq 1) or in. (eq 2), measured between the tips of opposite tubes
when the tubes are in their rotationing position.
14. After 5 minute test time is complete turn off motor power.
15. Immediately after the centrifuge comes to rest, verify the temperature. Do not disturb the oil-water interface with the
thermometer. The test is invalid if the final temperature after centrifugation is below 52°C (125°F).
NOTE: If the final temperature is found to be below 52°C (125°F), adjust the centrifuge heater to increase the final test
temperature and reinitiate the procedure, beginning with Step 4.
16. Read and record the combined volume of sediment and water at the bottom of each tube.
17. Reheat the tubes to 60°C ± 3°C (140°F ± 5°F), return the tubes without agitation to the centrifuge, and spin for another
5 minutes at the same speed rate. Repeat this operation until two consecutive consistent readings are obtained on each
tube.
18. For the test to be considered valid, a clear interface must be observed between the oil layer and the separated water.
No identifiable layering (that is, an emulsion) should be present immediately above the oil-water interface. In such
cases, one or more of the following remedies may be effective:
1. Shake the mixture between whirlings in the centrifuge just enough to disperse the emulsion
2. Use a different or an increased amount of demulsifier. (The demulsifier should not, however, contribute to the
volume of sediment and water.)
3. Use a different or an increased amount of solvent. After a satisfactory procedure for a particular type of oil has been
worked out, it will ordinarily be suitable for all samples of the same crude oil.
6. Maintenance
WARNING: Disconnect power to the unit before servicing to avoid exposure to high voltages and/or temperatures which
may result in personal injury or death. If you have any questions about maintaining your equipment, then please do not hesitate
to contact the Koehler technical service department.
• Periodically, check the sample tube cushion inside the carousel shields. Replace if worn excessively.
• ALWAYS check moving parts, both mechanical and electrical, for wear and stress. Replace if necessary.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
7. Wiring Diagram
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
8. Troubleshooting
8.1. The test will not start
• Contact Koehler’s Customer Service Department.
• Check Fuses
• Check Fuses
9. Service
Under normal operating conditions and with routine maintenance, the K600X2 Heated Oil Test Centrifuge should not require
service. Any service problem can be quickly resolved by contacting Koehler’s technical service department either by letter, phone,
fax, or email. In order to assure the fastest possible service, please provide us with the following information.
10. Storage
This laboratory test instrument is equipped with electrical components. Storage facilities should be consistent with an indoor
laboratory environment. This testing equipment should not be subjected to extremes of temperature and/or moisture.
This equipment was shipped from the factory in a corrugated cardboard container. If long term storage is anticipated, re-
packing the instrument in a water-resistant container is recommended to ensure equipment safety and longevity.
11. Warranty
We, at Koehler, would like to thank you for your equipment purchase, which is protected by the following warranty. If within one
(1) year from the date of receipt, but no longer than fifteen (15) months from the date of shipment, Koehler equipment fails to
perform properly because of defects in materials or workmanship, Koehler Instrument Company, Inc. will repair or, at its sole
discretion, replace the equipment without charge F.O.B. its plant, provided the equipment has been properly installed, operated,
and maintained. Koehler Instrument Company must be advised in writing of the malfunction and authorize the return of the product
to the factory. The sole responsibility of Koehler Instrument Company and the purchaser’s exclusive remedy for any claim arising
out of the purchase of any product is the repair or replacement of the product. In no event shall the cost of the purchaser’s remedy
exceed the purchase price, nor shall Koehler Instrument Company be liable for any special, indirect, incidental, consequential, or
exemplary damages. KOEHLER INSTRUMENT COMPANY, INC. DISCLAIMS ALL OTHER WARRANTIES, EXPRESSED OR
IMPLIED, INCLUDING ANY IMPLIED WARRANTIES OF FITNESS FOR A PARTICULAR PURPOSE. Please save the shipping
carton in the event the equipment needs to be returned to the factory for warranty repair. If the carton is discarded, it will be the
purchaser’s responsibility to provide an appropriate shipping carton.
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
Notes
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Portable Heated Oil Test Centrifuge
Operation and Instruction Manual
Notes
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