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Datos Potenciometria 25-05-23

The document contains data from the standardization of sodium hydroxide (NaOH), phosphoric acid (H3PO4), and hydrochloric acid (HCl) solutions through titration. Graphs show pH measurements at increasing volumes of NaOH added. For NaOH, the steepest slope/maximum first derivative is seen at 7.2 mL indicating the equivalence point. For H3PO4, maximum first derivatives are seen at 3.8 mL and 8.7 mL. For HCl, the maximum first derivative is at 5.5 mL.

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Angela Villegas
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28 views6 pages

Datos Potenciometria 25-05-23

The document contains data from the standardization of sodium hydroxide (NaOH), phosphoric acid (H3PO4), and hydrochloric acid (HCl) solutions through titration. Graphs show pH measurements at increasing volumes of NaOH added. For NaOH, the steepest slope/maximum first derivative is seen at 7.2 mL indicating the equivalence point. For H3PO4, maximum first derivatives are seen at 3.8 mL and 8.7 mL. For HCl, the maximum first derivative is at 5.5 mL.

Uploaded by

Angela Villegas
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PDF, TXT or read online on Scribd
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Estandarización NaOH

10.70
9.70
8.70
Vlm pH DpH/dV 7.70

pH
0.0 3.87 6.70
0.5 4.08 0.42
5.70
1.0 4.23 0.3
1.5 4.36 0.26 4.70
2.0 4.42 0.12 3.70
2.5 4.57 0.3 0.0 2.0 4.0
3.0 4.67 0.2 Vlm NaOH (mL)
3.5 4.84 0.34
4.0 4.96 0.24 Primera derivada estandarización NaO
4.5 5.13 0.34 6
5.0 5.24 0.22
5
5.5 5.51 0.54
6.0 5.67 0.32 4
∆pH/∆V
6.5 6.03 0.72
3
7.0 7.02 1.98
7.2 8.01 4.95 2
7.5 8.60 1.96666667 1
7.8 8.80 0.66666667
8.0 8.84 0.2 0
0.0 2.0 4.0
8.5 9.03 0.38
9.0 9.10 0.14 Vlm NaOH (mL)
9.5 9.23 0.26 Vlm pH
10.0 9.32 0.18 0.0 2.69
10.5 9.45 0.26 0.5 2.73
1.0 2.89
1.5 3.02
2.0 3.32
2.2 3.42
2.4 3.48
2.6 3.62
2.8 3.89
3.0 4.01
3.2 4.23
3.4 4.52
3.6 4.78
3.8 5.23
4.1 5.36
4.4 5.46
4.7 5.48
5.0 5.53
5.5 5.56
6.0 5.63
6.5 5.66
7.0 5.68
7.5 5.73
8.0 5.86
8.5 5.96
8.7 6.24
9.0 6.64
9.2 6.78
9.4 6.84
9.6 6.91
9.8 7.02
10.0 7.14
10.5 7.18
11.0 7.21
11.5 7.24
12.0 7.26
Estandarización NaOH Vlm pH dp/dv
0.0 2.08
0.5 2.13 0.10
1.0 2.20 0.14 10.70
1.5 2.29 0.18 9.70
2.0 2.41 0.24 8.70
2.2 2.45 0.20 7.70
2.4 2.47 0.10 6.70

pH
2.9 2.55 0.16 5.70
3.4 2.63 0.16 4.70
4.0 2.80 0.28 3.70
6.0 8.0 10.0 12.0 4.5 3.00 0.40 2.70
Vlm NaOH (mL) 1.70
5.0 3.80 1.60
0.0
5.5 4.68 1.76
derivada estandarización NaOH 5.7 5.78 5.50
5.9 6.78 5.00
6.1 7.34 2.80
6.00
7.2 mL 6.3 7.89 2.75
6.5 8.26 1.85 5.00
7.0 9.01 1.50
4.00
7.5 9.34 0.66

∆pH/∆V
8.0 9.43 0.18 3.00
8.5 9.54 0.22 2.00
9.0 9.62 0.16
9.5 9.81 0.38 1.00
6.0 8.0 10.0 12.0
10.0 9.91 0.20 0.00
Vlm NaOH (mL)
0.0
D

0.08 Estandarización H3PO4


0.32
8.00
0.26
0.60
7.00
0.50
0.30
6.00
0.70
1.35
pH

5.00
0.60
1.10
4.00
1.45
1.30
3.00
2.25
0.43
2.00
0.33 0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0
0.07 Vlm NaOH (mL)
0.17
0.06
0.14 Primera derivada de la estandarización de H3PO4
0.06 2.50
0.04 3.8 mL
0.10 2.00
0.26 8.7 mL
1.50
∆pH/∆V
0.20
1.40 1.00
1.33
0.70 0.50
0.30
0.35 0.00
0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0
0.55
0.60 Vlm NaOH (mL)
0.08
0.06
0.06
0.04
Estandarización HCl

0.0 2.0 4.0 6.0 8.0 10.0 12.0


Vlm NaOH (mL)

Primera derivada de la estandarización de HCl


6.00
5.50 mL
5.00

4.00

3.00

2.00

1.00

0.00
0.0 2.0 4.0 6.0 8.0 10.0 12.0
Vlm NaOH (mL)

14.0
14.0

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