Fed STD 228
Fed STD 228
com
FED.TESTMETHODSTD,No. 228
April
14,1%7
SUPERSEDING
Fed.
Spec.
J-C-98
Sepiember
11,1951
FJC61A3
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‘)
INFORMATION SREET
on
FED.TCSTMETMOOSTD.W. 221
April 14, 1967
SECTIONi
SCOPE,CONTENTS,ANOWMBERIN6SYSTEM
1. SCOPE
1,1 This standard gives the general 1000 Geometrical !dessurements.
physical, electrical, and chemical methods 2000 — Mechanical Tests.
for testing insulated wire and cable for 3000 — Tension Tests.
electrical purposes for conformance with 4000 — Accelerated Aging Tests.
the requirements of Federal and Military 5000 -. Thermal Tests.
apscitications, and other related docu- 6000 - Electrical Tests.
ments. It was prepared in order to elimi- 7000 - Chemical Tests,
nate Unnecessmy or undesirable variation 0000 Miscellaneous Tests.
in testing procedures. This standard does
not include special test methods applicable 4. Subject Index.
to certain wires and cables which are de- 5. Definition of Terms.
cribed in the appropriate detail spacifica- 6. Temperature and Humidity of Condi-
tiona, nor does it include all the test tioning Room.
methods for wires and cables used in the 7. Notes.
industry. In case of conflict between the 8. Test Methods.
provisions of those methods and those of
the individual test procedures or specifi- 3. NUMBERING SYSTEM
cations for particular material, the latter
shall take precedence. 3.1 New methods. A method number will
be assigned so that the new method is lo-
2. CONTENTS cated close to methods of similar or relat-
ed tests.
2,1 The contents of this standard are as
follows: 3.2 Revision of existing methods. When
a teChLiCal change or modification is
Section issued, it will be identified by adding a
decimal poznt to the basic method number or
1, Scope, Contents. and Numberin~ System. by increasing the decimal by one digit;
2. Alphabetical Index of Test Method e.g., 3111, if modified or changed, would
SubJecrs. Be 3111.1; and 2v11.1, If modiXied or
3. Numerical Index of Test Methods. changed, would he 2011.2.
FED.TI?STMCTHOOSTD.
NO.228
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SECTION1
WD.TEST.MET100 STO.W.~
I
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Method Method
Tit 10 NO. Tit1, No.
SECTION 8
NUMERICAL INDEX OF TEST METHODS
1
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Resistance tDHeal Oxyge% Air, LighG Resistance to Ozone, Insulation and Sheath- 4111
and Ozone ; Genera l------ ------ 4001 Resistance to Ligh\ Insulation and Sheath - 4131
Oxygen Pressure Tes4 Lnsulatlon and I Resistance tn Petrolatum, Varnished
Sheath ----------------- ‘-~ 4011 ~ cloth -------------------- 4211
Air Pressure Tes~ Insulation and Sheath -~ 4021 Resistance to Oil, insulation and Sheath -- 4221
Air Oven TesL Insulabon and Sheath - - - 4031 Resistance @ 011,Insulation and Sheath
Test Tube Heat-Aging, Insulation and (Ttecovery Method) ------------- 4223
Sheath ---------------- --- 4041
-———-
Heat Sh6ck1nsulaUon ------ ----- 5011 Drip, Cable ------------- ---- 5141
Heat Distortion Insulation -- - - -- -- - 5021 Flammability, Horizontal -- -------- 5211
MeL Fibrou6 Covering ---------- 5111 Flammability, Vertical -- - -------- 5z21
Drip, Fibrous Covering - - - - - --- -- 5131 ~aLOMabtiiQ,~kMeW----- . . . 5231
.— 1. -——— —.. —----- - --
SECTION4
W2JECT INDEX
4
Angle: Cable and wire--—------—-. Method 1441
BraiL-----...——-------— Method 1611 Contictora----—--— --------- Method 1441
Metal armor, braide&----- Method 1631 Coatings:
Wrap----..-.---— ------- Method 1621 Armor, zinc coated steel-_— Method 7111
Armor: Conductor coatings:
1
Brtided metal: tiraulfste--——-----—-—_- Method 7123
Angle--------- --——- Uethod 1631 klyaulfide----------—--- Method 7121
Covarav---—----—----—- Method 6121 Completed wire and cable:
Elongatio~--—-----”—-- Uethod 2111 Definition of________ Section 5
Thickness_--__--— ----- Methods 1221 Composition:
Metal tape: Insulation and aheath------ Method 7251
Coating, uniformity--— Method 7111 Lead sheat~-------------—-- Method 7231
Elongatio~-.------_-_-—- Method 2111 Concentric lay: Definition
Flexibility, low of-------------------------- Section 5
tem~rature------------— Method 2021 Conductor:
Lay, direction of-----_— Method 8111 Circuderenca---—-— -------- Method 1441
Omning----—------------ Method 2181 Coating, uniformity:
Thickness------------.—— Method 1211 Nraulfate---—----------- Method 7123
Tightness-..------------—--Method 2171 ~l~ulfide---.------------- Method 7121
Width ---------------------Method 1411 Definition of------------ SectIon 5
Nonmetallic: Acid and Elongation:
..ae+e+.!,,,,e
~~~=~~ .---- ..... --------- ~et~@~ ?Q~~ Earc!-flraW- .__--___-__-_——___ jfPthnr!?21?
steel: Soft, annealed--—------ Method 3211
Coating, zinc, uniformity- Method 7111 Insulated, definition of-—-- Section S
Xlongatio~--—---------- Method 2111 Lay, direction of-------- Method 8111
Flexibility, low Reaiatance, electrical------ Method 6021
temperature--...---——— Method 2021 Size-_—-__—__—_—- Method 1431
~ning.----.-—.------— method 2181 Stranded, definitio~--——- Section 5
Resistance, electrical---- Method 6011 Tensile strength:
Tightneaa---—------— — Method 2171 H=d-draw~-.------—-.--—- Method 3212
uira: Dimmeter----_—_- Method 1421 Soft, annealeL__--_—---- Method 3211
Armor wire: Weight--------------------- Method 8311
Lay : Cord, electric: Flexibility- Method 2031
Direction of-—-— -------- Method 8111 Coveragw:
of twist--—.— ---------— Method 1511 Armor, braided •etal--~---_- Method”8121
Springiness-------------- — Method 2161 Wrap or nerving--------------Method 8131
Touglmesa---—--- ---e-- Method 2131 Covering, fibroun:
Bedding: Acid and alkali resistance--- Method 7011
Lay, direction of----_—_— Method 8111 Flammability:
Thitineaa-----.-— ------ Methods 1171 Horizontal_———-—_—— Method 5211
and 1173 Spuk -----—--— -—------- Method 5231
Braid: Vertical--------------- Method 5221
Angle----— ------------- Method 1611 Mineralcontent-----------W Method 7211
Csrriars------------------ method 8021 Moisture abeorptio&—---- - Method 8221
Ende—-.-__— ________ N6thod 8021 Yarns ‘per inch--_-_-—-- Method 8031
Picks per inck-_-------_- Method 8011 Weight---------------------- Method S311
Ply of ysrL.___-—_---—_ Method S3021 Defects:
Thickness------— -.-— Nethod 1111 Insulation, apsrk teat___— Method 6211
Buffing: Insulation and Definitions of terme------_- Section 5
sheath ----------------- Method 3011 Diameter: Armor, wi~e_---- Method 1421
Bunched lay: Definition of-- Section 5 Dielectric strength: Cloth
Calibration: Tension test- and ta~----__------_--.-- Method 6221
ing machine--—------- ---- Method 3016 Direction of lay:
Capacitance: Insulation, Definition of_— _________ Section 5
change-------------------- Method 6271 Determination of--------- Method 8111
FED.TE$TM=HDD S7D.m.Z2E
1
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4
$ieatshock—-—--——-——— Method 5011 and 4223
Light reBistance---—--- Method 4131 opening: Armor---------- Method 2181
Moisture absorption, Werlap: Cotton tape------- Method 1711
mechanical-----------——- Method 8211 Oxygen pressure test:
Oil resistance--------— Methods 4221 Insulation and Sheath—----- Method 4011
and 4223 OZone resistance: Insulation
Oxygen pressure test___— Method 4011 and sheat~----------------- Method 4111
Ozona resistance--------- Method 4111 Pair:
Petrolatum resistance----- Method 4211 Shielded, definition of----- I Section 5“
Resistance: . Twisted, definition of------- SeCtiOn 5
Defia.tion of----_------— Section 5 Petrolatum: Resistance,
Determination of--------q Method 6031 insulation and sheat~ ---—-y 1 Method 4211
PCD.TEST MH~D STD. W.22S
.
{
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SUBJECT INllEX-Continued
3
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FED. TES7MET~0STB. ==
4
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SECTION 5
DEFINITION OF TERMS
1. DEFiNITION
L 1 The following definitions cover general
2. Q End. An end is an individual warp yarn
terms.
2.10 Finished conductor. A finished con-
2. GENERAL TERMS ductor 1s the meTal COndUCtOr with insulation and
any covering present before assembling into a
2.1 Bunched lay. In a bunched lay conductor, complete cable.
the strands are twisted together in the same
dtrectton wtthout regard to geometrical arrange- 2.11 Insulated conductor (insulated wire). An
ment insulated conductor (Insulated wtre) is a conductor
(wf.re) surrounded by a layer or layers of non-
2.2 Carrier. A carrierIstheyarnor com- conducting matertal (insulation) which tsolates
bination of several yarns latrf parallel
inthe the conductor (wire) from other conducting
bratdby a single bobbin of the braiding
machine. materials or from ground,
2.7 Direction of Iry. The direction of lay ie a. When the number of values is odd, the
the lateral direction, either right-hand or left- medtan is the middle value in the eeries.
hand, fn which a atrand or insulated conductor
passes over the top as it recedes from an b, When the number of valuea is eve% the
observer looking a(ong the axis of the conductor median ts the arithmet.tc average of the two
or cable. middle valuee,
2.8 Elongation. Elongation is the perm-ent 2.17 Picks per inch. Picksper inchisthe
extension in the gage length of a test epeci~e~ number ofcarriersin either direcUon contained
measured after rupture, and expressed a9 a in 1 inch of the braid measured parallel to the
percentageof the original we length. Ultimate axis of the finished wire or cable,
elongation is the extension measured at the
moment of rupture and expressed as a percentage 2.18 Pitch diameter. The pitch diameter
oftheoriginal gagelength.For example,ifa of any layer of conductors of a cable M the dia-
1-inchgage is marked on an unstretched specimen meter of the circle passing through their centers.
and the specimen la stretched until the gage
marks are 7 inches apar$ elongation is 7 2.19 Ply. A ply is an individual stngle yarn
- 1 inch = 6 inches or 600 percenL in a ply yarn.
2.20 Ply yarn. A ply yarn is the product 2.2’7 Tension se~ Tension set is the elonga-
formed by twietmg together *O or more tion remaining after a specimen has been stretched
single yarns. and held at a spectiled elongation for a given
period of time, thenhas been relieved of the
2.21 Ro}e. lay. In a rope-lay conductor the force, and is allowed to rest for a definite
stranded meumers are *isLed together with a period of time. It is emreseed, as a percentage of
concentric lay, and the stranded members the distace between the bench marks on the
emselves may have either a bunch~ concen- unstretched spechnerb For e-lple, a specimen
b7 c, or rope lay. ‘is stretch~ from 1 to 5 inches for a period
of 10 minutes and then released. Itslengthafter
2.22 Shielded pair. A shielded pair M a the 10 minutes rest is 1.2 inches; therefore, the
iwis ted pti over which a close braid of copper set under these conditions is O. 2 inch or 20
wire has been applied. percenL
2.23 Stranded~onductor. A stranded con- 2.28 Twisted pair. A twtsted pair is com-
ductor is a conductor composed of more titan pcmd of two irrsdated conduckwa lwisted
one wire, together.
2.24 Tearing stravgth. Tearing strength is 2.29 Unidirectional lay. Unidirectional lay is
the ratio of the maximum force applied during that variation of concentric lay in which all the
tear of a specimen to the thicicness of the helical layers of strands comprising the concen-
unstretched specimen. tmc conductor have the same direction of lay.
The construction includes normal unidirecuonai
2.25 TensiJe strength. Tensile strength is lay, i]] which each successive layer has a greater
the maximum force per unit of the original lay length than the preceding layer, and unidirec-
cross-6 ectiomal area of the specimen which tional equal lay (unilay), generally limited to 19
~pqlj!t~ !n~h~ rq3tirpof t!he spectmen. rt is strands; in which all helical layers have the
calculated by riividimg the m~mum force in same length of lay.
pounds by the original cross-sectional area in
square inches. 2.30 Unilay. See “’unidirectional ecfud lay”
under Wn.i&zectionsl lay. “
2.26 Tensile stress. Tensile stress is the
force per unit of original cross-sectional area 2.31 Wire. A wire ta a slemier rod of ,
of the unstretched specimen rquired to stretch filament o! drawn metal.
the specimen to a stated elongation It is
expressed in pounds of tmaion force per squm-e 2.32 size.
Yam Yarn size (yarn number)
inch at the stated eiongatiom For example, is a conventionalrelative mexure of fineness
1, 000 pounds per square inch at S00 percent or dimension. it is expressed as the number of
eiongatiom It is often designated in rubber standard lengths per standard weight of the
techrmIogy by the term “’modulus” material.
SECTION G
TEMPERATURE AND HUMIDITY OF CONDITIONING ROOM
SECTION.
7
NOTES
(Activities outside the Federal ~vernment may obtain copies O! Federal Specifications.
Standards, and Handbooks as outlined under General Information in the index of Federal
Sy?cifications and Sttin rds and at the Prices indicated in the Index. The Index, which
includes cumulative monthly supplements as issued, is for sale on a subscription basis by
the Superintendent of Documents, U. S. Government Printing office, Washington, D.C. 20402.
(F ,le copies of this specification and other product specifications required by activ-
itie. outside the Federal (kwern!uent for bidding purposes are available without Charue at
tts General Services Administration Regional Offices in Soston, New York, Washington,
D, c,, Atlanta, chiCagO, Kansas City, MO., Dallas, Denver, San ?ranci.eco, Los Angeles, and
Seattle, Wash.
J2USTODIANS:
Army - EL Army - None
Navy - SH Navy - YD, MC
Air Force - 17 Air Force - None
1
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Method 1011
April 14, 1%7
Method 1011
# Method 1013
April 14, 1967
Method 1014
~PKll14, 1967
Method 1018
April 14, 1%7
Method 1018
‘&
%
Method 1051
APril 14, 1967
l$fethod 1111
Amil 14. 1%7
BRAID
L SCOPE over the laps of tape or over the tops of any
1.1 This method is intanded for win deter. braid marks in the insulatio~
mining the thickness of braids over the immla- 4.3 Three measurements eqmlly spaced
t:on of insulated wire and cable. along the length of the specimen shall be made.
2 SPECIMEN The diameter over the braid and over the core
!&I The specimen shall be a pica of the in. shall be determined aa nearly as practicable at
spection unit at least 2 feet in length from which the samepoink
any covering over the bmid has been removwi 4.4 If two braids are pmeen~ the thiclmeas
& APPARATUS AND REAGENTS of the outer braid ehall be determined from the
3.1 The appamtue and magenta shall be es the diameter over the inner braid.
follow?l : 43 in detenrdning the thicknas of the
over-all braid of s twin-conductor cable, the
w Acic?wmet+w odiper graduatedto read
in mileor U.UUI inch and having flat aurfacee diameter over the core, D, in 4.2, shall be equal
on both anvil and end of spindle, each approxi. to 1.64 times the diameter of the individual
matxly 026 inch in diameter. The surf- Of
conductor.
~nvil and spindle shall he parallel to within 5. RESULTS
0, ?001 inch. 5.1 Calculation. The thickness of the braid
at any point shall be calculated as f ollows:
u Wipiflyda%.
%13 (?h&TO&Wb
or other Juit&b 80k71t. TMckrteee, lnch~
LA-D,
4. PROCEDURE
where:
4.1 The specimen shall be fme from mec- D,-the diameter over the brnhi at thepointmeee-
hanical damage. Any saturnnts or extraneous ured. Inches
materials shall he removed fmm the braid by G=the diameter oTer the core at the point meaeured,
means of the cloth and aolvenk The microm. lnchee
etar caliper shall he applied directly over the 52 Unless otherwise specified in the detail
braid so that the specimen can just he moved specification, three specimens from each inspec-
between the anvil and spindle without distor- tion unit shall he tested.
tion cf the braid. Tbe diameter over the braid 53 The average thickneea of the bmid of
aldl be read from the micrometer caliper ecale the inspection unit ehall be the average of the
and the value recorded aa D,. results obtained from tbe specimens tested.
4.2 The bmid shall then be rwmoved froru %4 The minimum thMmess of the braid of
the speoimen and any eatumnts or other ax. the inspection unit shall be the smallest of all
traneous materials removed from the mwfaca of values averaged in detmmining the average
the CON (assembly under the braid) by means tbickneee, 6.3.
of the cloth and solvent. The diameter over 5.5 The average thickness and minimum
the core shall then be determined as described thickness of tbe braid of the inspection unit
for diameter over the braid and the value m- shall be recorded to the nearest mil or 0.001
recordedM D,, This me e.aurement shallhemade inch.
lkbthod 1121
ADtil 14, 1%7
8pecimen can just be moved between the snvil tion unit shall be =ed.
and the spindle without distortion of the tap S3 The wemge thicknees of the tape of the
TIM diameter over the tripe shrill be rnd from inspection anit almll be the avrruge of tho reP
the micrometer caliper scule and the due re- suits ob~ined from the epecinws tested.
corded ●s D,. If psible, the measurement &4 The ntirhum thickness of the tipe of
shrill be:made st places wham the tqe is rtot the inspection unit shall be tho emnllest of ●ll
lapped. WIluea ● veqed in determining the ●verage
42 The tape shall then be mnoved fmm the t.hic~ 5.8.
specimen and any aeturents or other erttmeoue 6.S The ●verage tbickneee ●nd minimum
matarids removed from the Burfam of the eom thickneee of the tape of the inspection unit shall
(~bly under the tqw) by means of the be recorded to the nearest mil or 0.001 inch.
Method 1124
April 14.1967
M@hod 1141
Amil 14. 1%7
THICKNESS, WRAP
1. SCOPM core shall be measured in the came manner as
1.1 This method is intended for use in deter- described for diameter over the wrap and the
mining the thickness of wraps of insulated wim value recorded as D~.
and cable. 43 Three m-urements equnlly spaced
Z SPECIMEN along the length of the specimen shall be madw
2.1 The specimen shall be a piece of the in- The diameter over the wrap and over the com
spection unit a~ least 2 feet in length from shall be measured as nearly as practicable at the
which any covering over the wrap has been same poin~
removed. 4.4 If two wraps are present, the thickneae
3 APPARATUS AND REAGENTS of the outer wrap shall be detemnined from the
3,1 The apparatus and reagente shall be as diameter over the inner wrap.
follows : 6. RESULTS
“3J.I M“wrornde cd+wr graduated to read 5.1 Calculation. The thiclmess of the
in mile or 0.001 inch and having flat surfaces on wrap at any point shall be calculated as follows: .
both anvil and end of spindle, each approxi- .
‘Xldckaeaa,hlCb=~I-~, -
mately 0.25 inch in diameter, The eurfaws of 2
anvil and spindle shaIl be parallel to within Where:
0.0001 inch, Z),=t.be dhmeteroverthewrap at thepointrDeaa-
3.12 Wiping cloth. ured, inches
3J9 Chloroform or other suitable uolvent. D,=the ,liamet@r o~er Lhe core at ths point m-
are.% inchee
4. PROCEDURE
4.1 ‘T’he specimen shail be free irom me- 52 I?iihxs ct!iervisc spc%cc! k t!:e dctsi!
chanical damage. The micrometer culiper shall specification, three specimens from each inspec-
be applied directly over the wrap so that the tion unit shall be tested.
specimen can just be moved between the anvil 53 The average thickness of the wrap uf
and the spindle without distortion of the wrap. the inspection unit shall be the average of the
The diameter over the wrap ehaIl be read from remdte obtained from the specimens tedd
the miorometar scale and the value recordod 6.4 The minimum thickness of the wmp of
m D,. the inspection unit ehall be the anmlleat of s11
4.2 The vrmp shall then be removed from values ave~ in determining the average
the specimen and any fibers, eaturant+ or othar thicknq 6.9.
extraneous materials removed from the surface ‘“53 The avenge thiclrnesa and minimum
of the core (msembly under the wrap) by meana thickncns of the wrap of the inspection unit shall
of the cloth and eolvent. The diameter over the be =orded to the neared mil or 0.001 inch
Method 1151
April 14, 1967
Method 1153
April 14, 1967
lkfethod 1171
April 14, 1%7
I
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Method 1173
April14, 1%7
Method 1211
A@l 14, 1%7
Method 1221
April 14, 1%7
Method 12z3
~pril 14, 1967
I
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Method 1311
~Dril 14, 1%7
Method 1313
Ad 14, 1%7
(
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,.,
Method 1331
April 14, 1%7
THICKNESS, SHEATH
L SCOPE same manner as described for diameter over
1.1 This method in intended for use in deter- the sheath nnd the value recorded as D,.
mining tie thiclmeas of rubber and plastic 4S Threa sets of measurements equslly
sheaths of insulated wire and cable. spaced along the length of the specimen shrill
Z SPECIMEN be mad~ Each eat of measurements al-ml) con-
21 The specimen shall be a piece of the in- aiat of the maximum and minimum diameter at
spection unit at least 2 feet in length from which the placa measured. The diameter over the
●ny covrring owr the sheath has been removed, sheath and over the core shall be determined
3. APPARATUS AND REAGENTS as nearly es practicable at the same point.
“3.1 Tha ●pparatus and reagenta shall be as 5. RESULTS
follows : 5.1 Calculation. The thickness of the
8.LI dfiorometerdim graduated to read sheath ●t any point shall be wdcdatod aa
in roils or 0.001 inch and having flat surfaces follows :
D,-Ds
on both the snvil ~nd end of spindle, ench q- ~iC&NM, Inch=T
proximntely 0,25 inch in diameter, The sur-
faces of anvil and spindle aball be parallel to Where:
D,-the dlnmeter orer th obeatb at the point meaa-
within 0.0001 inch. nred, Inchee
3X2 Wiping ckth. D,dbe die meter over tbe core ●t tbe point meaaur~
3.13 C’hioro#orm or other dtabZa Johwmt. taebes
4. PROCEDURE 5.2 Unless otherwise specified in the detail
4.1 The specimen shall be free from me- eJwcificaLion, two specimens from ench inspec-
chanical aumqm Any cii~ grea* or other tion urut shall be tested.
extraneous mnterids ahnll b rwno~bd from the S.S The average thickness of the sheath of
apecimtm by means of the cloth nnd eolven~ the inspection unit ehnll be the nvernge of the
TIIe micrometer caliper ah]] be applied directly results obtained from the specimene teated.
o~er the sheath so that the specimen can just be 5.4 The minimum thickness of the sheath of
moved betvreen the ●nvil and spindle without the inspection unit shidl be the amnlleet of all
distortion of the aheath. The diameter over the valuen averaged in determining the average
sheath shall be read from the micmmeter scale thickneda, 5.3.
and the value recorded as D,. 5.5 The ave~ge thiclmess and minimum
4.2 The sheath shall then be removed from thickness of the sheath of the inspection unit
the specimen and the diameter over the core SIIIW be recorded to the nearest mil or 0.001
(aaeembly under tha shenth) measured in the inch.
wthd a411
Aprif 14, 1%7
Method 1421
Arwil 14. 1%7
Method 1431
A@] 14, 1%7
SXZ& CONDUCXOR
1. SCOPE shall be proportional to the number of wires in
1.1 This method ia intended for use in deter- the Aayer.
mining the siqe of solid and stmnded concluctom 43 If tin or other metal coatinge m-a prea-
of insulnted wim and ca~]e. For the purpoee of anL the diameter measurements slmll be mude
this metha-1, the term %vhfi shall kmddned aS over the coatil~g.
a slender A or filament of drawn metal 5. RESULTS
2. SPECIMEN 5.1 Calculation.
2.1 The specimen shall tm the bare conduc- 5.Ll Solid conductor. The rnae of tho con-
tom removed from s piece of the inspection unit ductor at any point, in cimular mih shall be
at lenst 6 inches in length calculated by squaring the diameter expressed
& APPARATUS in mik
!Ll The spparatua droll &n&t ofs microm- 5.1,2 Strandd contiwtom. The size of the
eter caliper grnduated to mad in 0.1 mil or O.O@~l stranded wmiuotor in circular mjls shall be
inch and having flat surfaces on both anvil and calculated as follows:
end of spindle, ;ach approximate y 0.25 inch in - Size of wire, circular mIl=D?+Di’+---------- +~n’
din mete;. The surfs-&e of BJ’IVif and spindki where:
shn 11be parallel to within 0.0001 inch. D,=dlnme@r (nverage of two mensuremrnts W
4. PROCEDURE npnrt) of Hrst wire In the conductor, In rolls
D,=dJometer (arertigc of two measurements W
4.1 Solid conductoxa The specimen shall
apnrt ) of amwnd wire III the conductor. In mite
be free from mechanical damagw The microm- Dn={]lamotcr (n~~rnge of two mtnnurements 90”
eter caliper shall be applied directly over LIM npn rt ) of ~~th wire 10 the conductor, In wUa
conductor so that tha artvil end qi.ndl~ nre ]Iwt n-the nlmmer 0? -!rm m the Wmdn?to?
brought into contact wjth the specimen in mch She of stranded conductor, circubr mUs=&+&+_-
a manner that the conductor ix not diatorlod. +88
where:
The criterion of contact is the initial devclol~ S,=clra)ar.mll atxa of tit wire in mndoeter
meut of frictional ~ietanee to mt.mament of the (6.1.1 )
specimen bet ween the micrometer surfnm &=clrcnlar.mll ●las Or eeeond wire (5.1.1)
‘I%e diameter of the conductor shall be mad th=clrrulnr-rnll size of nth wire (5.1S)
from the micrometa caliper scale and the values a-the number of tw’ree in the conductor
recorded. Two meaeuremente of the diameter 5.2 Unless otherwise specified in the detail
●t positions approximately 90° apart on the qmcificotion, two specimens from each iuspec-
specimen shal~ be made. tJon unit shall be teste~
42 Stranded eondnctoru Individual 5.S The size of the conductor of the inspec.
vriree of a stranded conductor cable shall be tion unit shall be the average of the reeulte ob-
measured aepamtely as described for solid con- tained from the specimens tested.
ductom in 4.I. Unleaa otherwim apecided in the 5.4 The diameter of tho conductor of the in.-
detail specification, 10 percent of the wires ad apection unit shall be recorded to the nearest 0.1
in no caaa leas than mven wima shall be talwn mil or 0,0001 inch.
from the conductor for ML Whe shall be !U5 The cross-sectional area of the conductor
selected at random from each layer of the con- of the inspection unit shall be recorded to the
ductor md the number mlectd fmm each la~er nearest circular roil.
Method 1441
April 14, 1%7
CIRCUMFERENCE
1. SCOPE pamtus and one end of the thrend or wire
1.1 This method is intended for use in dt+r- attached to it by means of a chuck. The other
mining the circumference of insulated wire or end of the thread shall be placed over the pIIllcy
cable. It is applicable to the determination of and attached to the 10-=qam weight, which
the circumference of finished cable, insulated moves along a cnlibrnted scale. ‘17)esmle shtill
wires, bnre wires, conductors, circumference be calibrated so as to indicate the length of the
over sheaths, etc., with a circumference of 3 thread wound nround the specimen. At bat
inches or less, when the circumference is ro- 10 complete turns of the thread or wire shrill be
quircd or when it is desirable to calculate the wrapped nro~md the specimen under a kmd of
dinmcter from the circumference. 10 grams, and the number of turns recorded
2 SPECIMEN as N.
2J The specimen shall h a pitwe of the in- 42 The wrnps of thread shall be jnst in con-
tmlnted wire, cable, conductor, etc., nt least 12 tact with ench other, without any overlapping.
inches in length taken from the inspvct ion unit. The lel~gtl) of the N turns of thrend shall be
3. APPARATUS AND REAGENTS rend from tl]e scnle and tl]e vnlue mcordetl IIS 1..
3.1 The apparatus and reagents shall be as 4.3 The dinmeter of the smnll threod shul]
follows : be mensltred with the microscope and the value
3.1.1 Fine wire or thread with n length Rp- recorded m l?.
proxim~tely 10 times the nominal circumfem.nca 4.4 Unless otherwise specified in the detnil
of the specimen. specifirwti(lll. tlro mensurcments eqlmlly sp:tcecl
3.L2 Convenient equipment for wrapping along the length of the specimen shall be mad~
. . . G.&L,,*WU
*1%”.... A*C)
&,,L bl. .. . . ,,n.a.
u,luti -A & ~a
-;. VGIA
.?... +---: *.. “-. . .....4
LLaAatutLULUUAAU 5. P.EsTl~
Wu.~=u
the specimen. 5.1 Calculation
3.13 Convenient. equipment for mensuring 5.1.1 Cimumlenwwe. The circumference df
the length of wire or thread which is wrnpped the win, cnble, or com.1uctor, etc., at any place
around the specimen to an accurncy of 0.1 inch. shall be calculated as follovrs:
3.1.4 Satisfactory equipment for controlling L
c~rcumteren~ Inehen- ~ -.D
the tension of the wire or thread durin~ wrap-
where:
ping and for measuring the length of thread L=tbe Iengtb of the thread for X turns at the Plain
or wire in a given number of turns, Satisfac- me4t6urPd
tory equipment is shown in figure 1441. N-the number of turn. of the thread
9.15 The nppnmtus described in method D=tbe Jinmeter of tb? threnfl, loch
1018 for determining the diameter of the tlweacl. 5.1.2 Diame/er.—The dinmcter of the wir~
3.L6 wiping dvth. cable, or conductor, etc., at any plnce shall La
3.1.7 PA/ornfnrm, or other .witnb7P so?)$~nt. calculated by dividing the circumference by
4. PROCEDURE 3.1416.
4.1 The specimen shall be free from me- 52 Unless otherwise specified in the dctnil
chnnica 1dnmnge. Any tiher, antumnts, m other specification, three specimens from ench inqxsc-
extraneous matminis shrill be removed from the tion unit shall be tested.
specimen by means of th~ cloth nnd solvent. &3 The a rerage circumference of the mi~
The specimen ahnll be placed in the testing ap- cable, colldult(lr, etc., of the inspection unit
Method lU1
shall be the sverage of the results obtsined from ence of the wi~ ublq wnductar, ●’-, of the
the specimens W wb unit &all h recoded ta the naarmt
5.4 The minimum circumference of the Wim .
cabl~ mnductor, etc., of the inspection unit 5d The average diametar and minimum
shall be tbe amalle8t of mll Yaluea averaged in diameter of the wi~ mble, conductor, d.c., of
determining the average circumference, 6.9. the inspection unit elmll be recorded to the near-
5.5 The avernge and minimum circumfer- eat 0.001 inch.
.
: F!
o
*.
:
$I
I
●
Method 1511
‘ April 14, 1%7
&
Method 1521
Amil 14. 1%7
Method 1531
April 14, 1967
Method 1611
&yil 14, 1%7
ANGLE, BRAID
1. SCOPE sembly under the braid) determined m described
1.1 This method is intended for use in (deter- in method 1111 and the value recorded as D.
mining the anglII between the yarns of Lhe bmid 4.5 If two braids are present, the angle of
an(i the 8xis of (I)e insulnted wire or cnUe, the outer one shall be determined from the
2. SPECIMEN diameter over the inner braid.
21 The specimen shrill be R piece of the in- 5. (; AI, CllIJATION
spection unit at leaet 6 inches in length from 5J ‘l’he tangent of the angle of the braid nt
which any covering over the braid has been any place shall be calculated as follows:
removed.
2*P(D+T)
3. APPARATUS AND REAGENTS Tangent of mgle. -
C
S.1 The ●ppmtue ●nd magenta shall be as where:
described in the methods referenced in 4. P =the num~r of pi~ ~r \ncb of the br~~d
4. PROCEDURE D -the dhmeter o~er the core, Inch
4.1 The specimen shail be free from me- T =the thl=~~ ~ h~ld, Inch
chanical dnmnge, Any fiber, saturrmt, or other C -the nnm~r of ~rrie~ 10 the bra~~
~,dJ~8
extrweous mt~terinls shail be removal from the
surface of the specimen by means of the cloth 5.2 The angle of the braid shali be deter-
and solvent. The number of picks per inch mined from tile tangent, of the angle by refer-
shall be determined as deecribed in method8011 ence to a tabie of natured trigonometric func-
and the value recorded ns P, tions.
4.2 The number of carriers shall be deter- 53 Unlvss otherwise s~wcified in the detail
mined Rs described in method 8021 mti illc vuiue Sp?ci!lcatiori, trc ?Pecirmzs. me fmn cdl Lx?
recorded as c, of the inspection unit, shall be tedad.
4S The thickn~ of the braid akmil be de- - 5.4 The nngle of the braid of the inspection
termind as dwcnt@ in method 1111 and. unit shali be the average of the results obtained
recorded m T. from the specimens ti
4.4 The braid shaIl be remowd from the 53 The angle of the braid of the inspection
speeimen and the diameter orer the core (M- unit almll be recorded to the nearest. 5°.
Method 1621
Avril 14, 1%7
ANGLE, WRAP
L SCOPE 44 _lf two wraps am preeeng the mgle of
1.1 This method is intanded for use in deter- the outer wrap shall be determined from tho
mining the angle which the yarns of cotton diameter over the inner wrap.
wrap make with the axis of the i.nsulatad wire 6. RESULTS
or cable. 6J Calculatfom The tangent of the angle
Z SPECIMEN of the wrap at my place shall be calculated as
Z1 The specimen shall be a pica of the in- follows :
specticha unit at least 6 inches in length from T (D+ D%)
Taacent o! nade= ~
which iny covering over the wrap has been
removed. where:
~mtw dls~ew o?er the wrap or eemlng,hlch
& APPARATUS AND REAGENTS f),-~e timti over the col’q Inch
&l The apparatus and magenta shall be M L-the Iengtbof lay of one aplral of wrap
described in the methods mferaxmd in 4. rdt.14
4. PROCEDURE 5.2 The angle of: the wrap shall be deter-
4.1 The specimen shall be fme from me mined from the tangent of the angle by refer-
chanical dnma~ The length of lay shall be ence h a table of natural trigonometric func-
determined as described in method 1531 and the
tions.
vnlne recorded as L.
5.3 Unless otherwise speoificcl in the detail
4.2 The diametar over the wrap ahd.1 be d~
ten-mined as described in method 1141 and the specification, two specimens, one from each end
value recorded as D. of the inspection uni~ shall be tested.
43 -“ -.-. J ;...
~i16 wrap sha]l tfiaii ‘be relllu~cu -
i, U,,l 5.4 The angle of thr mmp of the inspection
the specimen and the diameter over the core unit shall be the nveroge of the results obtnined
(assembly under the vrrap) shall be detmnined from the apecirnens @ted.
as described in method 1141, and the vnlue re- 53 The angle of the wrap of the inspection
corded as D,. unit shall be recorded to the nearest 6°.
Method 1631
April 14, 1967
Method 1711
April 14, 1%7
METHOD 261 i
METHOD 20!1
Method 2021
April 14, 1%7
Method 2031
Aprif 14, 1%7
Method 2041
April 14, 1%7
(
FLEXIBILITY, FIBROUS COVERINGS
1. SCOPE with n!? to 2% inch straight length of the speci-
L1 This method is intended for use in deter- men ●t ~ch end. If the size of the wire or cable
mining the tistnnce to bmnkags of tbe yams ie larger than No. 2 AIW, B simple U-turn
of fibrous coverings of insulated wire and cable. shall be made about the mandml. The Speci.
It is particularly ● pplicable to wim ●nd oebha men shall be examined for broken yarns in the
of the bnilding type, fibrous covering both bcfom and after removal
2 SPECIMEN from the nmndre]. Exeminstion shall also be
21 1%0 apetimen shall be n pioca of the in- made for nny finking of the finishing material
spection ttnit 24* $$ inch in length. from thp wire or cnblc ass result of the bending
$ APPARATUS t~ withoutactusl rubbing of the vira Creck-
3.1 The appamt us sludl rormist of n mamhvl ing is not nmwsttnly flaking of the finish.
of the diameter required in table 1 of method &S Flat twin cable ehall be bent ou the
8221. minor As of its cm section only.
4. PROCEDURE L RESULTS
4.1 IJnles otherwise specified in tho detnil 5.1 Unless otherwiao ~pecithl in the detail
Bpwification, the specimen shall be conditioned qwcificntion, one specimen from ench inspection
nml tested at a temperature of 23° * 1° C. (78.5° unit shell be tested.
*2 °F.). 52 @ breaking of the pm in the fihroun
4S The apocimen shall he fne from mP-
covering of the specimen eball be recorded.
chsnieel damage nnd shall not be bent or flexcul
5.21 For wmps or nervings, the typo of yarn
until it has reached the temperntum specified in
lmken shall be mmded.
( 4.I. Handling
almll be reduced
nnd flexing of the specimen
to the absolute minimum necea- 53 Any finking of the linishmg materials of
eery in conducting the test, The specimen shall the specimen shall be recorded.
then b&bent around ● msnchvl of the diameter &4 The kibility of the fibrous corcring of
required in table I of method 8221. If the tira the inspection unit shall be the reeulta obtained
or cable is size No. 2 AW(3 or smaller, os many from the specimen or specimens teuted.
tuma shall bo made ●bout the mandrel es will L5 The tempentttm of the K elmll & re-
permit it to conform closely to the mandmi Oordd.
Method 204’3
ADrll 14. 1%7
T- I.-M&iipiyirM
fader for &#u+AQ m#ItflUl tit8r
OBeduaiwwtq
AWO &y dm upto4p 4paDdm upt04p 4p andowr &y da
lMIMiee web:
J%saadaaI&r 8 4 9. 0 8 12
Ovu%h* 4 s 7 ? 10 la
ova% o $ $ la la
Umttvrinab
bdanbeimtcmthe dhnat@raban banauiiahtammng ● “ Ubosize
Qinoraxbofi ta-aationordy. Tlwminor ofti~
MAomu .
&“-itmJLm3
sol u:dP%”tba+o”qmoMd
illtb9d9biI
spcvi&n*om _ frwI - ~
unit dml~ be =UL
S.2 Any bmkii of h ynnt in ho fhtun
wwin& Of the @eCimCn Ohall be morduL
W Focunpor mvi~tbotypof
yam bmkcn dull ~ xuwdai. J
..’ ‘i’, .
,. i
“. ,1..”. .
I
-...
..
. . ...-
------- ----- .
I ..- .”.
-. ..: ●
.’ .4 .f . 3. .
1
-METHOD 2051
April 14, 1967
Method 2111
@ril 14, 1967
ELONGATION, ARMOR
L SCOPE apparatus. The unweighterl end of the speci-
1.1 This method is intended for use in deter- men SIIIIIIk hoisted gently until tile weight 011
mi ]]ing t h~ rmistunce to stretching of nrmor on the odm el]d hangs freely withou~ swaying.
insulated wire and cable. The specimen shrill hang vcrticnlly and per-
2 SPECIMEN pendiculnr]y to the fnce of the clnmps, ‘l’lie
21 The spccirneu shrill be a pieca of the in- specimen shrill support the specified weight
slwct io]l unit at ]enst 44 inches in len~h from for one minute. The specimen and weight
which any covering over the armor has been shall be lowered, the clnmps removed, and the
removed. specimen me~sured for recession of the conduc-
3. APPARATUS tors into the armor at euch end. The measure-
3.1 The apparatus shall be as follows: ments shall be mndc to the nearest 1~2inch and
3.1.1 Two ckmp~ each 2 inches wide and of tho sum of the recessions recorded.
good fit on the cable to be testd 5. RESULTS
3.12 lVFiyAt ns required in 4.1. 5.1 Unless otherwise specified in the detail
3.1.3 VerticaZ hoisting equipment. specification, one specimen from each inspection
3.1.4 Std iwvdeor tape graduated to $7: unit shall be testwl.
inch or finer, or its decimal equivalent. 5.2 Tile elongnt ion of the mmmr it t any
4. PROCEDURE plare shnl] be tile sllm of the rccessio]ls of tlie
4.1 Unless otherwiea specified in the detail conductor iuto the armor at each end.
specification, n weight of 100 pounds shall be XI The elongation of the armor of the in-
used sper[ ion unit Sl]:ill be thv rmlllt {Ibtninwl front
4.2 0.lc clMnp dud] be f=’tiiie~ on each end the specimen testccl.
of the specimen, leaving 2 inches of the cable 53.1 When I]iore than one specimen is
pmj=ted beyond the clnmps, This leaves a tested, the clong:~tion of the armor of tile in-
distance of 36 inches of the specimen between spection unit shn l! be the nvernge of the results
the clampg The clamps shall be fastened oht nined from the specimens tested.
firmly enough to prevent slipping but not tight 5A The-elongation of the srmor of the in-
enough to crush the armor. spection unit shall be recorded to the nearest
43 One clamp shrill be connected to the ~s inch.
weight and the other attached to o hoisting 5.5 The weight used shall be recorded.
Method 2161
April 14, 1%7
Method 2171
April 14, 1967
(
TIGHTNESS, ARMOR
1.SCOPE shall be cut wpmly and any burrs remomd by
Ll This method .ia intended for use in menns of a fib. The cable shall be inserted into
determining the tightness of braided armor on the pipe so &t the conductcm protrudea from
the eonductm assembly. the thmeded eml Tha cap shall be applied so
2 SPECIMEN as to contin the armor within the pipe and
Zl The specimen ehall be ● piece of the pennit the &inch length of protrmii.ug condu~
inspection unit 10~ feet in hngthfrom which tor to move freely. The protmding oonduetor
any cuvering orer the armor hae km removed ehall be eecurely faetened into a loop md this
3. APPARATUS attached to the weigh~ The pipe containing
3.1 The apparatus shall be os follows: the epecimen shall be mid to ● vertical pad-
8&l ~;IJ~I approximately 10 feet long and tion with the weight at the bottmn and then
having an inside d“iameter slightly larger than gently hoisted till the weight hangs freely with-
the outside diameter of the ,specimen to be out swaying.
tested so as to permit the cable to move frrely 4.3 After the weight haa been suspended, for
but not loosely through the pipe. One end of 1 minuta the pipe shall be lowered and the dis-
the pipe cxt.erior shall be thrmded to receive tance the conductor has receded into the armor
a cnp which shall contain a round, &mooth hole at the end opposite the weighted end shall be
large enough to allow the cnble conductors to measured by means of the scale to the nearest
pasa freely, but small enough that ● flange m- %2 inch.
mnins to support nnd contain the nrmor within 5. RESULTS
the pipe. 5.1 Unless otherwise specilled in the detail
~.~~ w~jq}f p~ q* *#*w=
G-A A:r A
●
1
=.*. !!ipecific~ticn, one s~ccimcn frcm Caclhinspection
S.U Nrel wale gradunted to ~z inch or unit thal,l be kted.
6ner or ita decimnl quivalent. 5.2 The tightness of the armor of the inspec-
3.1.4 Vert~*? hm’.ding quipwvnt. tion unit shall be the nsult obtained from the
4.PROCEDURE specimen tested.
4.1UnleEYI
otherwise speeificd in the detail !521 When more than one specimen is tastad
specification, B 15-pound weight shall be ueed from each inspection uni~ the tightness of the
in testing numbers 18, 16 and 14 stranded con- armor shall be the avemge of the results ob-
ductor cable (armored cord), and a 40-pound tained fmm the specimens tested.
weight for testing all other cabk 5.3 The tightn- of the armor wim of the
4.2 ‘he armor and shenthing ehd be m- inspection unit shall be twarded to the nearest
mowxi from one end of the epecimen eo se to ~a inch.
eqca 6 inchee of the conduotor, The armor &4 The weight used shall be recorded.
( (“
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Method 2281
Auril 14. 1%7
OPENING, ARMOR
L SCOPE clamps shall he fastened firmly enough to hold
L1 This method is intanded for use in deter- the specimen but not tight enough to damage
mining the resistance of armor of insulated wire the armor. One clamp shall be connected ro
and cable to opening. the specified weight and the other attached to s
2 SPECIMEN hoisting apparatus. The unweighed end of
3.1 The specimen shall be the nrmor from a the specimen shall be hoisted gently until the
piece of the inspection unit at least 44 inches in weight on the other end hangs freely without
length. The specimen shall be prepared by swaying, The specimen shall hang vertically,
m.moving the conductor from the cable without and perpendicularly to the face of the clamps.
mechnnicn] damage to the armor. The specimen shall support the speoified weight
3. APPARATUS for one minut.a The specimen nnd weight shall
U The *pparatus shaU he as foIlows: he lowed, the clamps removed, and the armor
3.1.1 Two cliwnpa each 2 indhes wide and of examined visually for openings. .kn y open inga
good fit on the specimen to be tested. in the specimen of sufficient size to expose nny
3.L2 Weiqht as required in 4.1. material under the armor shall he recorded.
3.L3 Vertical hoisting equipment.
5, RESULTS
4. PROCEDURE
5.1 Unless otherwise specified in the detail
4.1 Urdeas otherwise specikd “in the detail
specification, one specimen from each insption
specification, specimens of an.nor from sizee
unit shall be teated.
AWG 18, 16, and 14 stranded conductmr cnble
and all sizes having nrm(,: of flattened cross 5.2 The opening of the rumor of the inspec-
wtinn sihnll b ktd with a 150-pound weitzht tion unit shall be the results obtained from the
and cables of all other sizes shall be tested with spmmen tested.
s WI-pound weight. “53 Any openings in the armor of suf6cient
4J One clamp shall he fastened on each end size to expose any materinl under it shall he
of the specimen, leaving about 2 inches of tho recorded
armor p@mted beyond the champs. The 594 The weight used shall he recorded.
METHoD 22(1
APril 14, 1967
ABRASION RESISTANCE
Method 3001
APnl 14, 1967
ber and thermoplastic compounds, the material of 36 pounds is necessnry (o tww n specimen
strotchee with sn accompan~ng reduction in 0.082 inch thick, the tearing strength would be
cmse-sectionnl ara Sirm precise meaaure 36 divided by 0.082, or 439 pounds per inch.
menta of the specimen cannot be made ●t the 2.6 Median. If the numerical values for ●
moment the specimen bremka, calculation of the given property are ● rranged in an ascending or
tensile etrength at break is based on the croes- descending order, tho median is obtained as
sectionnl area of the specimen before applica- follows :
tion of any load. 26.1 If the number of values is odd, the
22 Elongation. Elongation is the exten- median is the value in the middlo d the eerics.
sion between bench marks produced by a ten- 2.62 If the number of values is even, the
sion force applied to a specimen and is ex- median is the arithmetic average of the two
pressed aa a percentage or origkml distance be- middle values.
tween the marks on the unstretched specimen, 3. SPECIMEN
Ultimate elongation is the elongation at the 3.1 Typaa.
moment of rupture For examplq if a l-inch 3J.1 Two shapes of specimens maybe used
bench length in marked on an unstretched speci- for tensile strength, elongation, tensile st~
men and the specimen is stretched untiI the nnd set of rubber or thermoplastic insulation.
bench marks us 7 inchee apa~ elongation is These are the dumbbell nnd straight specimens.
7 inches-1 inch-6 inches or 600 perwmt. .i dumbbell specimen, m described in method
23 Tensile stress. Tensile stress k the 3021, shall be used whenever it is pr~cticable
force per unit of original cross-sectional area of to prqxm it from the pime (varnished cam-
the unstretched specimen required to stretch bric insulation rxcepted) to be t~sted, Straight
Method 3001
specimens in the form of tubes shall be used 43 If the piece from which the specimen ia
for rubber nnd thermoplastic insulation and to be prepared is too thick or has an uneven sur-
sheaths Then it i’snot practicable to prepare a face that may interfere with the determination
dumbbell. A straight specimen 1 inch wide or of thickness, the piece or portion of the piece
the full width of the tape if less than 1 inch shrill be bufiecl IIS described in method 3011,
wide shall be used for determining the tensile The specimen shall be permitted to rest at least
strength of varnished cambric insulation. 30 minutes between bllffing nnd testing. Speci-
3.12 Specimens for use in the determina- mens for tension tests shall be buffed in tile strip
tion of tearing strength are shown in figure form before cutting with a die.
3111, 5. RESULTS
3.2 Direction. Specimens shall be taken in 5.1 Unlms otherwise specifiwl in the detnil
the length clirection of the wire or cable for rub- specification, three specimens from each in-
ber or thermoplastic insulation and sheaths and spection unit .dmll be tested for teusilc streugth,
in the ]cngth direction of the tripe for varnished elongnt ion, tcusile stress, nnd set of rubber and
cambric insulation. thermoplastic insulation nnd sheath except that
4. PROCEDURE under the following condit ious five specimens
4.1 Unless otherwise spcrified in the clebil shrill be tested:
specification, tsmsile strength, elougat.ion, and 5.1.X If one or more values do not meet the
tensile stress of rubber or thermoplastic insula- specifie(l reqllirmnents rl)en tested for com-
tion and shcztlls shun bc determined on the plinnro with speviticntions.
S:LIIIespw’i)n(m al]d during il si:)gle test. 5.1.2 If referee tests are bei]g mnde.
4.2 If five specimens nre reqtlired for deter- 5.2 Tlw chnrnctcristic of the insulation or
mining nny one of the nbove properLies, 4.1, sheath nf the il)spection uuit shall be the medinn
these five q)ecimcns shall be used for determin- of the rewlts obtained from the specimens
ing all of these properties. tested.
Method-3011
@il 14, 1967
Method 3016
April 14, 1967
Method 3021
Ad 14. 1967
TI
M-
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Ii
it
f3-
N.[
I
“-- ----- h,
●
‘%?
~d
d
+h
‘+
FED, TEST NETHOD STD. MO.
Downloaded from http://www.everyspec.com
Method S021
A * %a 1 1 1 ){ % % %
hhximum 1% l)f l!i l!~ 1$8 1% 1%
B 4;5
c Minimum 5% 5H 4 5 5 4)f
D *~~1 1% 1% 1% 1)-4 1% 1)4 1)4
D-r * ?4s % !f !4 N H % ~
+){s 1!4 1!4 w ~ 1% lx ‘
F
G ● %9
8J, %* ;8 p %* )h %*
1 1 1 % % !~
H *H*
L ● HV 2%. 2%. 1%6 l%, 2)f. 2!40( 1%s
w 660 agun o.Soo 0.250 0.250 0.125 0.125 0.250 0.250
1For dice wrd in clicking mnchWa, Itb Pmfe-le that We toler-e b +%4 Inch.
,30~ nml not more llmn n~”. The ollter fnce une~e]l surfiwe that mny interfere with the de-
shall extend nt this angle from the cutting edge termination of thickness, ti;c piece or portion
fur npproximntely ?~.t inch :lnd thrn shall form of [IN pirw sII:L1l ho lJutTc~l:1s (Iescribcd in
nil angle between 18° and 22° with the in]~er me! lwd 3011. The specimen shall be pwnittccl
face. The dies shall be sharp and free fr~jm to rest at Icnst :;0 minutes between buthng and
nicks in order to prevhnt leaving ragged edges t~stiw Swilnens shn]l be buffed in ~~~e*rip
on the specimen. form before cutting with 8 die.
~.~,~.l (!nrrfll] niujJi@l)iilm.3 Of dic-clltting 4.1.2 I)llwr)ht)f. Slxvinlen.s of the required
edges is of extreme importance and mny he ob- shnpe nnd sizr s?mll be cut or strtmpwl from
tuind by dnily light honing and touching up tlm piece of mntcrinl with the required die. To
the cutting edges with jeweler’s hard Arkansas facilitate cutting, the edge of ‘the die may be
honing stones. The condition of the die may lubricated with wwt~r containing a wetting
be judged by inveetigding the rupture point ngent snd a corrosion inhibitor before each
on uny series of btwken specimens. When specimen is cut. The cut cd=% shrill be per-
Inwkcn specimens nrs removed from the grips pendicular to the other surfaces of the speci-
of the teetin~ mnchin~, “it is sdvantageona to men, have a minimum of concavity, nm.1be free
pi 10 t lwse specimens nnd noto if there is nny from rngged edges.
ten(lvl wy to brrnk nt or near the samo portion of 4.13 Struiqht specimen. A specimen of
ench specinwn. Rupture points consistently nt proper length for clamping in the grips of the
the snme pluce nmy indicate that the die is testing machine shall be cnt from the unit or
dull, nicked, or bent at t hnt ptwticular position. piece to be tested. The specimen shall be free
3.12 C%ttinq mlppd. Rubber belting, from nicks. If possible, the specimen should ho
leather belting, light cardboard, or other mn- cut with a die or with a single stroke of the
terinl with a smooth, slightly yielding surfsce cutting tool.
that will not inj Nre tho cutting edge of the die 42 Cro-ectional area of specimen
during the cutting or stamping of the specimen. 43.1 Dumbbell.
4. PROCEDURE 42.1.1 Thirhnem. The thickness of the
4.1 Preparation of specimen. specime~ shall be determined as deseriberl in
4.1S l;ulfin~. If the pieco from which the method” 1124 except that three measurements
specimen is to be prepared is too thick or has an shall be made, one at the center and one near
&
Method ml
each end of the reduced section of the specimen. @ps of the machine knd adjusted symmetri-
If the specimen is narrower than the diameter cally in order that the tension will be distrib-
of the foot, rnensuremertte shall be IImde with uted uniformly over the cross section. If the
the canter of the micrometer foot coinciding tension is greater on one side of the specimen
with the longitudinal center line of the speci- than on the other, the maximum .v@@h of the
men so that there will be an equal orerlap of the specimen will not be developed. The force
foot on em-h side. The median of tlic three shrill be appIied to the specimen at such a rate
measllrement.s shall be used as the thickness in that the power actuated grip will travel at a
calculating the cros9-sectional arm of the speci- uniform speed of 20=1 inch per minute. After
men except that specimens fur which the differ- rupture of the specimen, the breaking force
ence between mnximum and minimum tllic.lulcss shall be noted from the (linl or scale or by means
exceeds 0.0(J3 inch shall he rliscartlcd. of :In nlltogruphic or spark recorclcr and the
4.2.1.2 Wldt4. ‘1’]w widlll of a spwimcn vnl ue recorded.
shsll be tbe dlstmce, W in the legend for figure 5. RESULTS
8021, between the cutling edges of tile die in the 5.1 Calculation. The tensile strength of
reduced section. the specimen shall be cdculnted as follows:
4.2.103 The cross-scctiorml arm of t hc speci- Tcnslle strength, p, a. l.=?
men shall be cdculatod by multi plyill~ the where : u
width of the specimen by the mwl ian tliicli!)~ss ~=breaklm! force in pounds
of the specimen. (?=cross. sectlorml orp,ll of the unstretch~ a~l~en
in square Ihcbes, 4.2.1.3 or 4,2.2.1.
4.2.2 %tight.
4.2.21 ‘1’lwwclcht of tllc spmljn(,ll it) gr:inls, N Ul)lw% otherwise specified in tile detni]
the Iengtli of the specimen in centimeters, rmtl specification, three specimens frnm each inspec-
the dollsity in grams per cubic cent imettv shrill t ion lll~it shall be tested cxcrpt tllnt ul)der the
full, )winy conditions fire specimens shall be
bc (Irtrrmincd. The cross-scction~l nt-rn s]~;~ll
then be calcl)lated from these mcnsllrernent.s ilk t Csted :
-m.
t lie following manner: d.:.l I.i tiw iensiic stre~~gti) (Ii ~JINIf~r lnore
specimens does not meet the specified require-
!l,lrbq;7
(’rfwwwtiwal area. ~unrv lIIch2s_ -
1)9 L-
ment for tensile strength “in the detail epsci.
where: licution.
11’-the weight OCthe aperhocn ioy]r IUgrnms ~.~ If referee tests nre being made.
J)=rlIO d,tmit~ of iht~ upeclmtw Ii) Krnulx ]wr cuhk 5.3 The tensile stremgtb nf the insulnt km or
c,lntlrnetw sllcat)l of the inspmtion unit sIMII he the me-
1.=! ti~,l~m~tl of the sl)m.imrn in mv)lln),qr.r<.
dian of the results obtained from the specimens
4.3 Determination of tensile strength. tested.
43.1 Tlic lost ing mnrhinc slmi] be culibrntwj 5.4 The.tensile Strength of the insulation or
as Josmibml in method 3016. shc:~th of tho inspection unit shall be recorded
4.X2 rho si~~imm dull] IN’ l}lncml in tho to the ncurest 10 pounc19 per square inch.
Method 3031
Avril 14.1967
containing ink of (he desired color nnd @ity D-the dlstn nm betwe@n tk beach marks ●t the
for msrkinq the specimen. Tlw ink SIJIIIIhnve moment It rnwutw of Inckthe *pAmm
O-the dlstnoce between the Mnrb mnrks on tbe
no deteriorating effect on rubber or plastic nnal retcMl *men. tncba
~~ enmpounch+ nnd shall be of contrasting color to
= t-hiese Othertvim ;lnYif%*d ill 1ho dct:~il
thrit of the specimen.
\ 3.1.4 Mmmm%.g mate .fiv oth~r ddce gmd- specification, three specimens from cinch inspect-
unted in 0.1 inch for indirsting elongation. , ion unit shrill be tested except thnt under the
4. PROCEDURE following conditions be specimens shall be
4J Unless otherwise specifimi in t ha detail t@skd :
specification, the elongnt ion shall be dmmnined 5.21 If tlw Ampti[m of ~)twIIr IIIIIIW●lnvi -
on the same specimen and nt the earn? time as mens does not nmeL the specifird requirmwlt
the tensile strength. for Amgntion in the detail specification,
42 Preparation of specimen. The npeoi- 5= If refcnw toxt~ rtrv Iwillg III:IIIV.
rnwl dm,il be prepntwl as tleacribed in method M “11}0 t+mgat ion of the insuhlt irm or
M)21. Two poralkl bench tnarks shrill be phimf sheath of the inspection unit shrill Im tllc nwdinn
ywnmetrieally on the strnight slmcuneti umi on uc tiw rcsu!ts obtamcd frml thG .spccimtnz
the mductxl section of the dumbbell specimen tsted.
perpendicular to the longitudinttl nxis of the 5.4 The eimlgntion of tllc inrmlntion or
spwinmn by menns of the bench marker nncl dmth of thr inqn~tion unit shrill b’ mcor(led
i~~l;, The rnnrks shrill ho not more thrm 0.010 to the nrnred 5 percent.
Method 3041
Aoril 14. 1%7
i
:
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Method 3111
APnl 14, 1%7
Method 3161
April 14, 1967
Method 3161
Method 3171
April 14, 1%7
Method 3171
U Unless otherwise spectied in the dekil 5.4 The tile strength of each tape tasted
spedcation, two specimen9 from emh tap9 - shall be recmrded to the nearest 10 pounds per
lscted shall be &ted. square in&
5S The tanstie strength of the tripe shall be
the nverage of the resulti obtained from tbe
specimens tested.
Method 3211
April 14, 1967
Method S2U
S.S The tande atrengtb or elongation of the
conduotor or wire of the inspection unit shall
be the amqe of the remdte obtained from the
Specimens tasted
wherb: S.4 The tensile atrengt.h of the conductor or
~mtie dls@nee betwewy (hch marks on the spcl- wire of the inspection unit shall be recoded to
men Imm+tely after ruptore, ilxk the neareat 10 pounds per square inch.
au Unlem otherwise specified in the detajl 55 ‘I’be elongation of the conductor or wire
specification, three spacimena from each inspec- of theirqection unitahallberam’ded to the
tion unit shall be t4utacL neamat O*5percenL
Method 3212
AD~ 14.1967
on the specimen es described in method 9211. &2 Unle.m otherwise specified in the dekil
4.3 The elongation of wira with diarnetar specification, three specimens from each inspec-
lass thnn 0.208 inch shd be determined by tion unit shall be tested.
measurement made between the grips of the 503 The tensile strength or elongation of the
testing machine. The zero length shall be the conductor or wire of the inspection unit shall be
Method 3ZlZ
the ●vemge of the rwulta obtaintd from the 5.S The elon@ion of the conductor or wim
qecimens * of the inqection unit Shll h reoorde!d to the
5.4 The teneile strength of the conauctor or nearest 0.05 percent for lo-inch apaci.mew and
wire of the inspection unit ahsll be recorded to to the nea- 0.01 percant for #-inch
the nemist 10 pounde per equam inch. qecimam
Method 4001
April 14, 1%7
Mdisod 4001
3.15 Automatic ternpemture controle shall 3J.1O If ● liquid !. -sting m~iw is &
be used and a recording thermometer employed the liquid or ite rape shall not ooxne ia eontaet
to record the temperature. with the ~pecimu
3.1.6 The test chamber shall be preheated 4. CONDITIONS OF EXPOSURE
to the expusure temperature before the speci-
4.1 The conditions of exposure shall be RS
men is placed in it. If the temperature within
the container changes while the spwimen is be- described in the ciehil specification. Many
ing plnqed in i~ the container and conte]lts combinations of tempmature, pressure, ml
ehall reach the specified temperature within 16 time of expam may be used, AE an aid to.
minutes after the specimen haa been placed in wade standardisation, it is recommended that
the chamber. the temperature and preMUrS specikl in the
S.1.7 The exposure period shall start at the detail spedlcationa be selected from the follow-
time the specimen is placed in the ohamber. ing suggested con~.ione. In genenl, the con-
At the end of the exposure period, the specimen dition eekwtad should be euch that the deteri-
ahnll be removed from the chamber and par- oralhm will not he so great as to prevent the
mitted to rest at room temperature for not ke determination of the final physical properti-
than 16 nor more tlmn 96 hours before deter- u nkea the aging characteristic of the com-
mining it9 properti=
pound are known to be poor.
3.1.8 The material used for marking bench
lines or other markings on the specimen shall 42 In the oxygen pressure teat the increase
not be detrimental to the rubber compound. iu temperature from 700 to 80° C. would k
3.1.9 Copper or braas parte shall not be ex- expected to approxi:.lately double the rati of
posed to the Btmoaphera used in the aging oxidation of the robber or other oxidizable
chamber. materinl.
tiinimtam volume
Tem~ of aging timber
Test Medium “J?& [email protected]. s. L .%J%08L
oxidi~le ma- \
tariak, mfliliitem \
.—
Oxygen pmsure Oxygen 70 m b 310 10
Modi6ed oxygen pmimure Do. 80 a to 52 10
Do. Do. 80 290 to 310 10
Air plwaum Ah 127 78 ti 82 100
Air OVOXl Air oircukted by 00nV@ttOU 70 Atmoepbde 10
eoestoobangeatlti
once par hour.
90 10
R
Do. Do.
Do. Do. 100 10
Do. Do. 121 Do. 10
Do. Do. 149 Do. 10
Teat tube Air oiraulated by conmetioa 112140 Do.
149
Method 4011
April14, 1967
,, Mdbod 4011 . -.
‘: time ruder the required conditions withoat ridsinqgetl ImdarprmmdDos tllarBt90f
opening the veal. reationms ybecomo~npidia mmoq
4.4 At the and of th CIPOSUN! period, the particularly if ● large W1’faa@-is erpaod
pmwre in the ● ging chmnber shall be mlemd md very hii ~ms may &v&p. (km
●t ● S1OWsnd uniform rate, rquiring ●t M till be taken to ●oid the intmmktion of
6 fninutee for a comp)ete rekssc of the prt%sureL
This proredw is neremwy to smid posible ~R:s#~~m * ~.
fortnntion of porosity in the SpeciInem ‘W &l CdCUh* The kngs in We
specimw shall be remowd from the ● ging S@@& aloagsti~ or other ckmcMstk of
chambrr immediately ●fter the mlmse of tho the insulation or shsath of th inspedm unit
prexsuw and tkn ed aside on * flat surface to due to @rig, shall bo omlollkted u follows:
# for not 1- thnn 16 houm @ not mom
wts~.~ ‘=~ Xloo
than 9G hontn at room tempcmtun before t-
●re made.
*:
o-tM?@mS@MatBednthe~ a
L! At the ml o{ the rest period. unbs titb or ttw i—l—d— tit
O(Iwrwiw qwwi fkl in the detail qwiflcnt ion, s-the do% abtdnd a tboamd ~ =
4.!L trnsile strength ●nd akmgntion shall ba de- ahssthotrbstmmett-mtt
@mlinccl on the aged sperimen ns dmrribed in S4 Wnlea othewiae spwifbd In’& Al
methods 3021 and 3(x31, rqmctivrly. If ofhcr qwritktion, the number of 8peckM &@9d
propet[irn are rrquirfd, the specimen Shall be frnm emch inspection unit shrill be as mqmirtd
testd as desrrild in the sperilird meLII(d. in the method oft* 4% d for**
The snmc test shall bs conductod on agml mIKl the deterioration of tbe insulation or .hh~
wmgwi qmcirnens for ths purpose of comjmri- 53 The changs in ths chsm- of the
son in determining the degree of dcteriomtion insulation or shesth of tb. irwpdk @ M
of thp ngml nlnterinls. k mm ~lcd to the ?l*iltSSt one percent.’
4.6 A&quntr safety prmutiom shall he 5.4 1110 tmnpemtu~ prwmu~ Utci tltno of
tnkm when hcuting osidiznbie orgauic nmm- ●xpwum used shall b%%9codo&
Method 4011
I
I I
I
I
I SUDPL y
I I
I
i
I
J19QU 40UAL
Method 4011
Method 4021
. . . . . Aprit 14, 1%7
M@hod m
●vaihhlo inthscbnhe rfordgrun of oxi-
d@ble mtdaL The --.rmlm P&d shall
8tart8t tkatime theqw&nan i8plaoodin thd
ohunbe+r and till ccntinue for tho rqui.md
time under the requirul conditions without
Opeuling the vmeld.
,,1
-W U
Method 40ZI
Chnagela Chamctsrlmlc! perceat= J&wlo from euh inspction nnit shall be as required in
the method of teat 42 used for determining the
Wlwlw:
o=~e val~e obtilned on tbe nal~ ~Uk~On Or deterioration of the insulation or sheuth.
sheetb of the lnmectloa unlt~ 53 The change in the cka.cteristic of the
B= tie v~~ue ob~lo~ on the sged WOhtbll Or
insulation or sheath of the inspection unit ahnll
sheath 0! the lnepectlon uolt t he recorded to the nearest one percent.
6.2 Unless otherwise specified in the detail 5.4 The temperatum, pr=mre, and time of
specibtion, the number of spaimens tastad exposure used shall be recorded.
Method 4031
*d 14, 1%7
I
AIR OVEN TEST, INSULATION AND SHEATH
L SCOPE heating medium to recmd tbe actual @ng tem-
Ll This method ie intended for uee in deter- pemtum in. v8rioue @a of the oren.
mining the effect of elevated tempemtmu ~d M Liqtid ass hectiog medium.
tir It normal dm+eric preunme on m.dhr 3JLl Avpwtw omployinq u U@d bating
and rubber-like ineuhtion and sheathe of insu- sdhun consisting of Bweml smd ● ging con-
lstad wire and mlk tb uubmerged in ● thermo9t9tic811y-con-
Z SPECIMEN trolled liquid U The equipment shown in
Z1 The specimen ahdl be m described in 5gure 4031 has beuI found suibblo for the
mcthodn 8021 ●nd 8(IB1or other method of uw P-
required for de@rmMng the mnount of * ~ A &CtiO?l Of tk buth SboWiXig OIM
terioratiq a. @q -+= ia sbom in figure 40S1. The
3. APPARATUS
W The qlpamtn, till be s, follows :
SJJ The equipment listed in 8A! may he IT
tuml where air ie amployed m the heating me-
dium. Appwatus in S3 mny be used where the
heating medium consists of a liquid bath,
M Air na L h-ting medium.
8-21 A okdatkg uiT own with pmtions
for suspending spcimens without crowding ad
without touching eecb other or the sides of the
Ovcrl. ‘ilne volume ehoul(i *be not km thnn
19x12x12h~umdntimm~WxWx~
ineben.
W A ML= of -, which is optiona~
shall be louted outide of tbe 8ging chambu
Properg
W A t~gulutor for ●tomtic tmn-
pexmtum control of the hdng medium
PWL -
M.4 E@#ipnWt #w olnnplcto o$’m&&m
of the heating medium * u to keep the tan- oontier oonsks of s nickel-platad brase cyl-
pemture of the sir tbroughcut the omn within inder ~ inti in diameter and”8% _ high
=10 C. (2° F.). The foUowing pmuutione with s cover which reota on ● flange ineide the
8haUbetaken: (u) Ifamotordri?enfan iaG cylinder about !2incha from the top. The epnca
theurin thaoven shall notmmeinoontaot ●bove the oovar ti !Uled with thermal insulating
with the f8n motor-hmsb d-rge beuuse of matorid Cumulation of air ie by convecticm
danger of 060ne forrnstion, (b) Mle8 shall he threughs ~-inch inside dkmeter tube mounted
wed as mquimd to pmwent local overheating in the metal cover. One of the tubee extends to
●nd dead ~ snd (c) the thermostatic con- within about ~ inch of the bottom of the eon-
tmd ohall be eo k8tad M to give ●ccurate tun- tsinerand tlmothera_akut6 inchrn
paratura control of the he8ting medium. The dxwe the cover. l%a Mar tube is insulstad
preferred location ie adjacant to the moording with ml’k
thermometer, 8S3 A & or otkr Ibid MA ~apable
W Reroding thmnmwtzw 1- in the of holding several submerged specimen con-
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bMhod 4021 .-
ti ad apipped with an sutomatic tbermo- kiner~dmt aside oaaflatmmfaoeto-for
datic oontml end means for obtaining a uni- not k than 16 houm and not mom k X
form temperature in all parts of the bath The houn&tmomt8!nper8tu* befom@steamcon-
tempatum of the air at the specimen will be duotd
●pProximatdy &5’ C. ( 1“ F.) bdOW that of 45 Attheend of themst@~nnleee
the liquid bath The bath is quippd with s otherwise speci&d in the detail @&
cover antaining about 1 inch of therms.1 id- tansi]e atmngth and dOt@im ahdl be d4ar-
●dsting material. Several aging eontainem m ini.ned ontheaged ~imenaedtibed in
fittad into the bath with the top being flush with methods WU and $(X3L If other propertk ●m
the cover of the bath required the specimen shall be tinted as de-
3S4 Mem ior 8u~]vmdim7 t?te Rpeekna emibedi nthea#6edl netho& The-t#st
vetiieally m the aging container svitlmut toudk- AaIlbeo onductedo nsgedandu nagedapaoi-
ing each other or the sides of the contiiner. mensfor thepurpae ofoomparkn indetar-
This can be aocompliahed by fastening hooks to mining the d-of detariorstion of the qd
the undemide of the cover. matarisl
4. PROCEDURE & RISSULT’S
4J Unks otkmriae specified in the detail lufklcallWnL Tha&ngeilltaneUs
specification, the ~ shall be cnrried out ●t s
8t_ elongation or other &mctarW “ .C of
tanpsratum of 70°=10 C (158°=20 F.) for s
the insulation or +aath of tha inqaAkn unit
period of 166 houm= 1 hour.
42 Unlese otherwise specified in the detail due to aging shall be cdoulated aafdlowa:
spdcation, tensile strength and elongation change In aaracterim% P-t4~—Xlw
tes@ methods 8021 and S081 respectively, ekdl Wk!re :
be used to det.mnine the det.erkrttion of the in- O.* ~loe ~la 00 * ~ xtion or
sulation or sheath due to aging. Sbath of the llupecuoo mlt
z.me Tame nbtahul eo * eawll blmoa or
43 After adjusting the aging container to 8tNouIiuthel~wlt
the required temperuLur~ the specimen simii ‘im u T.7ukl otherwise qa@atl in the datail
suspended vertically and the rmnteiner obad
epecidcatim the number of qmcimeaa _
immedistdy. At least 10 milliliter of cspacity
from each inspctiou unit ehnll b u required in
shall be ●vailable in the container for each gmm
of oxidizable material. The expocure period thematlmdo f~4&umdfor dm@n@ng the
shall start at the time the specimen is placed in deterioration 0{ the inauletion or sheath
the aging container and shs]l continue for the 63 Theohange incbeobere&cofthe
required time under the rwquired conditions insulation or she8th of the inspection unit shall
without opening the container. rerecorded tothewrwtlpelwmt-
44 At &e end of the axpoaum psri~ the 6A l!hatam~—dtimeof=poanm
speoimen ahdl be remored from the aging oon- Ileeddaallb
sreiorad
Method 4041
.@il 14, 1%7
Method 4041
estimating the degree of deterioration of the E-the vaIue obtained on tbe aced bulatlon or
aged mntcrhd. sheath of tbe i~oo unit
Method 4111
April 14, 1967
E%uax al.
Method 4111
U-tube hygrometer containing anhydrous cop- &L4 &.an&rd W&m thi08dfat# Bollbtiom
per aulfah &Ls Pota8abn idide, 1 parcent mlution
%1.1.4 A 0darat4d @lo mder having 8 S.L6 Acetio acid, 10 percent 00h1tiOIL
capacity of St least 25 cu. k per hour, for mw 4. PROCEDURE
uring the rata of flow of air through the sys- 4.1 Preparation and standardization of
tan. eolutiorw-’l%e solutions shall be prepared
3.1L5 J Qenera.tor forozonizing the air con- rmd shndardized as follows:
aista of two mncentnc eJectrod~ separated by 4.I.I Sta~h indicator uolutiom A fresh
a thin glaee dielectric, between which voltage is solution may be prepared for use each day by
applied. The generator is supplied by a po- dissolving 1 gram of soluble starch in 100 mL
tential transformer equipped with variable of boiling distilled water. A solution that may
voltage eont.rol of 20 to 30 kilovolt rating. be used for several daya shall be prepared by
3.1.1.6 An aging chumhw of ozone-resisting mixing 1 gram of soluble starch with 40 mL
material and of sufficient sti to accommodate of cold dist.iIled water, boiling until solution is
the largest speeimen to be tested. A chamber complete, diluting to about i!OOmL with cold
of about 18 to 20 inches in height with ● capac- water and adding 2 grams of zinc chlorida TIM
ity of from 2,OOO h 5,000 cubic inches is solution shall be set aside for several houra and
usually required. A convenient form of cham- then decanted.
ber is a glass jar with cover which permits eaey 4.12 Iodina - ~olution. A weighing bottle
access to the interior and allows inspection of containing 9 gmms of potassium iodide and 10
the specimen without opening the chamber, grams of distilled water ahail be weighed nnd
The chamber is equipped with a mineral wool then about 0,1 gmm of reagent grade iodiie
filter placed between two perforatd grills near cryatala added to the solution on the balana
the bottom. The ozcmized air is led from the The solution shall be accurately weighd to de.
generator to u space below the lilter. If an air. termine the amount of iodine added. The solu-
conditioned room is not available, the tempera- tion shall then be accuxataly transferred to ●
ture of the chamber may be controlled by im- volumetric flask and the volume made to 1 liter
mersing it in a water bath with accumtely con- with distilled watar. The solution should be
trolled temperature. A thermometer is placed stored in n dark bottle in a cod, dark plain
in the chamber with the bulb as near the speci- 4.LS Sodhwn thiom+lfate aoldon, A ~
men as possible. The chamber is equipped with dium thioeulfab solution of appronmately tha
a two-way stopcock, one acting as a discharge same strength aa the iodine solution shall be
ta the outside and the other as a bypass. prepared by dissolving ox gram of reagen~
3.L1.7 A mawrnetcr for measuring the grade sodium thioaulfate (Na,StO,.5H,0) in
prwure is connected ta the outl@ pipe of the distilled water and diluting to 1 liter. The
aging chnmber, solution shall be standardized against the iodine
3.LL8 A mnpling both for collecting s solution. Since the eolution gradually lotma its
specimen for the detm-mination of oaone con- streng@ the strength of this solution shall be
centration is connected to the outlet tube of the checked against the iodine solution at frequent
chamber, intervals. The atrvmgth of the thiosulfate. aolu.
tion shall be calculated as foIlows:
S&l.9 A &@&. gae cobatdnq burette ie
oonnected through a two-way stopcock to the ,-FXO
. T
sampling bottle. A 500-mL aspirator bottle is where :
connected to the gas burette by meana of rub- E=the kxllne aqulvalent of sodium thiaedfate es.
ber tubing. preaeed ● S mg. of iodine pw ml, of N-
3.12 Starch indicator solution. ~=~e n~~r Of ml- of the l~dlne ~l~tlon
C==the wmentratlon of the iodine In mg. per mL
3.13 Standan.i iodine uolution, 100 mg. per
S=the number of ml. of eodlum thloeulfate ueed to
liter. titrate the solution
Methed 4111
Method 4131
April 14, 1967
sunlight. The method is not applicable to hard designed to carry specimen helders in such a
or semihard robbers. The deterioration result- way that the surface of the specimens are 18%
ing from the exposure is determined by ob- inches *IA inch from the center of the arc. The
serving the nature and degree of cracking and frame work shall rotate around the arc at a
checking and by comparing the tensile atmngth uniform speed of one complete revolution every
and elongation of the exposed specimen with 2 hours.
that of unexposed specimen taken from the same 3.1.4 Spem”nwn holder suitnble for mount-
piece of mnterinl. The specimen is expwd in ing tlie specimen verticnlly while it is rotated
.tQestretched condition. The quantity of rndia- about tile carbon arc to provide uniform dis-
tiOn to which the specimen is exposed is meu- tribution of light, The holders shall be de-
sured by means of the decomposition of uranyl signed ta accommodate either one specimen 2
oxalate solution. by 6 inches or two specimens each 1 by 6 inches
2. SPECIMEN in size and to stretch them to nny elongation
2.1 The specimen shall be a piece of the in- up to 20 pcrcento A suitable holder is shown
Sulst.ion or !&ath tah frwn the inq?w!i or. iii figure WM.
uni~ It shall be not lass than % inch in width 3.1.S A cylindrical d~m of corrosion-
and 6 inches in length, and shall be buffed to resisting material for enclosing the lamps and
a uniform thickness of 0.35 Y 0.005 inch, If the framework. The cylinder shall be equipped
size of the insulation ia too small to permit prep- with a protective cover for shielding the opera-
aration ofs specimen of the above dimensions, tor from radiation from the nrc, and overflow
a tube specimen six inches in length maybe used. for carrying away the water from a spray, and
3. APPARATUS AND REGEANTS n sliding door to permit access to the specimens.
W The appm-atus and reagents shall be as 3.1.6 .4 fresh water nvray no2de mounted
follows : inside the cylindrical drum in such n position
3.1.1 A 2i9ht wwce consisting of a vertical that each specimen will be exposed to n complete
ventilated, flaming carbon arc designed to ac- wetting throughout its length one time during
commodate two or three pairs of carbons, num- onch revolution of the framework. Each noz-
ber.22 upper and number 13 lower; the arc to zle shall be adjusted so m not to strike the Corex
bum between only one pair of carbons at a time. D filters and to deliver between l% and 2 gal-
The carbons shall be of the cored type sunshine lons of water per hour. The water shall lM
carbons (of the National Carbon Company or maintained between 10° and 25”C. (50° and
qual ) designed to duplicate as closely as pos- 77°F. ) during the test.
sible the spectral distribution of sunlight. The 3.1.7 An ezhau.@ ,fam for effective y venti-
arc shall operate on 60 amperes and 50 volts lating the arc, with a capacity of 100a 20 cubic
ncross the arc on altexmating current or on 50 fept per minute.
nmperes and 60 volts across the nrc on direct 3.1.8 A thermometer for determining the
current. temperature of the air at the position of the
Method 4131
I-,esd
I I l-t-”-
II
U--)--&
I
L
\ J
C.ao—
-L
?
SW
FXOUU 41NA. Rubber holder for Hebt axtnz All ~rts exc-mt rods to k made of aluminum. Rods to be made
‘of mod. -
specimen in the drum. The bulb Qf the ther- taining the current of the arc approximately
momet.ar shall be shielded by a cylinder of c-onatanL The equipment shall include s con-
bright metal foil 2 inches in diametar and 2 stant voltage regulator to maintain the input
inches in lengtL voltage at 220=1 volt. It shall also contdu
3.19 A uuita~k frumework, complete with a push-button station for starting and stopping
oablea, pulleys, and counterweights for raising the unit, interlocked with the main line cxm-
the lamp for inspection and repkement of car- taetor to insure complete electrical isolation of
bons. the am equipment when changing ohms or
3.L1O Electrical control equipment for au- working on the interior mechanism of the lamp.
tomatic operation of the entire unit and main- 3.1.11 A cell of transparent fused quartz for
Method
U81
4 mtoclmum!l
u PlqMMionl 8torwfad di8puhw
of da ~ 90hltiO~ 8.L14 and 8.L15,
mRy be ~~ in OdiM~ difkd ligh~
UI AU R pottasiumprmsnpmte Bolu-
tioa Sha be prepw’ed by dbolviag 8.16 g’mms
Ofresgerlt gmdeindistilled wdarand making
the mdume b 1 liter. The Dolution ddl be
wtssideforl mdinc&kplscs thm Wrod
qcwtiglu~h~ndtiti
hlcgbtippered boulepmtcda dfrtlmthe
l@&?y&haqooding of bM@nL
wl’lta~ solution shall be
plupall)d by didtig 640 gr8ms of Teqent
@a hydmtad OXdiO aoid (H,(&O, ● 9H,0) or
4.80 grams Of snhydrtms oxdio aoid (IWO,)
=P-* the ●tinometar 00h1tion to the radi8- and4.90gXWr@ofresgwXtg18&my18ulplWta
tion fmm rho m of the desiga uid dinmsions
ShOWI) in iigm 4181B.
(uOwso.
“azo) illdistilled wstarand dihtad
U3.2 A * for anclosing the cell uoept
for tha faca which in expoeed to the light being
melm’eld. The exposed Crom-motiod - of
theoell ahdlbemeauured withui~ of
●tleult=lpamrtk ‘rheiddeoftheold
holder shall be completely cxwered with s dull,
black enamel paink The holder shall be de-
signed to take the ph~ . UA-
.4 “ .S{m-
or..- -. ho!d?r
andsooomtructa dthatth ooultarofthmodl
ocoupiw the- mlatire horixmtal pociti= u
b canter of 8 rubber 8pecimn.
SS.13 A ~~m~
4181c.
&L14 Rodiation adbWm4w dutio%
&Lls &uzuan#wkdoR
I t
Method 4181 --
to 1 littr. The solution shall be stored in ● glaa oall shall be hnroedktel~ placed in the holder
stoppemd bottle paintd with s heavy ooat of to p!lwant axpoaum of b dutioo to light.
black paint to protact the solution frmn light. The all holder shall be mounted 00 the cylin-
An mwtnstic dispensing burette shown in 6g- drical rotating framework in the 4ighting unit
um 4xMB when heavily coated wi~ black paint in s similar position as that of ● rubber speci-
to exclude light in euitable for storing and dia- men holder. The ‘solution shall be expomd to
- the 60]utio~ the @ht under ZIO~] opmting con(htiona for
4.2 Stuuk.rdization of aolutio~ The s suitable period of tinm The time of azpoeure
evaluating solution (potamium permanganste) of the actinometer eolutiou shall be eu6eient to
shall be standardized against ~nt grade dacompom not k than 10 pemant nor more
eodium oxalsta in the usual wsy, with such pre- than 60 pemant of the oxalic acid in the call.
cautions that its etmngth ahnll be known within At the end of the expoeum peri~ the actinom-
an socumcy of ●t J- =1 pement, The ebzr solution shall b transferred fmm the mll
stmngtb of the potamium pernmnganata shall to ● 200-mL beaker and then titmted with the
be expmaed in terms of miuigrama of anhy- -~ ~ e~l-=lution ss
droua oxalic tcid per mL of solution. The B&L deecribed in 4.% The quantity of the evaiuab
nometer solution hall be titrated against the ing BoMion ~aimd for the titmtioa till he
Andard potaaaium permanganate, An accu- d~gnated as V,. A rolume of the adwmeter
rately measured volume of 50 milliliters of the acdution qua] to that used in the ~ OeU
actinometer solution shall be transferred to a shall be titmti under the ~tditions,
tall form 200-milliliter beaker, 20 to 25 milli- cnmtting & expouure to iigh~ and Qlmquantity
Iibm of distilled vmt.cr addc~ and the solution af parmangarmte solution mquimd fomthe titm-
acid&d with 5 milliliters of 1 to 3 sulf uric acid. tionrwordedu T’* T&qWlt@ofoZalic
The beaker elmll be covered with ● porcelain ●cid in reg., Q, decompcA by the ndiat.ion is
dish a~ld the solution heated to 95° C. (203° F,) giren in the quutiun Q-u ( VFVJ ‘ivhem a
b ● light-proof water ba~ tranafermd to an is the number of mg. of oxalic aoid quivalent
o-pen glare water bnth and maidabecl at t~b to 1 ml, of evaluating dutiou. The qunnuty
tarnpemtum while -g on ● fla~ whita-glas ordoaageofdiatknie~aa Q/A and
ham The solution shall be clearly aeon by lighl the intanaity of Mdiation U Q/At where A is
from the glam”baae illuminated by a Wnylight” the~ofthe~inquam~md t
lamp. The hot eolution shall be titmted v@th iathetimeofeqmmiu~
the tindard potsmium permanganate eTsluat- 44 Expomm of Spedmea
ing solution from a dispensing bumtta while 4.44 Unka ~ specibi in the de.
stiming constantly until ●n orangs color is ob- tail qmcifidon, fhe total doeagu of radiation
tained which pemiste for at least 80 eeconds shall be lJ6XllP rug, perquam docimoter with
while stirring. The titration shall be conducted ● pine or minus tohmaoe of 9 pertark Ap
in such ● way that the ?ohun~ of solution used P maimat+ 60 houm axpoaum should b d-
am precim to within *0.05 milliliter, ciant for thin donge.
4d Calibration of radiation. The in- 442 Unleaaotherwiae spededinthedetail
tanaityof radiation of the light shall be m- eti~ tile S&U@ and dongation
umd in tame of the milligmms of oxalic acid ~rnothode 8021aad 6061, andthenatum
&ompaed per square decimetar per minut+ and degree of emaking and checking, L4.5, shall
and the quantit~ of mliation in any given pe- be used to detarmiue the detariomtion of the
riod of time ehall be measured in terms of the matarial due to aging.
milligrams of oxalic acid decomposed per equam 4AS UnI~ otherwiaa specided in the ded
decimeter. An accumtely meazured volume of epecidcatio~ the ~ mounted in the
the actinome&r solution shall be tmnsferred to holder, shall be etmtched to an elongation of
the quatiz mll from t dispensing bmwt.t~ The 10pament within 8bouraaft4rit haa k
Method 4131
buffed. The specimen shall be held in the be determined of the specimen as described in
stretched position for 16 to 24 hours at a tam- methods 3021 and 3031. If other properties am
peruture of 38° = 1“ C. (100° =2° F.) to aid in required the specimen shall be tested ~ de-
the blooming of the protective waxea. scribed in the specified method. The same
4.4.4 Within 1 hour after the precondition- physical tests shall be conducted on aged and
ing period, the stretched specimen mounted in unaged sp.ximens for the purpose of compari-
the holder shrdl be placed in the aging container son in debrmining tho degree of deterioration
in such a position as to receive full mdktion of the aged mat..arial. The dimensions of the
from the arc. It shall be exposed to the light specimens for use in calculating the tensile
until the total exposure is equivalent to that strength and elongation shall be determined
required to decompose the specified quantity after exposure.
of oxalic acid (4.4,1). At least one xneaswe- 5. RESULTS
ment of intensity of radiation shall be made, as 5.1 Calculation. The change in tensile
described in 4.3, at the start end the end of each strengt& elcmgation or other charactariatic of
exposure and at intervals of not more than the insulation or sheath of the inspection unit
24 hours during the period of exposure. The due to aging shall be calculated as follows:
temperature of the air in the vicinity of the o-E
specimen shall be maintained at 45° A 5° C. Change In charscterlstlc, percent=~x lW
——
(113” = 9° F.) during the exposure period, by where:
controlling the temperature of the room and the O=the valoe obtnlned on the unnged insolation or
ventilation of the space surrounding the speci- sheath of the Inepedon unit
E=the value obtained on the nged Insulation or
men. The filters or other enclosure shall be
sheath of the lnspmtlon unit
cleaned at least once every 24 hours during the
exposure period. 6.2 Unless otherwise specfied in the detail
4.4.5 .\tthe end of the exposilre period, the spezificntion, the number of specimens tested
hnldw with specimen shall be removed and the from each inspection unit shidl be as required
specimen examined immediately by means of m the method of kit, 4.4.2, used for determin-
binocular microscope for cracking and check- ing the deterioration of the insulation or
ing. The specimen shall be removed from the sheuth.
holder and set aside on s flat surfaoe to rest for 5.3 The change in the characteristic of the
not less than 16 hours nor more than 96 hours Cumulation or aheith of the inspection unit shall
at room tern pemture before physical tests are be recorded to the nearest 1 percent.
made. 5.4 by cracking or checking of the ma-
4.4.6 At the end of the rest period, unless terial of the inspection unit shall be recorded.
otherwise specified in the detail apecfication, 55 The dosage and the elon@ion used for
4.4.2, tensile strength and elongation ahdl alao stretching of the specimen shall be recorded.
Method 41s1
buffed. The specimen shall be held in the be detmnined of the specimen as deaoribed in
stretched position for 16 to 24 hours St s tam- methods 3021 and 3031. If other properties Bm
pemtum of 38” * 1° C. (100° *2’ F.) to aid in required the specimen shall be tested as d-
the blooming of the protective waxes. scribed in the specified method. The same
4.4.4 Within 1 hour after the precondition- physical &ts shall be conducted on aged nnd
ing period, the stretched specimen mountsd in unaged specimens for the purpose of compari-
the holder shall be plnced in the aging container son in determining the degree of deterioration
in such a position as to receive full mdintion of the aged material, The dimensions of the
from the arc. It shall be exposed to the light specimens for use in calculating the tensile
until the total exposure is equivalent to that strength and elongation shall & determined
required to decompose the specified quantity after exposure.
of oxalic acid (4.4. I ), At least one measure- 5. RESULTS
ment of intensity of radiation shall be made, se 5.1 Calculation. The change in tensile
described in 4.3, at the start and the end of each stren~ elongation or other characteristic of
exposure and at intervals of not mom than the insulation or abed of the inspection unit
24 hours during the period of exposure. The due to aging shall be calcuhtad as follows:
temperature of the air in the vicinity of the O-B
specimen shall be maintained at 45°35° C. Change In cbaracterlstlc, ~rcent==—~ Xloo
——
(113° =9” F.) during the exposure period, by where:
controlling the temperature of the room and the O-the Talne obtained on the Unng@ Insulation or
ventilation of the space surrounding the speci- sheath of the Inepwion unit
E-the value obtained on the aged Insulation or
men. The filters or other enclosure shall be ahedh of the inspection unit
cleaned at least once every 24 hours during the
exposure period. 5.2 Unless otherwise specified in the detail
specification, the number of specimens tested
4.4.5 -\t the end of the expos~lre period, the
hnldm with specimen shall k removed and the from each inspection unit shidl be as required
specimen examined immediately by means of m the method of test, 4.4.2, used for determin-
binocular microscope for cracking and cheok- ing the deterioration of the insulation or
ing. The speeimen shall be removed from the shedh.
holder and set aside on a flat surface to rest for 5.3 The change in the characteristic of the
not less than 16 hours nor more than 96 hours iRaulation or sheath of the inspection unit shall
at room temperature before physical t@s are be recorded to the nearest 1 Pe.rcenti
made. 6.4 by cracking or checking of the ma-
4.4.6 At the end of the ra period, unless terial of the inspection unit shall be rewrded,
otherwise specified in the detail specification, 5.5 The dosage snd the elon~tion used for
4.4.2, tensile strength and elongation shall also stretching of the specimen shall be recorded.
Method 4211
April 14, 1%7
Method 4221
April 14, 1%7
Method 42Zl
52 Unlesn otherwise specified in the detail 698 The ohange in the ch8r@&atic of the
specification, the number of specimens testad insulation or sheath of &c Qection unit ehdl
from each inspection unit shall be ae required be moorded to the nemd 1 pement.
in the method of tes~ 4.2,uaed for determining 5A The tempemtur~ and time of expomwe
the deterioration of the insulation or sheath. !&all be lmoorded.
Method 4223
April 14, 1%7
1
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Method ~
Mtxh(MI 5011
April 14, 1967
~mdrei b, W*
.. the nominalOutdda
Sias ~ aonduti AW(3 0? drouiar & Nknber Ofadjaod turns cuu.;atf&a
multlpliad by tho
following ktor
No.8arldarnal&r 6
No. 7 * No. 2, Inalualw 6 ;
No. 1 1 a
N& OtOWOO 180” band 2
226,000 &Ukudob 1S0” band 6
Method 5021
Agsil 14, 1%7
Method Sa@l
Where :
T.-the th!cknea n! tba bsnhlon o! tba sgdmea
Mom beat t?ea-~ lnc&
)
Method 5111
April 14, 1967
1
Downloaded from http://www.everyspec.com
Method 5131
April 14, 1%7
Method 5141
April 14, 1%7
DRIP, CABLE
L SCOPE speeimen for s dietance of approximdely ~
11 This method is intended for use in debw- inch The specimen ahnll be supported ver-
mining the ability of eutumnta and tiniehing tially by the &e end of the conductor in the
ma.bwids in cable to resist flow at elevated tem- oven which baa been preheated to the required
peratures when the cable ie “m c vertical pcmi- tamperatum. A ehmt of white pnper or any
tiom suitable container shall be placed beneath the
% SPECXMEN Bpecimen in such s poeition thst it will catch
Z1 The epecimen shall be 8 piece of the in. any matial which dripe from the spec”ixne.m
epection unit not k than 30 timee the over- The epecimen shall be heated for the required
) all diamehr of the U&lQL time and .st the required temperature. At the
& APPARATUS ●nd of thee-m period, the {ower end of the
u The Sppamtue ehdl be as follows : epechnen shall he examined for globules of the
S&l A c+cw?uting nir oven of sufficient eize eaturanta or finiahkg materide and bubbles on
to accomndat.a the specimen in a vertical po- the surfn~ The paper or container shall bs
sition m}d c~pnble of nmintaining tbe specimen examined for any drippings.
at the required tamperatura within* 1° C. (2° 5. RESULTS
F.). 5.1 Unless otherwise specified in the dehil
U2 Means for supporting the specimen in specification, epecimens from ench inspection
s vertical poaitiom
unit aid be tested.
\J? 3.1.$! A .*Av~tof pnprr or a cnnto%~r for CO1.
Y \ 54! The resistance to dripping of the fibrous
]ecting any drippinge from the specimen,
rnvnnng n? ths irqwtim unit Rhall he the re-
4* I% OCEDU-M
U Unlesg otherwim epdled in the detail eulw obtained from the specimens tested.
epeci!kntion, the apeeimen shall be uubjccted to 5S Any exudation, formation of bubbke on
s tempemture of 80° * 1° C. ( 176° = 2“ F.) fors the inspection uni~ or drippings on the paper
period of 1 hour. ehall be Mconled.
42 All comring xnd iM&tiOll ahd be m- L4 The time and tanpemtura of expoeure
mowxl from one end of the eonduotor of the shall be recorded.
Method 5211
April 14, 1%7
( .
FUIKMABILITY, HORIZONTAL
L SCOPE epecimen wham the inner blue cone of the flame
L1 This method ia intended for UMin detm- ia to in applied. The indiator paper ahail be
mining the tlame-ratadant propertied of in- motied just sullicient for proper dheaion
sulatad wire and oable without metallic cov- and wrapped onoe around the epecimen with the
m. St ie particularly ●pplicable to b _ aide towarda the wim and the en&
hne-retdant fibrous wvaring of vmiiahed paated evenly togethw sad projected ~ inch
dOth inadatd ti and cshb fmntheapecben ontheoppoeiternde towhich
Z SPECIMEN the be u to be sppiid The Tirrd bunmr
() 21 Theapecimen ahalibeapiece
apection unit St Met 10 incht, in length
of thein- shall be phead in a mrti~
9ameadjueted to6inchea
padtion and the
in height with the
8, APPARATUS inner blue ame l% inh in haighk
Xl The apparatw shall be aa follows: 4S The burner, in ● mrtical poaitio~ shall
2Ll ?’iwtA4mnikr appmxinmtoly B inciu9 bepiaoedeo thattbeinneroone jwttouchesthe
( wide, 14 inchee deep, ●id !24 inch high made
of sheet metal. The chamber ahai.i be opn at
under aide of the epirnen at a point midway
between the two indicator pqera. T’he flame
the top and front and quipped with aupporta shall be directed against the specimen for
8 inchee ●part for. hoiding the specimen in ● exactly 80 aeconda and then removed. After
horizontal position during the test= -of the epecimen haa~ the indicator
u rid bum having ● bom of ~ inoh” papem aid he examined to determine the
-d ● 4-incI.I iengch dove the primary air irdeta. maximum diatanca the 9ame extanded in either
V
{{J, $ 3.13 Supp?v of fuel qua, butzne or eov;w- direction from the center point of application
i, ,U W. The gua aym.eu ahail be quipped with of the *
( oontroia for maintaining the flow of gas to the 6. RESULTS
burner U Unifom pmre. &l Unk othemiee qpecibd in the detail
U*4 watch m dhu d-i- Which will mg- =.y SPBcJn from 4 inapeo-
hter the tie in mconda.
SJJ L!kd ad ~duati to % inch or bar U The llammahility of the fibrous covering
or its decimal equivaien~ of the kaiation or ehesth of the inapotion
L PROCEDURE unitahallbe the~tobtained from thespeci-
UThea#xnenah allbefmefromme - Inentmtad.
0h8nicai damag& T&l 9ammAMutyteatahau UWhenmom than one specimen ia
( bearried outin~mom free frwndrdt or a the ilammabiiity of the fibmua owering
under s hood in which the 90W of air ia not of the hwpection unit ahail be the average of
sukient to ●ffect the tlama. theramlts obtained fmmtbaapecirnwti
.
42 The apeoimen till be placed in B hori- 63 aammabiity
The (lwimum diaknoa
( I zontal position in the chamber on supports 8 the 8pecimm burned in either direction from
inohea ●part. Two stripe of indicator paper the oemter point of cppiication of the fiarne) of
shall be attached to the epedmen 4 inch- ●* the inapmtia unit ahail be recorded to the near-
each paper being 2 inches from the point on the cat~inoh
( ..
Downloaded from http://www.everyspec.com
Method 5221
ApdI 14, 1%7
FLAMMABILITY, VERTICAL
L SCOPE ‘ 4 PROCEDUBE
lJ This method is intanded for use in d*r- &l T’heflammabili~ tdshallbecanied
mining the flame-resistant prop@im of firms outinaroom fifran drafter mders hood
ooverings, other than tapeq of insnlati wire in which the flow of air is not sudicient to dad
●nd oable without metallic co~- It is dso theke. [email protected] ehallbefrea from
applioeble to the determination of the flame- mdaltioel -
amtardmt propert.k of plastic .bnlation and 43 Oneendofthespecbenshallbefastaned
jacketd. inthechamberbymunaof sckmp. Theflame
2 SPECIMEN i.ndioator paper ehdl be ~ to the speci-
21 The specimen shall bes pieca of the in- amn 10 inch= ●bove the point where the inner
spection unit ● pproximately 18 inch in length blue coneoftheflame is to be applied. The indi-
from which ●ny cxwering over the oovering to oator paper h?i be moistaned just dcient for
be t@ad has bean removed. proper abion and mpped onoe aronnd the
& APPARATUS ‘specimen vrith the gummed side toward the
3.1 The apparntus shall be M follows: specimen and the ends pasted evenly together
S&l Test chamber ● pproximately 12 inohes and projectad M inch from the specimen on the
wide, 14 inches deep, aud 24 inches high made of aide opposite to where the fhme is to be ● pplied.
meld shes~ The chmber shall be open at the 43 Tho burner shall he adjusted to produce
tQp and front and equipped with supports for a fhune S inches high and ● i) mer blue cone Lb
hohiing the specimen in a mwtial position and irmhsa high The burner n- .ted on the 520°
keeping it taut dining the test. angle blo.~k shrill be placed agriinst the jig in
o ““-- ?““ WI
3.:4? Uuvfny ..84,7
~w. ,Gc;, h..t-e~ .-IMe~~~?bfi.
B,U-.WW“. a-.. .b WA
-a bb. - +h. t +k .+;*O1nlmnm
A& Uk VM6 ~~~= & -.. d! ye . . . . . ~.....
&ttt. The pa systmn A-d] be equipped with through the stem of the burner passes through
controls for cnaintiitiing ~he flow of p to the the axis of the epecimem The jig shall be ad-
burner nt a uniform prmmre. juti so that there is ● distance of 1.5 inches
&13 A ak42 & gnduated to %2 inch or between the tip of the burner stem and the sur-
finer or its decimal quivalen~ faoe of the speoime% as memmd along the
8J.4 Watch or other timiay device which ●xis of the burner etmm The height of the
will register the time in eeconds. . ______ _ specimen shrill be ● djusted so that the point of
9.13 A Tirrell burner hnving a bore of ~ oontact with the dame ahd] be not less than 8
inch and 4-inch length above the primq ti inches from the lower end of the speeimen.
inlets. The bumcr shall hnve an sttached pilot 4.4 The pilot of the burner shall be tightad.
light and shall be mounted on a !MOengle block The valve supplying the fuel gas to the burner
in the heating ckamber. shall be opened and tho dame Automatically
3J.6 An a$j@abk atsel an g 1e (#g) spplied to the specimen for 15 seeonds and then
attached tu the bottom of the cbmntm to insnm the valve cloeed for 15 eaoonds This operation
the correct location of the burner with relation Shell be XqJeatad 4 additional times.
to the specimem 45 At the end of the fifth application of the
S.1.7 FZanM Jmficutom cnnrnstin~ of strips flnrne the perczmt of the extended portion of
of gummed krnft paper, 5 nlils iii uumilml dJuk- the indicator paper which is burned shall k
nesa and ~ inch in width. This paper shall con- eetimatuf and recorded. The duration of the
form to type III, grade B, PPP-T-4S. burning period of tie specimen ●fter the fifth
application of the flame ahdl be observed and
the valve mxzmkKL
Method -
Method 5231
April 14, 1%7
.
FLAMMABILITY, SPARK METHOD
1
4J3 Unk othemiea qded in the detail d end the PIIWS*f&d ●WBy from the-k
~iktion, for d unrmnomd =ble+ where !IIM maximum dksnee which tbe ikne tmv-
tho ikmition time is lees than 60 eocmn* the eis along the mwfsoe of the spdrnen before eS-
current in the heating coil ehsll be turned off tincticm Alf be miemmmdfrom the top of the
60 -de after being turnd o~ bester coil ●nd modad as the &etuM8 whi~ .
4.L3 Unless otherwise qwcilied in the detail the fhme *rek
epeciiicntion, for rdl unarmored eablq where 4,s Time reuahed for aetf+stinctiom
tbo ignition time’ is gmmter than 80 MXWA the The timq in H* that the specimen con-
current in the heating coil shd] bs turued off tinues to bum after the current u cut on in the
when ignition OrxUrh bester coil un!il the ~tion of ●ll flaming
4Z ‘i%e lower ml of tha specimen ehaIl be 8hall be mrorded u the time of eelktinctiom
wappcd with varnished cambric or, similar & llESUL’!%
rnnterial in such a manner that say gasu rs- u one spmimen fmun each inspection nait
lessed though this cnd shell be diserted t~ ebalI be *
wad the Spark pla~ L1.1 The ihmmebility of the inspection /l&
43 Time of igdion. we specimen shall unit shrill be the results obtained ~ the npeci-
be renterad in the hater eoiL The spnrk PIW rncn turte&
●nd flume ~b~ shall be placed in pofdtion tmd 62 If the reenlhrfzmm one spec”hkn f~il to
the chamber sh:tll k closed and the rcntiluting me& the spwified rqnimnents, four additional
fan sturted. The wntch or timing device dml~ spmimens shall iM t@d
be Kt.arte(l simulltuwously with the oncrgizing 5.21 The fianlrnnbility of the jnspertion
of the hm tcr coil hy the current in :wcordnncm unit shall ho the avemge of the mmdta obtained
with tublo I and tl~c energizing of the spark from the fin epmimens *
plus Ibmition elmll be ronsidored as occur- 63 The iime required for the ignition of
ring wlm)t the fi:lmc transfm-s frwl} tllc csrnping
tb kpwtion unit elm!] be reccrtkd to th~
gnscs to the surfnre of II]e specimen and con-
nearest second
tinws [here. Fl;lshes which nmy occur in the
5.4 ‘I’lie time mcprimcl for enlf+xt inrtion of
gaseous space prior b oblaining s sustained
flame shall be disregarded. The tinie from tho the inspection unit ebaii be mxonled to the near-
stmtiug of the current until ignition shsll be - eeconcL
recorded ss the ignition time. 6.S The dtieeI the fbuns.tre?ele along the
4.4 Distance of frame travd Immedi- inspection unit eimll h mmx?iad to the nammst
ately after ignitiou has occurred, 4.3 the cIG ~ incib
tricnl cupply to the spark plugs shall be turned S3 Thetime of btiag8bubmdd
wthod 6011
Aptil 14, 1%7
Method 6021
April 14, 1%7
Method 6021
value recorded as L. If a W%eatstone bridge R
Xtedstince ●t 20° C., ohms= —
1+0.00S96 N (T-20)
is used for measurement the length of the speci-
whine :
men shun not include the portion of the-con- R-the reststnace of the spedmen ●t the test tempe~
ductor held between tho jnws of the binding ature, ohm-
poets. IQ order to avoid raising the tcmpem- ?’=th~ *nD:~rature of tbe test, “C.
ture of the specimen nbcwe tlmt of tlje surround- h’=tbe trmpernture cuerl!clent of reslstnnce of the
ing medium (air or ]iqllid both), tile mngnitude conductor rclntl Ve to soft cowwr. The follow.
lng mlues of N shall be used:
of the current shall be kept low nnd the time of Soft or mmmled copper-L6fW0s
its flow through the conductor shall be kept Mert!usu-hnrd.drnwn: SIZW 1/0 and lsLrL?er~.976.
short to minimize the change in resistance due Smuller than l/lL&M6S.
to rise in tempature of the specimen. The Hard-drawn: Sizes 1/0 tlnd larger+l.f)716 -
specimen shrill be connectad to the testing in- S1- smaller t!snn 1/0-0.0616.
strument as described in Al. 5J! Factory tesL
43.1 The resistance of the specimen shall 5.2.1 Unless otherwise specified in the detail
be maaured nnd the value recorded in ohms as specific:.tion, the entire delivery of the wire or
R after indications have been steady for not kss cable shall he tested.
than 1 minute. The ambient temperature shall 53.2 The resistance of the conductor of the
entire delivery in ohms per 1,000 feat shall be f? JQ
be measured to an soouracy of 0.s” C. and the
vnlue recorded ns T. recorded to tho ncnrest 1 percent.
5. RESULTS 5.3 Laboratory test.
5.3.1 Vnlesq otllerwiw sl)ecitied in the d~tail
5.1 Calculation.
spcci fication, one specimen from each inspection
5.1.1 The resistance of the conductor per
unit shrill bc tested.
1,000 feet shall be cdculat.ed as folknrs: 5.32 The resistance of the conductor of the
Resistance, ohms RGS1,000feet-+x 1~ inspection unit shall be tho result obtained from
where: the speci nen tested.
R-tiIe rssisunce
or tbe specimen or the Ienatb of 5X3 When more. thnn one specimen is tested
aptximen potential conductors, ohms,
between from each inspect ion unit, the resistance of the
L-the length of the s~men or the Iezsgtb of ~1-
conductor shall be the avcmge of the results
men between potenthl conductom feet.
obtnined from the specimens tested.
5.12 Resistance measurement made ●t S3.4 The resistance of the conductor of the
te.mperntures other than 20” C. shall be cor- inspect ion unit in ohms pm 1~~ fet ehall be
rectedto 20” c. as follows: recorded b the nearest 1 percent.
k 1 The lQf)=stuS %hd be ●% fOi~OWS: 4.3 The teet vol~e shall be as specified tn
the detail epeclflcatlon or epecfficaUon sheet.
3. 1.1 A %ui@le eontatner, q- with “
stirrer, in whtch the specimen may be immersed 4.4 The Inmktton resistance tsst may be
L-bwatt r. m=+ &for@ tlw braiding or finishing operatton
during manufacture, but not before nnv vulcaNz-
3. 1.2 A standard res{@ance, scale, ●td tng procees. Stngle conductor cable shall be
shunu of any 8uI@le pattern. tested tmtween the cmductor and water in which
it is immereed, Lead covered single cmtuctor
3.1.3 A d. c. vol?a@ source preferably a cable As.11 be tested prim to application of the
LWtery of dry cells, that will supply a voltage ‘ lead sheath. Individual conductors of a
of tmt less than thatepedftedinthedetatl multiple cmiuctm cable shall be bsted before
8pecXtcatton or specification hee~ aeeembl y se described for single codwtor
cable. After aesembly, the multipk-oomtuctor
3. 1.4 A suitable instrument for rneneurtng cable Aall be tested between a stngle comiuctor
the resistance that wlI1 give an Rccumcy of auahwt alf other cmatuctors arranued in two or
wtthtn 10 percent ad a sensithtty of 1 percent more groups for tes~ these tests may be
of full scale deflecttm comfucted withnut immerelon or witi immersion
uetag the water se a groti Mer covering, a
3.1.4.1 A gahoometer of fatrly high lea+cowrd cable abalI be tested betwxm ●ach
eensiuvtty and havtql the loflowim (fuaMfIcauone oomiuctor ad the lead she or be-en each
has been feud to meet the accuracy rerfutre& cmductor ad Its contiguous comtuctors and to
The gatwummeter constant 9hall ha mt less than the ~ wtthout tmmeratom
50,000. The means for tndtca* the denectlon
shall produce a sharply outlhed t@kation on b &5 TIWepectmen sballbetlnmereedtn
BCS2eI,and the ~enecttna shallbeaot less thuI water for a period of at least 12 hours before
100 ctMsionn (measured from aero) when the applkation d the potenfiaL Unleea otherwiee
vartable shunt has been stt to determine the con- speetfted tn the detail epectfkation or spoctfica-
stant of the gahmmeter. The reststmce of Uonahee$ tapwaterwltfbeusd The water
tha shunts and the calibrating redetor shall be Ln which ti epectmen te tested whtle tmmerseq
checked from the @ Ume. as well as the lead covered ad mulUple txm-
~r cable, ehall be at a temperature between
3. 1.4.2 Any other eultable qutpmtnt 10* ad 27” C for at haet 30 mtrutes before the
arranged to apply a voltage of not iess than that tes~ Tba ●rxts of the specimen 8hall be kept
epeclfktIn the de&aJl spectfkation or apecUka- welf above the surface of the water and the
Uon sheeL covertng removed from the surface Df the
lnsulstton for several inches at each em! in order seriec wtth the @mmmcter m prfxhw a gslvs-
to reduce surface leaksge. The ●nds of the speci- tmmeter sale deflectbn of on tie dlvbkq
men 8heU be dippm4 @o melted psrntfln or other either wtth m shunt or for shunt coaat8at equal
satisfactory materl.sl to mhhntae the effect of tountty aldthetiue ofvohs.geequal tothai
moisture tn reductng tnaulation resistance be- required tn4. L (lap4rqF@e 4.8 Md5ti
ween the covering a.rd comiuctor. The water in conetits Sasdsfordnmt*~ *ae-
the bath shall be ctlrred well to rnatnt81a a eumedto bethe1’8ii00f tbeisppedr9$tSkoce
untform temperature throughout the batb during the tothetotal twtst8aoe ~tishuat (Ayrt0atype)
test, The specimen shall be sssemtded in tbe test rm~y ~ct8d stm+es * galealumebr
circuit es deocrtbed in 4,6. . termtasl. )
.
4.8 Totiowf oranykahgecunwatto
4.6 The test Instruments shall be mounted grourd -m @ -ry, Irntrumoats, esd ell
so thst they wilt be reasonably !ree from vtbra-
mwcttmw thegahaometer defhctkw rmt
tton end wU1 not be tiecteci sdversely by kcsl correspomltag shuatsmetsntssbsll blW-
cmdttions. A typical test C&CUt~ 8S - in
Curded fitb the ~ bew9ea m battery
figure 6031, shall constst of 8 K!’OUWMgaN8no- lesd C @ eldter the speetmenarx opm
metsr wtth Amton shunt b seriet wfth ● suttsble Tbe ~~r Mkctioa aad m.#USctUIt :
swttc~ s kmmn resistance, and a battery wtth & *r tbe IosulsUon re8tstaaoe of ti~ctmeq
the negative terminal connected to. one Qnd of the shdlthen berecordedwfththe~ hdC
conductor of the specimerb The circuit shall be connected b one ed of the coducbr of the
completed through the inter ●lectrode or metaltic specimen at potnt 11. The galvsnometer deflec-
sheath which shall be &!ounded. tion shall be recorded after an eiectrtftcation
period of 1 minute. U the cm af 8 sl@e coil
“ 4.7 The gdvammeter constant K shall be de where the deflection ts SMS.Had is &cre&;ing,
determmod with the battery lead C connected to the galvamxnetsr scale readtq -y & tsken
f
grvufd at& The Qvammetsr shunt constant at the end of 15 seconds.
IS defil]ed as Uie vzlue of resMance required m
GALVANOMETERS
/
b GALV
SHUNT
I I
i+$fa-’
FIGuRE6&l
METHOO 6031
TABLE L
-.. - . .. —--- ------ .- —.—— --. —
,. . . .. . ..
Temp?raturc
------
● ~ ~ -“=-; “-;- “;;;*;,
I
:
RW TW
----- J .- .—------ . .-— -- i
.. . .. .
i—
50 0.60 0.79 0.73
0.63 ; n. Cl 1
0.76
I
:: 0.07 0.82 f 0.78
53 0.71 0.84 0.80
&75 I 0. Bti .0.53
54 J
55 o. ?9 0.88 0.80
,
56 o. &!2 0.90 0.88
57 ‘0.86 0.92 0. !]I
0.90 0.95 0.94
:: 0.95 I 0.97 0.97
60 1.00 L 00 1.00
61 1.05 1.03 1.03
62 1.10 1.06 1.07
63 1. 1s ~ 1.10 L 10
64 1.22 1.14 L 13
85 L 28 1.19 L 17
60 L 34 i L 23 j 1.20
67 1.41 1.27 L 24
1.48 L M I 1.28
68 ~
1.55 1.39 i 1.32
% ! 21:1 1063 L 46 I L 36
I 1.55
71
72
! 21.7 1.71
1.80 I 1.67
1.40
1.45
?3 1.89 1.78 , 1,50
74 23.3 1.88 I 1*91 1.55
75 23.9 2.06 I 1.59
76 .:: I 1.64
77 i g; z 29 :: [ 1.89
78 25.6 2*40 2.56 I 1.75
79
—80
26.1
26.7 —:-
z 52
2.65 i.-
-. .-
2.75
— 2.93 —. L I 1.80
1.86
3 FED. TEST METNOD STO. NO. 228
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)lETHOOW41
Aprii 14, 1%7
METHOD 6111
ADrll 14, 1%7
—
IUETHOD 6111
)
possible so that 100 percent of the rated voltage 5.1 Unless ntherwtse speclfled tn the detatl
Of the specimen Ls reached in tmt less than 10 specification or specifkatton sheeg the entire
seconds and not more than 00 seconds. Failure delivery of the wire or cable shall be tasted.
can usually be determined by & midden current
increa..e and may be indicated by the trtpptng of
5.2 Whether the hedatton of the enttre
a circuit-bre.n.ker in series wtth the test coil, or
deltvery withstood the spuclfkt test vvltage
by other mewm, 1! may also h idicated by a
flash at the point on the specimen where break- wtthout fat lure shall be recorded
down occurs. If other means fal~ the lnamlatioa
resistance readings described in method 6021 5.3 The test voltage and ttme of application
will detect the voltsge wtthetand failure. shall be recorded.
S. RESULTS
)
. )
- Method 6121
April 14, 1%7
Method 6131
t
FED. TEST METHOD STD. ND. 2X
Downloaded from http://www.everyspec.com
Method 6211
Apil 14, 1%7
*
1
Downloaded from http://www.everyspec.com
●
Mothodtzll ✍✎
✎
Method 6221
“AwN 14, 1%7
I
Downloaded from http://www.everyspec.com
Method 6271
Au* 14. 1%7
&l
3.1.1 .4 -g;f~?J,’ W?nrwww hr;tl.”” Tim 5. RESULTS
bridge d)nl! IW (wlml~lo t, I 1,,, a .,, I i~)g t]w 5.1 Calculation. Thr di~lectric constant
n
‘t cnpwitance with a limit of error of 1 n\irromi - (K) of tlm insulntilm shall be cnhmhlted after
crofamd. It shnil be eapnble of mmwuring tha each immemion period ~ follows:
utpacitanm of a spcimen one side of whirh is x-ltMOO c b% r)ld
gromvlml. Trovicions S]lill) IN? m:ldc for wwk-
wbprr:
rmrt.irtg nnd disconnecting tlm specimen ~t the ~=!~~ ~.~e!tanm !a m!erdnrndm nf th? irnmm=d
spocirnrn ml of the leads conducting tho qwci- 10 feIMof the qwclrnen
men to the bridge. ~-~ dl~~r “-r ~~ i-nlati~ l~b~
3.1.2 4 *fi~’..- Anth in vrhich tho sptwimen d-the dismetw mm t be conductor, hcb
can bu JlnUVM!4$d. S~ Unlew otherwise specified in the detail
L PROCEDURE specificnt ion, one specimen f mm each inspection
4.1 17nlcse otherwise speciiied in tho detail unit shall be tested.
apecihcntkm, tho speeinw droll Iw imlnrmcd 5.3 Tlw cnpneitirwe change of the insn]ation
in vmter nt room tempemtnm not lew tball 21° of thp. inspcci.ion unit shall he the result ob-
C. (70° F.) f! r a period of 14 duy~ tained from the specimen taated.
4.2 Unless dherwiw s]wifiw] ill tIw {Ivtnil 5S1 lVhOn nwro than one specimen is tested
qwci6rntinn, rcndin~m Fhull b iaktw nftw !?2, from each inspect ion uni~ tha capncibma
1M, and 334 hotm of inlnwmirm in wntm at clwtge of the insulation of the inspection unit
morn lenqmnturc not lm thnu i?l” C. (it)’ F.). An] I lm tho nmnge of the IWUlta obtained
! 4.2 Tlte dian~ctrr of t hr slmcimen over the from the apminmns teatd
insulntiml nml ovw t.hr romluctor ahnll be dcter- 5.4 The capnritnnce c)mnge of the insnlmtion
minod as d~rilml il~ mkhod 1o11 nlld Iho of the inspction unib slut]] be ~rdod to the
valuo rwxwded as I) nud d *pert irely. ll~ei neamt 0.1 parcanL
middle 10 feet of t,ho specimen nhnll he im- 65 The temperature and time of immersion
mersed in did i!led wa*r for tho required shall be Kuxdd
Method 7001
April 14, 1%7
mtlmd 7011
April 14, 1%7
Method 7011
62 Unless otherwise specified in the detail ‘be the svemge of the meulta obtained from the )
specification, one epecirncu from ench inspection qmimcme tested.
unit shall be tested in each eolutiom 6A Any attaok on the fibrous covering or
●rmor of the inepeetion unit by the eolut ion
5.3 The absorption of the covering or irmor
ehnll be recorded.
of the’ inspe%ion unit for the particular solu-
5.5 The atmorption of the corerin: of the
tion used shrill be the results obtained from the
inspwtion unit ~hnll be recordrd to the nenrest
specimen tested. 0.1 percent.
53.1 When mom than ono specimen is teet~ 5.6 The immemion solution, expoeuro pe-
the nbeorption of the covering or amw of the riod, and expoeure tempexnture shrill be re-
inspection unit for the particular xdution 81MM !Xmied.
‘)
Met],,,,l 7111
ADtil 14, 1%7
h?ctht)d 7121
April 14, 1=7
-Cyclrs :
.-. . ,.. - ———- 1
-- - —-- ——
M8ximum num-
hcr of nprcimeoo
Win, diaw%cr (idll tf~tod for 2 c@H
in l~#l~nSOM
o.vifimil]- .. ... . . 2
O.l WO.OMI. . .. . .. . . . . . 4
O.I-IN.WO.(LW1 . ---- .-. . . . . . . . G,
“M O.MCS)11.0:;s1 . ..-
11.IHWIn o.m I .
.. .. . ‘If’)
32 “
(u-mm)l) IMl:ul. -. . - - - 14
I
. ..- -.. .-— ------- —
Method 71Zf
434 The name 4~-irmb length shall be im- be immemed for 80 aeoon& in the sodium poly-
memed in the hydrochloric acid solution, S.1 9,
for a period of 1 minute, washed in clean run-
auMde solution, waehed in clean running wat.a,
and shaken to remo?e extzm water,
)
IUng water, and shnken to remove excess water. 4.5 At the end of the above cycles of immer-
4.3.3 The snme 4~2-ilwl~ length shal] ngkkr sion, the o~imen shall then be examined for
be immemed for 30 seconds in the sodium poly- the presence of blackened areas resulting from
sulfide solution, wmhcd in clean running water, the action of sodium polytndfide. Blackening
cnd shnken to remove excess water. that occum wjthin 0.5 inch of the cut ends shall
43.4 The snme 4}~-inch length shrrll agnin be disregmled. Blackening of the catted sur-
bc immerwd for 1 minuto in the hydrochloric face caused by treating the specimen with
acid solution, washed in CIP:LIIrunning water: sodium pol@6de ebould disappenr when
and All km to wlIKw excwm wntrv. treated with hyhchlorio ●cid ltmving black-
4.4 Immen3ion of specimen, tin-coatet ened amns only wham copper is exposed.
Uniess otherwise specified in the dct.ail qeci- 4.6 T’ho percentage of the total arm of the
lkmtion, for tin-coated conductors n 4+@wh specimen showing exposed copper (blackened )
hngt h of the clcnn qxwimrn ddl be immersed aren) shall he ddem]ined by visual txu,ninn-
in accordance with the follmvin~ ryrlc= nt a tion.
tmllpellltura of lR” Z2” c. (I;3”*.40 F.). $ RESULTS
4.4.1 One minuto in the IIydrovhloric ncid 5.1 Unless otherwise spccitkd in the detrril )
solution, 3.1.2, wnshd in clenn rnrrning water, spwifiratinn, three qwcimens from aach inspec- ~$v
nml dmkfw to remove emws wutfv. tiorl !Illit dml] I* tesled.
4.4.2 TIIe srurw 4Y:-inClI Iwgth shall bc im- 5.2 TiI*s mli fwrnity of the routing of tlw
mersed for %) swrrmis in the sodium polysIIl!idc conductor nf (IIC insertion unit shall h the
Solutim. 3.1.3. w:mhed in clcnn running water, arom~q of (he mmJks ohtnined from tllr qwri -
:m(l slI~lwII to remove cx~:es~wntcr. mrws te.ted,
4.4.3 l’hr mnw +}~-illcl] lcngt h sh:Ill ngnin 53 ‘1’Iw imnwmwl nr-m of the iuqwrt ion
bv iir]nww~ll f(,r 1 nlir)litv ir] tli(~ I)ytirotl)l,,ric Ilnit Jjulvi]lg l.xlNIwvl q>!wr shrill 1]{*rerordcd
acid solution, vvnsi]ed iII clmm nmning water, to tim nearest 5 percent.
and A&en to remove exw% writer. 5.4 TIIO nunrhcr of immemifm ryclm nnd
4.4.4 The same 4~&inch [email protected] shrill again tmnlmnt.rlm of solu~iou shall be recmded.
t
Downloaded from http://www.everyspec.com
Method 7123
- April 14, 1%7
Method ?12#
)
Downloaded from http://www.everyspec.com
Method 7211
April 14, 1%?
Method 7291
April 14, 1%7
Method ml
ttmgs$tw ah ft ●ttached tos 1,000 r: p. n~ motor a blackening ●ound the colunlw When this
gm rrd so t hnt tlm solution is drnwn townnls
I 11Pr:tthtmll’. me nl~pnrntus shrill he eql[ippetl
dnrk layer hss eztemlexl ono-htdf to tJNVM-
fauths of tbe hngtlt of the tube dowv~ the
)
wit h :tu :inoly[ e reservoir for flushing out the
nnt KICrhnnllwm during the Awt rolysis. The
:I]Jlmrnl tw slwll bo equipfwl with UIInnodc of
column; the silver chlorido nntl silver AILII be
tmrtsferred to ● benker and cmerml with 1 to
190 sulfuric acid solution and 8 zinc rod placed
.
l)lll.(l cf)ljl~.r will,, ~ mm. in dinn)ctt”r, silwr-fw in the henkm so thnt the zinc ie iu crmtnct with
1111~1IIImnWmkWl) for we iu detem~inatinn of the silver chloride. The silr~r chloride i~ tw-
si lyrr. dueed to siker which shell be wzzhed *nd
3,1.14 ,u:)t’t’r
P#”,l?&*tor. rdumd to the inductor column for fud~r urn.
3.1.14.1 ‘l”h IS npparatus shall be similar in
l]~i~ll ~11f@l~ ~~:)1~, JInd S]lJLII(X)llff}J7ntO the
f,,1h,wi ng d inmlmions:
Inhwml dlnnlctvr ------------------
Length et rednrtor rel!tmn -------
W tn W mm.
120 to I:*1 n~.
)
CnwickY of r-rudr--- 73
.---------—— 50 to ml.
3JJ42 Pr#,pmz@m nf dtw wihrfor.
Sixty gmms ot silver nitrttte shall he diwnlvwl
in W) Id. of wtttcr and n few drolIS of nitric WRETTE
TIP MOLE
.)
ncid ridded. A sheet of medic copper, nhout
10 cm, squn m., shall be suspended in the siJver
uit.rute and the solution stirred mechnnimd Iy
until all the silver hzs precipitated, as shown by
the hence of silver chloride precipitate on n(l-
{Iitirm of hydrochloric ncid to a few n)illilit~’r=
uf the solution. The sheet of copper shrill k
rcmorcd from Limsolution and the l}recil~it.nLc~i
~ilvcr wrbahod by decantatioo with sulfuric acid
stdut ion (I t,o l!M) until ~ of the dissolwd
copper is removed. lVzt8r zhsll be addwl to the
silver precipitate and the mixture poured irtt o
the reductor eolunq the 10WQW end of whicJ
crmtnins n plug of glass wool placad over n few
gbs bends. Aftm t he solution has dmhed to
the top of the silver column, the silver precipi-
tate shall be wmhed rupeatdy with 1 h 100
tndf uric acid ul~t.il all the copper has been re-
)
mo7ed, ns shown by the nbmrwe of a LJIUO rohm
t-mthe addition of mnmonium hydroxide to the 3.L15 Tin reduction aPPIJmvtua. The sppa.
washings. The inductor ehzll then be tllkd with
I to 9 hydrochloric acid eolutiort. When not in
mttte *own in f~ 7YW3 shzu Oomist of ●
flnsk cbed with s three-hole rubber stopper
)
use. t.ho reductor shall km kept full of hycl ro- containing an inlet tube for carbon dioxid% an
.chloric neitl solution (1 to f)). ttir wnclen.sor, and a hole for n burette (glare
WWI RcqvwwWwI d i+hw. During plugged ).
tho reducI ton w terric iron by paasmg u hydro- 32 ‘Me JVIY~JltRldlnll he Rs follows :
cldoric nrid sfdution of iron through the mrluc- 321 A mmnnivw ,,?w)I dv~ion, ‘Il~e W] II.
tnr, silver chloride fomns at the top of the lioJl Shll k pt%pmd by dlsedvmg W gmns
column. This silver chloride dttrke~ knving of nmrnunium alum ( AlNH, (S04) ,.~tf J)
Method 7Z31
ia 100 ml. of distillsd water. (One ml. of the wmml” with water ●nd evaporating agsin to
enlut iou cont~irte qqwoximrkely 2 nig. of AL) demo white fumq snd diluting to 1 liter with
3.2# A tntnow”*mt Wimidc, 1 rwrwni wlu- Wiled wster in a Volumetric flask. This pri-
tbn. maqy mJlutinn shall b dihhed 1 to 10 for bk-
323 Am-”twn pwtitate, 10 pawnt mutk standards.
#o/ti”on, pqmmd fresh M mquimd.
324 J m.modwb nutfatc, SS prrent dv- RC,KWan
WoTQ?s M& *WOW
timk-l%e sohtion should m.mtain law than -<
mnFeaAtm ..
0.0005 pwwnt twannic. Fo;w:w ‘ .
‘.,
3.2!5 .4 ftl)tlO?N’U7?b thioeymte, @ fWTWt
dwtion.
. . AMALOAMATCO
snm
3.26 Ant;mony cMW mktion. The -“ @o To so mslo
●
Ml]lttit)n sIKJI & prqvnrwj hy ditvmlving ? gtnms
of nllt imony chloride (SM’ll) in 200 ml. of
hydrcwhkic aci~ sp. gr. 1.10, nnd dihtting to 1
Iitcr with distilled water. .SLASS WOOL
t
.-9 MIA
.@&lmT II
,- -v
?0 SUC:IOU PL49tl
IJwmu WID. Wwr rmluctor.
1
“As ‘ 32.8 nt’8 VRfl t A Colorhlw$c Iltandurd-1.
w LLAt ThaBO shndards shrill hc prquwd hy trans-
rust
ferring to 100 pd. tmlorimctric tuk, 0.2 to 1.4
rng. of bismuth, in intnunen~ of 0.1 reg., from
—. .. t.h stnndnrd snlution in 8.2.7, utl(liug 2 ml. of
---s00 40 pwawt pdnasium iodid% 9 ml. of 20 percant
\ FLA8u sodium thiocyanwto snlution, 0.5 ml. of etsrch
sol utio]l, nnd 2 ml. of 0.1 N tmdi~yn thiomtlfate
-- solution t.ueach tu~ diluting to 90 ml. with dis-
---- tilled water, adding 1 ml. of 1 to 1 sulfnric wi~
-.
-.-- ---- and dihlx to I@ d These StJU&X’dS
@ = should he pmpamd jti before the test is txm-
~GUM ~lC. A~mtw tOr dlmtlllnt~ooOt ●rDACIlC ducta4L
329 8mndard d &f& m)lktiivnq OJ
327. Bimwtii ed@e, dandavd 80&diaL N. This srhtion shall be prepared by dimmlT-
The solution shall be prwpamd by dimol~ing ing 64 grameof C8(HS0.), in SOOm.1.of dis-
1.0000 gram of metallic bknuth in s end ex- tilled wat.ar oon&ining 16 ml of sdfuric X@
cess of nitric ●
cid, sp. gr. 1,49, adding 20 ml of ep. gr. 1.83, and diluting to 1 Iitar. ‘The eolu-
sulfuric aci~ Ep. ~. 1,83, evaporating b dcuta tion shall be standardixod by either of the fol-
white fumq cooling, rinsing the sidtu of tho lowing methods :
Melhod 7231
...\
S29.1 MethadA. ApproxinwtdY
of iron of known composition sbd be trans-
W ~ MIS Forw& add ~. ‘Ills Bohltion
ahaIl be prwpamd by miring 200 mL of fomnio )
ferred to B 250-ml. beaker ar.d &uhd sin aci& Sp.gr. 1.20,970 ml. of d%tilled water and
20 ml. of 1 to 1 hydrochloric acid and 1 to $?ml. 30 ml. of ammonium hydroxide, sp. gr. 0.90.
of satumtd bromine water. The solution shall =6 Fomtic oaid ddUIW wudb ddiom
ho boiled to expeI exct== bromine, stwmns The solution shall be pmpmed by dil@ng 2S
chloride solution (150 grnms of SnCl,.2H,0 ml. of formic acid mixture, 3.!!.15, to 1 liter
in 1 liter of 1 to 2 hydrochloric ncid) added with distilled water and satumting the solution
dropwiae while stirring, until the yellow culor with hydrogen sulfide.
just disnppws, and exactly I drop in excess. 33.17 Rykrdne m!lfl?t~,
The solution shrill be cooled to rwm tempera- 3.2.18 Llydmqw prr-”dP, .9 prrernt wZu-
ture and 10 ml. of 5 pnrcent mercuric chloride tioll .
added all at once. The precipitate should be
whjte and milky. (If it is grny, the solution
QL19 IZydwgen aulflde wad 8olntiom
Tho solutirm shrrfl be plqwod by saturating
)
shall be discarded.) One drop of ortbo-pheunn- @furic ●cid aolutio~ $! to 96, with bydrogeu
throline ferrous complex indicator ahnll be sulfide
added and the solution titmted with eerie sul-
fwe to a pale blue or colorless end point.
32.92 Method B. Twenty-the mL of 0.1 N
3.220 Iodine. 0. T N solutk. The solution
sliall ho pmpnred hy rlixsolving 12.7 grams of
iodine and 40 grmru of pntmsiurn iodide in 2fi
)1
arsenous acid solution sh:dl be rrch.led to a 400- nlI. of distilled writer. When solution is com-
rnl. beaker, 10 ml. of 1 to 1 sulfuric acid, 3 drops plete it sh:lll he dilutal to one liter and stored
of osmium tetroxide (2.5 gmrus per IIter of in a cool plnrc in n Ark botde. The eo)ution
0.1 N sulfuric ncid), as ● catalyst, rmd 1 drop of shrill bs al nm-larrlid as follmva: Tern ml. of R
ortl]o-phenarrthroline ferrous complex indica- tin solutiou (1 ml. cquir) to 0.001 gram of tin)
tor added. The solution shn!l l-w titrated to a shall b )Jipettwl iuto n NM-ml. flnsk, 10 ml. of
pale blue or colorless end point wllh the standa- sulfuric acit~ sp. gr. 1.t3. ~! ,grams of sodium
rd ccric sulfate solution. Clllurillv, 73 JII1. of ll~dmchloric acid, sp. gr.
3.2.10 Cilm’c acid, W percent aol~ltiom 1.]9, nnd 5 grnma of h-t lend ruhkd. The snlu-
U-11 Copper nitti anolyte solution. tit-m shrill he rwlucml and titrated with the iodine
The anolyte solution shall be prepared by dis- solution rrs dmrrihed in 4.3.4.
solving 4 grams of metallic copper in nitric 32.21 Irm ~ttwrdad wAItion The eolo-
acid, sp. gr, 1.43, evaporating I ust to drynessi tiori shall he {,rvprred i}}di.wolvitlg {).1000graur
adding 30 ml. of nitric acid, and diluting to 1 of iron (Nat ionnl Xhn-eau of Standards standa-
liter. rd ~ mplv R’o.55b of ingot iron is ad is fartory)
3.212 Copper urblfate dixnduni adution in 10 ml. of 1 to 1 hydrochloric ●cid and 1 ml. of )
The solution shall be prepared by dissolving bromine n-atrr, baling to rwnova tho em=
1.0000 grab, af metnllic copper in 15 ml. of 1 bromine, ● dding !M ml. of tho hyclroehhmic acid,
to 3 nitric acid, adding s ml. of sulfuric acid, snd dihating to 1 liter in s volumetric floak.
W. gr. 1.W, and evaporating to vrhite fum- $2Q3 iilanvanene nitraleb 10 pemcn4 oolu- )
The beaker shall be coded, the walls washed tion.
down with 20 ml. of distilled wster nnd the 32ZI Mrmyane.ee d?nt~. M ywvrt MIW -
solution rrgnin evaporated @ dense whiw fumes. tt”on ,
Two hundred ml. of 1 to 1 sulfuric acid ohall 3224 Md?tyt mvvnqe {nttiflator. The solu-
be added and the eolution made to 1 liter in a tion shall bc prqwcd by dissolving 0.1 gram of
volumetric flask. mrthyl mrnge in 100 ml, of distilled water ad
3213 ~o}’pf’r M!rlutc, 04 yr-nf ~chffon, filtering off nny residue.
3.214 Fomic am~, 8P P. 130. 3.2.25 Uetal’tio merewy,
)
Downloaded from http://www.everyspec.com
Method 7231
---
tmlizfwl As f(dlow: Trft ml. of Mnudttml wppr+ mei) U* II will dipcnrl on the rqqw wIl )lis-
mdf:~tr w)llltion shnlf he transferred 10 a 2:AI-1111. ImIfl I c(mre~lt nnct SIUIII b us imli~mtcd in bhe
wide-nmuth flunk, the ~lution diluted to 25 f,,ll,,u”irl: 1,,1.lr :
.
Weight of npcchnsn
1-
?ypa Of toad “ c!!per Ekmutb
‘
(%rlper Bismuth
dstortnination dcwmhmtioa
Method 7231 ,
M9tltod7zu
fermi to ● MO-ml. Erlenmeyer flask and MO-ML then bdd over m open flame until the volume
dltollnitric acidadded. hemixturaddl haabaan duatdtOaboutlOmL TheameniG
#e heated gant.ly to dkdve the lead and than ●ntimony, and tin shall he debrmined as b
boiied to expel the brown fum= The oolu- ~ibad in AS% 4.53, and 4.8.4, or in 4.9.5, 4A.%
tion absll be diluted to 800 ml,, heated to boiling, ●nd 4.8.7.
10 ml. of 9 pement potaaaiumpemnanganate snd 49802 Am-’e & -w ?q( bwmJM%
90 mL of 10 percent manganeae nitrate add~ tibmt$om The solution froJn 4.q.l Rhall be
●nd then boiled. gently for about 9 minu~ cooled tmrmom temperature, the oidm of tho flnslc
The hot solution ebdl he filt.crad thrtmgh a washed down with !50 ml. of distilled water,
rapid filter paper and the precipitate washed 20 ml of hydrochloric acid added, an~ the aohl-
with bot writer. The filtrnta shall be labelad tion heated to abut 90° C. ( 104° F.) to dissolve
(a) and meervad. The pnp containing the all of the lend aalk One drop of m?thyl omnge
precipitate shall bo returned to the originrd inrlicutur Aal] be added and the solution ti-
Erlmneyer flask, 15 ML of sulfuric acid, q. gr. t~tecl with 0.01 2? potassium bromnta until the
l.tRLand M ml. of nitric aci~ sp, gr. 1.43, ad- red color weakexm A eerond drop of methyl
and the solution bettted ~ntly tn hui}ing to de. orange shnU h added and the titration con-
tiroy the Mcr pnper. The solution shall be timwd slowly until 1he odor chnuges to yellow
labeled (b) and JWJMWed. One-hundred ml., or or culorl~ fie titrnted solution sh~~llbe rw-
enrmgh tn rmlih-o 811of lIw lrwl nf :UI prrrent servcIl for um in 4.3.3. A ld;~lik ~lrtw[lfimition
ammfminm wtlf:~lr, shrill k nlltl(.,1 ti, thli tlltrllte sII:I1l k J,II:UIIStf+ing t hc wnc ntnfl~int I)f rno~wnts
htbdwl (n) whiht stirring, tlw wdllti(m mnlPIi nml following the snme prumlurr. The ntffuhw
to room temlw.mt we, filtered fl)rongh a ClQSC- of millilitrm of potassium I.momntc rcquilml to
txwurml papw on n BIIchImr funnel, nnd titrutc tlw arsenic and antimony (A) is equal
washed onto with distilled wnte.r. ‘UK: pwci - to the totnl ti~rutioii minus the IAwk t itmt.ion.
pitot~ of )WJd .wlfnto dl:tll IW IIisrnrflrtl. TIw 4.3 ? A )~tin)my fiy ?~ronl.otr iitra!ion.
fi!tP-!o e!:::!! !* nw~!rn!izpf! wi!!l nl!w!wiw! (;I:Iss in.:tilS Aa]l b utlI]fd 10 the t itr:l(e(l sOlll-
hy(lrnxide, lfi ml. JJ(l{leIl iu {xt”fw. Imntcd to Liou rfw.mcd iu 4.3~J uml lhu solut if!li Imiltxl
boiling. 10 inl. of 10 pmwnt amnwliium pwxnl- unl il tho volume is rmlucwl to 100 ml. The
fato ttddwl. IIIId then hnihwl vigor(}lwly for 1 solution shall k trnusfwml to n W@ml. glms-
minute. TIM solution shall he filtertxl through strIppered iodiue thk, the 500-ml. Erlennwycr
a mpid filter pnper, the prtwipitnto tmnsfcrrml fbmdcriJwod with 40 ml. of hydtwehhwic m“id nnd
to the paper. mshd four timca with hnt wdcr, the wnshin~ added to thr. imliuv flnsk. TWO
and the fflt rntc diwwdod. The pnpor nwl pw - ml. of 0,4 percent cnpper Slll[nto Sllitll Im udllc~
ripitnto shrill be tmn~fwmd to the snlntion in the snlution cool~ to rootn twl~prrntllre, 5 III].
the .500-Inl. l?rlalm~yer fhwk lnheled (h). This of metallic mcrmry Juk.hvl (if mcr(,ut”tuw clllo-
fhwk cmt uins nl] tho marnic, Ilntimmiy. and” rido is pmci] Iitated more hythw”l~lorif. ni!iil
tin plus snmc mungnnwe, led, anfl a tnm of should & nflckxi), ml the flfisk stoppeml nml
copper. Thirty-livo ml. of nitric aoid ftp. LT. tdmkml vi~rmwly for 5 minuks. The snlnt ion
1A, shall br ndhd to t he ~lnsk n ml the tmlution An]] ho dofwdd itdu t hf~ MO-III!. Yh+wmvyer
h-ted gently to destroy tho enrhonaceoue ma- fhwk nnd the mcrcmy wnshed, ridding the WtISIJ
tennl, mhling more nitric acid if necetmnry. to I Ifn snllltirnt. The solution sh:dl he dilutd to
T)Je &dution dm][ he wfqwtmlwl 10 ~hvvx!whito olrnwt :x(} ml. and. with nir bulddil~g slowly
fumm. IIfe rmiduo roolcd, 3 gtxni,q of potns. through it, hctttetl to !lo” C. (l!) in F.). Ttm nir
siurn bisulfnto aofl0.1~pwrn of hytlruzine SIJL atraam ~hnll he discontinued, 1 drop of methyl
fate adIhxl, nnd the sides of the flask wzhed omngo indicntur addeIl, nnfl t hc fffltlhony t i-
dowu with water, mnking uvrtnin tlm( no Ilydm. trntf3i slowly d M“ C’. ( IW’ F.) with U.[)1 S
zinv sulfate remaina on t]lc nvL]js. ‘1’JIc~lllti~n potnfshm hmntm ‘1’hLI titr:iLmi SoIulioll s]: II]
ahull be evnpornted to dense white fume+ and be nservcd for tin detcrminrftion in 4.0.4. A
Method ml
blank determination shall be made using the apparatw% %.1.1,900 ml. of water ploeed in the
JMIIWumounts of rrapywts and following the rmiving tkk, the distillation desk lwmted to
INL)IIL![)tWWdU1
l’. ‘h number of miHilitere of boiling, nnd continued until the tempmntmv of
fwluk~ium bromate nqllirwl to titmte the nuti- k distillwl vapor ~hm 105° C. (?21° F.).
nmny (1/) is Cqllill tLJ lhe Iutal Litmtion minus ‘I%P distillation flask s@Il be unstoppered, the
tile Illnllk ti\r:ition. hot plate remuwd, mid the r+dution rescrvc([ for
43.4 Tin Ly iwlilw /iJrufiow Thixty mih antimony detmninntiotl iu 4.3.0. The delirery
lilit.cm of IIydrochlwic ncid, sp. gr. 1.19, ●nd tube shnl] be rinoed into the mceivh~g flask and
sufficient 0.2 percent nnl inmny chloride solution thn distillate heated ntnrly to boiling. ‘I%(I
to nmkc the total nntimony content of the flask solution shall be titrated at W *EQ C. ( 165° *
equnl to nbout 10 mg. shun be ridded to the 9° F.) with 0.01 N potsssium bromate solution,
tit rnt Pd wdut ion reserved ill 4.3.3. Five gmms adding methyl orange indicator near the end
of trst lend slmU be added m-id ti:n solution of the titration. A bhnk determinant ion @hnl!
)
boiled gmt ly for 15 minutes. When the dep- bo mndvlming the same nmounts of mqents nnd
osit ion of nohla met nls is eompletc, the solu- following tbtt same pmmiurm The nnmbw
tion Ann be filtcrvvl through Mton w glnss of mil]ilitem of potnosium hrnrnate soluticm re.
WOOI iut.o a wille-mm~th fiIHI-IIil. EA*nnqw quiml to titmte the nrwnic (4) k eqtld to th
flnsk Pnjitni]lij]g s prims I,f twt lVJII1 nm! QI~ tntnItitrnt inn nlims the Mnnk t itmticm. )
gr:tnts of mt{ium cIIliwitlc. ’17w fl:~-k ~lI;~ll Lo L7.tl .1 Ptiniony d, fcrrn ;nvf;nn. Twn llun-
IIsselIIIIlcIl into N t ill rml~wtirm aplmmt IIS n~ drwi ml. {If watm shttll he nddwl tn ~bc s,}l~tion ~1
+
{Iew.rilw{ in 3. I.15. J4 strwm {*f r:lr)m]l in the (list illnt im tlnds rxwervml in 4.3.5 nml the
dinxi!l~ slm]l 110IVVWO{l fhr~wdl th (ln*k. tlm solutinn Imikxl t,} diwudre nll of tlm MIIS. The
solu{itlll ~mdlmlly lmtml 10 Ltililtg. nnd lMIilrII hot solution A:II1 1101it ml IW1mit.h 0.01 N potu~
for 11 I(NIr. ‘1110 llnsk stroll bu t mnsfmw[ 10 nn SiIIrII bmmt;tte. mlding mr! }I)f nrnngc indientor
i~w lxttll :IIItl (1111(WIIJIjII tlt~txi(](~ It. L~IIl,III.] .SO rw:ir llIP P!III I)f IIIC titr:~ti~jjl. TIII\ ti[r:ltwl so-
lht n!) uir wiii im sIIckud Iiit{.k IIItI) Ilw ll:I+k. iutlOll 41:111 1* IWSMVI[ ftlr tilt fldermiwtion
Tlto S(,IUIill!, JI;III Iw ,wJII*(l tI) ;IIY)III If) (’. III ,1.3.7. dl.i~’rtl]ij~:~lil~llSII,IUIn mwh;
.i hluuk
(W’ F.) II I~Ilrr aII nlmosphwe of mrbon uqing llm same nmmmts nf rmgrnts mId fcdlow-
dioxide, t h plII: JWl]fWPil frllm tlw tIlirll Imle ing the snnm ~mwmhm. w numhrw nf milli-
of I hc ruhtrnw ~tolqrr. n~I~l5 ml. of III pvrumlt lit em of potuwium Immnto HIM ion rquired
potnssiurn iodiile Solutiuli aml 5 ml. of 1 pcr- to titntte the antimony (8) in qunl to the total
fw)t stnrrll dutiw Iuldml. ‘l%! tip of Iho 1ittul ion minns 1he hkmk t itmticm.
b!lrottv rontnillillg 0.1 N iwiirw s~lntioll +Itu!l 4.3.7 Tin ~y ;nf?ifl~ titrvftiIJn. Thr SfdNtiOII
be imn)edinl~ly insortetl i)lto t}w other htdc of lvw!rv~ in 4~3.tJ~]m]l k diluted to Wit)ml.,75
tIw rlill}wr d q)lwr rInrl lhe solution titrntrd to Inl. of hydrochloric aci~ sp. &r. 1.J9, f~ildc’~,nlld
the first [wrnument d~utle IIf blue. ,i bl:mk tho t in cWcrminnt ion completed nn drsvribwi in
determinntio~l nhnll lx! mwle using the same 4.3.4, adding only 10 granw ?f sodium chlo-
anmunts of rmgentti nmi following (ho same rklo in~eatl of he !?ograms specified in the
prmmlum. The numlwr of millilitrm of iodine Jmoedum
mlution required to titrntc tlm [in (f?) is ~Nal 4A Iron by ~ohnetrlc or eolorimetrie
t.o 1)W 1.oQII t itrntion miltus tke Idnt]k tit mlioh metho~
4.3.S .4 rmnic Ljt diafiilflfion. The solution 4.4.1 Pnymdon O! xoludon of irnn. A
of nmwir, nntinwny, and tin hludl bu lwepnred qweimen mntaining about 50 giams of tbe lead
w dexribcd in 4.3.1. This nohtion shrill be sheath sMl be trmsforrod to a WtO-ml.beaker,
cooled to mom tcmperatmn, 50 ml. of hydro- UN ml, of I to 4 nitric ncid nrlded, the nlixtl~~
cl~loric nrid, sp. gr. 1,19, alul R to 10 grwns of I:mtd gently to dissolve the lead, nnd then
sodi urn chloridu Tile 500-1111.Erhm-
nddd. tmilcd to expel the brown flzme~ The Iwnker
nl~ycr fli~sk shall & connvctw] to tlm distillation shall be removed from the hnt platn, 35 roil. of
Metbod 72Sl
1 to 1 sulfuric sold adde4 the scdution Wn’ed mination shall he made using the same ●mounts
through s clom-texture psper m ● Bachner of mqents and follow’mg the same procedure
funnel, and tho beaker and psper washed with Tit. number of milliliters of ccric sill fate solu-
hot water. l%. fikmte and washings ebdl be tion rwquimd to titrate the iron (A) is rqunl to
collected in s 600-mL beaker, evqorated to thri totalIitmtion minus the blank titrnt ion.
white funw+ the besting continued until the 4.43 hwn by cobrimetric mcfhod. The fe~
~olume of the sulfuric acid is mducad to about ric hydroxide preripit.cte from 4.4.1 sh::ll h
9 ml., snd then oooled to mom tsmperatum dixeolved in 20 ml. of bot 1 to 3 hydrochloric
One hundred mL of wster shall h add~ acid nnd IXWIMIto room tcmpmature. The solu-
the solution boiled for ~veml minutq cool~ tion nhnll he tranefcrred to a 100-mI. cArinwt-
made neutral with ●nmonium bgdroxid~ and nc tube, 2 ml. of 20 pemrnt ammonium thio-
9 ml. of hydrochloric SC@ sp. gr. 1.19, sdde& cyansts addwl, clilutnd to 100 ml., and mixed
Hydrngsn sulfide ahd be @ into the xJlu- well. Tho color of the solution shall be com-
tion for ●bout 15 minuttq the precipitate al- pamd with a standmd cnntnining a known
lowed to settlq and then filbrd Tbe pre- amount of iron. ‘he stsndmd shall be prepsred
cipitate shall he wnsbed with hydrogen sulfide by ridding drnpvrk stanrkd iron solution to
water snd then discarded. The filtrate snd a calorimetric tube mntaining 75 ml. of dis-
vvsahinge shall be baled to expel tbe hydrogen tilled vmter.2 ml. of 20 perrcnt ammonium thio-
m]lfide and the iron oxidkxl by tho addition eyw-mte, nnd 20 ml. of 1 to 3 hylrocl~lnric ncid.
of a few drops of 3 percent hydrogrm pwoxide. The sduf ion shall be mixed well nnd ~ornpnrrd
The solution shall he ● vapomted to 50 to 75 ml., with the nnknmvn boyvisual obwrvat ion ngn iww
cooled slightly, ●nd 5 mL of anunoninm alum n white bavkgrouncl. If nmtil:~hlc~ n twlnrimetcr
solution ●dded. The solution shall be neutrsl- or tqmctrophutmneter mny be used for making
ixed with ammonium bydroxidq uhiiqj 2 the color comparisons. The st.andurd iron solu-
ml. in esccs~ boilvd for 1 rninutq and t)len tion slmll 1~ mhiwl until the vo]or m~ttchw tlmt
mt sside for ●bout 1 hour. The precipi- of t lie specimen, Lringillg t.lm volume of the
tated iron shall be filtered on to rapid filter iki comparison IJI) to ii)fi mi. in ~iw iiik. A
PSW, W* with hot 1 percent ammonium Mmdc &trmlinntion shall be made usiqg the
chloride, and the fihute rtserved for tho de- enme amounts of mngmts rind f ollovring the
termination of xiac in 44. Ths iron shall be enme prncedure. ‘1’huJmJdwr of milliliters of
detemnined on the precipitate by the volumetric irrm solution required to match the specimen
method described in 4.4.2 or by the oolorimetric (B) is equal to the totnl iron volume milms the
method as dmribed in 4.4A volume of iron solution requird to match the
k~ lson * valumstrie mathud. The fer- blank
ric hydroxide precipitate from 4.A1 shall h 4.5 Zinc determhtstion. The arnmonical
d~lved in 20 ml. of 1 to $ hydrochloric acid, erhtion in a tWO-mL besker maerved in 4.4.1
the solution diluted to 50 B& ooolo& ●nd then sl&l be made just acid to litmus with 20 pwwnt
passed through the SUvsr rdlctor, SolJ& St citric acid. The solution shall be noutmliaed
therate of80mL per minute. ‘Ilwmductor with ammonium hydroxide 25 ml. of formic
shall bewashed witblOOmLof lto80hydm acid add~ the solution diluted to about 200 ml.
ddO!iC ui~ adding the SOhltkm in sevsrd por- and 1 mL, of tile mwpension ridded. The n~ix-
tinn~ and mllowing each eddition to grain to ture dd be heatsd to about 95” C, (90..0 F.)
the top of the sliver column Mom the nsxt is and hydrogtn aulfhlo pamcd thrnJlgh for 30
edded. TenmLof ltilsalfuricuddsnd minutes while allowing to am], The baker
1 drop of ortho-phenanthmlino indiutor sbsn shslI he set aside for nbout 1 hour, the pmcipi-
be added and the Awed iron solution titratal tite flltsred on ● 9-cm. clnse-texture paper, aod
with standmd cerio sulfate solution to the dis- washed with formic acid mixture mash solution.
appesmnca of the pink oolor. A hlsnk detsr- The xiuc sulfide shall be dhrdved from tho filter
9
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Method 7231
Wbcrs:
~.tbe ~~ ~ @ of pI#~~ b~te -
to titratetbe●-k
r=the gmrmcof-menk per ml. ofpohnalum bromate
~=t* ~~ght ~ * tad abeatb apclmen
B-the numkr or ML Of ptsDIum b?oma~ ~
to tkram tbe aDtiDoW
E=theb~~~ of ●tlmony per rd. o! potanlum
lnm, P&tnt- ~
Axc x 100
whew:
A -lbe weight of Nte dhe? deposit on ekt?ede -
U =tbe wetght of the lead sheath 8-II -
I
Method 7231
I
S.L7 The lead content .ef the epet&em shall M The metal coxkmt (had copper, bis-
ba Calcddad aa folhlm “ o ! muth •rneni~ antimony, tiz+ iron, tine, or 8il-
~er) of the tthed,h of the htupaction unit shall
.)
bad, prrcont=100-(lwr’mt eapmr, blsmut& ●rnak
anttumny, W, lr~ 8111C,MId be tile aversge of the mndta obtained from the
slt~ xh specimens tustad.
52 TJnless otherwiss I@Afied in the detail S,4 Tbe lead content of the sheath of the in-
spwitlcnt ivn, two spwimena from each inspx - spection unit shall be -KM to the nem-n5t
tion tit shall be tested. 0.01pntwmtm
Method 7251
April 14, 1%7
Method 72S1
)
paper. To conduct the tut this paper till be ~ PROCEDURE
moistened with the wetting solution in 8Q11.1. 4J PWOl@U tak A specimen contain-
32.12 spot tale piape? (Polyieohutykw). ing about 0.5 grum of the rubber cnmpcwd,
3.2.121 Mercur& od$e-eulfurie acid lrwtting ftw from adhering fnbrirs or other mnterial,
sozution Eiye grams of yellow mercuric oxide shall ho trmwfermd to the distillation tube of
shall ~ ridded @s mixtura of 15 ml.. of sulfuric the dietillntifm ●pparat us %1.S ●nd a condmwr
acid, sp. gr. 1.83, in 80 mL of watar, and the tube sttached. Tho distillnt ion t ulrn ntmll be
mixture boiled until the mercuric oxide baa fextened in position by mennn of a chmp and
diaschd. The eolution ehatl be coded and di- then hrated with n very low tlams until the
luted to l(Ki mL with diatilhd wstar. specinm lwgins to deeompae. When vnpor
32122 Teat appears in tlw tube,the end of tho condeneer
+%%e:%ig%x%
shall be HiOIStO tbe eha]l be immemrd in 1.5 ml of eulut ion
ecribd in 8M!M and then cut into xtripa No. ~ contained in ● M tub and the distilla- )
3ZJ3 spot ted ppef (A%w’-etymne). tion continmd until it hae tin determined
3JM3.1 %Abvao& 40 i &wornvlm nol whet }wr a rolor chnnga will derclop. TIM oon-
wetti ng 8ohJtim ‘T%irty gram of trichlo~ t.iemuwhh rdmll then I* rwnnml kom eolution
acetic acid droll -be dimmbod in impropanol No. 2 nnd tm]ufcr~i ton Remnd N!CCiTingtllh
)
●nd the solution diluted to 100 mL with the contninillg I.fi ml. of wht(ion No. 1, -ml the
anme solvenk The eolution should not be al- distillation rImt inlml flw a [mr minuios. Tho
.
lowed to come in direet contact with the skin. disli]ln(e in the two recciring tubee slmll lm
P
3213Jl Tent paw . The eolution shall be roolcd sh:lkrn. TINI tub ccmtnining eolu-
n~d
prepared by dissolving 8 gmme of p-dimethyln- tmn No. J nhall IM cxnminexl to determina
mine benxaldehyde ●l 0.05 grout of hydro- wh(~tlier the (lrnps of distillate sink or tlont on
quinone in 100 ml. of ethyl ether. Filter pnpers
solution No. 1. Both aolutiotrs No. 1 ●nd
ohall he irnpreegnnted in t!~is du!iou, dried, nnd
cut into strips, The paps shall be stored in a
No. 2 shl I Iw Awwxl
Mulion NrJ. 1 dtnll k
for nn,v rohw rhnp.
tmnsfrrrd ton 16- by
)
brown glue bottle. Pmpera I$omd under aurh
condition are stable fnr eewvaI months, but M()-mm. tmt tub, 5 ml, of dxvdute mdtyl nleo-
lose their eilkiency if ctored in the light, Ta Im] nddw{, the mixtum bested on writer bath
conduct the t.cut for natuml rubber rmd atyrene nt 100” C. (212° k’.) for 3 miwltm+ nnd nnyoolor
polymer them pap shall be moistened with thnt dcvclrqm mcm+d. All ohewations made
the wetting eolution deecrm m 3JL13.L WI both snhltinns RhaM hr rrrnrd{’d nml the ma-
&2914 %oj gromwod. , terinl cla~.ified hy menne of tnbie I.
..
- —---- -— .- .-—- T-
-.-— ..— )
Soiulion No. 1 pdwim”rh.3
Ms@Al
dor
fniuai
)
BIank Palo yditw I%ioyniiow Own.
Polyvinyl ddor+b Yellow Yeiinw M.
Cbiom$mae . his yellow$- l-h.
lwtdie
Cbiomprsndtrsb
ora2”Kd
m.
Ned
Do.
mom
Yaibw to rd.
Stpm Yeiiowgmmb Gmn Cheri.
Natural robber Bmn Vkbt Mlw no.
&o at~nO-50 rubbur Ouvo gmoll Gwn the Do.
Pot@eobutybne Yoiiow(drophrt floats] Peie blue gmcm m.
PolyTiIlyl Mew Youow MO yotiow gmon Yellow.
— ——
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42 spot kw9
421 Chborrrwwru “t.riie 8Vot teat. A lMLt-
iJIgrlwnent such ns ● lmi f% file, or iron sbnll
k hwlted, either chxtricslly or Lrymeats of a
gns flwu~ to a temperature su5cient to produoe
~h.tl~ofllnms bllt ~Jot ]iigll enough to ibmi~ t}~e
— IIIIIIIW slwcimrn. T)m ruihr trpccimett slmll
be lmwd ngninst thr hentin: element until
fmnrs arc Iihernted. A N rip-ofthe ehloroprenc-
nit rilo t M. lmpor Am II be lnoistwml with tlic
Imlzilli)m i)y(lnwlllori~lo.]~ydql~ il)(lno wetting
ftoIII~i~jl~ ;III~l t]lcli Iwhl jn a pnmllc] position
~}utIII ~ I)im. nbovc tho surface of the herding
) unit, which is pmrssed ngainst the rubber qwci-
nwn Imtil s gmxl color is probed on the side
oft Iw pnper f sting the fumes without srorching
the IMpvr or lho impmgnnting matM+rLlrL
TAttI.E 114
----- -. —-.
i
Materiil Chkwqmmo-nit rilo trst ~ ]’,,lyidm,tl.} 161M lost
ltutllw~r-ql yrQIIP
t-l
.—. - ..-. — —. —.-—. . I. . .
.. . ----- —----- --- .- — -— .-. -—.
—.-—
.
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.-
warmed to remora tho cmbon tetmchloride. A
bluo or rwl-tiobt odor indicntett. the prtmence
of natural robber. (Oil-type reclshned rubber
gives this fast but alkali-type mwlnirn does ~
Polyi%prene ah givee i poeitive tcsL)
4.X3.3 rf~r ,r ~,h’ f,,r R+VWW* ;Sdfpwrn. The
prtqtlre of stymue polsniwn nl~y bt) further
mufirnwd hy I itis trst, One or two -pros of the
sjmimcn Hlmll he extrncted with scetone and
driwi n~ desrritwd in 4.8.3.2 The dried speci-
men slmll be plnced iu a xmnll flask 20 mL of
nit rir ncid, sp. gr. 1.43, added nnd then rdluxed
for 1 hour. Tm refluxcd mistnre ahull bo di-
)utcd by pouring into NM ml. of water, then
ext m rted with 50-, 25. and 25-nA portions of
cl her. llM ethw extrncta ehall & oombkd,
wnshrd twice with IS nd. of water and the wnsh-
i)lgs rejrcted. The dlwr solution nhdl & ex-
trnrtm! with threw lfi-n)l. II(wt ions of” 5 perent
~nliltllt hy,irt)si~lc. f,dl~meJ by extinction with -
~1) ,,, !. “f ~J-OIVr, nnt[ tho e[lwr discnrded. The
s(~{lilllll l~ylrosido nnd wrwhing shrill be
extracts
c(mlbi 11011,f hci, ncid with hy&ochlo-
nmde just
ric aci~l, sp. gr. 1.19, :Iml ?~t ml. added in cxces
Tile c~llllfi~)n -i, Ill IW lICfiIId {m tlIc stmm bath
r,itti tIii iu !K,IIzII;c urid r(,tiucwi with 5 *W of
~?’xflllhlfl’fi XI I:(!. ion dIall be made
‘LJW si)]ttt
nlknlinc wi[l~?0 perrtmt sodium hydroxide, xdd-
iug st(fli(’ietlt e.wcs 10 just di.ssrdvc lhe zinc
h) llroxide precipitate that furms The solntion
shnl I h! ext meted t wire with r(lmr and the@ hr
disrnr(lvd. ‘h nqu~xJnesolution tdmll he rrmde
nrid wJth hyd rochlnric nci~ sp. gr. 1.19, tmnlml
to roum temlwmtum, nnd 2 ml, of 0.5 N eotiiurn
nil rite addtd. The solution shall be poured into
mI cxresa of s sniution of 11-nuphthol in 5 per-
ctwt sodium hydroxide, A vivid scarlet color
indicatrs tho p~ce of ctyrene polymem in the
ehetnmer.
43.4 PoJyiwbty7cnr pdynmm. The pm
mm of polyi.aobutylwm polymer may h fu~.er
cnnfirnmd by the fol)owing: A bat delivery
tube shall be sttached to a test tube No. 1 by
Iw:Im nf n rubhor d qqwr. Thn ddiwry tube
dL;Il1 pm through w S(oppcr nlmmt to the bot-
tnm of t-t tutw ‘No. 2 l~~ring a side arm. Test
tribe No. 2 shall be plmcd in nn ice bath. A
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Method ml
.
second delimry tube ehall be ●ttached b the sido mined. The derkative ie believed to b meth-
stm of teat tub No. 2 and extended into an open oxy-i-butyl-mereuri-soetate with s melting
& tube No. 3 containing 0.5 gmm of mercuric point of about 55° C. ( 131° F.). The test shall
acetate in 10 mL of methyl ●lcohol. A l-gram be further confirmed by s mixed melting point
epwimen of the rubber compound that has been determination with the mercury derivative of
extracted with acetone and dried as described in known pdyiaobutylene or isobutylenc.
4.3.33 shall be phwed in the fimt test tube and 435 Po@J+dt nifihma. The pnlysulfid~
heated strongly to decompose and distill off the nabbers are easily identified by menns of odor
compound into the second and third teat tubes. ●nd high sulfur content. Additional qualitative
The liquid thnt collects in the second test tubo teeta include the pronounced swelling action of
shrill be rejected. The third ~ tube shall be acetone (unlike other rubbers except unvulcan-
heated to evaporate the methyl rnlcoho~ svoidixtg iacd nitriles) ●nd the extremely mpid reaction
excessive heating near the end of the erapom- (5 t~ 35 aeconda) at 40° C. (104° F.) with a
tion. Twenty-five ml. of petroleum ether (b. p. mixture of M@ volumes of concentrated ]litric
SO”* ]0° C, ( 122° A 18° F.) shall be ●dded to the and sulfuric acich
tet ttt~ and the mixture huHed and filtered. S. RESULTS
The lilt IYIIeshatl bP cvnporeted to a SUMIIvol- 6.1 Unless otherwime specified in the detuil
ume nnci chilled in kc to mystullixe the mercury qwcificat ion, otle specimen from each inspection
dcrivatiw. The rrystals slmll be dri(~d at M“ Y unit S}M11be tested.
!ie C. (95 °2!)0 F.) and4he nmltil~g point ckter- 52 The ulnato:uem found shtill be recorded.
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..
Method 8011
Aoril 14, 1%7
‘ethod 8kl
April 14, 1%7
Mclhod 8031
April 14, 1%7
Method 8033
April 14, 1%7
5. Ill?St.11.TS
5.1 1;nlms ot Iwrwiw specified in the detail
sperilicntirm. one specimen from each Inspection
unit shrill be tested.
5.2 “17wNNIS [ w:lrl) yRrII~\ IWr inch nf the
lnycr O( tnlw ~hall Itc the rewllts oh:tiuwl from
the specimen t-tad .
53 Tlw pirk.s [ Iillitlg ynrns) pw it@i of the
lnyer U( lnpc Atnll h the results ohlnincd from
thr specimen tested.
5&l When mom tlmn one’ specimen is
trdd, the ends (wnrp pm) per inch nnd the
picks (filling yarnsi per inrh ot fhr Inyer of
tnl)c shall he tlm avwmge nf the msul~a ob(nined
from the spw=imens tested.
5.4 ‘1’lIe emls per inch nnd the picks per inch
Of ench tape tested shrill be recordctl to the near-
eat whole number.
Mctbd 8041
April 14, 1%7
3.13 AnaZyt{cal balanre and weights. L=tiIe lengtlt of Lhe specimen, Inches
P=EtlIe ply d the cotton yarn
3.L4 Wd ecde graduatad to ~z inch or W-tie ueightd tbe Speelmen,Vam5
fhwr or its decimal equivahmL S2 Unless othcrvviao specified in the detail
3.13 a~ciworw. specificntirm, one qmcimcn from ench inspection
3.1.6 {’Alornf ornt or other suitable so] vent, unit shall bc testml.
~. p~(jc-~~1~~ 5+% The size of the ynm in tho wrttp or wrv-
4J The ends of the spcimen shall be cut ing of the inspct.ion unit shall be the result
quare, the length measumd with a std scale obtiinod from the specimen tested.
to the newest ?42 inch and the who recorded es 53.1 When moro *8n onc specimen is
L. The specimen shall be foIded and trnnsfmrod tuked, tho sise of the pm in the wrnp or serv-
to nn extinction appamtu~ ing of the inspection unit shrill be the svemge
43 Tho specimen shall he extracted with the of tho roeults obtmined from the specimene
solvent. until all the aaturanta and finishing ma- t4!sted.
terisls hn~e been removed. The extraction is 5.4 Yam size of the ynm in the wrnp or
mmplote when the solvent from the siphon tuii serving of tbe inspection unit shall be reoorded
is dam. The apecinmn shall then be mmowd to the nenmt whole number.
Mctbod 8111
APril 14, 1967
DIRECTION OF LAY
L SCOPE 4. PROCEDURE
1.1 I“llis nwt hod is i~~tcnded for w-in deter- 4.1 The corrring nmtcrinl shrill b relnovrwl
mining tl)o di!tctirm of twist of my lw!icol t+. from tho sprcimcn nnd the chwcnts t[! 110IOX;UII-
mfmt such a.. S1rJtl& conduclor% tapq cottou iw+d cxposwl Bud clrnncxl if necowwry with tho
WJ21]H or scrvinph jute budding, ●rmoring solvent un{l cloth. Tho rlirwtion of lay of the
t JIIW.n rmlming wirn, jute Swvil)g, ●k., of insu- ●hmmc dull k rwodod u right-hmi or left”
lated wim and cmbl~ For of this
pqxmm hmd The fol)owing defhit ions ~hnll ripply to
specification, direct ion of lny is dohed as the the kms right-hand lay and Icft-hnud lny:
Intcrx! tiircct ion, eithnr right-kind or left- (6) Ri@t-hd lcy A ckkwiss twist of
hnml, in whirh an element pnsws over the top the eknwnt awny from the obsorver.
as it rccdcs frmu an observer looking along tho (b) L@-hud &y. A counterclockwise
nxis of the wire or cabk twist of the demont away from the observer.
2 SPEC1hfEN
5. RESULTS
2.1 “l”IIQqwwimm droll tw n piece nf the in- 5.1 l~tllrss tdwrvrisc spccifird in tllc d~tail
spection unit of sufhcient length to iIKluJe at
+rificntim. 0110sprciiomi frntu e:;cll in.+wt iot~
hulst t~rt) spirals of the (+nlwlt ttl h,! (Cstell
relit sh:lll bc Ii*still.
from which nny cm-wing over the demeut to be
63 ‘no tlirertion of lny of the IIelicnl clc-
tated hns ken removed.
metlt of IIN+iqm[ ion unit dtnll ho tho mwlt
S. AP1’ARATUS AND REAGENTS
3.1 The uppnrntus nnd rw~gw~ts shfi]l he ss obtnined frwu ttw qwrimm lcsted.
follows: 5.3 The Plolnvtit of LIlc itlspcrtio]l ul~it slInll
3.1.1 ll-;il~. - .7.C~ ho designotel EIV! its ilirrctim of lny (right-
3U L’hhmnforvn or other nuitulde solwmL tubml or Il!fbhlmtl) rom’dd
Method 8121
April 14, 1%7
●
hfCthOd 8131
froml which nny wwcriug over tho wmp or 5J Calculation Th6 coremgm of the cob
serving has beeu remrnwL (see methods re- tan wmps or twvin~ of ths spmimen alult be
rfllird ill 4.) eallwlntd an follown :
E#lm
3. APPARATUS AND REAGENTS C4nwucc of servlnc or wmr. pwfwnt= -
x
whwo :
3.1 The n~qmmt us 1!nd rengent:; sha] i bc m
.~ ~ f I,w lllin]l~r O( CWrlmof yarn In rll~ np~”tl~~o.
tlcscrilwd in Ihe nwt hndc rnfmmred in 4. .t =1 Iw rII14tI
lm~twww Ihv ynrn nd nstk ctf WIW W
rnhh .
4. PROCEDURE (,=tho l~nglh Of ]fiy ~r tlu. srrnp m msrvlnc, ID*W.O
4.1 The length of )ny of the serving or wrap 1)--- tb rwdnot W ynw 917* [ tnhl~ I).
slI:Ill Iw tll’tcrltlint’11 :1+{Im-rilml ill Ill:! lI(x1 1531 Ii_=-llw wlunl to J’ t“lls. A.
I’=-’lho @qIIJIl tt} 1, TaII. ,\ ●
and thp wdue recorded as L.
52 ‘Uhilws 01 imrwiw? slwI-i LoIi iii Ilifi dcti:i!
42 TIIP nngln of th swving ddl h deter.
qn.rilhvlt il!ll. onr qwitlwu fr4mi ench irtspac=
mind ns duscribd in mcthlti lW1 nml tllc WIIIO
ti4~ll uuit Auillb [Ad.
rec’ol”(lwl ns .’1.
54 “l”lw rwvwxgo 0( t III’ u riIp ur serving of
43 The tntn] numlnw of ends of ytrjl in the t ho imq uwl.iolt unit A II Ix the rvwdt ubtuincd
Fp=imcn shn II b dctwmirted as drscrihvd ill from Ihe qwimwl testcwL
met Id WMl A tho vnlur merwtlwl rw N. q”! j \YiIwl IIIOIW Ih: III {w FINW
.-. illltw is
4.4 TIIe ynrn sim slinll Iw (Irl rrllti Id as tmlt.fl. 1II(. (wwrngc of tlm wruIl or wwving of
drserilwd in me(hod ~1~41 and tlw \.nlIIP ~ t.lw iuslwt i,m uhit droll k tile nwrug~ of the
cortlod, The constnnt-l~ for ynrn twulls 01)1Ninwl from tho S]mrimcns tcstrd.
iu tnldv 1. 5.4 ‘1’he rrwrrngo of fhe wmp or seining of
4.5 If two mnp9 or servings the innpect ion unit shall bn rorwrdcd to the
ewh shall be tested Oepntately. nearest 1.0 percent.
Method 8211
Aprif 14, 1%7
commodato the ends of the epecimen. ‘1’lte U-portion of the epacimen immersed in the
cover SIIOIIbe of corrasion-resisting metal. wctm. The water level ehall h mdntsined
3M0 C%Mwm ch?m+fc, •nhydrm~ for flush with the under aide of the ccmer plnte
desiccnnL during the ~ dare being taken that no water
391.11 mtzzcd UMtar. ~ in contact with the ends of the specimen.
Mdltod ml -.
4.L6 TIM qeoitnan shall be exposed in th water. The raroaining aurfem water 8h811 be
water bath fors period of 166 hours nts tam- removed by blotting lightly with clean, Iintlq
pcrnture of 70° =2” C. {153” *4’ F.) ●fter abeorbent gause sad tk specimen weighed as
which the corm plste with the specimen shall be demribed in 4.1.5. T%e epecimen ehsll be
mmored from the bath and transferred to s dried, amle& and weighed as dwcribed in 4.1A
similar vml filled with distilled water at s & RESULT’S
tampemtum of 94”=8” C. (766 *8° F.). The M cdcnMOa
qwcimen shall be nllovwd to remain in this bath 5J.1 The area of the irnmerwd portion of the
for not leas thnn 6 minutee nor more than 15 specimen shall be calculated be follom:
minutes The vraahere shrill then be cnmfully Conductor eke No. 1 AWG or smaller:
remowd from the specimen. The specimen AIvla,#muare~xL
ahnll be removed from the bath ●nd shaken to where :
remo~e Inoae water. The remaining surfnee c-me et~ of Speclmea becom wtll&
Iocbee.
water shall be removed by Motting the qxwiroen L=tbe len@h of lbe Imnwrml speclmm. tocbos.
lightly with clean, lintleas, absorbent gnuze,
Conductor k Xc. Oor ia~.r:
The qwcimcn shell then he weighed 10 the
ncnrest nlilli~=m within 3 minutm nfter rc- Ares, 8 quare lw+wa=~(~X W) +ST(L+W)
movnl from the water. This wright ALU be wlm~:
W’-tlw whltlt of the qwrlmon, Inch . ‘
recorded ns W’r, Ldhe lm:th of Ibc qurlmen, lncb.
4.1.6 Tho epecinwn dI:~ll he dried in the T-the Ihkkm.en of the g~wvltuen ●fter buglng, Iuch.
vncuurn, 4.1.1, over cnlcium chlorido at rt tem-
6.1.2 The moisi.nrs Asm@ion of tbe spu5-
ptwature of 70” *2” C. (158°=40 F.) for 24 nmn droll be cahmlnted nn folhwe:
hmm, cooled to room temprrnt ure in n rlesima- Where the original wriuhtt TV,, is Iew than
(or, :~nd weighed LO the ncrmst Iuilligmm the tinnl weigl~t, II’,, of the dried spmimcn:
witl)in
The tirying
3 nliltutc~
nn(! WPighing
after rermmil
shtdl be continued
from
at
(ltwimmt{m.
MnMnw nl-qwkw :W egmre !;r.* grsw——
Tr,- w,
m
-J”
24-hour Mervale untiI the weight is conebmt Wlmre the origimd weight, W,,. is grenter
within I milligram in two coneccutivo w-eigh- t hnn the final weight, lV,, of the drkd qmci-
in~ or until any one weight is greater than the men:
previous wei@L The lowed weight shall be W*-WS
Mdsture dnwrptlon per mmere Inrh. croulrn~ --N—
worded ns W4
lrhcrs :
42 Conductor Nm O AWG and larger. W,=tb+ crktnal ~Eht of spertmcn. xvnnw.
42.1 The huffed qmcimen shun be Awncd, lF,-tlte weight ~wlmen afwr bnmersiw. fmnrna ~
cooled, and the thickness drtcrmined as de-
ecribwl iu method 112L ‘1’hevnluu hdl be re-
W,- lhe wdght
S=1 he urm
c rzum.
of the qcdmen after
eqLW9
)
corded as T.
inch .
422 ‘J%o specimen shall tkn be we;f$md ae
described in 4.1.2 and immersed in the water 52 UIJlms othcrwirn spocidcd in the dctnil
bath at a tempemture of 7[)- z!!” (;. ( 158° =4°
upecifhation, three specimens from coch hwpco-
tirm unit shall he tested.
)
F.) for n yeriod of lfi bourn, At the cnd of the
expoeure period, the tprimcn shall k t rnns- 5.3 mO ntOiA UIV absorption of the imnda-
ferred to a similar bath of distilled water at s t.ion of the inqmction unit 8haU be the ●verage
temperature of 24°att0 C. (75’’=5° F.). The of the results obta.med fmm the qecimam
spcrirncn ahnll be ●llowed to remain in this tested. ,.,.
b~tth for mt lFSSthnrt 5 minutes nor more than S4 Mnishm nheorptinn of the inauhdion of
15 minuka Tlte specimen shsl] be removed from the inspection unit shall be recorded ta the
the bath and ~hnken to remove loose surfnee nenreet 0.01 gram per quare inch.
Mcthotl 8221
ADti 14, ‘1%7
~ ............... ~E:::::::::::i
............ #
No. 6-.......--------.........-----
UO. L.---- ........ . .. ... .. ... ... .
NO.2------------------------------
11$
1!;
:fi,
lL50,tNKleir, roils. . ------------------
7n0,0tMlcir. milk.
~wcb dr. m,,”
7AIMMNI
.-. --- . . . . . . . .. . ..-
mih. --------------------
- ltl~
Al!i
t.,
.-
NW 1.- . . . . . . . . . . ------------------ . . . . . . . . . . --------- --- l~lf
t Tbo whros for mandmt tiismrtrr in the table apply thrfmhmt to Itwlstod conductors hsvin~ two fikwn
oovwhqm. For Ntm 14, 12, III, nwt R A ~~u cnmtuctura havhm mm 6twoua mverlIw the rnandrcl tioIMu~ arc to
b %* !L fib and ‘Mo Iuch, raspectiwtv
METHOD S231
ADril 14, 1967
Method 8311
April 14, 1%7
Method 8321
Ad 14. 1%7
,?-
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