THE E3500 HAND HELD EXPLOSIVE

DETECTOR
User Guide

MANUAL PART NUMBER D350600

REVISION F
APRIL 2009
FOREWORD

Copyright ©2009 Scintrex Trace Corp. All rights reserved.

The manufacturer (MFR) reserves the right to make changes to this document and the products, which it
describes without notice. The MFR shall not be liable for technical or editorial errors or omissions made
herein; nor for incidental or consequential damages resulting from the furnishing, performance, or use of this
material or of the accompanying Software or any files derived from the Software.

The product supplied by the MFR, when properly maintained, operated and calibrated in accordance with the
instructions in this User Guide, will detect specific explosives or narcotics residues at such levels and under
the conditions described in the MFR’s published specifications. The MFR disclaims responsibility for the
detection of any particular explosives compound under any particular circumstances.

The customer and/or user releases and agrees to hold harmless the MFR, its officers, servants, employees,
agents and contractors, against any and all claims, demands, actions and liabilities whatsoever, arising from
the use or operation of the product.

No part of this document may be reproduced or transmitted in any form or by any means, electronic or
mechanical, for any purpose, without the expressed written permission from Scintrex Trace Corp.

E3500, Scintrex Trace Corp, and the Scintrex Trace Corp logo are trademarks of Scintrex Trace Corp.

Other company or product names referenced may be the trademark or registered trademark of their respective
companies.

Scintrex Trace Corp

300 Parkdale Avenue
Ottawa, Ontario K1Y 1G2
CANADA
Phone: 613-224-1061
Fax: 613-224-2603
Email: [email protected]
Internet: http://www.scintrextrace.com

Printed in Canada

- ii - The E3500 Hand Held Explosive Detector

 FOREWORD

Standard Warranty
Scintrex Trace Corp warrants that the products it manufactures and sells will be free from defects in materials
and workmanship for a period of one (1) year from the date of shipment from an authorized Scintrex Trace
Corp distributor or reseller. If a product proves to be defective within the respective period, Scintrex Trace
Corp, at its option, will repair the defective product without charge for parts or labour, or will provide a
replacement in exchange for the defective product. Batteries are excluded from this warranty.

To obtain service under this warranty, customers must notify Scintrex Trace Corp of the defect before the
expiration of the warranty period and make suitable arrangements for the performance of service. Our toll-
free number within North America is 1-877-877-7147. If calling outside North America, our number is 1-
613-224-1061. Support is available during normal working hours, 8:00 a.m. to 5:00 p.m., EST. Customers
shall be responsible for packaging and shipping the defective product to the service center designated by
Scintrex Trace Corp, shipping charges prepaid, and with a copy of customer proof of purchase. Scintrex
Trace Corp shall pay for the return of the product to the customer if the shipment is to a location within the
country in which the Scintrex Trace Corp.service center is located. Customers shall be responsible for paying
all shipping charges, duties, taxes, and any other charges for products returned to any other locations.

This warranty shall not apply to any defect, failure or damage caused by improper use or improper or
inadequate maintenance and care. Scintrex Trace Corp shall not be obliged to furnish service under this
warranty:
To repair damage resulting from attempts by personnel other than certified Scintrex Trace Corp
representatives to install, repair, or service the product;
To repair damage resulting from improper use or connection to incompatible equipment;
To repair any damage or malfunction caused by the use of non-Scintrex Trace Corp supplies; or
To service a product that has been modified or integrated with other products when the effect of
such modification or integration increases the time or difficulty of servicing the product.

Except as provided in this warranty, Scintrex Trace Corp makes no warranty of any kind, expressed or
implied, including, but not limited to, the implied warranties or merchantability and fitness for a particular
purpose. In no event shall Scintrex Trace Corp be liable for indirect, special, incidental or consequential
damages.

All servicing to be performed by Qualified Service Personnel only.

Before operating the E3500, become familiar with all the safety symbols and instructions in this guide to
ensure that the equipment is operated and maintained safely.

Regulatory Statement
This equipment has been tested and complies with the emission limits for “Class A” and immunity
requirements of EN 61326:1997 + Amendment A1: 1998. A2: 2001, A3: 2003. Electrical equipment for
measurement, control and laboratory use – EMC requirements and verification, in accordance with EMC
directive 89/336/EEC (including amendments). For products safety, it complies to EN 61010-1:2001 in
accordance with the Low Voltage Directive 72/23/EEC (amended by 93/68/EEC).

Software Version
This User Guide covers operation of the E3500 with Operating Software, release date January 2009.

Safety Instructions
The following safety instructions must be observed whenever the E3500 is operated, serviced, or repaired.
Failure to comply with any of these instructions or with any other precaution or warning in the E3500 User
Guide is in direct violation of the standards of design, manufacture, and intended use of the equipment.
Scintrex Trace Corp assumes no responsibility for the customer's failure to comply with any of these safety
instructions.

The E3500 Hand Held Explosive Detector - iii -

FOREWORD

Safety Symbols
The following safety symbols are used in this guide. The instructions and precautions associated with these
symbols must be observed whenever the E3500 is operated, serviced, or repaired.

WARNING This procedure can result in serious injury or loss of life if not carried out in
proper compliance with all safety instructions. Ensure that all conditions necessary for
safe handling and operation are met before proceeding

Caution. Always refer to the text accompanying this symbol for instructions.

Caution. Risk of electric shock.

On (Power)

Off (Power)

When operated on an external DC power source, the E3500 is connected

directly to earth via a power supply cord. The following symbol is used to
indicate a protective earthing conductor terminal in the equipment

Before Operation
Become familiar with all the safety symbols and instructions in this guide, to ensure safe operation and
maintenance of the E3500.

Inspect the equipment for any signs of damage and read the User Guide completely.

Set up and verify the performance of the E3500 as specified in Section 2 – Getting Started.

Ensure that equipment and any devices or cords connected to it are properly grounded.

While Operating
Do not operate the equipment when its covers or panels have been removed.
Do not interrupt the protective earthing connection. Any such action can lead to a potential shock
hazard that could result in serious personal injury or death.
Do not operate the equipment if an interruption to the protective earthing is suspected ensure that
the equipment remains inoperative until it is confirmed to be in a safe operating position.
Use only the type and rating of fuse specified by the manufacturer as appropriate for the equipment.
Do not use repaired or modified fuses. Avoid any situations that could short-circuit the fuse(s).
Do not attempt adjustments or perform any maintenance or repair procedure if the cover or panels
are opened while the equipment is connected to a power source. Only qualified service personnel
should perform any procedures required under these conditions.
Do not operate the equipment in the presence of flammable gasses or fumes – this is extremely
hazardous.
Do not attempt to perform any adjustment, maintenance or repair procedure that is not described in
the User Guide.

Electrical Safety
To avoid risk of injury or death, always observe the following precautions before operating the E5000.

Use only a power supply cord with a protective earthing terminal.

- iv - The E3500 Hand Held Explosive Detector

 FOREWORD

Connect the power supply cord only to a power outlet (3-prong receptacle) equipped with a protective earth
contact. Never connect to an extension cord that is not equipped with a functioning protective earth contact.

Willfully interrupting the protective earth connection is prohibited.

SENSITIVITY TO SOLVENT COMPOUNDs: The E3500 is highly sensitive to certain

solvent compounds commonly found in laboratories. Solvents such as carbon tetrachloride,
chloroform or methylene chloride should never be introduced into the unit, as such
compounds will severely diminish detector sensitivity.

POTENTIAL ELECTRICAL HAZARD: The E3500 operates at high voltages and

amperages. No component of the electrical system should ever be serviced with the power
on. The electrical system includes all power supplies, transformers, electrical connections
and fuses. Only qualified personnel should attempt repair or maintenance of the E3500
electrical system.

SENSITIVITY TO MOISTURE: Liquids should never be introduced into the E3500.

Direct exposure to liquids may cause serious damage to system components. The E3500 is
not water resistant, and should always be adequately protected from exposure to high
humidity, precipitation and other sources of moisture.

DAMAGE: Do not operate the equipment if it bears any sign of damage to any portion of its
exterior surface such as the outer casing or panels.

ELECTRICAL SHOCK: Some of the equipment’s capacitors may retain an electrical

charge even when the equipment is disconnected from its power source.

E3500 SENSOR: The E3500 sensor contains a dilute Alkaline solution of potassium
hydroxide. This solution is mildly caustic and can cause skin irritation or damage sensitive
surfaces (MSDS sheets). Do not ingest or get contents on skin. In case of skin contact, flush
immediately with water. Care should be exercised to prevent rupture of the E3500 sensor
membrane. Should the membrane be damaged and leakage occur, the sensor and area
should be washed with a dilute solution of household vinegar. Used or damaged sensors
should be stored in a Ziplok or equivalent bag. The E3500 sensor cannot be discarded
without treatment (Section 5 - Troubleshooting and Maintenance).

The E3500 Hand Held Explosive Detector -v-

TABLE OF CONTENTS

Table of Contents

SECTION 1 – OVERVIEW................................................................................. 1-1

1.1 General Background.................................................................................. 1-1

1.2 Principles of Operation.............................................................................. 1-1
1.2.1 Sample Collection Cycle ................................................................... 1-2
1.2.2 Vapour Mode ...................................................................................... 1-2
1.2.3 Particulate Mode ................................................................................ 1-3
1.3 Analysis Cycle............................................................................................ 1-3
1.3.1 Vapour Mode ...................................................................................... 1-3
1.3.2 Particulate Mode ................................................................................ 1-3
1.4 Results Phase............................................................................................. 1-3
1.5 Description of Parts ................................................................................... 1-6
1.6 Rear Panel................................................................................................... 1-7
1.7 Keypad and Display Panel ........................................................................ 1-7
1.7.1 Status Indicators (LED) ..................................................................... 1-8

SECTION 2 – GETTING STARTED .................................................................. 2-1

2.1 Unpacking and Inspection ........................................................................ 2-1

2.2 Powering the E3500 ................................................................................... 2-2
2.3 Connecting the Battery.............................................................................. 2-3
2.4 Installing the E3500 Sensor ...................................................................... 2-3
2.5 Turning on the E3500................................................................................. 2-3
2.6 Verifying Performance of the E3500......................................................... 2-4
2.6.1 Vapour Mode ...................................................................................... 2-4
2.6.2 Particulate Mode ................................................................................ 2-7
2.7 Turning Off the E3500................................................................................ 2-8

SECTION 3 – OPERATIONS ............................................................................ 3-1

3.1 Battery Operating Requirements .............................................................. 3-1

3.2 Changing the Battery................................................................................. 3-2
3.3 Self Test Mode............................................................................................ 3-2
3.4 Changing the E3500 Sensor Cartridge..................................................... 3-3
3.5 How to Sample Vapours ............................................................................ 3-5
3.6 How to Sample Particulates ...................................................................... 3-5
3.7 Clearing the Alarm ..................................................................................... 3-6
3.8 Decontamination Cycle ............................................................................. 3-6

- vi - The E3500 Hand Held Explosive Detector

 TABLE OF CONTENTS

SECTION 4 – APPLICATIONS ......................................................................... 4-1

4.1 Sample Collection ...................................................................................... 4-1

4.1.1 Vapour Pressure ................................................................................ 4-1
4.1.2 Vapour Sampling Background.......................................................... 4-1
4.2 Vapour Sampling Methods ........................................................................ 4-1
4.3 Particulate Sampling Background............................................................ 4-2
4.4 Particulate Sampling Method .................................................................... 4-2
4.4.1 Glove Sampling .................................................................................. 4-3
4.4.2 Direct Sampling with a Screen.......................................................... 4-4
4.5 Smart Sampling Area Identification ......................................................... 4-4

SECTION 5 – TROUBLESHOOTING AND MAINTENANCE ........................... 5-1

5.1 Troubleshooting......................................................................................... 5-1

5.2 Maitenance.................................................................................................. 5-2
5.2.1 Decontaminating Sample Screens ................................................... 5-2
5.2.2 Replacing the Fuse ............................................................................ 5-3
5.2.3 Recovering from Severe Contamination.......................................... 5-3
5.2.4 Vapour Contamination....................................................................... 5-3
5.2.5 Refurbishing Vapour Inlet Assembly ............................................... 5-3
5.2.6 Particulate Contamination................................................................. 5-4
5.2.7 Replacing Particulate Pyrolyzer ....................................................... 5-4
5.3 Service and Maintenance Call Procedures .............................................. 5-5
5.4 Return of Goods for Repair or Disposal .................................................. 5-5
5.5 Handling and Storage of E3500 Sensors ................................................. 5-6
5.5.1 Neutralization Method........................................................................ 5-6

APPENDIX A – E3500 BATTERY .................................................................... A-1

APPENDIX B – COMMUNICATIONS............................................................... B-1

APPENDIX C – SPECIFICATIONS .................................................................. C-1

The E3500 Hand Held Explosive Detector - vii -

TABLE OF CONTENTS

THIS PAGE IS INTENTIONALLY LEFT BLANK

- viii - The E3500 Hand Held Explosive Detector

 OVERVIEW

SECTION 1 – OVERVIEW
1.1 General Background

The E3500 is a lightweight, hand-held, rapid-response explosives detector. It is

used for detection of vapour or residue, which may indicate the presence of one
or more of the following explosives:

EGDN NG PN TNT
EGMN DNT Semtex Black Powder
DMNB RDX C-4 TATP
O-MNT PETN Detasheet HMX
P-MNT AN Primacord Dynamite

Individuals may unknowingly contact trace amounts of explosives during their

daily activities. An alarm generated by the E3500 indicates a need for further
investigation by authorized personnel. Alarms do not imply guilt of
possession of an explosive substance on the part of any individual.

Vapour sampling is performed by sampling the air in and around an area where
explosives are suspected to be present. Particulate sampling is performed by
wiping the surfaces of suspect articles and transferring the particulates collected
onto a metal sample screen. The sample screen is then inserted into the E3500
for analysis. The analysis is usually completed within 20 seconds and the results
displayed on the LCD (liquid crystal display). An alarm is indicated by a red light
and an audible signal.

Under normal conditions, a fully charged NiMH battery will provide two to three
hours of continuous operation (or analysis of more than 200 samples). The
E3500 is supplied with a spare battery, and a charger capable of fully recharging
a battery in one hour. Typical warm up time is one minute.

1.2 Principles of Operation

The E3500 is a dual mode explosive detector capable of operating in vapour as

well as in particle mode. The detection technology relies on thermal
decomposition of explosives such as RDX, PETN, AN, Urea Nitrate, TNT, NG,
TATP, and Taggants yielding to the formation of chemicals which specifically
react with luminol to generate light. The amount of light generated by this
chemiluminescence reaction is directly proportional to the amount of explosives
analyzed.

The three phases of the E3500 explosives detection process are the sample
collection cycle, analysis, and results phase.

The E3500 Hand Held Explosive Detector 1-1

 OVERVIEW

1.2.1 Sample Collection Cycle

The E3500 operates in the vapour and particulate modes. The only difference
between the two modes is in the sample collection cycle. The analysis cycle and
results display are common to both modes. The Mode Selector Switch sets the
E3500 to vapour or particulate mode. A schematic of the basic operation is
shown in Figure 1-1 below.

Explosive Particulates
Sampling
Screen Pyrolyzer

Pump:
Desorber 0.8 LPM Processing
1.5 LPM Sampling
N O2
Mode Selection Valve Luminol Cell Chamber

Luminol
Explosive Vapours Solution
PMT Signal
Desorber

Vapour trap Pyrolyzer

Photomultiplier Tube (PMT)

Figure 1-1 E3500 Basic Operation Schematic

1.2.2 Vapour Mode

With the E3500 set to vapour mode, pressing the Sample Button starts the
Sample Pump that draws air into the unit through the Vapour Inlet at a flow rate
of approximately 1.5 liters per minute. The air drawn into the E3500 passes
through a Vapour Collector Tab that selectively adsorbs explosive vapour
molecules. The duration of the sample time is adjusted by the Technician
during calibration. Typically, sample times of five to fifteen seconds are used.
During this time, the LCD message center will show Sampling. Following the
sample collection cycle, the analysis cycle is initiated.

1-2 The E3500 Hand Held Explosive Detector

 OVERVIEW

Following the sample collection cycle, the Sample Pump switches into a lower
flow mode and the analysis cycle is initiated, the LCD will show Processing. The
E3500 may be moved to another location while the analysis is being performed.

1.2.3 Particulate Mode

Using the Mode Selector Switch, the operator sets the E3500 to particulate
mode. In the particle-sampling mode, sample collection is performed by the
operator using a metal sample screen or cotton glove. In the case of glove
sampling, the operator wipes the surface with a cotton glove, then rubs the glove
onto the sampling screen. This screen is then inserted into the particle injector
See Figure 1-4 (page 1-6).

The operator then presses the blue Sample Button to initiate the analysis cycle.

1.3 Analysis Cycle

1.3.1 Vapour Mode

The first step in the analysis cycle is the rapid heating of the Vapour collector
tab for approximately 2.5 seconds. The tab is indirectly heated electrically to
desorb the explosives which then move to the pyrolyzer. The elevated
temperature of the pyrolyzer converts the organo-nitrate-based explosives
molecules to NO2 that is easily measured by the chemiluminescence detector.
This method is known as thermo-chemiluminescence.

1.3.2 Particulate Mode

In the Particulate mode, the explosives are directly desorbed from the sampling
screen to the pyrolyzer where they are converted to NO2.

The NO2 is picked up in the air stream and transferred directly to the
chemiluminescence sensor. As the NO2 passes across the sensing surface of the
detector, light is generated. The light is collected by a highly sensitive
photomultiplier tube (designed for single photon counting), which converts light
into an electrical signal. The electrical signal is sent to a micro-processor that
measures the signal strength.

The overall sampling and analysis time is about 20 seconds. During this time,
the LCD message center will show Processing.

1.4 Results Phase

The presence of explosives is verified when the signal strength exceeds the
alarm threshold within a time window expected for the explosives. If explosives
are detected, an “ALARM” message will be displayed (see figure 1-2). The
microprocessor calculates a number that represents the strength of the

The E3500 Hand Held Explosive Detector 1-3

OVERVIEW

measured signal. This number is displayed on the LCD screen as the Peak
Height = xxxx and Peak Area = xxxx values at the end of the analysis period,
Figure 1-3 on page 1-5. The displayed value is already corrected (i.e. minus
threshold value (THH), for instance if THH is 2000 and the total signal is 5000
then the displayed number will be 3000). At the end of the sampling process the
result is graphically displayed on the LCD and an alarm sound will be audible if a
trace of explosives was found. At the same time the Red LED will be lit.

Message Centre
ALARM
12.1V Battery Voltage
023548 PMT Output

P04X Zoom Level

(01-20X)

WL1 Mode

Figure 1-2 E3500 Graphical Result Display

a) Curve: the curve depicts the signal output from the sensor versus time.
Whenever a suspicious material is found, the graph should show two
peaks with different intensities (peak I > peak II).
b) Alarm: if a positive identification has been found, then the Red LED and
an audible sound will turn on. At the same time ALARM on READY will
appear on the LCD.
c) Battery Voltage: the number represents the strength of the battery in
volts. When the value blinks the unit will still be operational for about 30
minutes.
d) PMT output: the number represents the idle baseline value from the
sensor. The typical value for this number is between 10,000 to 100,000.
This number can be higher when the instrument is constantly being used
e) Zoom Level: the user can change the scale of the graph and zoom in
and out by pressing the up and down arrow keys. The zoom level is
indicated on the display (1-20X).
f) Mode: the mode is indicated next to the zoom level. P is for Particle
mode and V is for Vapour mode.
g) WL1: the cursor indicates the reference point that the software is using to
determine if an alarm condition exists. If the peak position is to the left of

1-4 The E3500 Hand Held Explosive Detector

 OVERVIEW

WL1 the alarm will not sound; if the peak position is to the right of WL1
the alarm will activate.

By pressing the user can switch to the text window, where the
numerical results are displayed.

Run Number

Mode
PARTICLE RN 0189 Peak Height
PEAK HEIGHT + 0025
PEAK AREA 022354 Peak Area

PK POS 35
Peak Position

Figure 1-3 E3500 Numerical Result Display

a) MODE: PARTICLE or VAPOUR.

b) RUN NUMBER (RN): this value indicates the number of samples taken
with one E3500 Sensor Cartridge.
c) PEAK HEIGHT: the value represents the intensity of the signal. When an
alarm is found, a positive number is displayed.
d) PEAK AREA: this value is a different representation of the signal
intensity. When an alarm is found a positive number is displayed.
e) PEAK POS: the value represents position of the peak in time (Figure 1-3,
i.e.: 35 is equivalent to 3.5 seconds). If the PK Pos is less than the WL1
there will be no alarm.

The E3500 Hand Held Explosive Detector 1-5

 OVERVIEW

1.5 Description of Parts

Mode Switch
Selection Sample Screen
Injector Sample Button

Vapour Inlet

Battery

LCD Keypad

Rear Panel

Access to the
E3500 Sensor

Figure 1-4 The E3500

a) Sample Button: The blue Sample Button on the handle is used to

initiate a sample cycle when the E3500 is in READY mode. It is also used
to start the decontamination cycle.
b) LCD – Keypad: The LCD allows the user to visualize and navigate
through various screens.
c) Mode Selector Switch: The Mode Selector Switch is used to switch
between Vapour and Particulate sampling modes.
d) Sample Screen Injector: After a particulate sample is collected on a
sample screen, the screen is inserted into the Sample Screen Injector.
e) Vapour Inlet Nozzle: The Vapour Inlet Nozzle is used to draw vapour
samples directly into the E3500 for analysis.
f) Battery: The E3500 is powered by a 12-Volt rechargeable NiMH Battery
that plugs into a receptacle in the Rear Panel of the unit.

1-6 The E3500 Hand Held Explosive Detector

 OVERVIEW

1.6 Rear Panel

On/Off Switch
Earphone Receptacle

Volume Control
5 Amp Fuse
Battery Receptacle

RS-232 Terminal External Power

Figure 1-5 Rear Panel of the E3500

a) Power Switch: The Power Switch is a push-on/push-off switch. It is used

to start up the E3500 and to shut it off.
b) Volume Control: The volume of the audible alarm can be adjusted by
turning the Volume Control knob located on the left Rear Panel.
Alternatively, the audible alarm can be immediately shut off by pressing
any keys on the Keypad of the Display Panel. When another sample is
initiated, the volume will return to the default setting of the control knob.
c) Earphone: Operators can connect an Earphone to the earphone
receptacle in order to monitor for audible alarm signals, without disturbing
other persons in the vicinity. Inserting an earphone jack into the
earphone receptacle on the left Rear Panel disables the internal speaker
of the E3500.
d) External Power: The External Power Receptacle is used to connect the
external 12 VDC battery vehicle adapter or an external AC power supply.
e) RS-232 Terminal: The RS-232 Terminal is used to connect a computer
terminal to download analysis results data.
f) Fuse Holder: The fuse holder is mounted in the right Rear Panel which
allows easy replacement of the 5 Amp main fuse.

The E3500 Hand Held Explosive Detector 1-7

OVERVIEW

1.7 Keypad and Display Panel

The Keypad and Display Panel in Figure 1-6 indicates the operating status and
allows the Supervisor or Technician to change detection parameters.

It is recommended that parameter settings be adjusted only by designated,

trained personnel.

1.7.1 Status Indicators (LED)

There are two status LED’s (light emitting diodes) located at the top of the
Keypad and Display Panel illustrated in Figure1-6 below.

The green READY LED illuminates when the E3500 is first turned on to verify
that the LED is functioning; and when the unit is in READY mode (waiting for the
operator to initiate a sample analysis).

The red ALARM LED illuminates when the E3500 is first turned on to verify that
the LED is functioning. The red LED ALARM is also initiated as a result of a
positive detection; or if an error message is displayed on the LCD screen.

PARTICLE RN 0189
PEAK HEIGHT + 0025
PEAK AREA 022354
PK POS 35

Figure 1-6 Keypad and Display Panel

1-8 The E3500 Hand Held Explosive Detector

 GETTING STARTED

SECTION 2 – GETTING STARTED

2.1 Unpacking and Inspection

The E3500 and its accessories are contained in a transportable carrying case.
The case should only be opened when it is lying down flat. All items should be
accounted for and should have been received in good condition. Open the case
by unfastening the two latches at the front of the case. Remove each item from
the case and verify it against the checklist shown in Table 2-1.

Inspect the exterior of the E3500 and its accessories for any evidence of damage
resulting from shipping. If there are any discrepancies between the checklist and
the items received, or if there is any evidence of damage, contact your Scintrex
Trace Corp Sales Representative immediately.

Refrigerate unused E3500 sensors for long-term storage.

The E3500 Hand Held Explosive Detector 2-1

GETTING STARTED

CHECK-
ITEM QTY DESCRIPTION PART NUMBER
LIST
1 1 Carrying Case 943 213
2 1 E3500 D350 505
3 2 NiMH Battery D100 513
Universal Battery Charger
4 1 D100 550
(90 V – 240 V)
5 1 Vapour Test Kit D1000524
6 1 Particulate Test Kit D1000526
7 12 Particulate Sample Screen D350 532
8 20 Cotton Glove 943 019
9 1 Audio Earphone 943 018
10 5 5 Amp Fuse 943 009
11 1 User Guide D350 600
12 1 E3500 Sensor (pack of 12) D350 548
13 1 RS-232 Cable 1002813
14 1 Shoulder Strap 1002866
Screwdrivers; Philips, Flat 540 006,000 359,
15 3
Head, Allen Key 1002662
Sample Accessory Kit
16 1 D350 549
(includes)
1 Vapour Injector Assembly D350 520
1 Particle Pyrolyzer D350 514
2 Needle Probe, 2 inch long 250 302
1 Nozzle Vapour 943 210

2.2 Powering the E3500

The E3500 can be powered by a re-chargeable Scintrex Trace Corp 12 Volt

NiMH battery, an optional external 12 Volt DC battery, car adaptor, or an optional
AC power supply. Under normal conditions, a fully charged NiMHattery can
provide up to three hours of continuous operation.

The E3500 is supplied with a spare NiMH battery, and a charger capable of fully
recharging a battery in approximately one hour. The NiMH battery is shipped in
storage mode. The customer must provide a first time charge of two hours. It is
recommended that both of the batteries be fully charged before using the E3500.
The battery charging procedure is described in Appendix A.

2-2 The E3500 Hand Held Explosive Detector

 GETTING STARTED

2.3 Connecting the Battery

To connect the battery, remove the E3500, both batteries, and the charger from
the carrying case. Then insert the battery into the receptacle at the rear of the
E3500 and slide it forward, as shown in Figure 2-1 below. The battery should
snap into place to ensure a proper connection.

Slide battery forward until it

snaps into place

Figure 2-1 Connecting the battery

2.4 Installing the E3500 Sensor

Make sure that the E3500 Sensor is installed right side up and the cover closed.

2.5 Turning on the E3500

After the battery has been installed, and the external battery or AC power supply
has been connected, the E3500 can be turned on.

On the Rear Panel of the E3500, press the on/off power switch. It takes two to
three seconds for the E3500 to initialize, after which time the display will
indicate:

SCINTREX TRACE

E3500 V X.XX (Software version number)

Following an internal system check, the E3500 enters a initialization mode for a
period of approximately sixty seconds. The LCD will display SELF-TEST with a
timer indicating the number of seconds remaining. When SELF-TEST mode
ends, the E3500 enters READY mode shown in Figure 2-2. The green Ready
LED remains illuminated and the red Alarm LED goes out.

The E3500 Hand Held Explosive Detector 2-3

GETTING STARTED

The E3500 is operational if the measured and displayed baseline value is

between 10,000 and 100,000. If the baseline is not within the recommended
range, see Section 5 - Troubleshooting and Maintenance.

If the battery indicator is steady in the graphical window, turn the E3500 off and recharge
the battery or replace it with a fully charged battery.

PARTICLE RN 0189
Self Test PEAL HEIGTH + 0025
PEAK AREA 022354
PK POS 35

Figure 2-2 Display in Self Test mode

2.6 Verifying Performance of the E3500

Prior to sampling for explosives, it is recommended that the operator verify that
the E3500 is functioning properly by testing its performance using the appropriate
test vials supplied. The Vapour Test Kit contains DMNB, while the Particulate
Test Kit contains PETN.

The performance verification of the E3500 should be done on an ongoing basis.

Some instances include:
after transportation,
before it is first used for sampling operations,
at the beginning of each work day or shift,
whenever the unit has been unused for an extended period of time, or the
unit has been turned off, or
whenever a malfunction is suspected.

Performance is verified using background testing and vapour and particulate test
kits.

2.6.1 Vapour Mode

Background Testing
Background testing should be completed before verifying performance with the
test kit. Background testing consists of an analysis that is done in a clean

2-4 The E3500 Hand Held Explosive Detector

 GETTING STARTED

environment, free of explosives and explosives residues. The procedure is as

follows:

1. When the unit has entered READY mode, set the E3500 to vapour
sampling mode by pressing the Mode Selector Switch toward the front
of the unit, as shown in Figure 2-3.

2. Initiate a sample by pressing the blue Sample Button on the handle of the
E3500. Do not hold the button down - press it only once. Once pressed:
The Sample Pump will be activated.
The green Ready LED will go out.
The LCD message center shows SAMPLING.

3. After approximately ten seconds, depending on the factory-set sampling

time, the pump will switch to a lower flow mode. The E3500 will then
analyze the sample for approximately 15 seconds, after which time
(depending on the pre-set sample delay period) the green Ready LED
will stay on. At this point the unit is ready for another sample. If an alarm
occurs, it may have resulted from vapours that were trapped inside the
pre-concentrator and the process should be repeated by depressing the
sample button again.

4. At the end of the analysis, the LCD will show the graphical representation
of the result. When in the text window, if the numbers displayed (PEAK
HEIGHT or PEAK AREA) are greater than the factory-set alarm
threshold, an alarm will be initiated.

Mode Selector Switch in Vapour

Sampling Position

Vapour Inlet
Nozzle

Figure 2-3 Mode selector switch to front for vapour sampling

Subsequent background test samples that consistently produce no alarms indicate that
the background level and alarm threshold of the E3500 are set correctly for vapour
sampling mode. It is common for the E3500 to initiate an alarm in response to the first few
samples taken when the unit is turned on after an extended shut down period. This is a
normal part of the initialization process and should be disregarded.

The E3500 Hand Held Explosive Detector 2-5

GETTING STARTED

Testing with the Vapour Kit

To verify that the E3500 responds properly to explosives vapours, a vapour test
is performed using a vial containing DMNB. This test should be performed only
after background testing has been completed.

Remove the vapour test vial from the E3500 carrying case. With the E3500 in
READY mode, press the blue Sample Button, unscrew the lid of the test vial,
and immediately place the opening of the vial over the Vapour Inlet Nozzle for
approximately two seconds (see Figure 2-4 below).

The test vial contains a small source of explosives vapours. To preserve

the contents always ensure that the lid of the vial is kept tightly closed
when it is not in use. When using the test vial partially cover the inlet
nozzle with the opening of the vial to ensure accurate sampling.
NOTE: The calibration should be done at near room temperature.

Figure 2-4 Vapour Mode Performance Verification

The pump switches to a low flow mode when the sample cycle is finished.
Remove the test vial from the nozzle and screw the lid on.

2-6 The E3500 Hand Held Explosive Detector

 GETTING STARTED

Following the analysis, an alarm should be initiated. The alarm should activate
and an audible signal heard (unless the volume was set low). If the numbers
displayed (PEAK HEIGHT or PEAK AREA) are greater than the factory-set alarm
threshold, an alarm will be initiated. If an alarm is not initiated by the vapour
sampling test, refer to Section 5 - Troubleshooting and Maintenance.

After the alarm is presented, run another test to clear the residue in the system.
This is known as a blank test. Subsequent background test samples that
consistently produce no alarms indicate that the background level and alarm
thresholds of the E3500 are set correctly for particulate sampling mode. The unit
should not alarm again, if so refer to Section 5 - Troubleshooting and
Maintenance.

2.6.2 Particulate Mode

Background Testing
Background testing should be done in a clean environment, before verifying
performance with the particulate test kit.

When the unit has entered the READY mode, set the E3500 to particulate
sampling mode by pressing the Mode Selector Switch toward the rear of the
unit (Note that each time the mode switch is activated, the instrument will
go into a self-test mode). With a clean sample screen inserted into the Injector
Inlet, (See Figure 2-6 on page 2-8) sample by pressing the Sample Button on
the handle of the E3500. Do not hold the button down - press it only once for
each sample. The LCD message center shows Processing.

The E3500 will then analyze the sample for approximately 15 seconds, after
which time (depending on the pre-set sample delay period) the green Ready
LED will illuminate. At this point the unit is ready for another sample.

Subsequent background test samples that consistently produce no alarms

indicate that the background level and alarm thresholds of the E3500 are set
correctly for particulate sampling mode.

Never handle sampling screens with your bare hands. The oil from human
skin, if introduced into the E3500, interferes with the detection of
explosives.

Testing with the Particulate Test Kit

Prior to sampling for explosives it is recommended that the performance of the

E3500 be verified using the particulate test kit supplied with the unit. The test kit
contains a PETN verification pen. This test should be performed only after
background testing has been completed, and after the background level and
alarm threshold have been set. The procedure is as follows:

The E3500 Hand Held Explosive Detector 2-7

GETTING STARTED

Figure 2-5 Particulate verification

Put the cotton gloves supplied with the unit on one of your hands, to ensure that
you do not contaminate the unit or yourself. Remove the test kit from the E3500
carrying case. Remove the verification pen from the test kit. Gently apply
medium pressure on the middle of the screen with the verification pen (as shown
above). A small deposit of liquid should appear. Wait approximately 30 seconds
to allow the deposit to dry.

Insert the sample screen into the Injector Inlet illustrated below, and then press
the Sample Button to initiate an analysis cycle. The analysis should initiate an
alarm.

2-8 The E3500 Hand Held Explosive Detector

 GETTING STARTED

Figure 2-6 Inserting the sample screen

If the unit fails to respond with an alarm, repeat the procedure with an additional
drop of liquid from the pen. If no alarm occurs after the second analysis cycle,
refer to Section 5 – Troubleshooting and Maintenance.

After an alarm, start another test to make sure there is no explosive

residue left in the system. This procedure is known as a blank test. If an
alarm is still present, refer to Section 5 – Troubleshooting and
Maintenance.

2.7 Turning Off the E3500

Whenever the E3500 is not to be used for an extended period of time, it should
be turned off. Press the on/off power switch on the Rear Panel.

The E3500 Hand Held Explosive Detector 2-9

GETTING STARTED

THIS PAGE IS INTENTIONALLY LEFT BLANK

2 - 10 The E3500 Hand Held Explosive Detector

 OPERATION

SECTION 3 – OPERATION
After the E3500 has been set up, its self-test cycle completed, and the unit’s
performance verified, sampling can begin. As discussed previously, sampling is
performed by either vapour sampling or particulate sampling.

Vapour sampling is performed by sampling the air in and around an area where
explosives are suspected to be present. Particulate sampling is performed by
wiping the surfaces of suspect articles and transferring the particulates gathered
onto a metal sample screen. The screen is then inserted into the Sample
Screen Injector Inlet of the E3500 for analysis. The sample analysis is usually
completed within 15-20 seconds and the results displayed on the LCD. An alarm
or hit, is indicated by a red light, audible signal, and a value displayed on the
LCD. If the analysis does not initiate an alarm, the next sample can be taken and
analyzed. If a sample initiates an alarm, the operator must follow the appropriate
procedures for the security environment they are working in and initiate the alarm
clearing procedure (see Section 3.7 for more details on Clearing an Alarm).

3.1 Battery Operating Requirements

Under normal conditions, a fully charged battery will provide up to 3 hours (or
approximately 200 samples) of continuous operation. When the battery voltage
falls to approximately 12 volts, the battery voltage indicator will blink until 11.5
Volts, as shown below in Figure 3-1.

READY
11.8V
023548
P04X

Figure 3-1

The E3500 Hand Held Explosive Detector 3-1

OPERATION

When the battery indicator is blinking, the E3500 will operate for an additional
thirty minutes before the battery is fully discharged and the E3500 stops
operating.

When the battery voltage drops to 10.8 volts, the BATTERY BELOW 10.8 V –
SHUT DOWN message appears on the LCD and samples can no longer be
taken. (Figure 3-2). While one battery is being used to power the E3500, the
other battery should be charging or fully charged and ready for use. It takes
approximately one hour to fully charge a battery.

ERR-BAT RN 0950
PK HEIGHT +0200
PK AREA +02000
PK POS 023

Figure 3-2 Low Battery Message Displayed on LCD

3.2 Changing the Battery

To change the battery turn off the E3500 by pressing the on/off power switch on
the Rear Panel. Press the battery lock mechanism and slide the battery out of
the back of the unit. Slide a fully charged battery into place, and ensure that it
snaps into position. Turn the unit on by pressing the on/off power switch on the
Rear Panel. The unit will automatically enter SELF TEST mode.

3.3 Self Test Mode

The SELF TEST mode will be initiated when the user performs one of the
following operations:
Turning on the unit.
Switching from Vapour to Particle Mode and vice versa.
After editing any operational parameters (not applicable to DATE or
THRESHOLD values THA and THH).
If the unit is left idle for 1 hour.
Opening and closing the E3500 Sensor Cartridge tray.

3-2 The E3500 Hand Held Explosive Detector

 OPERATION

At the end of each SELF TEST cycle the unit will automatically display the result
of the last blank sample. (See Figure 3-3).

PARTICLE RN 0950
PK HEIGHT +0200
PK AREA +02000
PK POS 23

Figure 3-3 Text Window

3.4 Changing the E3500 Sensor Cartridge

The E3500 Sensor Cartridge will need to be changed every 2000 samples. The
number of samples taken is indicated in the text window as RN (RN1500 would
mean that the E3500 sensor was used 1500 times) (Figure 3-4).

PARTICLE 1 RN 1500
PK HEIGHT +0256
PK AREA 02563
PK POS 23

Figure 3-4 Numerical Results Display

NOTE: If the unit has been stored in a cool place for a long period of time, the
E3500 sensor may have a longer lifetime. Make sure that the sensor is installed
right side up.

The E3500 Hand Held Explosive Detector 3-3

OPERATION

NOTE: It is recommended to refrigerate the E3500 Sensors not in use, in its

original package. However, the sensor may still be operational after 3 months
stored at room temperature if they are remain in the sealed package. If the RN is
between 1800 and 2000, then a symbol for the E3500 sensor will appear and
blink, warning the user that the E3500 sensor is either close to its lifetime (2000
samples) or the expiration date is approaching 1 month, see Figure 3-5.

READY
12.1V
023548
P04X

Figure 3-5 Luminol Cell Status Window

If the cartridge has been inside the unit for more than a month, an error message
ERR-CELL will be displayed on the LCD to warn the user about the status of the
cartridge. Within 1 or 2 days from the expiration date, a number 1 or 2 will be
displayed respectively as shown in Figure 3-4 (page 3-3).

ERR-CELL RN 0950
PK HEIGHT +0256
PK AREA 02563
PK POS 23

Figure 3-6 Error E3500 Sensor Cartridge Message

3-4 The E3500 Hand Held Explosive Detector

 OPERATION

With the power on, use a flat screw driver to open the door on the side of the
unit and open the tray to change the E3500 Sensor. An ERR-PMT-D message
window will appear in the text window: (figure 3-7). Remove the sensor from the
aluminum pouch and place the sensor inside the tray with the membrane facing
up (soft side) and then close the tray.

ERR-PMT-D RN 0950
PK HEIGHT +0256
PK AREA 02563
PK POS 23

Figure 3-7 Error PMT Door Message

At this point the user will be asked to reset the run number. When a new E3500
Sensor is used this number should be reset to zero. After the E3500 sensor has
been replaced, the unit will go into SELF TEST mode and then will be ready for
sampling.

3.5 How to Sample Vapours

Place the Vapour Inlet Nozzle of the E3500 near the area to be sampled. Press
the blue Sample Button on the handle and the Sample Pump will immediately
draw an air sample into the Vapour Inlet Nozzle, The LCD will display
SAMPLING . The pump will remain on for five to fifteen seconds. This time can
be adjusted by the user for specific applications. The PROCESSING message
will be displayed on the LCD during the analysis cycle. After the pump switches
to a low flow regime, the E3500 can be moved to a new location while the
analysis is being performed. At the end of the analysis, the results will be
displayed on the LCD. The overall time for a sample to be analyzed will vary
from 15 to 20 seconds.

3.6 How to Sample Particulates

Take a sample from the suspect article and transfer it to a clean sample screen.
With the E3500 in READY mode, insert the sample screen into the Sample
Screen Injector Inlet of the E3500. Do not force the screen into the Sample

The E3500 Hand Held Explosive Detector 3-5

OPERATION

Screen Injector Inlet or the screen may be damaged (if inserted correctly, the
screen will slide in with little resistance). Press the blue Sample Button on the
handle and the Sample Pump should immediately draw air into the E3500. The
PROCESSING message will be displayed on the LCD during the analysis cycle.
At the end of the analysis, the results will be displayed on the LCD similar to the
default window shown in figure 1-2 on page 1-4 where the sample resulted in an
alarm.

3.7 Clearing the Alarm

NOTE: Remove the Sample Screen before clearing an alarm in Particulate

Sample Mode.

Following the correct procedure to clear an alarm is a critical operational

requirement. The alarm clearing procedure for the E3500 must be carried out in
the proper sequence. Whenever an alarm condition is initiated, it is
recommended that the operator verify that the unit has not been contaminated.
This is done by pressing the Sample Button to initiate another analysis cycle. In
most cases, this second cycle should result in a non-alarm condition, indicating
that the unit is clean and is ready for another sample. In particulate sampling, the
risk of contamination is much greater, since the explosive residue is desorbed
entirely from the sample screen or the collector tube during the first cycle.

When this occurs, the E3500 may continue to respond with alarms on
subsequent sample cycles, even when no sample has been taken. The alarm
clearing procedure is the same for nuisance alarms and alarms caused by the
presence of explosives. When a repeated alarm condition is identified, remove
the sample screen from the unit and thoroughly clean it with soap and water.
Ensure that the decontaminated screen is rinsed with alcohol or acetone solution
and thoroughly air-dried before reinserting it into the E3500.

Re-insert a new or decontaminated screen and press the Sample Button to

ensure that there is no contamination still present. If contamination is still present
a decontamination cycle must be run.

3.8 Decontamination Cycle

1. Press to return to the numerical result display.

2. Simultaneously press the keys to obtain the

Decontamination window seen below (see figure 3-8).

3-6 The E3500 Hand Held Explosive Detector

 OPERATION

Decontaminate ?

No Yes

Figure 3-8 Decontamination Cycle Option

3. After choosing yes the unit will proceed with the decontamination cycle,
which lasts 60 seconds.

60
STANDBY

Figure 3-9 Decomtamination Cycle

4. The unit should be clear after the decontamination cycle has

processed. If the unit is still not clear refer to Section 5 – Troubleshooting
and Maintenance.

The E3500 Hand Held Explosive Detector 3-7

OPERATION

THIS PAGE IS INTENTIONALLY LEFT BLANK

3-8 The E3500 Hand Held Explosive Detector

 APPLICATIONS

SECTION 4 – APPLICATIONS

4.1 Sample Collection

4.1.1 Vapour Pressure

Explosive compounds can be characterized according by their tendency to

evaporate and release material into the air (vapour pressure). Explosives with a
high vapour pressure (EGDN, Dynamite) produce and release more vapour at a
given temperature. Explosives with a low vapour pressure (C-4, Semtex) release
very little vapour. However, these materials can be detected if they are tagged
according to the ICAO standard.

4.1.2 Vapour Sampling Background

High vapour pressure explosives can be detected by the E3500 in the vapour
sampling mode. In an enclosed area, explosive vapours slowly fill the area until
there is an almost equal distribution of vapour anywhere within the containment
area.

The longer the explosive is present, the greater the amount, or concentration, of
vapours present. Therefore, you would not have to be in the immediate vicinity of
an explosive to collect a sample.

4.2 Vapour Sampling Methods

To collect a sample keep the nozzle of the E3500 pointed in the direction of the
suspected vapour. Push the sample button on the handle of the unit and hold the
nozzle until the LCD displays PROCESSING.

Vapours escape from rooms and other enclosed areas or containers through any
available opening. Table 4-1 below indicates examples of specific areas where
vapour samples should be taken.

The E3500 Hand Held Explosive Detector 4-1

APPLICATIONS

Table 4-1 Vapour Sampling Area Identification Guide

SUSPECT ARTICLE SAMPLING AREAS

LUGGAGE Zippers and seams
LARGE AREAS Samples in large buildings can be taken at
exhaust ventilation openings
VEHICLES Edges of trunk, doors, and windows
BOXES Box lid
ROOMS Door cracks, windows, and vents
LARGE AIRCRAFT Samples can be taken at air exchange
ventilation openings
OUTDOORS Take samples downwind of the suspect area or
object

4.3 Particulate Sampling Background

Explosives residues, particularly those of plastic explosives, tend to stick to

surfaces. When a person touches an explosive some residue may stick to their
hands, and each time they touch an object some of the residue may be
transferred to it.

Collecting samples for analysis requires the operator to think like a person trying
to conceal explosives. The operator must consider where the person may have
touched the suspect article. This applies to any container. The goal is to take
samples from the most probable locations on the suspect containers that may
have been contaminated (handels, zipper).

The E3500 can detect very small traces, but it is the operator’s responsibility to
introduce these traces (when present) by using the proper sampling technique.

4.4 Particulate Sampling Method

Particulate samples are taken from suspect articles by wiping with a clean cotton
glove or wiping with a sample screen. Each sampling method has advantages
and disadvantages, however, wiping with a clean cotton glove is the preferred
method. Using a sample screen is the second recommended method.

When using either of the two methods, it is very important that all sampling of
suspect articles be done with the operator wearing clean cotton gloves on
both hands. The gloves must be discarded and a fresh pair put on whenever
the gloves become soiled, the gloves show signs of deterioration, or a sample
results in an alarm.

4-2 The E3500 Hand Held Explosive Detector

 APPLICATIONS

It is not necessary to aggressively rub a surface to collect a sample. Sample

screens and cotton gloves are designed to lift material off surfaces with gentle
pressure so that damage to surfaces is minimized.

NOTE: For example, any amount of particulates large enough to be visible

to the naked eye will overload the E3500.

4.4.1 Glove Sampling

The suspect article is wiped with a gloved finger. The material is then transferred
to a clean sample screen by rubbing the gloved finger against the screen
surface. The screen is then inserted into the Injector Inlet of the E3500, and an
analysis cycle initiated.

The glove sampling method produces the lowest rate of nuisance alarms, permits
the setting of the lowest alarm thresholds, and is the least prone to interference
from the operator’s hands.

However, because particulates must be transferred from the glove to the screen,
some could be lost in the process. If this happens, the amount deposited on the
screen could be less than that required to initiate an alarm.

Note: Using a clean cotton glove for sampling is currently recommended by

Scintrex Trace Corp. Other sampling protocols have proven effective in
special circumstances, and some institutional users have adopted alternate
techniques. For more information on sampling techniques, contact Scintrex
Trace Corp. or your local representative.

The position of the glove refers to how it is held while wiping suspected areas.
The glove should be held firmly to minimize movement, to ensure that the area of
the glove or wipe that contacted the suspect article remains fixed, and to ensure
that the maximum amount of the sample is transferred to the screen.

Apply a moderate amount of pressure when sampling, and in a circular wiping

motion. The area of the glove that contacted the suspect article should be
applied to the sample screen, to transfer the maximum possible amount of
explosive.

The E3500 Hand Held Explosive Detector 4-3

APPLICATIONS

4.4.2 Direct Sampling with a Screen

This method of sampling is the most efficient, but the suspect article may be
scratched or damaged when rubbed by the sample screen. Furthermore, the
chances of picking up and introducing foreign particles and debris into the E3500
Sample Screen Injector Inlet is increased over the glove sampling technique.

Sampling screens require careful handling. Gently rub the surface and keep your
fingers away from the metal mesh when handling screens.

If a particulate sample screen is bent or frayed and cannot be restored, then

it should be discarded. A bent or frayed screen may damage the E3500
when it is inserted into the Injector Inlet. It may also damage the surface
being sampled.

4.5 Smart Sampling Area Identification

Smart sampling area identification can be defined as: intelligent determination of

those areas of a suspect article most likely to be contaminated with a target
compound. In the case of baggage, these areas would logically be handles,
latches, buttons, and exterior edges.

Table 4-2 Particulate Sampling Area Identification Guide

SUSPECT ARTICLE SAMPLING AREAS

DOCUMENTS Outer cover and inner pages

LUGGAGE Zippers, handles, and latches
PHONES, RADIOS, Carrying handles, switches, knobs,
COMPUTERS keypads, and keyboards
Doors, glovebox, trunk locks and handles,
VEHICLES steering wheel, shift lever and radio
controls
BOXES Box lid
ROOMS Door knobs, handles, and windows, locks
FURNITURE Handles and armrests

4-4 The E3500 Hand Held Explosive Detector

 TROUBLESHOOTING AND
MAINTENANCE

SECTION 5 – TROUBLESHOOTING
AND MAINTENANCE

5.1 TROUBLESHOOTING

At times, the E3500 may show symptoms of faults or errors. Table 5-1 lists
potential problems and related troubleshooting procedures.

Table 5-1 Troubleshooting Procedures

PROBLEM PROCEDURE
Battery Troubleshooting
• Replace battery with fully charged battery.
• Ensure that the battery is installed securely.
• Ensure that the unit is turned on.
UNIT DOES NOT
POWER UP (WITH • Inspect the 5 Amp fuse and replace if necessary.
BATTERY INSTALLED) • Check the battery and battery contacts and clean them
if necessary.
• If the E3500 still does not power up, contact Scintrex
Trace Corp Technical Service Support.

• Replace battery with fully charged battery or connect

unit to an external power source.
POWER TURNED ON
BUT LCD BLANK • Inspect the 5 Amp fuse and replace it if necessary.
• Contact Scintrex Trace Corp Technical Service
Support.

• Battery is discharged. Replace the battery with a fully

charged battery or connect unit to an external power
UNIT OPERATES ON source.
EXTERNAL POWER
SOURCE BUT NOT ON • Check the battery and battery contacts and clean them
BATTERY if necessary. Contacts may be damaged.
• Contact Scintrex Trace Corp Technical Service
Support.

BATTERY DOES NOT • The battery is a consumable device and has a limited
HOLD A CHARGE OR number of recharge cycles. Safely dispose of Ni-Cd
CHARGER DOES NOT battery and obtain new battery from Scintrex Trace
CHARGE BATTERY Corp Technical Service Support.

The E3500 Hand Held Explosive Detector 5-1

TROUBLESHOOTING AND
MAINTENANCE

Pump Troubleshooting
AIR PUMP DOES NOT • Turn off and turn on the unit.
START WHEN THE • Contact Scintrex Trace Corp Technical Service Support.
UNIT IS TURNED ON

PUMP OPERATES, • With the E3500 in vapour sampling mode, initiate a

BUT UNIT DOES NOT sample cycle and place a finger over the nozzle opening,
RESPOND TO TEST then remove it from the opening. A change in sound
SAMPLES should occur when the nozzle is blocked by your finger
during the sample cycle. This change in sound indicates
that the pump is drawing air into the unit and creating air
flow.
• Disconnect the nose cone and check that the 9-pin
connector is securely plugged in.
• Tighten the connection.
• Ensure that the Teflon tube is not loose or disconnected.
Do not use excessive force to move the tube.

PMT OUTPUT HIGH • High level of oxidant in the atmosphere such as Nox,
peroxides.
• Old E3500 sensor (stored at room temperature.)

E3500 Troubleshooting
UNIT IS • Remove E3500 to a clean area.
CONTAMINATED • If Unit was contaminated in particle mode – Remove
BY EXPLOSIVES particle screen.
RESIDUE • Initiate a sample cycle and note the value.
• If the value is still too high, repeat until the value has
decreased to the background value noted at start-up.
• If the value does not decrease, contact Scintrex Trace
Corp Technical Service Support.

5.2 Maintenance

Effective operation of the E3500 depends on regular maintenance.

5.2.1 Decontamination of Sample Screens

Screens with visible dirt accumulation should be discarded or cleaned. Dirt
reduces the collection and desorption efficiency of the screen. A dirty sampling
screen should be thoroughly cleaned with soap and water, and then rinsed in
acetone or a similar solvent. The screen should then be thoroughly air-dried (if
possible heat dried) before being re-inserted into the E3500. If a particulate
sampling screen is bent or frayed and cannot be restored, it should be discarded.
Bent or frayed screens may damage the E3500 and the surface being sampled.

5-2 The E3500 Hand Held Explosive Detector

 TROUBLESHOOTING AND
MAINTENANCE

5.2.2 Replacing the 5-amp Fuse

Unscrew the fuse holder cover on the rear panel by turning counterclockwise.
Carefully remove the fuse and inspect it. If it requires replacement, install one of
the fuses supplied with your unit (stored in your case). Re-install the fuse holder
in the rear panel.

5.2.3 Recovering from Severe Contamination

The following components of the E3500 could be adversely affected by severe
contamination:
The vapour inlet nozzle and its components,
The vapour and particulate sample tubes,
The internal tubing,
The three-way solenoid valve,
The particulate screen desorber assembly,
The carrier pump.

Severe contamination can occur in both vapour sampling and particulate

sampling modes. If this occurs, the nose cone assembly of the unit must be
either cleaned or replaced. If these procedures do not work, contact Scintrex
Trace Corp Technical Service Support.

5.2.4 Vapour Contamination

In most cases of an overload condition, two or three blank sample cycles will
usually cleanse the E3500 of any residual explosives vapours. A blank sample
cycle is one in which no actual sample is taken. The blank samples should be
taken away from the location where the sample that caused the overload was
taken. If a series of blank cycles fail to clear the contamination, refurbish
the vapour inlet assembly.

5.2.5 Refurbishing Vapour Inlet Assembly

The vapour inlet assembly is refurbished by removing the steel screw nut from
the front of the vapour inlet nozzle then removing the vapour sample collector
tube from its housing and cleaning the inside of the steel screw nut, the O-ring,
and the steel mesh screen. Contamination may mainly occur at the Steel mesh
screen or the Vapour trap (see figure 5-1).
Install a new vapour sample collector tube (Vapour desorber + Vapour
trap + Vapour Pyrolyzer) and reassemble the vapour inlet assembly.
Turn on the E3500 and wait until it enters READY mode. Perform three
blank sample cycles.

The E3500 Hand Held Explosive Detector 5-3

TROUBLESHOOTING AND
MAINTENANCE

Steel mesh Vapour Vapour

Black Nut screen desorber pyrolyzer
O-ring

Vapour Vapour trap

inlet Steel screw Vapour tube
nut adapter

Figure 5-1 Vapour Inlet Assembly

5.2.6 Particulate Contamination

The most common contamination in the particulate sampling mode is in the
screen desorber. Performing a series of blank sample cycles without a sample
screen in the injector inlet should cleanse the screen desorber of contamination.
If this fails, replace the particulate sample tube collector.

5.2.7 Replacing Particulate Pyrolyzer

The particulate pyrolyzer tube is replaced by first removing the nose cone
assembly from the E3500. Remove the protective casing from the particulate
sample tube collector housing. Remove the teflon tubing from the housing. Open
the case that holds the particulate pyrolyzer tube shown in figure 5-2. Then insert
a new particulate sample tube collector in the housing and reinstall the tube
collector. Re-install the nose cone assembly. Turn on the E3500. When the
E3500 enters READY mode, perform three blank sample cycles.

5-4 The E3500 Hand Held Explosive Detector

 TROUBLESHOOTING AND
MAINTENANCE

Pyrolyzer holder
assembly

Figure 5-2 Particulate Pyrolyzer Tube Replacement

5.3 Service and Maintenance Call Procedures

When additional technical information or support is required, contact your local

representative or call Scintrex Trace Corp during standard business hours of
8:00 a.m. to 5:00 p.m., EST.

Toll free in North America 1-877-877-7147

Outside of North America 1-613-224-1061
Email: [email protected]

Please have the following information on hand prior to calling Scintrex Trace
Corp Technical Service Support as it will be required to process your request:
The serial number of the unit
The location of the unit
A contact person on-site and their telephone number
A detailed explanation of the problem

5.4 Return of Goods for Repair or Disposal

The E3500 or any of its parts may be returned to Scintrex Trace Corp for repair
or disposal. Shipping of a complete unit or parts requires special handling.

Pack the unit in its original factory shipping crate. Parts must be well packed and
protected against any possible damage they may be exposed to during shipping.
Contact Scintrex Trace Corp. to order a replacement shipping crate if required.

Disconnect battery and remove E3500 Sensor from E3500 prior to shipping.
Protect battery terminals from electrical short circuit to prevent fire or personal
injury.

The E3500 Hand Held Explosive Detector 5-5

TROUBLESHOOTING AND
MAINTENANCE

Contact Scintrex Trace Corp to coordinate shipping details such as customs and
other documentation required, pickup times, and required signatures for
insurance purposes.

After all shipping arrangements have been made and confirmed with Scintrex
Trace Corp., all returned goods should be shipped to the following address or a
DDU (Delivery Duty Unpaid) service from outside Canada.

Scintrex Trace Corp.

Technical Service Department
300 Parkdale Avenue
Ottawa, Ontario K1Y 1G2
CANADA

5.5 Handling and Storage of E3500 Sensors

New E3500 Sensors should be stored in a refrigerator. This simple procedure will
extend the life of the sensor.

Used E3500 Sensors should be stored in a plastic bag (Ziploc® or equivalent).

Used E3500 Sensors cannot be discarded unless the contents are chemically
neutralized. Care should be exercised during the procedure to prevent skin
contact or contact of the contents with sensitive surfaces. Latex or vinyl gloves
and protective glasses should be worn. Should skin contact or spillage occur
flush immediately with water or a dilute solution of vinegar.

5.5.1 Neutralization Method

Equipment

One liter glass bowl

Household vinegar
Sharp knife or tool for puncturing E3500 Sensor membrane

Process

Carefully puncture the sensor membrane located on the top of the sensor
with a sharp knife
Immerse the sensor in a liter of water (in a bowl)
Add some household vinegar
Pour the solution down the drain and flush with water
Discard the empty container

5-6 The E3500 Hand Held Explosive Detector

 APPENDIX A

APPENDIX A – E3500 BATTERY

How to Charge the NiMH Battery Using the Scintrex Trace Corp
Universal Battery Charger (PN D100550)

Use the Universal Battery Charger PN D100550 with the recommended Scintrex
Trace Corp NiMH battery. Charging a battery other than the recommended
battery provided may cause irreparable damage to the incompatible battery
and/or the charger. Recharge batteries at ambient temperatures of 18°C to 24°C.

Connect the Universal Battery Charger to a compatible AC outlet which provides

a ground connection for safe operation. The Universal Battery Charger is
designed to operate within the voltage range indicated on the label affixed to the
charger.

Activate the Universal Battery Charger by switching to the appropriate “POWER

ON” indication. The red power lamp should be lit. The green charge state lamp
should be lit prior to installing a discharged battery.

Inspect the battery for any damage prior to connecting it to the charger. If any
physical damage to the battery is apparent do not attempt to charge it. Obtain a
replacement battery.

After connecting the battery to the charger the red power lamp should remain lit
and the green mode lamp should change colour to orange while the charging is
in progress the mode lamp should change back to green when the charging
process has been completed (about one hour). If the red lamp and the green
lamp both extinguish and the fan stops, this may indicate a battery which has
defective cells and can no longer be safely charged. Obtain a replacement.

When the mode lamp changes to green, after about an hour the battery is
normally charged and is safe to use. Although this is a multistage type charger, it
is good practice not to leave the battery connected for longer than one hour as
the battery may be damaged.

If a battery quickly heats up during the charging process, it may no longer charge
properly and needs to be replaced. A temperature sensor in the battery will
disconnect it in such an event. Disconnect and remove the defective battery. If
the battery does not hold a charge above 13V for the normal expected time this
also indicates a replacement battery may be necessary. The battery is a
consumable device and has a limited number of recharge cycles. To avoid loss
of run time or unexpected battery failure, replace batteries every two years.

The E3500 Hand Held Explosive Detector A-1

APPENDIX A

The battery charger should be switched to the off position when not in use to
extend the life of the built in cooling fan.

LED Function of Charger

LED WILL ILLUMINATE TO INDICATE STATUS

OF CHARGER AND BATTERY
LED 1 Red = Power ON
LED 2 Orange = Charging
LED 2 Green = Full Charge

A-2 The E3500 Hand Held Explosive Detector

 APPENDIX B

APPENDIX B – COMMUNICATIONS
Communications

There are a number of techniques that can be used to communicate with the
E3500. Hyper-Terminal, LabView, Internet Browsers and Pocket PCs are all able
to communicate with the E3500.

Embedded Software

The E3500 has several frames that the user can browse through to view results,
operational parameters or settings. The user can navigate through these frames
by pressing onto the keypad located at the bottom of the LCD.

• INITIAL SCREEN

• First Screen when unit is turned on

• SELF TEST SCREEN

• SELF TEST mode (in particle mode

ensure that no sampling screen is
inside the injector inlet).

The E3500 Hand Held Explosive Detector B-1

APPENDIX B

• TEXT SCREEN

• After each SELF TEST mode the

following screen will appear. This
screen will show the correction values.
In order to switch to the graphical
window press the MENU button.

• GRAPHICAL SCREEN

• Graphical representation of the result.

READY
By pressing the up and down arrows 12.1 V
the user can zoom in and out of the 023548
graph. The zoom level is indicated at 004X
the bottom right corner of the screen.
The user can switch back to the text
window by pressing the Menu button.

• VIEW PARAMTERS SCREEN 1

• To view the parameters press the

ENTER button from the TEXT or
GRAPHICAL windows. Then press
ENTER again.
• To exit from this window press the
MENU button.

B-2 The E3500 Hand Held Explosive Detector

 APPENDIX B

• VIEW PARAMETERS SCREEN 2

• Select which parameters to view with

the up and down buttons, then press
the ENTER button to select.
• To go back to the previous screen
press the MENU button.

• VIEW VAPOUR PARAMETERS

SCREEN 1

• H1P: duty cycle for vapour desorber

(0-100).
• H2P: duty cycle for vapour pyrolyzer
(0-100).
• WL1: reference point for the peak
position (0-80).
• H1T: duration of vapour desorber (0-
6s).
• H2T: duration of vapour pyrolyzer (0-
6s).
• PWD: peak width for peak area
calculation (0-20).
• Press the Menu button to exit or the up
and down buttons to move to the next
window.

• VIEW VAPOUR PARAMETERS

SCREEN 2

• ST: sampling time (5-15s).

• THH: threshold for peak height (0-
99990).
• THA: threshold for peak area (0-
99990).
• Press the Menu button to exit or the up
and down buttons to move to the next
window.

The E3500 Hand Held Explosive Detector B-3

APPENDIX B

• VIEW PARTICLE PARAMETERS

SCREEN 1

• H1P: duty cycle for particle pyrolyzer

(0-100).
• H2P: duty cycle for particle desorber
(0-100).
• WL1: reference point for the peak
position (0-80).
• H1T: duration of particle desorber (0-
6s).
• H2T: duration of particle pyrolyzer (0-
6s).
• PWD: peak width for peak area
calculation (0-20).
• Press the Menu button to exit or the up
and down buttons to move to the next
window.

• VIEW PARTICLE PARAMETERS

SCREEN 2

• THH: threshold for peak height (0-

99990).
• THA: threshold for peak area (0-
99990).
• Press the Menu button to exit or the up
and down buttons to move to the next
window.

B-4 The E3500 Hand Held Explosive Detector

 APPENDIX B

• EDIT PARAMETERS SCREEN 1

• Select Edit parameters using the up

and down keys, then press the ENTER VIEW PARAMETERS
button to select.  EDIT PARAMETERS
• To go back to the previous screen
press the MENU button.

• EDIT PARAMETERS SCREEN 2

• The unit will now prompt the user to

enter a password. Using the keypad
Password
enter the appropriate password. &&&

• EDIT PARAMETERS SCREEN 1

• Once the appropriate password has

VAPOR
been entered, the following screen will PARTICLE
appear. Choose the RESET MEM OPTIONS
option using the keypad to clear the RESET MEM
memory.
• To go back to the previous screen
press the MENU button

The E3500 Hand Held Explosive Detector B-5

APPENDIX B

• EDIT PARAMETERS SCREEN 2

• By choosing the RESET MEM option

the following screen will be displayed. RESET MEM ?
• Choose Yes to reset the buffer memory
No Yes

B-6 The E3500 Hand Held Explosive Detector

 APPENDIX B

• LOW BATTERY •
MESSAGE •
DISPLAYED ON •
LCD •
READY
• 12.1 V
• 023548
004X
•
•
•
•
•
• If the battery indicator is blinking, the unit will be operational for
about 30 minutes.

ERR-BAT RN 0201
PK HEIGHT +0256
PK AREA 02563
PK POS 23

•
• If the battery indicator has a value less than 11.5V, the unit will not
be operational. The display will automatically switch to the text
window.
• Replace the battery with a fully charged battery.
• Recharge the battery that was removed.
• E3500 SENSOR •
ERROR •
DISPLAYED ON •
LCD READY
12.1V
023548
• P04X
•
•
•
•

• If Luminol sign ( ) is blinking, the unit will be operational for 1 to 2

days.
• If Luminol sign ( ) is steady, the unit will not be operational until
the Luminol cartridge is changed.

The E3500 Hand Held Explosive Detector B-7

APPENDIX B

• ERR-CELL •
•
•
• ERR-CELL 1 RN 2001
PK HEIGHT +0256
• PK AREA 02563
• PK POS 23

•
•
•

• If RN run number is equal to 2000.

• If elapse time since the last time the Luminol tray has been opened
exceeds 1 month.

• ERR-PMT-D •
•
•
•
• ERR-PMT-D RN 0950
PK HEIGHT +0256
• PK AREA 02563
PK POS 23

•
•
•

• To clear this message close the tray and the door on the side of the
unit.

Hyperterminal Communication

Hyperterminal is a program that is available on most PCs. Connect the E3500 to

the PC using the RS-232 cable provided. Once HyperTerminal has opened,
create a new connection called E3500 (or any other such name that is desired).
Setup the connection using the settings found in the figures below and then turn
on the E3500 and allow it to go through its warming cycle.

B-8 The E3500 Hand Held Explosive Detector

 APPENDIX B

Click on the Settings tab and adjusts the parameters.

Once Hyperterminal has opened the connection, there a number of commands

which can be sent to communicate with the E3500. In order to send the
commands, there are a number of options must be changed (in HyperTerminal)
from the factory default settings. Under the File menu, choose the Properties
selection.

The E3500 Hand Held Explosive Detector B-9

APPENDIX B

Once the window has opened, choose the Settings Tab.

B - 10 The E3500 Hand Held Explosive Detector

 APPENDIX B

Next, select the ASCII Setup button.

Once completed, click OK to leave the ASCII Setup window, and then OK once
more to leave the Properties window. To save the settings, choose File->Save As
and choose a filename/location under which to save the file. The next time the
settings are required, File-> Load and choose the appropriate file.

The E3500 Hand Held Explosive Detector B - 11

APPENDIX B

To start an analysis, type 1. The E3500 will start sampling, and the following data
will appear in the HyperTerminal window. This data can be displayed again by
pressing L.

If more detail on the run is desired, the entire set of data points used to create
the graph shown on the primary display can be obtained by entering d (or D) in
the HyperTerminal window.

B - 12 The E3500 Hand Held Explosive Detector

 APPENDIX B

The user can also download all the results stored (895 samples) in the memory
by pressing A and Enter. To stop the process type S and Enter.

To retrieve the parameters for both modes type P, the following window will
appear:

The E3500 Hand Held Explosive Detector B - 13

APPENDIX B

THIS PAGE IS INTENTIONALLY LEFT BLANK

B - 14 The E3500 Hand Held Explosive Detector

 APPENDIX C

APPENDIX C - SPECIFICATIONS

Electrical

VOLTAGE 12 VDC Scintrex Trace Corp. rechargeable battery

Optional 12 VDC external battery
Optional external AC power supply

RATED CURRENT 5 Amperes

FUSE TYPE AND RATING 5 Amperes

Mechanical

WEIGHT 3 kg (6.6 lbs)

DIMENSIONS (L x W x H) 51 x 11 x 14 cm
20 x 4.3 x 5.5 in

SHIPPING WEIGHT 15.5 - 16 kg (boxed)

SHIPPING DIMENSIONS 57 x 26 x 39 (cm)

22 x 10 x 15 (in)
(L x W x H) (L x W x H)

Environmental

TEMPERATURE The E3500 may be operated at temperatures ranging from

-10°C to +55°C (23°F to 131°F). The E3500 may be stored
at temperatures ranging from 5°C to +65°C (32°F to
149°F).
HUMIDITY The E3500 may be operated in environments with up to
90% humidity (non-condensing). Do not expose the
equipment to any condition or change in conditions that
may cause condensation.
VENTILATION The E3500 has ventilation holes that allow dissipation of
the heat generated by its operation. Do not use the
equipment in any location that restricts the ventilation
holes. Preventing air circulation around the equipment
may cause overheating that could damage the equipment
or compromise its reliability. For optimum performance,
provide clearance adequate for ventilation and ease of
operation.

The E3500 Hand Held Explosive Detector C-1

APPENDIX C

General Specifications

DETECTION SYSTEM Chemiluminescence

SAMPLING METHODOLOGY Vapour and particulate sampling
WARM-UP TIME 1 minute with regular use
SAMPLING TIME 5 to 15 seconds (user selectable)
ANALYSIS TIME Less than 10 seconds
SENSITIVITY PPB Level-Vapours / Nanograms - Particulates
DETECTABLE COMPOUNDS EGDN P-MNT NG Semtex Black powder
EGMN DNT AN Detasheet TATP
DMNB RDX PN Primacord HMTD
O-MNT PETN C-4 TNT HMX
DETECTION INDICATORS LCD displays ALARM
Red light on
Volume adjustable audible alarm
OPTIONS 12 VDC external battery
External AC power supply
External battery charger
Replacement nose cone assembly
Cotton sampling gloves (pkg. of 20)
4 inch needle probe
Flexible probe
Neoprene Cover (D1000009)
Universal Ethernet Kit (D1000520)
Universal Wireless Kit (D1000515)
Universal Printer Kit (D1000500)
DATA RECORDING STORAGE RS-232 terminal for data transmission
Data storage capacity of 896 analysis results

NOTE: All specifications are approximate and are subject to change.

C-2 The E3500 Hand Held Explosive Detector