Certificate No.

XXXXXXXX 04 April 2023

Certificate of Sampling and Analysis

In pursuance of an order received form Messrs. EMDAD, we (Cotecna) attended for inspection of the
cargo described below:Cargo Basic Information

Issuing Date : XX.XX.XXXX

Our ref. : XXXXXXXXXXX XX
Origin : XXX
Shipper As Per B/L No.1 : XXX
Buyer as Per B/L No.1 : XXXsss
Vessel : M/V XXX
Bill of Loading : NO.1 Dated XX.XX.XXXX, Port
Port : XXX Port
Cargo : Material: Anthracite Coal
Sizes:
 ASH 1-6 mm
 AMSKO 625-80 25 mm
 AKO 20-80 mm

Total Weight : XX,XXX mt

Lot : Average
Sampling Commence Date : XX. XX. XXXX
Sampling End Date : XX. XX. XXXX
HS Code : 27011100

Confirmation Statement

We (Cotecna) cConfirm that we have attended the loading and sampling the material of
Anthracite, which was loaded on the board of the vessel “XXX” on Date XX.XX.XXX at the port of
“XXX”.

1 Sampling
As per ISO 18283:2016, samples are taken at the time of loadingtwo times. :

 In-Take Sampling: At Time of Wagon Arrivals.

 During the Loading of See Going Vessel.

The weight and the number of increments collected for the chemical and physical analysis of ASHSH,
& AMS, and AKOKO mateiralsmaterials are illustrated as shown below.

Material For Chemical # of Increments Sampling Date

Analysis

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 Certificate No.XXXXXXXX 04 April 2023

Sample Weight
ASH (1-6 mm) XXX Kg X From XX to XX/XX/XXXX
AMS (6-25 mm) XXX Kg X From XX to XX/XX/XXXX
AKO (20-80 mm) XXX Kg X From XX to XX/XX/XXXX

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 Certificate No.XXXXXXXX 04 April 2023

2 In-Take Analysis
2.1 ASH (1-6 mm)
2.1.1 Chemical Analysis
The Below table illustrates the weighted average chemical results for ASH (1-6 mm). ISO 1170:2020 is followed to calculate the results to different basis.

Test Test Procedure Unit On Dry Basis As Received Basis Standard (Contract Annex1) Compliance

Total Moisture ISO 579 :2008 % XX.XX XX.XX 11 % max (AR)1 ☒Yes ☐No
Ash ISO 1171:2010 % XX.XX XX.XX 7% % max (DB)2 ☐Yes ☐No

Volatile Matter ISO 562:2010 % XX.XX XX.XX 3 % max (DP) ☐Yes ☐No

Hydrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Carbon (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Nitrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Total Sulphur ISO 334:2020 % XXXX.XX XXXX.XX 1% max (DP) ☐Yes ☐No
Gross Calorific Value ISO 1928:2020 Kcal/Kg XXXX.XX XXXX.XX 7800 Kcal/Kg min (DP) ☐Yes ☐No

Net Calorific Value ISO 1928:2020 Kcal/Kg XX.XX XX.XX 7200 Kcal/ Kg min (DP) ☐Yes ☐No

Fixed Carbon ISO 17246:2010 % XX.XX XX.XX 90 % min (DP) ☐Yes ☐No
Phosphorus ISO 622:2016 % XX.XX XX.XX 0.025 % max (DP) ☐Yes ☐No
Hardgrove grindability index (HGI) ISO 5074:2015 -- XX

1
AR: As Received Basis
2
DB: Dry Basis
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 Certificate No.XXXXXXXX 04 April 2023

2.1.2 Physical Analysis

Sieving tests for ASH (1-6 mm) are carried out using ISO 1953:2015 as shown in the below table.

Size Range %
+ 25 mm : 0XX.XX
+ 20 mm : 0XX.XX
+ 15 mm : 0.2XX.XX
+ 13 mm : 1.1XX.XX
+ 10 mm : 1.8XX.XX
+ 8 mm : 2.0XX.XX
+ 6.3.3 mm : 5.0XX.XX
+ 3.1515 mm : 45.3XX.XX
+ 1 mm : 24.2XX.XX
+ 0.5 mm : 14.8XX.XX
0.31521 2.7XX.XX
+ 2 mm :
+ 0.212 mm : 1.7XX.XX
+ 0.200 mm : 1.7XX.XX
+ 0.075 mm : 0.7XX.XX
- 0.075 mm : 0.5XX.XX
Total 100 %
Quantity of the materials with size below 1 mm is XX.XX Metric Tons, and
it represents XX.XX % of the total ASH quantity.

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2.2 AMS (6-25 mm)

2.2.1 Chemical Analysis
The Below table illustrates the weighted average chemical results for AMS (6-25 mm). ISO 1170:2020 is followed to calculate the results to different basis.

Test Test Procedure Unit On Dry Basis As Received Basis Standard (Contract Annex1) Compliance

Total Moisture ISO 579 :2008 % XX.XX XX.XX 11 % max (AR)1 ☒Yes ☐No
Ash ISO 1171:2010 % XX.XX XX.XX 7% % max (DB)2 ☐Yes ☐No

Volatile Matter ISO 562:2010 % XX.XX XX.XX 3 % max (DP) ☐Yes ☐No

Hydrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Carbon (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Nitrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Total Sulphur ISO 334:2020 % XXXX.XX XXXX.XX 1% max (DP) ☐Yes ☐No
Gross Calorific Value ISO 1928:2020 Kcal/Kg XXXX.XX XXXX.XX 7800 Kcal/Kg min (DP) ☐Yes ☐No

Net Calorific Value ISO 1928:2020 Kcal/Kg XX.XX XX.XX 7200 Kcal/ Kg min (DP) ☐Yes ☐No

Fixed Carbon ISO 17246:2010 % XX.XX XX.XX 90 % min (DP) ☐Yes ☐No
Phosphorus ISO 622:2016 % XX.XX XX.XX 0.025 % max (DP) ☐Yes ☐No
Hardgrove grindability index (HGI) ISO 5074:2015 -- XX

1
AR: As Received Basis
2
DB: Dry Basis
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 Certificate No.XXXXXXXX 04 April 2023

2.2.2 Physical Analysis

Sieving tests for AMS (6-25 mm) are carried out using ISO 1953:2015 as shown in the below table.

Size Range %
+ 25 mm : 0
+ 13 mm : 29.7
+ 6 mm : 53.4
- 6 mm : 16.9
Total 100 %

2.3 AKO (205-100 80 mm)

2.3.1 Chemical Analysis
The Below table illustrates the weighted average chemical results for AKO (205-100 80 mm). ISO 1170:2020 is followed to calculate the results to different
basis.

Test Test Procedure Unit On Dry Basis As Received Basis Standard (Contract Annex1) Compliance

Total Moisture ISO 579 :2008 % XX.XX XX.XX 11 % max (AR)1 ☒Yes ☐No

1
AR: As Received Basis
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 Certificate No.XXXXXXXX 04 April 2023

Ash ISO 1171:2010 % XX.XX XX.XX 7% % max (DB)2 ☐Yes ☐No

Volatile Matter ISO 562:2010 % XX.XX XX.XX 3 % max (DP) ☐Yes ☐No

Hydrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Carbon (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Nitrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Total Sulphur ISO 334:2020 % XXXX.XX XXXX.XX 1% max (DP) ☐Yes ☐No
Gross Calorific Value ISO 1928:2020 Kcal/Kg XXXX.XX XXXX.XX 7800 Kcal/Kg min (DP) ☐Yes ☐No

Net Calorific Value ISO 1928:2020 Kcal/Kg XX.XX XX.XX 7200 Kcal/ Kg min (DP) ☐Yes ☐No

Fixed Carbon ISO 17246:2010 % XX.XX XX.XX 90 % min (DP) ☐Yes ☐No
Phosphorus ISO 622:2016 % XX.XX XX.XX 0.025 % max (DP) ☐Yes ☐No
Hardgrove grindability index (HGI) ISO 5074:2015 -- XX

2.3.2 Physical Analysis

Sieving test for AKO (205-80 mm) is carried out using ISO 1953:2015 as shown in the below table.

Quantit
y
Size Range %
(Metric
Tons)
+ 25 mm : XX.XX XX.XX

2
DB: Dry Basis
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+ 20 mm : XX.XX XX.XX
+ 15 mm : XX.XX XX.XX
+ 13 mm : XX.XX XX.XX
+ 10 mm : XX.XX XX.XX
+ 8 mm : XX.XX XX.XX
+ 6.3 mm : XX.XX XX.XX
+ 3.15 mm : XX.XX XX.XX
+ 1 mm : XX.XX XX.XX
+ 0.5 mm : XX.XX XX.XX
+ 0.315 mm : XX.XX XX.XX
+ 0.212 mm : XX.XX XX.XX
+ 0.200 mm : XX.XX XX.XX
+ 0.075 mm : XX.XX XX.XX
- 0.075 mm : XX.XX XX.XX
(28,0000
+/- 10 %
Total 100 %
Metric
Tons)
Quantity of the materials with size below 25 mm is XX.XX Metric Tons, and it
represents XX.XX % of the total ASH quantity.

Size Range %
+ X mm : XX.XX
+ X mm : XX.XX
+ X mm : XX.XX
+ X mm : XX.XX
+ X mm : XX.XX
+ X mm : XX.XX
+ X mm : XX.XX
+ X mm : XX.XX
+ X mm : XX.XX
+ X mm : XX.XX
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 Certificate No.XXXXXXXX 04 April 2023

+ X mm : XX.XX
+ X mm : XX.XX
+ X mm : XX.XX
- X mm : XX.XX
Total 100 %

3 During Loading Analysis

3.1 ASH (1-6 mm)
3.1.1 Chemical Analysis
The Below table illustrates the chemical results for ASH (1-6 mm). ISO 1170:2020 is followed to calculate the results to different basis.

Test Test Procedure Unit On Dry Basis As Received Basis Standard (Contract Annex1) Compliance

Total Moisture ISO 579 :2008 % XX.XX XX.XX 11 % max (AR) ☒Yes ☐No
Ash ISO 1171:2010 % XX.XX XX.XX 7% % max (DB) ☐Yes ☐No

Volatile Matter ISO 562:2010 % XX.XX XX.XX 3 % max (DP) ☐Yes ☐No

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 Certificate No.XXXXXXXX 04 April 2023

Hydrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Carbon (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Nitrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Total Sulphur ISO 334:2020 % XXXX.XX XXXX.XX 1% max (DP) ☐Yes ☐No
Gross Calorific Value ISO 1928:2020 Kcal/Kg XXXX.XX XXXX.XX 7800 Kcal/Kg min (DP) ☐Yes ☐No

Net Calorific Value ISO 1928:2020 Kcal/Kg XX.XX XX.XX 7200 Kcal/ Kg min (DP) ☐Yes ☐No

Fixed Carbon ISO 17246:2010 % XX.XX XX.XX 90 % min (DP) ☐Yes ☐No
Phosphorus ISO 622:2016 % XX.XX XX.XX 0.025 % max (DP) ☐Yes ☐No
Hardgrove grindability index (HGI) ISO 5074:2015 -- XX

3.1.2 Physical Analysis

Quantity
Sieving test for ASH (1-6 mm) is carried out using ISO
% (Metric
1953:2015 as showm in the below table.Size Range
Tons)
+ 25 mm : XX.XX XX.XX
+ 20 mm : XX.XX XX.XX
+ 15 mm : XX.XX XX.XX
+ 13 mm : XX.XX XX.XX
+ 10 mm : XX.XX XX.XX
+ 8 mm : XX.XX XX.XX
+ 6.3 mm : XX.XX XX.XX
+ 3.15 mm : XX.XX XX.XX
+ 1 mm : XX.XX XX.XX

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 Certificate No.XXXXXXXX 04 April 2023

+ 0.5 mm : XX.XX XX.XX

+ 0.315 mm : XX.XX XX.XX
+ 0.212 mm : XX.XX XX.XX
+ 0.200 mm : XX.XX XX.XX
+ 0.075 mm : XX.XX XX.XX
- 0.075 mm : XX.XX XX.XX
(28,0000
+/- 10 %
Total 100 %
Metric
Tons)
Quantity of the materials with size below 1 mm is XX.XX Metric Tons, and it represents XX.XX % of the total ASH quantity.

3.2 AKO (25-100 mm)

3.2.1 Chemical Analysis
The Below table illustrates the chemical results for AKO (25-100 mm). ISO 1170:2020 is followed to calculate the results to different basis.

Test Test Procedure Unit On Dry Basis As Received Basis Standard (Contract Annex1) Compliance

Total Moisture ISO 579 :2008 % XX.XX XX.XX 11 % max (AR) ☒Yes ☐No
Ash ISO 1171:2010 % XX.XX XX.XX 7% % max (DB) ☐Yes ☐No

Volatile Matter ISO 562:2010 % XX.XX XX.XX 3 % max (DP) ☐Yes ☐No

Hydrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Carbon (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

Nitrogen (from Ultimate Analysis) ISO 29541:2010 % XX.XX XX.XX -- -- --

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 Certificate No.XXXXXXXX 04 April 2023

Total Sulphur ISO 334:2020 % XXXX.XX XXXX.XX 1% max (DP) ☐Yes ☐No
Gross Calorific Value ISO 1928:2020 Kcal/Kg XXXX.XX XXXX.XX 7800 Kcal/Kg min (DP) ☐Yes ☐No

Net Calorific Value ISO 1928:2020 Kcal/Kg XX.XX XX.XX 7200 Kcal/ Kg min (DP) ☐Yes ☐No

Fixed Carbon ISO 17246:2010 % XX.XX XX.XX 90 % min (DP) ☐Yes ☐No
Phosphorus ISO 622:2016 % XX.XX XX.XX 0.025 % max (DP) ☐Yes ☐No
Hardgrove grindability index (HGI) ISO 5074:2015 -- XX

3.2.2 Physical Analysis

Sieving test for AKO (25-80 mm) is carried out using ISO 1953:2015 as shown in the below
table.%
XX.XX
XX.XX
XX.XX
XX.XX
XX.XX
XX.XX
XX.XX
XX.XX
XX.XX
XX.XX
XX.XX
XX.XX
XX.XX

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Certificate No.XXXXXXXX 04 April 2023

XX.XX
XX.XX
100 %

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4 Draft Surveying
Materia Hold Number (s) Weight Date
ASH (1-6mm) X XX,XXX mt XX.XX.XXXX
AMS (6-25 mm) X XX,XXX mt XX.XX.XXXX
AKO (20-80 mm) X XX,XXX mt XX.XX.XXXX

This Certificate of Sampling & Analysis is issued at (Place) on (Date).

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