HPCL-MITTAL ENERGY LIMITED

DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC1-1101 Crude - Before 18/09/2023 6:00 BS&W ASTM D 4007 Vol % 0.5 0.10
Desalter
Density at 15°C ASTM D 1298 kg/m³ 865.44 895.57 882.5
Salt Content ASTM D 3230 PTB 57 10.70
Total Acid Number (TAN) ASTM D 664 mg 0.1 0.5 0.2000
KOH/g
Total Sulphur ASTM D 4294 Wt% 2.9 2.49
501-SC1-4901 Swing naphtha 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 749.5
Initial Boling Point ASTM D 86 °C 84.7
Temperature at 5% Volume ASTM D 86 °C 123 132 118.7
Recovery
Temperature at 10% Volume ASTM D 86 °C 123.9
Recovery
Temperature at 30% Volume ASTM D 86 °C 133.0
Recovery
Temperature at 50% Volume ASTM D 86 °C 138.1
Recovery
Temperature at 70% Volume ASTM D 86 °C 141.8
Recovery
Temperature at 90% Volume ASTM D 86 °C 146.0
Recovery
Temperature at 95% Volume ASTM D 86 °C 143 147 148.9
Recovery
Final Boiling Point ASTM D 86 °C 160.2
Total Sulphur ASTM D 4294 Mass% 0.06
501-SC1-5001 LT. Kerosene 18/09/2023 6:00 Total Acid Number (TAN) IS 1448:P 113 mgKOH/ 0.0170
gm
Copper Strip Corrosion for 3 hrs @ ASTM D 130 Rating 1b
50°C
Doctor Test IS 1448:P 19 Negative
Page 1 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC1-5002 Hy. Kerosene to 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 822 811.1
Sour diesel
Initial Boling Point ASTM D 86 °C 139.8 150.6
Storage
Temperature at 5% Volume ASTM D 86 °C 178.9 173.8
Recovery
Temperature at 10% Volume ASTM D 86 °C 182.5
Recovery
Temperature at 30% Volume ASTM D 86 °C 205.7
Recovery
Temperature at 50% Volume ASTM D 86 °C 223.8
Recovery
Temperature at 70% Volume ASTM D 86 °C 241.4
Recovery
Temperature at 90% Volume ASTM D 86 °C 266.4
Recovery
Temperature at 95% Volume ASTM D 86 °C 281.2 280.8
Recovery
Final Boiling Point ASTM D 86 °C 285.9
Total Acid Number (TAN) IS 1448:P 113 mg 0.05
KOH/g
Total Sulphur ASTM D 4294 Mass% 0.612 0.59
501-SC1-5101 LGO Product to 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m3 841.5
Storage
Initial Boling Point ASTM D 86 °C 143.6
Temperature at 5% Volume ASTM D 86 °C 201.4
Recovery
Temperature at 10% Volume ASTM D 86 °C 222.4
Recovery
Temperature at 30% Volume ASTM D 86 °C 259.6
Recovery
Temperature at 50% Volume ASTM D 86 °C 281.8
Recovery

Page 2 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC1-5101 LGO Product to 18/09/2023 6:00 Temperature at 70% Volume ASTM D 86 °C 303.0
Storage Recovery
Temperature at 90% Volume ASTM D 86 °C 331.7
Recovery
Temperature at 95% Volume ASTM D 86 °C 344.5
Recovery
Final Boiling Point ASTM D 86 °C 354.6
Total Acid Number (TAN) IS 1448:P 113 mg 0.1100
KOH/g
Total Sulphur ASTM D 4294 % wt 1.23
501-SC1-5201 Hot HGO 18/09/2023 6:00 Initial Boling Point ASTM D 86 °C 189.4
Temperature at 5% Volume ASTM D 86 °C 272.3
Recovery
Temperature at 10% Volume ASTM D 86 °C 294.0
Recovery
Temperature at 30% Volume ASTM D 86 °C 327.5
Recovery
Temperature at 50% Volume ASTM D 86 °C 348.2
Recovery
Temperature at 70% Volume ASTM D 86 °C 364.6
Recovery
Temperature at 90% Volume ASTM D 86 °C 384.2
Recovery
Temperature at 95% Volume ASTM D 86 °C 393.1
Recovery
Final Boiling Point ASTM D 86 °C 396.0
Total Acid Number (TAN) ASTM D 664 mg 0.16
KOH/g
501-SC2-059 HVGO 18/09/2023 6:00 Density at 15°C ASTM D 1298 kg/m³ 942.9
Temperature at 5% Mass Recovery ASTM D 6352 °C 394.0

Page 3 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC2-059 HVGO 18/09/2023 6:00 Temperature at 10% Mass Recovery ASTM D 6352 °C 415.0
Temperature at 20% Mass Recovery ASTM D 6352 °C 442.0
Temperature at 30% Mass Recovery ASTM D 6352 °C 462.0
Temperature at 40% Mass Recovery ASTM D 6352 °C 478.0
Temperature at 50% Mass Recovery ASTM D 6352 °C 494.0
Temperature at 60% Mass Recovery ASTM D 6352 °C 508.0
Temperature at 70% Mass Recovery ASTM D 6352 °C 523.0
Temperature at 80% Mass Recovery ASTM D 6352 °C 538.0
Temperature at 90% Mass Recovery ASTM D 6352 °C 557.0
Temperature at 95% Mass Recovery ASTM D 6352 °C 571.0
Temperature at Max. Recovery ASTM D 6352 °C 598.0
Micro Carbon Residue ASTM D 4530 Wt% 1.04
Total Acid Number (TAN) ASTM D 664 mg 0.17
KOH/g
501-SC2-060 VGO 18/09/2023 6:00 Density at 15°C ASTM D 1298 kg/m³ 931.4
Temperature at 5% Volume ASTM D 6352 °C 381.0
Recovery
Temperature at 10% Volume ASTM D 6352 °C 402.0
Recovery
Temperature at 20% Volume ASTM D 6352 °C 422.0
Recovery
Temperature at 30% Volume ASTM D 6352 °C 435.0
Recovery
Temperature at 40% Volume ASTM D 6352 °C 447.0
Recovery
Temperature at 50% Volume ASTM D 6352 °C 461.0
Recovery

Page 4 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC2-060 VGO 18/09/2023 6:00 Temperature at 60% Volume ASTM D 6352 °C 477.0
Recovery
Temperature at 70% Volume ASTM D 6352 °C 492.0
Recovery
Temperature at 80% Volume ASTM D 6352 °C 509.0
Recovery
Temperature at 90% Volume ASTM D 6352 °C 530.0
Recovery
Temperature at 95% Volume ASTM D 6352 °C 545.0
Recovery
Temperature at 5% Mass Recovery ASTM D 6352 °C 362.0
Temperature at 10% Mass Recovery ASTM D 6352 °C 382.0
Temperature at 20% Mass Recovery ASTM D 6352 °C 410.0
Temperature at 30% Mass Recovery ASTM D 6352 °C 426.0
Temperature at 40% Mass Recovery ASTM D 6352 °C 445.0
Temperature at 50% Mass Recovery ASTM D 6352 °C 461.0
Temperature at 60% Mass Recovery ASTM D 6352 °C 477.0
Temperature at 70% Mass Recovery ASTM D 6352 °C 495.0
Temperature at 80% Mass Recovery ASTM D 6352 °C 514.0
Temperature at 90% Mass Recovery ASTM D 6352 °C 536.0
Temperature at 95% Mass Recovery ASTM D 6352 °C 555.0
Temp at FBP for Vol% ASTM D 6352 °C 559.0
Temp at FBP for Mass% ASTM D 6352 °C 588.0
Micro Carbon Residue ASTM D 4530 Wt% 1 0.50
Nitrogen Content ASTM D 4629 mg/kg 1079.0
Total Sulphur ASTM D 4294 Mass% 2.87
501-SC2-062 LVGO 18/09/2023 6:00 Density at 15°C ASTM D 1298 kg/m³ 928.7

Page 5 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC2-062 LVGO 18/09/2023 6:00 Temperature at 5% Volume ASTM D 6352 °C 386.4 375.0
Recovery
Temperature at 10% Volume ASTM D 6352 °C 394.0
Recovery
Temperature at 20% Volume ASTM D 6352 °C 407.0
Recovery
Temperature at 30% Volume ASTM D 6352 °C 422.0
Recovery
Temperature at 40% Volume ASTM D 6352 °C 430.0
Recovery
Temperature at 50% Volume ASTM D 6352 °C 440.0
Recovery
Temperature at 60% Volume ASTM D 6352 °C 458.0
Recovery
Temperature at 70% Volume ASTM D 6352 °C 472.0
Recovery
Temperature at 80% Volume ASTM D 6352 °C 489.0
Recovery
Temperature at 90% Volume ASTM D 6352 °C 511.0
Recovery
Temperature at 95% Volume ASTM D 6352 °C 517.2 530.0
Recovery
FBP Vol% ASTM D 6352 °C 548.0
Total Acid Number (TAN) ASTM D 664 mg 0.1800
KOH/g
Total Sulphur ASTM D 4294 Mass% 2.88
501-SC2-086 Vacuum diesel 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 867.3
Initial Boling Point ASTM D 86 °C 238.9
Temperature at 5% Volume ASTM D 86 °C 268.2
Recovery

Page 6 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC2-086 Vacuum diesel 18/09/2023 6:00 Temperature at 10% Volume ASTM D 86 °C 280.4
Recovery
Temperature at 30% Volume ASTM D 86 °C 302.7
Recovery
Temperature at 50% Volume ASTM D 86 °C 318.8
Recovery
Temperature at 70% Volume ASTM D 86 °C 334.1
Recovery
Temperature at 90% Volume ASTM D 86 °C 351.8
Recovery
Temperature at 95% Volume ASTM D 86 °C 358.2
Recovery
Final Boiling Point ASTM D 86 °C 365.1
Inorganic Chloride Titration mg/kg 3.8
Total Acid Number (TAN) ASTM D 664 mg 0.2000
KOH/g
Total Sulphur ASTM D 4294 Mass% 2.28
501-SC2-096B Crude-2nd Stage 18/09/2023 6:00 BS&W ASTM D 4007 Vol % 0.3 0.10
Desalter Outlet
Salt Content IP 77 PTB 1.3 0.79
501-SC2-5601 Vacuum Residue 18/09/2023 6:00 Density at 15°C ASTM D 1298 kg/m³ 1026.1
Temperature at 5% Mass Recovery ASTM 1160 °C 550 554.0
Equivalent
Temperature at 10% Mass Recovery ASTM 1160 °C 598.0
Equivalent
Temperature at 20% Mass Recovery ASTM 1160 °C 611.0
Equivalent
Temperature at 30% Mass Recovery ASTM 1160 °C 639.0
Equivalent
Temperature at 40% Mass Recovery ASTM 1160 °C 661.0
Equivalent

Page 7 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC2-5601 Vacuum Residue 18/09/2023 6:00 Temperature at 50% Mass Recovery ASTM 1160 °C 695.0
Equivalent
Temperature at 55% Mass Recovery ASTM 1160 °C 711.0
Equivalent
501-SC3-5301 MP steam Blow 18/09/2023 6:00 Conductivity ASTM D 1125 µS/cm 9.00
down
Phosphate APHA 4500 mg/l 6.70
P.D
pH ASTM D 1293 12.8
501-SC3-5401 LP steam Blow 18/09/2023 6:00 Conductivity ASTM D 1125 µS/cm 9.42
down
Phosphate APHA 4500 mg/l 6.42
P.D
pH ASTM D 1293 9.8
501-SC2-086 Vacuum diesel 18/09/2023 6:02 Initial Boling Point ASTM D 86 °C 238.9
Temperature at 5% Volume ASTM D 86 °C 268.2
Recovery
Temperature at 10% Volume ASTM D 86 °C 280.4
Recovery
Temperature at 30% Volume ASTM D 86 °C 302.7
Recovery
Temperature at 50% Volume ASTM D 86 °C 318.8
Recovery
Temperature at 70% Volume ASTM D 86 °C 334.1
Recovery
Temperature at 90% Volume ASTM D 86 °C 351.8
Recovery
Temperature at 95% Volume ASTM D 86 °C 358.2
Recovery
Final Boiling Point ASTM D 86 °C 365.1
501-SC3-084 Stabilised naphtha 18/09/2023 14:00
(UnTreated to

Page 8 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
NHT) Density at 15°C ASTM D 4052 kg/m³ 702.7
Initial Boling Point ASTM D 86 °C 36.3
Temperature at 5% Volume ASTM D 86 °C 57.5
Recovery
Temperature at 10% Volume ASTM D 86 °C 62.0
Recovery
Temperature at 30% Volume ASTM D 86 °C 75.4
Recovery
Temperature at 50% Volume ASTM D 86 °C 89.5
Recovery
Temperature at 70% Volume ASTM D 86 °C 103.8
Recovery
Temperature at 90% Volume ASTM D 86 °C 119.2
Recovery
Temperature at 95% Volume ASTM D 86 °C 123 140 124.6
Recovery
Final Boiling Point ASTM D 86 °C 134.8
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 50 47.4
501-SC1-1401 Brine to ETP at 18/09/2023 22:00 Oil & Grease IS 3025:P 39 mg/l 100 58.0
B/L
pH Vendor 5.7
Method
501-SC4-2901 Reflux Drum sour 18/09/2023 22:00 Chloride IS 3025:P 32 mg/l 40 12.0
water
Iron Content ASTM D 1068 mg/kg 1.0 0.30
pH ASTM D 1293 7.5
501-V-107 Hot well Drum sour 18/09/2023 22:00 Chloride IS 3025:P 32 mg/l 3.9
water
Iron Content ASTM D 1068 mg/l 0.33
Sulphide IS 3025:P 29 mg/l 296.0
pH ASTM D 1293 6.0

Page 9 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
# of Samples in Unit: 20
# of Analytes in Unit: 169

Page 10 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

502-NHU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
502-SC.B-2302 Stripper Reflux 18/09/2023 6:00 Chloride IS 3025:P 32 mg/l 15 40 16.0
Drum Boot
Iron Content APHA 3500 D mg/l 2 1.42
pH IS 3025:P 11 5.5 8.5 6.5
502-SC.B-2701 Light Hydrotreated 18/09/2023 6:00 Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 80 95 88.3
Naphtha
502-SC.K-1201 NHT Combined 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 685 710 701.2
Feed
502-SC-8203 PSA off gas 18/09/2023 6:00 Hydrogen Sulfide DRAEGER Vol % 0.0012
TUBE
Total Volatile Sulphur ASTM D 3246 ppm(w) 25.0
502-SC.A-1901 Hydrotreated 19/09/2023 6:00 Total Sulphur ASTM D 5453 ppm(w) 0.3 0.10
Naphtha from
Storage
502-SC.E-1901 Heavy 19/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 0.3 0.10
Hydrotreated
Naphtha
502-SC.G-2401 Splitter Inlet Feed 19/09/2023 6:00 Nitrogen Content ASTM D 4629 mg/kg 0.2 0.1
Total Sulphur ASTM D 5453 mg/kg 0.2 0.10
502-SC.H-1101 SR Naphtha From 19/09/2023 6:00 Nitrogen Content ASTM D 4629 mg/kg 1 0.5
CDU/VDU
502-SC.K-1201 NHT Combined 19/09/2023 6:00 Nitrogen Content ASTM D 4629 mg/kg 1 0.5
Feed
Total Chloride ASTM D 4929 mg/kg 1 <0.3
# of Samples in Unit: 9
# of Analytes in Unit: 14

Page 11 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

503-ISOM
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
503-SC.B-1102 Fresh Feed+DIH 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 650 675 663.7
Recycle
Total Sulphur ASTM D 5453 mg/kg 0.2 0.10
503-SC.D-2104 Isomerate product 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 670 655.7
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 95.0 92.0
Research Octane Number (RON) ASTM D 2699 84 87 86.6
503-SC.K-2403 SCRUBBER 18/09/2023 6:00 % strength UOP 209 Wt% 2 3.0
CIRCULATING
CAUSTIC
503-SC.D-2104 Isomerate product 18/09/2023 14:00 Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 95.0 89.9
503-SC.K-2403 SCRUBBER 18/09/2023 14:00 % strength UOP 209 Wt% 2 2.3
CIRCULATING
CAUSTIC
503-SC.D-2104 Isomerate product 18/09/2023 22:00 Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 95.0 93.9
503-SC.K-2403 SCRUBBER 18/09/2023 22:00 % strength UOP 209 Wt% 2 2.2
CIRCULATING
CAUSTIC
# of Samples in Unit: 7
# of Analytes in Unit: 10

Page 12 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

504-CCR
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
504-SC.K-1101 CCR Feed 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 730 740 738.2
Total Sulphur ASTM D 5453 ppm(w) 0.2 0.5 0.2
504-SC-2602 Reformate 18/09/2023 6:00 Benzene Content ASTM D 3606 Vol % 0.81
Density at 15°C ASTM D 4052 kg/m3 800.0 805 799.2
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 25.6
Research Octane Number (RON) ASTM D 2699 95.0
504-SC-2602 Reformate 18/09/2023 14:00 Benzene Content ASTM D 3606 Vol % 0.6 1.0 0.84
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 20 30 23.9
504-SC-2602 Reformate 18/09/2023 22:00 Benzene Content ASTM D 3606 Vol % 0.6 1.0 0.80

# of Samples in Unit: 4
# of Analytes in Unit: 9

Page 13 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

505-CCR Regeneration
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
505-SC-1103 Caustic Recycle 18/09/2023 6:00 % strength UOP 209 % 0.2 1.0 0.2
Solution
505-SC-2101 Spent Catalyst 18/09/2023 6:00 Chloride IS 3025:P 32 Wt% 0.9 1.0 0.85
505-SC-2301 Regenerated 18/09/2023 6:00 Chloride IS 3025:P 32 Wt% 1.0 1.1 1.02
Catalyst
# of Samples in Unit: 3
# of Analytes in Unit: 3

Page 14 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

506-HRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
506-P-05 Liquid Hydro 18/09/2023 2:00 Initial Boling Point ASTM D 1078 °C 64.6
Discharge Carbon
Distillation between 64 to 70°C ASTM D 1078 Vol % 88.0
Dry Point ASTM D 1078 °C 77.7
506-P-05 Liquid Hydro 18/09/2023 4:00 Initial Boling Point ASTM D 1078 °C 64.6
Discharge Carbon
Distillation between 64 to 70°C ASTM D 1078 Vol % 86.0
Dry Point ASTM D 1078 °C 76.5
506-SC.3-1901 Stripped Naphtha 18/09/2023 22:00 Initial Boling Point ASTM D 1078 °C 64.2
(C-03 bottom)
Dry Point ASTM D 1078 °C 0.1 67.7
Recovery up to 70°C (E70) ASTM D 1078 Vol % 96.3
Total Sulphur ASTM D 5453 mg/kg 0.2 0.10
506-SC.3-1901 Stripped Naphtha 19/09/2023 0:00 Total Sulphur ASTM D 5453 mg/kg 0.2 0.10
(C-03 bottom)
506-SC.3-1901 Stripped Naphtha 19/09/2023 2:00 Initial Boling Point ASTM D 1078 °C 64.1
(C-03 bottom)
Dry Point ASTM D 1078 °C 0.1 67.4
Recovery up to 70°C (E70) ASTM D 1078 Vol % 95.6
Total Sulphur ASTM D 5453 mg/kg 0.2 0.10
506-SC.1-2305 Hexane(FG) 19/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 0.5 0.1

# of Samples in Unit: 7
# of Analytes in Unit: 16

Page 15 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

507-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
507-SC-C-3803 Diesel Product 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 820 860 831.1
Total Sulphur ASTM D 5453 mg/kg 5 10 6.00
507-SC-C-4002 Kerosene Product 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 775 840 796.1
Initial Boling Point ASTM D 86 °C 155.6
Temperature at 5% Volume ASTM D 86 °C 171.3
Recovery
Temperature at 10% Volume ASTM D 86 °C 174.3
Recovery
Temperature at 30% Volume ASTM D 86 °C 182.2
Recovery
Temperature at 50% Volume ASTM D 86 °C 189.3
Recovery
Temperature at 70% Volume ASTM D 86 °C 197.4
Recovery
Temperature at 90% Volume ASTM D 86 °C 210.0
Recovery
Temperature at 95% Volume ASTM D 86 °C 216.0
Recovery
Final Boiling Point ASTM D 86 °C 300 224.4
507-SC-G-2001 Recycle Gas 18/09/2023 6:00 Methane UOP 539 Vol % 3.25
Ethane UOP 539 Vol % 0.93
Propane UOP 539 Vol % 0.52
Iso Butane UOP 539 Vol % 0.12
N Butane UOP 539 Vol % 0.42
Iso Pentane UOP 539 Vol % 0.14
n-Pentane UOP 539 Vol % 0.21
C6+ heaviers UOP 539 Vol % 0.20
Carbon Dioxide UOP 539 Vol % 0.04
Page 16 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

507-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
507-SC-G-2001 Recycle Gas 18/09/2023 6:00 Oxygen UOP 539 Vol % 0.01
Nitrogen UOP 539 Vol % 0.35
Hydrogen UOP 539 Vol % 93.81
Hydrogen Sulfide UOP 539 Vol % 0.0020
Gross Calorific Value ASTM D 3588 Kcal/kg 22753
Net Calorific Value ASTM D 3588 Kcal/kg 19625
Molecular Weight Default 3.78
507-SC-G-8401 DHDT Light 18/09/2023 6:00 Doctor Test ASTM D 4952 Negative
Naphtha
Reid Vapour Pressure @ 38°C ISO 3007 kPa 96.7
507-SC-H-1201 Feed TO DHDT 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 850 841.5
Total Sulphur ASTM D 4294 Mass% 1.65 1.42
507-SC-G-8401 DHDT Light 18/09/2023 6:06 Initial Boling Point ASTM D 86 °C 26.9
Naphtha
Temperature at 5% Volume ASTM D 86 °C 35.3
Recovery
Temperature at 10% Volume ASTM D 86 °C 37.9
Recovery
Temperature at 30% Volume ASTM D 86 °C 46.0
Recovery
Temperature at 50% Volume ASTM D 86 °C 54.6
Recovery
Temperature at 70% Volume ASTM D 86 °C 66.4
Recovery
Temperature at 90% Volume ASTM D 86 °C 88.9
Recovery
Temperature at 95% Volume ASTM D 86 °C 101.8
Recovery
Final Boiling Point ASTM D 86 °C 108.5 130.0
507-SC-B-3210 Fractionator 18/09/2023 10:00
Page 17 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

507-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
Naphtha Density at 15°C ASTM D 4052 kg/m³ 751.8
Initial Boling Point ASTM D 86 °C 75.0
Final Boiling Point ASTM D 86 °C 171.6
Temp. at 50% Vol. Recovery ASTM D 86 °C 130.5
Temp. at 95 % Vol. Recovery ASTM D 86 °C 160.8
Doctor Test IS 1448:P 19 Negative
507-SC-B-3201 DHDT Heavy 18/09/2023 14:00 Density at 15°C ASTM D 4052 kg/m³ 748.3
Naptha
Initial Boling Point ASTM D 86 °C 40 88.0
Temperature at 5% Volume ASTM D 86 °C 101.3
Recovery
Temperature at 10% Volume ASTM D 86 °C 104.2
Recovery
Temperature at 30% Volume ASTM D 86 °C 114.9
Recovery
Temperature at 50% Volume ASTM D 86 °C 126.9
Recovery
Temperature at 70% Volume ASTM D 86 °C 139.0
Recovery
Temperature at 90% Volume ASTM D 86 °C 152.9
Recovery
Temperature at 95% Volume ASTM D 86 °C 159.8
Recovery
Final Boiling Point ASTM D 86 °C 180 172.8
507-SC-C-3803 Diesel Product 18/09/2023 14:00 Total Sulphur ASTM D 5453 mg/kg 5 10 5.50
507-SC-C-3803 Diesel Product 18/09/2023 22:00 Total Sulphur ASTM D 5453 mg/kg 5 10 5.50
507-SC-C-3803 Diesel Product 19/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 5 10 5.00

Page 18 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

507-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
# of Samples in Unit: 13
# of Analytes in Unit: 60

Page 19 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

508-DCU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
508-SC-2-1902 Hot HCGO 18/09/2023 8:00 Density at 15°C ASTM D 1298 kg/m³ 969.7
Micro Carbon Residue ASTM D 4530 Wt% 1.0 1.02
508-SC-3-3601 Hot LCGO 18/09/2023 8:00 Density at 15°C ASTM D 4052 kg/m³ 873.3
Initial Boling Point ASTM D 86 °C 194.3
Temperature at 5% Volume ASTM D 86 °C 215.1
Recovery
Temperature at 10% Volume ASTM D 86 °C 223.0
Recovery
Temperature at 30% Volume ASTM D 86 °C 249.1
Recovery
Temperature at 50% Volume ASTM D 86 °C 278.3
Recovery
Temperature at 70% Volume ASTM D 86 °C 308.8
Recovery
Temperature at 90% Volume ASTM D 86 °C 346.5
Recovery
Temperature at 95% Volume ASTM D 86 °C 350 370 368.7
Recovery
Final Boiling Point ASTM D 86 °C 377.5
508-SC-4-3906 LPG Product at 18/09/2023 9:00 Ethane ASTM D 2163 Vol % 0.5 0.02
B/L
Propane ASTM D 2163 Vol % 46.66
Propylene ASTM D 2163 Vol % 23.37
Iso Butane ASTM D 2163 Vol % 2.96
N Butane ASTM D 2163 Vol % 12.14
trans-2-Butene ASTM D 2163 Vol % 2.16
1-Butene ASTM D 2163 Vol % 5.80
Iso Butylene ASTM D 2163 Vol % 4.43
cis-2-Butene ASTM D 2163 Vol % 1.52
Page 20 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

508-DCU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
508-SC-4-3906 LPG Product at 18/09/2023 9:00 Iso Pentane ASTM D 2163 Vol % 0.17
B/L
n-Pentane ASTM D 2163 Vol % 1 0.07
1,3 Butadiene ASTM D 2163 Vol % 0.31
Trance-2-Pentene ASTM D 2163 Vol % 0.16
1 Pentene ASTM D 2163 Vol % 0.12
2 Methyl 2 Butene ASTM D 2163 Vol % 0.02
Cis 2 Penten ASTM D 2163 Vol % 0.07
C5 Hydrocarbons and Heavier ASTM D 2163 Vol % 1 0.62
Density at 15°C IP 432 kg/m³ 538.0
Vapour Pressure at 40°C IP 432 -2000 kPa 1046
508-SC-2-1201 Vacuum Residue 18/09/2023 12:00 Asphaltenes (Heptane Insoluble) ASTM D 3279 Wt% 29 10.84
Feed
Density at 15°C ASTM D 1298 kg/m³ 1020 1050 1028.5
Micro Carbon Residue ASTM D 4530 Wt% 28.42 24.16
508-SC-4-2801 Fractionator O/H 18/09/2023 12:00 Chloride IS 3025:P 32 mg/l 13.7
sour water
Iron Content ASTM D 1068 mg/l 0.32
pH IS 3025:P 11 8.4
508-SC-4-3102 WGC Interstage 18/09/2023 12:00 Chloride IS 3025:P 32 mg/l 17
(508-V005) boot
Iron Content ASTM D 1068 mg/l 0.39
sour water
pH IS 3025:P 11 7.3
508-SC-4-3203 Recontacting 18/09/2023 12:00 Iron Content ASTM D 1068 mg/l 0.29
Drum (508-V006)
pH IS 3025:P 11 7.5
boot sour water
# of Samples in Unit: 7
# of Analytes in Unit: 42

Page 21 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

509-VGO HDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
509-SC-B-4102 VGO Naphtha 18/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 20 5.5
Product
Doctor Test ASTM D 4952 Negative
509-SC-F-4302 HDT VGO Product 18/09/2023 6:00 Density at 15°C ASTM D 1298 kg/m3 896.5
Temperature at 5% Volume ASTM D 6352 °C 368.0
Recovery
Temperature at 10% Volume ASTM D 6352 °C 392.0
Recovery
Temperature at 20% Volume ASTM D 6352 °C 402.0
Recovery
Temperature at 30% Volume ASTM D 6352 °C 420.0
Recovery
Temperature at 40% Volume ASTM D 6352 °C 428.0
Recovery
Temperature at 50% Volume ASTM D 6352 °C 441.0
Recovery
Temperature at 60% Volume ASTM D 6352 °C 460.0
Recovery
Temperature at 70% Volume ASTM D 6352 °C 474.0
Recovery
Temperature at 80% Volume ASTM D 6352 °C 491.0
Recovery
Temperature at 90% Volume ASTM D 6352 °C 512.0
Recovery
Temperature at 95% Volume ASTM D 6352 °C 531.0
Recovery
Temperature at Max. Recovery ASTM D 6352 °C 548.0
Total Sulphur ASTM D 4294 mg/kg 230 170
509-SC-G-4401 Sweet Gas 18/09/2023 6:00 H2S DRAEGER Vol % 0.0010 0.0012
Sample TUBE
509-SC-B-4102 VGO Naphtha 18/09/2023 14:00 Density at 15°C ASTM D 4052 kg/m³ 770.0 735.8
Product
Page 22 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

509-VGO HDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
509-SC-B-4102 VGO Naphtha 18/09/2023 14:00 Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 50 51.3
Product
Total Sulphur ASTM D 5453 mg/kg 20 7.0
509-SC-E-3603 Diesel Product 18/09/2023 14:00 Density at 15°C ASTM D 4052 kg/m³ 880.0 875.7
Initial Boling Point ASTM D 86 °C 170.6
Temperature at 5% Volume ASTM D 86 °C 199.6
Recovery
Temperature at 10% Volume ASTM D 86 °C 215.0
Recovery
Temperature at 30% Volume ASTM D 86 °C 259.7
Recovery
Temperature at 50% Volume ASTM D 86 °C 289.6
Recovery
Temperature at 70% Volume ASTM D 86 °C 309.8
Recovery
Temperature at 90% Volume ASTM D 86 °C 333.2
Recovery
Temperature at 95% Volume ASTM D 86 °C 378 341.4
Recovery
Final Boiling Point ASTM D 86 °C 345.2
Total Sulphur ASTM D 5453 mg/kg 50 32.0
509-SC-F-4302 HDT VGO Product 18/09/2023 14:00 Total Sulphur ASTM D 4294 mg/kg 230 183
509-SC-G-4401 Sweet Gas 18/09/2023 14:00 Methane UOP 539 Vol % 9.34
Sample
Ethane UOP 539 Vol % 6.13
Propane UOP 539 Vol % 2.17
Iso Butane UOP 539 Vol % 0.59
N Butane UOP 539 Vol % 3.64
Iso Pentane UOP 539 Vol % 1.00
n-Pentane UOP 539 Vol % 1.70
Page 23 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

509-VGO HDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
509-SC-G-4401 Sweet Gas 18/09/2023 14:00 C6+ heaviers UOP 539 Vol % 4.39
Sample
Carbon Dioxide UOP 539 Vol % <0.01
Oxygen UOP 539 Vol % 0.01
Nitrogen UOP 539 Vol % 0.42
Carbon Monoxide UOP 539 Vol % <0.01
Hydrogen UOP 539 Vol % 70.59
Molecular Weight UOP 539 14.0
Net Calorific Value UOP 539 Kcal/kg 12745.00
Gross Calorific Value UOP 539 Kcal/kg 14139.00
H2S DRAEGER Vol % 0.0010 0.0018
TUBE
509-SC-J-1201 Total Feed 18/09/2023 14:00 Total Sulphur ASTM D 4294 Mass% 3.5 2.920
DownStream of
Filter
509-SC-B-4102 VGO Naphtha 18/09/2023 22:00 Total Sulphur ASTM D 5453 mg/kg 20 6.0
Product
Doctor Test ASTM D 4952 Negative
509-SC-F-4302 HDT VGO Product 18/09/2023 22:00 Total Sulphur ASTM D 4294 mg/kg 230 173
509-SC-G-4401 Sweet Gas 18/09/2023 22:00 H2S DRAEGER Vol % 0.0010 0.0018
Sample TUBE
509-SC-B-4102 VGO Naphtha 19/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 20 5.5
Product
# of Samples in Unit: 12
# of Analytes in Unit: 55

Page 24 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

510-FCCU PC
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
510-FB-8302 FCCU PP MIX 18/09/2023 6:00 Methane ASTM D 2712 ppm(v) <100
Ethane ASTM D 2712 ppm(v) 200 <200
Ethylene ASTM D 2712 ppm(v) <100
Propane ASTM D 2712 Vol % 13 11.49
Propylene ASTM D 2712 Vol % 87 88.41
Propadiene ASTM D 2712 ppm(v) 5 <5
Acetylene ASTM D 2712 ppm(v) <3
C4 Saturates ASTM D 2712 ppm(v) <200
C4 Unsaturated ASTM D 2712 ppm(v) <10
C5 Saturated ASTM D 2712 ppm(v) <200
Methyl Acetylene ASTM D 2712 ppm(v) 21.00
1,3 Butadiene ASTM D 2712 ppm(v) <5
C5 Unsaturated ASTM D 2712 ppm(v) <10
Moisture Content ASTM D 1142 ppm(w) 1788 17
COS ASTM D 5504 ppm(v) <0.02
Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5
Methyl Mercaptan ASTM D 5504 ppm(v) <0.5
Ethyl Mercaptan ASTM D 5504 ppm(v) <0.5
510-FV-8402 FCCU FV MIX 18/09/2023 6:00 Propane ASTM D 2163 Vol % 0.90
Propylene ASTM D 2163 Vol % 0.584 0.32
Iso Butane ASTM D 2163 Vol % 11.43
N Butane ASTM D 2163 Vol % 6.01
trans-2-Butene ASTM D 2163 Vol % 17.19
Butene ASTM D 2163 Vol % 14.13

Page 25 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

510-FCCU PC
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
510-FV-8402 FCCU FV MIX 18/09/2023 6:00 Iso Butylene ASTM D 2163 Vol % 29.64
cis-2-Butene ASTM D 2163 Vol % 12.87
Iso Pentane ASTM D 2163 Vol % 0.38
n-Pentane ASTM D 2163 Vol % 0.02
1,3 Butadiene ASTM D 2163 Vol % 0.38
Trance-2-Pentene ASTM D 2163 Vol % 0.62
2 Methyl 2 Butene ASTM D 2163 Vol % 0.02
1 Pentene ASTM D 2163 Vol % 0.07
C5+ heaviers ASTM D 2163 Vol % 1.12
Density at 15°C IP 432 kg/m³ 597.0
Vapour Pressure at 40°C IP 432 kPa 348
510-SC-1-8001 Circulating Caustic 18/09/2023 6:00 % strength IS 252 Wt% 5 8 7.1
Mercaptide UOP 209 ppm(w) 121.00
Sulphide IS 3025:P 29 ppm(w) 473.00
510-SC-4-7301 Fuel gas 18/09/2023 6:00 Methane UOP 539 Vol % 32.42
Ethane UOP 539 Vol % 9.95
Ethylene UOP 539 Vol % 33.52
Propane UOP 539 Vol % 0.07
Propylene UOP 539 Vol % 1.83 0.62
Iso Butane UOP 539 Vol % 0.04
N Butane UOP 539 Vol % 0.03
C4 Unsaturated UOP 539 Vol % 0.2
Iso Pentane UOP 539 Vol % 0.02
C6+ heaviers UOP 539 Vol % 0.02

Page 26 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

510-FCCU PC
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
510-SC-4-7301 Fuel gas 18/09/2023 6:00 Carbon Dioxide UOP 539 Vol % 1.31
Oxygen UOP 539 Vol % 0.08
Nitrogen UOP 539 Vol % 9.74
Carbon Monoxide UOP 539 Vol % 0.26
Hydrogen UOP 539 Vol % 11.63
Hydrogen Sulfide UOP 539 Vol % 0.05 0.060
Gross Calorific Value ASTM D 3588 Kcal/kg 10725.00
Net Calorific Value ASTM D 3588 Kcal/kg 9861.00
Molecular Weight ASTM D 3588 Wt% 21.75
510-SC-4-7801 Debutanizer Ovhd 18/09/2023 6:00 H2S DRAEGER ppm 6.0
(LPG Befor TUBE
Caustic Treatment) Total Volatile Sulphur ASTM D 3246 ppm(w) 10
510-TV-1612 RCSV Catalyst 18/09/2023 13:00 0-20μ ASTM D 1921 Vol % 0.60
0-40μ ASTM D 1921 Vol % 6.07
0-80μ ASTM D 1921 Vol % 55.85
0-105μ ASTM D 1921 Vol % 86.48
0-149μ ASTM D 1921 Vol % 98.95
APS ASTM D 1921 µm 77
510-V-893 CFH fines 18/09/2023 13:00 0-20μ ASTM D 1921 Vol % 38.47
0-40μ ASTM D 1921 Vol % 90.79
0-80μ ASTM D 1921 Vol % 100.00
0-105μ ASTM D 1921 Vol % 100.00
0-149μ ASTM D 1921 Vol % 100.00
APS ASTM D 1921 µm 24

Page 27 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

510-FCCU PC
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
510-SC-1-8001 Circulating Caustic 18/09/2023 14:00 % strength IS 252 Wt% 5 8 7.2
510-SC-1-8002 Circulating Wash 18/09/2023 14:00 Free Caustic IS 252 Wt% 0.4 0.15
Water (LPG Wash
Section)
510-SC-1-9002 LCN 18/09/2023 14:00 Benzene Content ASTM D 3606 Vol % 4.7 3.09
Density at 15°C ASTM D 4052 kg/m³ 620 710 666.8
Initial Boling Point ASTM D 86 °C 29.4
Temperature at 5% Volume ASTM D 86 °C 33.8
Recovery
Temperature at 10% Volume ASTM D 86 °C 34.5
Recovery
Temperature at 30% Volume ASTM D 86 °C 37.0
Recovery
Temperature at 50% Volume ASTM D 86 °C 39.8
Recovery
Temperature at 70% Volume ASTM D 86 °C 44.7
Recovery
Temperature at 90% Volume ASTM D 86 °C 63.7
Recovery
Temperature at 95% Volume ASTM D 86 °C 67.3
Recovery
Final Boiling Point ASTM D 86 °C 67 73.2
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 110 106.6
510-SC-1-8001 Circulating Caustic 18/09/2023 22:00 % strength IS 252 Wt% 5 8 6.8
510-SC-1-9001 MCN 18/09/2023 22:00 Benzene Content ASTM D 3606 Vol % 10 10.57
Density at 15°C ASTM D 4052 kg/m³ 744.7
510-SC-1-9002 LCN 18/09/2023 22:00 Benzene Content ASTM D 3606 Vol % 4.7 3.30
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 110 107.3

Page 28 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

510-FCCU PC
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
510-SC-1-9101 Caustic 18/09/2023 22:00 % strength IS 252 % 5.6
510-SC-3-4201 LCO Product d/s 18/09/2023 22:00 Density at 15°C ASTM D 4052 kg/m³ 990 981.0
of coalescer
Water Content ISO 12937 ppm(w) 1560.0
510-SC-3-8701 HCN 18/09/2023 22:00 Benzene Content ASTM D 5580 Vol % <0.1 <0.1
Density at 15°C ASTM D 4052 kg/m³ 857.2
Total Sulphur ASTM D 5453 ppm(w) 21.0
# of Samples in Unit: 16
# of Analytes in Unit: 96

Page 29 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
511-SC-1155 Naphtha feed to 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 692 733 709.8
PDS section
Initial Boling Point ASTM D 86 °C 35.6
Temperature at 5% Volume ASTM D 86 °C 50.7
Recovery
Temperature at 10% Volume ASTM D 86 °C 56 80 56.9
Recovery
Temperature at 30% Volume ASTM D 86 °C 79.0
Recovery
Temperature at 50% Volume ASTM D 86 °C 105.2
Recovery
Temperature at 70% Volume ASTM D 86 °C 130.8
Recovery
Temperature at 90% Volume ASTM D 86 °C 146.0
Recovery
Temperature at 95% Volume ASTM D 86 °C 150.4
Recovery
Final Boiling Point ASTM D 86 °C 177 155.9
Total Chloride UOP 779 ppm(w) 2 <0.3
Total Sulphur ASTM D 5453 ppm(w) 5 500 324.00
C/H Ratio ASTM D 6839 5.78 5.4
511-SC-1754 Hydrogenated 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 709.3
naphtha to E-003
Total Sulphur ASTM D 5453 ppm(w) 155.0
A/B/C
511-SC-2255 Naphtha (liquid) to 18/09/2023 6:00 Total Sulphur ASTM D 7183 ppm(w) 2 5 0.4
HDS section
511-SC-2752-Ga Feed + H2 d/s 18/09/2023 6:00 Hydrogen Sulphide DRAEGER ppm(v) <0.2
s 511-R-101 TUBE
Total Sulphur ASTM D 5504 ppm(w) <1
511-SC-2757-Ga Process gas (1st 18/09/2023 6:00
s sulfur guard
Page 30 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
bed)-Train 1 Hydrogen Sulphide ASTM D 5504 ppm(v) <0.2
Total Sulphur ASTM D 5504 ppm(w) <1
511-SC-2955 Process gas 18/09/2023 6:00 Methane UOP 539 Vol % 57.4 61.62
prereformed (511-
Carbon Dioxide UOP 539 Vol % 19.87 18.14
R-103 O/L)
Carbon Monoxide UOP 539 Vol % 0.88 0.25
Hydrogen UOP 539 Vol % 21.85 19.98
511-SC-3353 Saturated HP 18/09/2023 6:00 Chloride Vendor ppb(v) 100 <50
steam from steam Method
drum-Train 1 Conductivity IS 3025:P 14 µS/cm 13.89
Silica ASTM D 859 ppm 0.02 <0.02
TDS IS 3025:P 16 ppm 9
pH IS 3025:P 11 8.3 10.0
511-SC-3355 Boiler blow-down 18/09/2023 6:00 Chloride IS 3025:P 32 ppb(v) 91.0
from steam
Conductivity IS 3025:P 14 µS/cm 5.63
drum-Train 1
Phosphate APHA 4500 mg/l 2.47
P.D
Silica ASTM D 859 mg/l <0.02
pH IS 3025:P 11 9.3
511-SC-3551 Process gas I/L to 18/09/2023 6:00 Methane UOP 539 Vol % 4.26 4.00
MT shift
Carbon Dioxide UOP 539 Vol % 6.88 7.95
convertor-Train 1
Carbon Monoxide UOP 539 Vol % 21.66 18.60
Hydrogen UOP 539 Vol % 67.2 69.44
511-SC-3553 Process gas O/L of 18/09/2023 6:00 Methane UOP 539 Vol % 3.59 3.53
MT shift
Carbon Dioxide UOP 539 Vol % 20.11 20.61
convertor-Train 1
Carbon Monoxide UOP 539 Vol % 5.03 2.10

Page 31 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
511-SC-3553 Process gas O/L of 18/09/2023 6:00 Hydrogen UOP 539 Vol % 71.21 73.76
MT shift
511-SC-3704 Reformer O/L to1 18/09/2023 6:00 Methane UOP 539 Vol % 3.78 3.15
convertor-Train
Heater I/L
Carbon Dioxide UOP 539 Vol % 8.79 8.73
Carbon Monoxide UOP 539 Vol % 19.7 19.06
Hydrogen UOP 539 Vol % 67.73 69.06
511-SC-3801 511-SC-3801 18/09/2023 6:00 Chloride IS 3025:P 32 mg/l 105.0
Conductivity IS 3025:P 14 µS/cm 301.00
511-SC-3802 511-SC-3802 18/09/2023 6:00 Chloride Vendor ppb 100 <50
Method
Conductivity IS 3025:P 14 µS/cm 659.00
511-SC-4752-Ga Feed + H2 d/s 18/09/2023 6:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.2
s 511-R-201
Total Sulphur ASTM D 5504 ppm(w) <1
511-SC-4757-Ga Process gas (1st 18/09/2023 6:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.2
s sulfur guard
Total Sulphur ASTM D 5504 ppm(w) <1
bed)-Train 2
511-SC-4758-Ga Feed+ H2 d/s 18/09/2023 6:00 Hydrogen Sulfide UOP 539 ppm(v) <0.2
s 511-R-202A
Total Sulphur ASTM D 5504 ppm(w) <1
511-SC-4955 Process gas 18/09/2023 6:00 Methane UOP 539 Vol % 57.82 76.75
prereformed (511-
Carbon Dioxide UOP 539 Vol % 20.8 3.97
R-203 O/L)
Carbon Monoxide UOP 539 Vol % 0.82 <0.01
Hydrogen UOP 539 Vol % 20.56 19.27
511-SC-5353 Saturated HP 18/09/2023 6:00 Chloride Vendor ppb(v) 100 98.0
steam from steam Method
drum-Train 2 Conductivity IS 3025:P 14 µS/cm 54.70
Silica ASTM D 859 ppm 0.02 <0.02

Page 32 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
511-SC-5353 Saturated HP 18/09/2023 6:00 TDS IS 3025:P 16 ppm 35
steam from steam
pH IS 3025:P 11 8.3 9.8
drum-Train 2
511-SC-5355 Boiler blow-down 18/09/2023 6:00 Chloride IS 3025:P 32 ppb(v) 93.0
from steam
Conductivity IS 3025:P 14 µS/cm 17.65
drum-Train 2
Phosphate APHA 4500 mg/l 3.53
P.D
Silica ASTM D 859 mg/l 0.04
pH IS 3025:P 11 9.8
511-SC-5551 Process gas I/L to 18/09/2023 6:00 Methane UOP 539 Vol % 4.83 5.02
MT shift
Carbon Dioxide UOP 539 Vol % 10.18 6.37
convertor-Train 2
Carbon Monoxide UOP 539 Vol % 17.8 16.47
Hydrogen UOP 539 Vol % 67.19 72.14
511-SC-5553 Process gas O/L of 18/09/2023 6:00 Methane UOP 539 Vol % 4.2 5.01
MT shift
Carbon Dioxide UOP 539 Vol % 22.3 15.50
convertor-Train 2
Carbon Monoxide UOP 539 Vol % 1.9 1.46
Hydrogen UOP 539 Vol % 71.6 70.16
511-SC-5801 Blow down for 18/09/2023 6:00 Chloride Vendor ppb 98.0
E-219 Method
Conductivity IS 3025:P 14 µS/cm 219.00
511-SC-5802 E-219 Saturated 18/09/2023 6:00 Chloride Vendor ppb 100 91.0
steam Method
Conductivity IS 3025:P 14 µS/cm 332.00
511-SC-6101 PSA off-gas 18/09/2023 6:00 Methane UOP 539 Vol % 11.57 12.75
Carbon Dioxide UOP 539 Vol % 54.56 52.85
Carbon Monoxide UOP 539 Vol % 4.21 5.25

Page 33 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
511-SC-6101 PSA off-gas 18/09/2023 6:00 Hydrogen UOP 539 Vol % 28.67 29.15
511-SC-6151 Product Hydrogen 18/09/2023 6:00 Methane UOP 539 ppm(v) 930 <0.2
from PSA unit
Carbon Dioxide UOP 539 ppm(v) 1.33
Carbon Monoxide UOP 539 ppm(v) 20 9.52
Hydrogen UOP 539 Vol % 99.9 99.99
511-SC-6853 Boiler feed water 18/09/2023 6:00 Conductivity IS 3025:P 14 µS/cm 16.80
from
Silica ASTM D 859 mg/l 0.02 <0.02
Dearator-Train 1
pH IS 3025:P 11 8.3 9.6
511-SC-7853 Boiler feed water 18/09/2023 6:00 Conductivity IS 3025:P 14 µS/cm 92.40
from
Silica ASTM D 859 ppm 0.02 <0.02
Dearator-Train 2
pH IS 3025:P 11 8.3 10.2
511-SC-2255 Naphtha (liquid) to 18/09/2023 14:00 Total Sulphur ASTM D 7183 ppm(w) 2 5 0.5
HDS section
511-SC-2255 Naphtha (liquid) to 18/09/2023 22:00 Total Sulphur ASTM D 7183 ppm(w) 2 5 0.5
HDS section
511-SC-2752-Liq Feed + H2 d/s 18/09/2023 22:00 Total Sulphur ASTM D 7183 ppm(w) <0.05
uid 511-R-101
511-SC-2758-Ga Feed+ H2 d/s 18/09/2023 22:00 Hydrogen Sulfide ASTM D 5504 ppm(w) <0.2
s 511-R-102A
Total Sulphur ASTM D 5504 ppm(w) <1.0
511-SC-2764-Ga Feed+ H2 d/s 18/09/2023 22:00 Hydrogen Sulfide ASTM D 5504 ppm(v) 0 <0.2
s 511-R-102B
Total Sulphur ASTM D 5504 ppm(w) 0.05 <1.0
511-SC-2764-Liq Feed+ H2 d/s 18/09/2023 22:00 Total Sulphur ASTM D 7183 ppm(w) 0.05 <0.05
uid 511-R-102B
511-SC-2775 Chloride guard 18/09/2023 22:00 Total Chloride ASTM D 4929 ppm(w) <0.2
Outlet
(511-R-102C)

Page 34 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
511-SC-4758-Ga Feed+ H2 d/s 18/09/2023 22:00 Hydrogen Sulfide UOP 539 ppm(v) <0.2
s 511-R-202A
Total Sulphur ASTM D 5504 ppm(w) <1.0
511-SC-1155 Naphtha feed to 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 692 733 710.4
PDS section
Total Chloride UOP 779 ppm(w) 2 <0.3
Total Sulphur ASTM D 5453 ppm(w) 5 500 296.00
C/H Ratio ASTM D 6839 5.78 5.4
511-SC-1754 Hydrogenated 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 709.5
naphtha to E-003
Total Sulphur ASTM D 5453 ppm(w) 132.0
A/B/C
511-SC-2255 Naphtha (liquid) to 19/09/2023 6:00 Total Sulphur ASTM D 7183 ppm(w) 2 5 0.4
HDS section
# of Samples in Unit: 38
# of Analytes in Unit: 114

Page 35 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

512-PRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
512-SC-4-1301 PP mix 18/09/2023 6:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5 <0.5
COS ASTM D 5504 ppm(v) <0.02 <0.02
Methyl Mercapton ASTM D 5504 ppm(v) <0.5 <0.5
Mercaptan Sulfur ASTM D 5504 ppm(v) <0.5 <0.5
Moisture Content ASTM D 1142 ppm(w) 0.60
512-SC-4-1302 PP mix 18/09/2023 6:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5
COS ASTM D 5504 ppm(v) <0.02
Methyl Mercapton ASTM D 5504 ppm <0.5
Mercaptan Sulfur ASTM D 5504 ppm(v) <0.5
Moisture Content ASTM D 1142 ppm(w) 1 0.60
512-SC-4-1401 LPG product from 18/09/2023 6:00 Propane ASTM D 2163 Vol % 99.14
C3 stripper bottom
Propylene ASTM D 2163 Vol % 2 0.80
Iso Butane ASTM D 2163 Vol % 0.04
N Butane ASTM D 2163 Vol % 0.01
Density at 15°C IP 432 kg/m³ 507.5
512-SC-4-2202 PGP product 18/09/2023 6:00 Ammonia Dragger ppm 2.0 <2
Arsine GC-MS ppm(v) 0.03 <0.03
Methane ASTM D 2712 ppm(v) 100.0 <100
Ethane ASTM D 2712 ppm(v) 279.9 <279.9
Ethylene ASTM D 2712 ppm(v) 100.0 <100
Propane ASTM D 2712 Vol % 0.4 0.390
Propylene ASTM D 2712 Vol % 99.50 99.52
Iso Butane ASTM D 2712 ppm(v) 100 <100
N Butane ASTM D 2712 ppm(v) 100 <100

Page 36 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

512-PRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
512-SC-4-2202 PGP product 18/09/2023 6:00 Propadiene ASTM D 2712 ppm(v) 5.0 <5
Acetylene ASTM D 2712 ppm(v) 4.85 <3
C4 Unsaturated ASTM D 2712 ppm(v) 10.0 <10
Iso Pentane ASTM D 2712 ppm(v) 100 <100
n-Pentane ASTM D 2712 ppm(v) 100 <100
1,3 Butadiene ASTM D 2712 ppm(v) 3.89 <3.89
Methyl Acetylene ASTM D 2712 ppm(v) 3.0 <3
C5 Unsaturated ASTM D 2712 ppm(v) 10.0 <10
Hexane + Nonene ASTM D 2712 ppm(v) 1.98 <1.98
Cyclopentadiene Vendor ppm(v) 0.05 <0.05
Method
Green Oil (C6,C9,C12) Vendor ppm(v) 20.0 <20
Method
H2S DRAEGER ppm(v) 0.50 <0.5
TUBE
Moisture Content By SHAW ppm(w) 1.0 0.4
Dew Point
Total Sulphur ASTM D 3246 ppm(w) 0.5 0.5
Carbon Dioxide ASTM D 8098 ppm(v) 1.91 <1.91
Hydrogen ASTM D 8098 ppm(v) 2.0 <1
Oxygen ASTM D 8098 ppm(v) 1.0 <1
Nitrogen ASTM D 8098 ppm(v) 100.0 <100
Carbon Monoxide ASTM D 8098 ppm(v) 0.03 <0.03
COS Default ppm(v) 0.02 <0.02.
Isopropyl alcohol UOP 960 ppm(v) 0.91 <0.91
Methanol UOP 960 ppm(v) 1.0 <1

Page 37 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

512-PRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
512-SC-4-2202 PGP product 18/09/2023 6:00 Phosphine GC-MS ppm(v) 0.03 <0.03
512-SC-4-1301 PP mix 18/09/2023 22:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5 <0.5
COS ASTM D 5504 ppm(v) <0.02 <0.02
Methyl Mercapton ASTM D 5504 ppm(v) <0.5 <0.5
Mercaptan Sulfur ASTM D 5504 ppm(v) <0.5 <0.5
Moisture Content ASTM D 1142 ppm(w) 0.60
512-SC-4-1302 PP mix 18/09/2023 22:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5
COS ASTM D 5504 ppm(v) <0.02
Methyl Mercapton ASTM D 5504 ppm <0.5
Mercaptan Sulfur ASTM D 5504 ppm(v) <0.5
Moisture Content ASTM D 1142 ppm(w) 1 0.60
512-SC-4-2202 PGP product 18/09/2023 22:00 Arsine GC-MS ppm(v) 0.03 <0.03
Methane ASTM D 2712 ppm(v) 100.0 <100
Ethane ASTM D 2712 ppm(v) 279.9 <279.9
Ethylene ASTM D 2712 ppm(v) 100.0 <100
Propane ASTM D 2712 Vol % 0.4 0.410
Propylene ASTM D 2712 Vol % 99.50 99.49
Iso Butane ASTM D 2712 ppm(v) 100 <100
N Butane ASTM D 2712 ppm(v) 100 <100
Propadiene ASTM D 2712 ppm(v) 5.0 <5
Acetylene ASTM D 2712 ppm(v) 4.85 <3
C4 Unsaturated ASTM D 2712 ppm(v) 10.0 <10
Iso Pentane ASTM D 2712 ppm(v) 100 <100
n-Pentane ASTM D 2712 ppm(v) 100 <100

Page 38 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

512-PRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
512-SC-4-2202 PGP product 18/09/2023 22:00 1,3 Butadiene ASTM D 2712 ppm(v) 3.89 <3.89
Methyl Acetylene ASTM D 2712 ppm(v) 3.0 <3
C5 Unsaturated ASTM D 2712 ppm(v) 10.0 <10
H2S DRAEGER ppm(v) 0.50 <0.5
TUBE
Moisture Content By SHAW ppm(w) 1.0 0.4
Dew Point
COS Default ppm(v) 0.02 <0.02
Phosphine GC-MS ppm(v) 0.03 <0.03
# of Samples in Unit: 7
# of Analytes in Unit: 77

Page 39 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331A Reactor1 18/09/2023 1:00 Melt Flow Rate ASTM D 1238 g/10min 4.38
513-S-331B Reactor2 18/09/2023 1:00 Melt Flow Rate ASTM D 1238 g/10min 3.92
513-S-415 Reactor 3 18/09/2023 1:00 Melt Flow Rate ASTM D 1238 g/10min 3.44
513-S-331A Reactor1 18/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 4.57
513-S-331B Reactor2 18/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.79
513-S-415 Reactor 3 18/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.44
R03RR PP Pellet 18/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.52
513-S-331A Reactor1 18/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 4.21
Xylene Solubility ASTM D 5492 Wt% 3.92
Xylene Solubility by NMR Default % 4.03
513-S-331B Reactor2 18/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.79
Xylene Solubility ASTM D 5492 Wt% 3.76
Xylene Solubility by NMR Default % 3.77
513-S-415 Reactor 3 18/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.06
Xylene Solubility ASTM D 5492 Wt% 3.46
Xylene Solubility by NMR Default % 3.74
R03RR PP Pellet 18/09/2023 4:00 Irg 1010 ASTM D 6247 ppm 380 520 340
I 168 ASTM D 6247 ppm 750 1050 600
DHT 4A ASTM D 6247 ppm 250 350 180
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.69
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 10

Page 40 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
R03RR PP Pellet 18/09/2023 4:00 Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
513-S-331A Reactor1 18/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.99
513-S-331B Reactor2 18/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.42
513-S-415 Reactor 3 18/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 2.87
R03RR PP Pellet 18/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.31
513-S-331A Reactor1 18/09/2023 8:00 Bulk Density ASTM D 1895 g/cc 0.468
Aluminium Content ASTM D 6247 ppm 60.0
Magnesium Content ASTM D 6247 ppm 13.0
Titanium Content ASTM D 6247 ppm 1.0
Chloride Content ASTM D 6247 ppm 38.0
Iron Content ASTM D 6247 ppm 1.0
Melt Flow Rate ASTM D 1238 g/10min 3.80
Retention on 10 mesh ASTM D 1921 Wt% 0.20
Retention on 18 mesh ASTM D 1921 Wt% 0.70
Retention on 35 mesh ASTM D 1921 Wt% 21.80
Retention on 60 mesh ASTM D 1921 Wt% 66.10
Retention on 120 mesh ASTM D 1921 Wt% 10.80
Retention on 230 mesh ASTM D 1921 Wt% 0.20
Retention on Pan ASTM D 1921 Wt% 0.20
APS ASTM D 1921 µ 446
Xylene Solubility ASTM D 5492 Wt% 3.94
Xylene Solubility by NMR Default % 3.99
Page 41 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331B Reactor2 18/09/2023 8:00 Bulk Density ASTM D 1895 g/cc 0.474
Aluminium Content ASTM D 6247 ppm 60.0
Magnesium Content ASTM D 6247 ppm 13.0
Titanium Content ASTM D 6247 ppm 1.0
Chloride Content ASTM D 6247 ppm 38.0
Iron Content ASTM D 6247 ppm 1.0
Melt Flow Rate ASTM D 1238 g/10min 3.50
Retention on 10 mesh ASTM D 1921 Wt% 0.20
Retention on 18 mesh ASTM D 1921 Wt% 0.70
Retention on 35 mesh ASTM D 1921 Wt% 21.80
Retention on 60 mesh ASTM D 1921 Wt% 66.10
Retention on 120 mesh ASTM D 1921 Wt% 10.80
Retention on 230 mesh ASTM D 1921 Wt% 0.20
Retention on Pan ASTM D 1921 Wt% 0.20
APS ASTM D 1921 µ 446
Xylene Solubility ASTM D 5492 Wt% 3.49
Xylene Solubility by NMR Default % 3.52
513-S-415 Reactor 3 18/09/2023 8:00 Bulk Density ASTM D 1895 g/cc 0.470
Aluminium Content ASTM D 6247 ppm 60.0
Magnesium Content ASTM D 6247 ppm 12.0
Titanium Content ASTM D 6247 ppm 1.0
Chloride Content ASTM D 6247 ppm 25.0
Iron Content ASTM D 6247 ppm 1.0
Melt Flow Rate ASTM D 1238 g/10min 2.92

Page 42 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-415 Reactor 3 18/09/2023 8:00 Xylene Solubility ASTM D 5492 Wt% 3.51
Xylene Solubility by NMR Default % 3.58
R03RR PP Pellet 18/09/2023 8:00 Irg 1010 ASTM D 6247 ppm 380 520 440
I 168 ASTM D 6247 ppm 750 1050 1105
DHT 4A ASTM D 6247 ppm 250 350 285
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.18
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 16
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 36
Under Size Default Wt% 0.2 0.0
Over Size Default Wt% 1 1.4
Size Default Wt% 98 98.6
Fines Default Wt% 0 0.0
Yellowness Index ASTM E 313 0 -4.63
513-S-331A Reactor1 18/09/2023 10:00 Melt Flow Rate ASTM D 1238 g/10min 3.86
513-S-331B Reactor2 18/09/2023 10:00 Melt Flow Rate ASTM D 1238 g/10min 3.24
513-S-415 Reactor 3 18/09/2023 10:00 Melt Flow Rate ASTM D 1238 g/10min 3.05
R03RR PP Pellet 18/09/2023 10:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.35
513-S-331A Reactor1 18/09/2023 12:00 Melt Flow Rate ASTM D 1238 g/10min 3.76
Xylene Solubility ASTM D 5492 Wt% 3.51
Page 43 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331A Reactor1 18/09/2023 12:00 Xylene Solubility by NMR Default % 3.58
513-S-331B Reactor2 18/09/2023 12:00 Melt Flow Rate ASTM D 1238 g/10min 3.35
Xylene Solubility ASTM D 5492 Wt% 3.50
Xylene Solubility by NMR Default % 3.66
513-S-415 Reactor 3 18/09/2023 12:00 Melt Flow Rate ASTM D 1238 g/10min 3.33
Xylene Solubility ASTM D 5492 Wt% 3.37
Xylene Solubility by NMR Default % 3.50
513-SP-60101 White oil+Atmer 18/09/2023 12:00 Aluminium Content Default % 1.48
Density at 15°C ASTM D 4052 kg/m3 902.7
Moisture Content ASTM D 2867 ppm 930
R03RR PP Pellet 18/09/2023 12:00 Irg 1010 ASTM D 6247 ppm 380 520 410
I 168 ASTM D 6247 ppm 750 1050 735
DHT 4A ASTM D 6247 ppm 250 350 210
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.32
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 18
Tails Default no/5kg 3 2
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
513-S-331A Reactor1 18/09/2023 14:00 Melt Flow Rate ASTM D 1238 g/10min 3.50
513-S-331B Reactor2 18/09/2023 14:00 Melt Flow Rate ASTM D 1238 g/10min 3.57
513-S-415 Reactor 3 18/09/2023 14:00 Melt Flow Rate ASTM D 1238 g/10min 3.46

Page 44 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
R03RR PP Pellet 18/09/2023 14:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.42
513-S-331A Reactor1 18/09/2023 16:00 Melt Flow Rate ASTM D 1238 g/10min 2.34
Xylene Solubility ASTM D 5492 Wt% 2.83
Xylene Solubility by NMR Default % 2.98
513-S-331B Reactor2 18/09/2023 16:00 Melt Flow Rate ASTM D 1238 g/10min 3.66
Xylene Solubility ASTM D 5492 Wt% 3.68
Xylene Solubility by NMR Default % 3.94
513-S-415 Reactor 3 18/09/2023 16:00 Melt Flow Rate ASTM D 1238 g/10min 3.67
Retention on 10 mesh ASTM D 1921 Wt% 0.20
Retention on 18 mesh ASTM D 1921 Wt% 0.40
Retention on 35 mesh ASTM D 1921 Wt% 22.30
Retention on 60 mesh ASTM D 1921 Wt% 63.20
Retention on 120 mesh ASTM D 1921 Wt% 12.30
Retention on 230 mesh ASTM D 1921 Wt% 1.5
Retention on Pan ASTM D 1921 Wt% 0.10
APS ASTM D 1921 µ 440
Xylene Solubility ASTM D 5492 Wt% 3.35
Xylene Solubility by NMR Default % 3.55
R03RR PP Pellet 18/09/2023 16:00 Irg 1010 ASTM D 6247 ppm 380 520 450
I 168 ASTM D 6247 ppm 750 1050 635
DHT 4A ASTM D 6247 ppm 250 350 295
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.20
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0

Page 45 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
R03RR PP Pellet 18/09/2023 16:00 Fused Pellet Default no/5kg 1 12
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 37
Under Size Default Wt% 0.2 0.0
Over Size Default Wt% 1 1.5
Size Default Wt% 98 98.5
Fines Default Wt% 0 0.0
Yellowness Index ASTM E 313 0 -452.00
513-S-331A Reactor1 18/09/2023 17:00 Melt Flow Rate ASTM D 1238 g/10min 2.29
Xylene Solubility by NMR Default % 2.63
513-S-331A Reactor1 18/09/2023 18:00 Melt Flow Rate ASTM D 1238 g/10min 2.50
Xylene Solubility by NMR Default % 2.96
513-S-331B Reactor2 18/09/2023 18:00 Melt Flow Rate ASTM D 1238 g/10min 3.56
513-S-415 Reactor 3 18/09/2023 18:00 Melt Flow Rate ASTM D 1238 g/10min 3.83
R03RR PP Pellet 18/09/2023 18:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.20
513-S-331A Reactor1 18/09/2023 19:00 Melt Flow Rate ASTM D 1238 g/10min 2.94
513-S-331A Reactor1 18/09/2023 20:00 Melt Flow Rate ASTM D 1238 g/10min 3.28
Xylene Solubility ASTM D 5492 Wt% 3.06
Xylene Solubility by NMR Default % 3.09
513-S-331B Reactor2 18/09/2023 20:00 Melt Flow Rate ASTM D 1238 g/10min 3.68
Xylene Solubility ASTM D 5492 Wt% 3.64

Page 46 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331B Reactor2 18/09/2023 20:00 Xylene Solubility by NMR Default % 3.71
513-S-415 Reactor 3 18/09/2023 20:00 Melt Flow Rate ASTM D 1238 g/10min 3.72
Xylene Solubility ASTM D 5492 Wt% 3.38
Xylene Solubility by NMR Default % 3.55
R03RR PP Pellet 18/09/2023 20:00 I 168 ASTM D 6247 ppm 750 1050 610
DHT 4A ASTM D 6247 ppm 250 350 265
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.17
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 16
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
513-S-331A Reactor1 18/09/2023 21:00 Melt Flow Rate ASTM D 1238 g/10min 3.69
513-S-331A Reactor1 18/09/2023 22:00 Melt Flow Rate ASTM D 1238 g/10min 4.05
513-S-331B Reactor2 18/09/2023 22:00 Melt Flow Rate ASTM D 1238 g/10min 3.98
513-S-415 Reactor 3 18/09/2023 22:00 Melt Flow Rate ASTM D 1238 g/10min 3.81
R03RR PP Pellet 18/09/2023 22:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.26
513-S-331A Reactor1 18/09/2023 23:00 Melt Flow Rate ASTM D 1238 g/10min 4.40
Xylene Solubility by NMR Default % 3.69
513-LZ-110B-I/L Propylene Dryer 19/09/2023 0:00 Methane UOP 539 ppm(v) 100 <5
I/L
Ethane UOP 539 ppm(v) 200 <5
Ethylene UOP 539 ppm(v) 100 <5

Page 47 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-LZ-110B-I/L Propylene Dryer 19/09/2023 0:00 Propane UOP 539 Vol % 0.4 0.370
I/L
Propylene UOP 539 Vol % 99.6 99.62
Propadiene UOP 539 ppm(v) 5 <5
Acetylene UOP 539 ppm(v) 3 <3
Iso Butane UOP 539 ppm(v) <5
N Butane UOP 539 ppm(v) <5
C4 Unsaturated UOP 539 ppm(v) 650 <5
Iso Pentane UOP 539 ppm(v) <5
n-Pentane UOP 539 ppm(v) <5
1,3 Butadiene UOP 539 ppm(v) 5 <5
Methyl Acetylene UOP 539 ppm(v) 3 <3
C5 Unsaturated UOP 539 ppm(v) 200 <5
Hydrogen Sulfide UOP 539 ppm(v) 500 <0.5
COS UOP 539 ppm(v) 0.02 <0.02
Arsine UOP 539 ppm(v) 0.03 <0.03
Phosphine UOP 539 ppm(v) 0.03 <0.03
Mercaptan Sulfur UOP 209 ppm <0.5
Moisture Content ASTM D 1142 ppm(w) 1 0.40
513-S-331A Reactor1 19/09/2023 0:00 Melt Flow Rate ASTM D 1238 g/10min 4.49
Xylene Solubility ASTM D 5492 Wt% 3.58
Xylene Solubility by NMR Default % 3.73
513-S-331B Reactor2 19/09/2023 0:00 Melt Flow Rate ASTM D 1238 g/10min 3.90
Xylene Solubility ASTM D 5492 Wt% 3.69
Xylene Solubility by NMR Default % 3.84

Page 48 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-415 Reactor 3 19/09/2023 0:00 Melt Flow Rate ASTM D 1238 g/10min 3.56
Xylene Solubility ASTM D 5492 Wt% 3.48
Xylene Solubility by NMR Default % 3.59
R03RR PP Pellet 19/09/2023 0:00 Irg 1010 ASTM D 6247 ppm 380 520 430
I 168 ASTM D 6247 ppm 750 1050 700
DHT 4A ASTM D 6247 ppm 250 350 260
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.53
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 18
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 35
Under Size Default Wt% 0.2 0.0
Over Size Default Wt% 1 1.3
Size Default Wt% 98 98.7
Fines Default Wt% 0 0.0
Yellowness Index ASTM E 313 0 -4.47
513-S-331A Reactor1 19/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 4.24
Xylene Solubility by NMR Default % 3.68
513-S-331B Reactor2 19/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 4.04
513-S-415 Reactor 3 19/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.63
R03RR PP Pellet 19/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.29
Page 49 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331A Reactor1 19/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.83
Xylene Solubility by NMR Default % 3.64
513-S-331B Reactor2 19/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.90
Xylene Solubility by NMR Default % 3.89
513-S-415 Reactor 3 19/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.53
Xylene Solubility by NMR Default % 3.51
R03RR PP Pellet 19/09/2023 4:00 Irg 1010 ASTM D 6247 ppm 380 520 360
I 168 ASTM D 6247 ppm 750 1050 550
DHT 4A ASTM D 6247 ppm 250 350 230
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.69
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 15
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
# of Samples in Unit: 65
# of Analytes in Unit: 252

Page 50 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

514-FGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
514-C-101 O/L RFG feed to DCU 18/09/2023 10:00 Methane UOP 539 Vol % 57.71
Ethane UOP 539 Vol % 19.44
Ethylene UOP 539 Vol % 3.12
Propane UOP 539 Vol % 1.80
Propylene UOP 539 Vol % 0.59
Iso Butane UOP 539 Vol % 0.45
N Butane UOP 539 Vol % 2.78
C4 Unsaturated UOP 539 Vol % 0.8
Iso Pentane UOP 539 Vol % 0.19
n-Pentane UOP 539 Vol % 0.20
C5 Unsaturated UOP 539 Vol % 0.2
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 0.02
Oxygen UOP 539 Vol % 0.03
Nitrogen UOP 539 Vol % 0.51
Carbon Monoxide UOP 539 Vol % 0.17
Hydrogen UOP 539 Vol % 12.00
Hydrogen Sulfide UOP 539 ppm(v) <0.5
COS UOP 539 ppm(v) <0.5
Gross Calorific Value ASTM D 5865 Kcal/kg 12815
Net Calorific Value ASTM D 3588 Kcal/kg 11640
Total Mercaptans ASTM D 6228 ppm(v) 14.0
Molecular Weight Default 20.20
Methyl Mercaptan ASTM D 5504 vol. ppm 12.00

Page 51 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

514-FGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
514-C-101 O/L RFG feed to DCU 18/09/2023 10:00 Ethyl Mercaptan ASTM D 6228 vol. ppm <0.5
Propyl Mercaptan ASTM D 6228 vol. ppm <0.5
Butyl Mercaptan ASTM D 6228 vol. ppm <0.5
514-SC4-2101 LP Fuel Gas 18/09/2023 14:00 Methane UOP 539 Vol % 73.10
Ethane UOP 539 Vol % 7.60
Ethylene UOP 539 Vol % 8.32
Propane UOP 539 Vol % 1.11
Propylene UOP 539 Vol % 0.26
Iso Butane UOP 539 Vol % 0.28
N Butane UOP 539 Vol % 0.77
C4 Unsaturated UOP 539 Vol % 0.2
Iso Pentane UOP 539 Vol % 0.05
n-Pentane UOP 539 Vol % 0.04
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 0.15
Oxygen UOP 539 Vol % 0.11
Nitrogen UOP 539 Vol % 2.86
Carbon Monoxide UOP 539 Vol % 0.12
Hydrogen UOP 539 Vol % 5.02
Hydrogen Sulfide UOP 539 Vol % 0.0100 0.0004
Molecular Weight UOP 539 18.78
Net Calorific Value UOP 539 Kcal/kg 11219.00
Gross Calorific Value UOP 539 Kcal/kg 12365.00
514-SC4-2102 HP Fuel Gas 18/09/2023 14:00 Methane UOP 539 Vol % 73.59

Page 52 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

514-FGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
514-SC4-2102 HP Fuel Gas 18/09/2023 14:00 Ethane UOP 539 Vol % 7.37
Ethylene UOP 539 Vol % 8.41
Propane UOP 539 Vol % 0.95
Propylene UOP 539 Vol % 0.26
Iso Butane UOP 539 Vol % 0.24
N Butane UOP 539 Vol % 0.5 0.68
C4 Unsaturated UOP 539 Vol % 0.18
Iso Pentane UOP 539 Vol % 0.05
n-Pentane UOP 539 Vol % 0.04
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 0.13
Oxygen UOP 539 Vol % 0.08
Nitrogen UOP 539 Vol % 2.71
Carbon Monoxide UOP 539 Vol % 0.12
Hydrogen UOP 539 Vol % 5.19
Hydrogen Sulfide UOP 539 Vol % 0.0100 0.0004
Molecular Weight UOP 539 18.60
Net Calorific Value UOP 539 Kcal/kg 11265.00
Gross Calorific Value UOP 539 Kcal/kg 11000 12000 12418
# of Samples in Unit: 3
# of Analytes in Unit: 67

Page 53 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

515-Sr LPG TU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
515-SC4-1501 LPG to B/L 18/09/2023 6:00 Total Volatile Sulphur ASTM D 3246 ppm(w) 500 10
Hydrogen Sulfide ASTM D 2420 ppm(v) Negative
515-SC4-1501 LPG to B/L 18/09/2023 14:00 Total Volatile Sulphur ASTM D 3246 ppm(w) 500 10
Hydrogen Sulfide ASTM D 2420 ppm(v) Negative
515-SC4-1501 LPG to B/L 18/09/2023 22:00 Copper Strip Corrosion for 1 hrs @ ASTM D 1838 1b
38°C
PHP Default Positive
Volatility:Evaporation Temp in°C for ASTM D 1837 °C -2 0.2
95%v at760mm
515-SC4-1501 LPG to B/L 19/09/2023 6:00 Total Volatile Sulphur ASTM D 3246 ppm(w) 500 10

# of Samples in Unit: 4
# of Analytes in Unit: 8

Page 54 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

516-Cr LPG TU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
516-SC4-2601 LPG 18/09/2023 22:00 Total Volatile Sulphur ASTM D 3246 ppm(w) 100 30
Copper Strip Corrosion for 1 hrs @ ASTM D 1838 1b
38°C
Hydrogen Sulfide ASTM D 2420 Negative
PHP Default Positive
Volatility:Evaporation Temp in°C for ASTM D 1837 °C 0.0
95%v at760mm
# of Samples in Unit: 1
# of Analytes in Unit: 5

Page 55 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

519-ATF Merox
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
519-SN-002 ATF After Prewash 18/09/2023 2:00 Acidity Total IS 1448:P 113 mg 0.0150 0.003
KOH/g
519-SN-001 ATF Feed to 18/09/2023 6:00 Acidity Total IS 1448:P 113 mg 0.015 1.5 0.0300
Prewash KOH/g
Density at 15°C ASTM D 4052 kg/m³ 783 789.1
Initial Boling Point IS 1448:P 18 °C 158.4
Temperature at 5% Volume IS 1448:P 18 °C 165.0
Recovery
Temperature at 10% Volume IS 1448:P 18 °C 166.9
Recovery
Temperature at 30% Volume IS 1448:P 18 °C 171.8
Recovery
Temperature at 50% Volume IS 1448:P 18 °C 179.4
Recovery
Temperature at 70% Volume IS 1448:P 18 °C 188.8
Recovery
Temperature at 90% Volume IS 1448:P 18 °C 211.6
Recovery
Temperature at 95% Volume IS 1448:P 18 °C 227.2
Recovery
Final Boiling Point IS 1448:P 18 °C 247.2 233.1
Flash Point, Abel IS 1448:P 20 °C 40 46.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.249
Color -Saybolt ASTM D 156 20 28
Doctor Test IS 1448:P 19 Negative
Sulphur Mercaptan IS 1448:P 109 ppm(w) 350 208
519-SN-008 ATF After Clay 18/09/2023 6:00 Acidity Total IS 1448:P 113 mg 0.015 0.0020
Filter KOH/g
Density at 15°C IS 1448:P 16 kg/m³ 783 788.9

Page 56 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

519-ATF Merox
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
519-SN-008 ATF After Clay 18/09/2023 6:00 Freezing Point IS 1448:P 11 °C -60 -62.4
Filter
Mercaptan Sulfur IS 1448:P 109 ppm(w) 18 20.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.253
Color -Saybolt ASTM D 156 16 17
Copper Strip Corrosion for 2 hrs @ IS 1448:P 15 1a
100°C
Doctor Test ASTM D 4952 Negative
Silver Strip Corrosion for 4hrs @ IP 227 0
50°C
Interface Rating IS 1448:P 42 1b
519-SN-001 ATF Feed to 18/09/2023 14:00 Density at 15°C ASTM D 4052 kg/m³ 783 788.3
Prewash
Flash Point, Abel IS 1448:P 20 °C 40 45.5
Total Sulphur ASTM D 4294 Wt% 0.25 0.227
Color -Saybolt ASTM D 156 +28
Doctor Test IS 1448:P 19 Negative
Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
50°C
519-SN-008 ATF After Clay 18/09/2023 14:00 Acidity Total IS 1448:P 113 mg 0.015 0.0014
Filter KOH/g
Density at 15°C IS 1448:P 16 kg/m³ 783 788.0
Mercaptan Sulfur IS 1448:P 109 ppm(w) 18 20.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.239
Color -Saybolt ASTM D 156 16 18
Copper Strip Corrosion for 2 hrs @ IS 1448:P 15 1a
100°C
Doctor Test ASTM D 4952 Negative

Page 57 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

519-ATF Merox
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
519-SN-008 ATF After Clay 18/09/2023 14:00 Silver Strip Corrosion for 4hrs @ IP 227 0
Filter 50°C
519-SN-001 ATF Feed to 18/09/2023 22:00 Density at 15°C ASTM D 4052 kg/m³ 783 788.6
Prewash
Flash Point, Abel IS 1448:P 20 °C 40 45.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.232
Color -Saybolt ASTM D 156 +26
Doctor Test IS 1448:P 19 Negative
Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 3a
50°C
519-SN-008 ATF After Clay 18/09/2023 22:00 Acidity Total IS 1448:P 113 mg 0.015 0.0016
Filter KOH/g
Density at 15°C IS 1448:P 16 kg/m³ 783 788.0
Mercaptan Sulfur IS 1448:P 109 ppm(w) 18 22.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.234
Color -Saybolt ASTM D 156 16 18
Copper Strip Corrosion for 2 hrs @ IS 1448:P 15 1a
100°C
Doctor Test ASTM D 4952 Negative
Silver Strip Corrosion for 4hrs @ IP 227 0
50°C
519-SN-012 3 Be Caustic 18/09/2023 22:00 % strength UOP 209 % wt 3.5
storage Drum
# of Samples in Unit: 10
# of Analytes in Unit: 56

Page 58 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

520-SWU-I
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
520-SC-1101 Sour water 18/09/2023 6:00 Ammonia IS 3025:P 34 ppm 930 376.00
Chloride IS 3025:P 32 ppm 100 5.6
H2S IS 3025:P 29 ppm 1300 436.0
Iron Content ASTM D 1068 ppm(w) 1.66
TSS IS 3025:P 17 ppm(v) 100 34
pH IS 3025:P 11 8 8.10
520-SC-1202 Stripped water 18/09/2023 22:00 Ammonia IS 3025:P 34 ppm 50 47.0
Chloride IS 3025:P 32 ppm 13.0
H2S IS 3025:P 29 ppm 50 6.3
TSS IS 3025:P 17 ppm 20 6
MDEA Concentration Default ND
pH IS 3025:P 11 7 9 9.3
# of Samples in Unit: 2
# of Analytes in Unit: 12

Page 59 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

521-SWU-II
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
521-SC-1202 Stripped water 18/09/2023 22:00 Ammonia IS 3025:P 34 ppm 50 19.40
Chloride IS 3025:P 32 ppm 100 15.9
H2S IS 3025:P 29 ppm 50 5.9
pH ASTM D 1293 5.5 9.2
# of Samples in Unit: 1
# of Analytes in Unit: 4

Page 60 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

522-ARU-I
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
522-E-105 Cooling water 18/09/2023 10:20 H2S IS 3025:P 29 ppm 291.0
return from lean
amine water cooler
522-E-205 522-E-205 18/09/2023 10:20 H2S IS 3025:P 29 ppm 270.0
522-SC-1501 Reflux amine 18/09/2023 14:00 Conductivity IS 3025:P 14 mS/cm 37.20
Iron Content ASTM D 1068 ppm 0.12
MDEA Concentration Default Wt% 0.5 0.06
522-SC-1601 Reflux amine 18/09/2023 14:00 Conductivity IS 3025:P 14 mS/cm 39.40
Iron Content ASTM D 1068 ppm(w) 0.10
MDEA Concentration Default Wt% 1 0.06
522-E-105 Cooling water 18/09/2023 17:30 H2S IS 3025:P 29 ppm 272.0
return from lean
amine water cooler
522-E-205 522-E-205 18/09/2023 17:30 H2S IS 3025:P 29 ppm 258.0
522-SC-1302 Lean Amine 18/09/2023 18:00 H2S IS 3025:P 29 ppm(w) 1500 211.0
TSS APHA 2540 C ppm 100 24
MDEA Concentration Default Wt% 38.0 40.4
# of Samples in Unit: 7
# of Analytes in Unit: 13

Page 61 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

524-SRU-I
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
524-SC-4501 Water 18/09/2023 14:00 Conductivity IS 3025:P 14 mS/cm 19.30
Iron Content N/A mg/l 0.14
MDEA Concentration Default Wt% 0.07
524-SC.H-4401 TGTU (Lean 18/09/2023 22:00 H2S IS 3025:P 29 ppm 233.0
Amine)
TSS IS 3025:P 17 ppm 30
MDEA Concentration Default Wt% 46.40
# of Samples in Unit: 2
# of Analytes in Unit: 6

Page 62 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

530-BBU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
530-SC-2903 Scrubber Wash 18/09/2023 6:00 pH IS 3025:P 11 8.4
Water
530-SC-2001. Reactor O/L 18/09/2023 11:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 213
530-SC-2001. Reactor O/L 18/09/2023 14:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 627
530-SC-2903 Scrubber Wash 18/09/2023 14:00 pH IS 3025:P 11 8.4
Water
530-SC-2001. Reactor O/L 18/09/2023 17:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 903
Penetration @ 25°C, 100g, 5Sec, IS 1203 mm 128.0
1/10mm
Softening Point (R & B) IS 1205 °C 42.3
Viscosity ratio at 60°C (Residue of IS 1206:P 2 3.8
RTFOT)
530-SC-2001. Reactor O/L 18/09/2023 20:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 1137
530-SC-2903 Scrubber Wash 18/09/2023 22:00 pH IS 3025:P 11 8.5
Water
530-SC-2001. Reactor O/L 18/09/2023 23:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 1839
Viscosity ratio at 60°C (Residue of IS 1206:P 2 4.6
RTFOT)
530-SC-2001. Reactor O/L 19/09/2023 1:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 2882
530-SC-2001. Reactor O/L 19/09/2023 4:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 4064

# of Samples in Unit: 10
# of Analytes in Unit: 14

Page 63 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

551-Crude Tanks
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
CRT Line 551-Crude Oil 18/09/2023 1:00 BS&W ASTM D 4007 Vol % 0.10 451750282
Tanks
Density at 15°C ASTM D 1298 kg/m3 881.0
CRT Line 551-Crude Oil 18/09/2023 9:00 BS&W ASTM D 4007 Vol % 0.10
Tanks
Density at 15°C ASTM D 1298 kg/m3 881.3 B. No.
451750282
CRT Line 551-Crude Oil 18/09/2023 17:00 BS&W ASTM D 4007 Vol % 0.10
Tanks
Density at 15°C ASTM D 1298 kg/m3 882.9 B.NO.
451761256
CRT Line 551-Crude Oil 19/09/2023 1:00 BS&W ASTM D 4007 Vol % 0.10
Tanks
Density at 15°C ASTM D 1298 kg/m3 882.7 451761256
# of Samples in Unit: 4
# of Analytes in Unit: 8

Page 64 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

552-Intermediate Tanks
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
552-T-04A 552-NHT Feed 18/09/2023 0:30 Density at 15°C ASTM D 4052 kg/m³ 670 720 696.0
Initial Boling Point ASTM D 86 °C 35.4
Temperature at 5% Volume ASTM D 86 °C 51.2
Recovery
Temperature at 10% Volume ASTM D 86 °C 56.6
Recovery
Temperature at 30% Volume ASTM D 86 °C 74.1
Recovery
Temperature at 50% Volume ASTM D 86 °C 95.5
Recovery
Temperature at 70% Volume ASTM D 86 °C 119.6
Recovery
Temperature at 90% Volume ASTM D 86 °C 140.1
Recovery
Temperature at 95% Volume ASTM D 86 °C 147.9
Recovery
Final Boiling Point ASTM D 86 °C 155.5
Mercaptan Sulfur ASTM D 3227 ppm(w) 92.00
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 61.6
Total Sulphur ASTM D 4294 ppm(w) 199
Color -Saybolt Visual 28
Aromatics ASTM D 5443 Vol % 5.88
i-Paraffin ASTM D 5443 Vol % 36.05
n Paraffin ASTM D 5443 Vol % 41.07
Naphthenes ASTM D 5443 Vol % 16.30
Olefines ASTM D 5443 Vol % 0.69
Paraffins ASTM D 5443 Vol % 77.12
Total Oxyganates UOP 960 ppm(w) 18.00

Page 65 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

552-Intermediate Tanks
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
552-T-04A 552-NHT Feed 18/09/2023 0:30 CS2 ASTM D 5623 ppm(w) 2.0
# of Samples in Unit: 2
# of Analytes in Unit: 22

Page 66 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

553-LPG Spheres
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
553-MB-01F LPG Storage 18/09/2023 6:00 Ethane ASTM D 2163 Vol % 1.04
Bullet
Propane ASTM D 2163 Vol % 23.61
Propylene ASTM D 2163 Vol % 2.74
Iso Butane ASTM D 2163 Vol % 14.34
N Butane ASTM D 2163 Vol % 12.76
trans-2-Butene ASTM D 2163 Vol % 9.93
1-Butene ASTM D 2163 Vol % 8.94
Iso Butylene ASTM D 2163 Vol % 18.16
cis-2-Butene ASTM D 2163 Vol % 7.33
Iso Pentane ASTM D 2163 Vol % 0.42
n-Pentane ASTM D 2163 Vol % 0.07
1,3 Butadiene ASTM D 2163 Vol % 0.24
Trance-2-Pentene ASTM D 2163 Vol % 0.35
2 Methyl 2 Butene ASTM D 2163 Vol % 0.02
1 Pentene ASTM D 2163 Vol % 0.03
C5 Hydrocarbons and Heavier ASTM D 2163 Vol % 0.89
COS ASTM D 2163 ppm(v) <0.02
Ethyle Mercapton ASTM D 2163 ppm <0.5
Moisture ASTM D 2163 ppm(v) 38.0
Total Volatile Sulphur ASTM D 3246 ppm(w) 10
Hydrogen Sulfide ASTM D 2420 Pass
# of Samples in Unit: 1
# of Analytes in Unit: 21

Page 67 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

558-ETP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
558-SC-0101 Spent caustic 18/09/2023 6:00 Sulphide IS 3025:P 29 ppm 25000 106.0
storage tank I/L
558-SC-0102 Treated Spent 18/09/2023 6:00 Sulphide IS 3025:P 29 ppm 20 16.0
Caustic
558-SC-0105 OWS SUMP 18/09/2023 6:00 Free Oil Visual Vol % 1.2 SLUDGE
OIL
PRESENT
558-SC-0106 Desalter Inlet 18/09/2023 6:00 Free Oil Visual Vol % 1.5 SLUGDE
OIL
PRESENT
558-SC-0107 Sour Water 18/09/2023 6:00 Alkalinity APHA 2320 D ppm 63.00
COD APHA 5220 C ppm 288
Nitrates APHA 4500 ppm 62.2
NO3-
Sulphide IS 3025:P 29 ppm 5.2
TDS IS 3025:P 16 ppm 85
pH IS 3025:P 11 9.2
558-SC-0201 API I/L 18/09/2023 6:00 Free Oil Visual Vol % 0.9 SLUDGE
OIL
PRESENT
558-SC-0202 TPI I/L 18/09/2023 6:00 Free Oil Visual Vol % NO FREE
OIL
PRESENT
TSS IS 3025:P 17 ppm 25 54
558-SC-0203 Outlet of TPI I/L of 18/09/2023 6:00 Oil & Grease IS 3025:P 39 ppm 4 525 <4
DAF super cell
TSS IS 3025:P 17 ppm 20 39
558-SC-0204 DAF outlet A 18/09/2023 6:00 Oil & Grease IS 3025:P 39 ppm 4 10 <4
TSS IS 3025:P 17 ppm 10 20

Page 68 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

558-ETP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
558-SC-0205 DAF outlet-B 18/09/2023 6:00 Oil & Grease IS 3025:P 39 ppm 4 10 <4
TSS IS 3025:P 17 ppm 10 16
558-SC-0206 SBR I/L 18/09/2023 6:00 Alkalinity IS 3025:P 23 ppm 65.00
Ammonia IS 3025:P 34 ppm 50 49.00
BOD(3days at 27° C) IS 3025:P 44 ppm 600 37 15/09/2023
COD APHA 5220 C ppm 1000 247
Nitrite Default ppm 57
Ortho phosphate APHA 4500 P ppm 25.00
Phenol APHA 5530 C ppm 100 6.000
Sulphide IS 3025:P 29 ppm 50 6.70
TSS APHA 2540 C ppm 20 36
pH IS 3025:P 11 7 8 7.2
558-SC-0301 MBR Inlet 18/09/2023 6:00 Alkalinity APHA 2320 D ppm 54.00
Ammonia IS 3025:P 34 ppm 40 46.00
COD APHA 5220 C ppm 500 165
Sulphide IS 3025:P 29 ppm 6
TSS IS 3025:P 17 ppm 30 40
pH IS 3025:P 11 7 8 7.0
558-SC-0302 Treated Effluent 18/09/2023 6:00 Alkalinity IS 3025:P 23 mg/l 83.0
Pump Discharge
Ammonia IS 3025:P 34 mg/l 1.65
BOD(3days at 27° C) IS 3025:P 44 mg/l 5.0 15/09/2023
COD APHA 5220 C mg/l 45.0
Conductivity IS 3025:P 14 uS/cm 775.00
Oil & Grease IS 3025:P 39 mg/l <4

Page 69 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

558-ETP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
558-SC-0302 Treated Effluent 18/09/2023 6:00 Phenol APHA 5530 C mg/l <0.1
Pump Discharge
Phosphate APHA 4500 mg/l <0.5
P.D
Sulphide IS 3025:P 29 mg/l <0.5
TDS APHA 2540 D mg/l 503.0
TSS IS 3025:P 17 mg/l 5.0
pH IS 3025:P 11 7.2
558-SC-0803 CRW System DMF 18/09/2023 6:00 COD APHA 5220 C mg/l 62
Outlet
Oil & Grease IS 3025:P 39 mg/l 4 <4
Sulphide IS 3025:P 29 mg/l <0.5
TDS APHA 2540 D mg/l 524
TSS APHA 2540 C mg/l 15
pH ASTM D 1293 7.4
558-SC-0804 Strom Pond A 18/09/2023 10:00 Alkalinity ASTM D 1067 ppm 52.00
COD APHA 5220 C ppm 74
Oil & Grease IS 3025:P 39 ppm 4 <4
Sulphide IS 3025:P 29 ppm 1.1
TDS IS 3025:P 16 ppm 806
pH IS 3025:P 11 9.1
558-SC-0805 Strom Water 18/09/2023 10:00 Alkalinity ASTM D 1067 ppm 54.00
Pond B
COD APHA 5220 C ppm 82
Oil & Grease IS 3025:P 39 ppm 4 <4
Sulphide IS 3025:P 29 ppm 1.2
TDS IS 3025:P 16 ppm 794
pH IS 3025:P 11 9.2
Page 70 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

558-ETP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
558-SC-0102 Treated Spent 18/09/2023 14:00 Sulphide IS 3025:P 29 ppm 20 22.0
Caustic
558-SC-0102 Treated Spent 18/09/2023 22:00 Sulphide IS 3025:P 29 ppm 20 23.0
Caustic
558-SC-0107 Sour Water 18/09/2023 22:00 Ammonia IS 3025:P 34 ppm 46.00

# of Samples in Unit: 19
# of Analytes in Unit: 68

Page 71 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

561-Process Blending
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
561-SC-1401 MS-VI Blending 18/09/2023 2:00 Doctor Test ASTM D 4952 Negative
(BS VI) station
561-SC-1901 HSD-VI Blending 18/09/2023 2:00 Cetane Number ASTM D 613 No 51.5 50.90
(BS VI) Station
Total Sulphur ASTM D 5453 mg/kg 10 8.0
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 18/09/2023 6:00 Benzene Content ASTM D 3606 Vol % 0.95 0.84
(BS VI) station
Aromatics ASTM D 1319 Vol % 35.0 29.8
Olefines ASTM D 1319 Vol % 12.1
Saturates ASTM D 1319 Vol % 58.1
Copper Strip Corrosion for 3 hrs @ ASTM D 130 1b
50°C
Density at 15°C ASTM D 4052 kg/m³ 741.6
Initial Boling Point ASTM D 86 °C 34.3
Final Boiling Point ASTM D 86 °C 195 193.9
Recovery up to 70°C (E70) ASTM D 86 Vol % 10 45 34.9
Recovery up to 100°C (E100) ASTM D 86 Vol % 40 70 54.1
Recovery up to 150°C (E150) ASTM D 86 Vol % 75 84.8
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 58 58.4
Total Sulphur ASTM D 5453 mg/kg 10 7.0
Doctor Test ASTM D 4952 Negative
Research Octane Number (RON) ASTM D 2699 92.0 91.8
561-SC-1901 HSD-VI Blending 18/09/2023 6:00 Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
(BS VI) Station 50°C
Density at 15°C ASTM D 4052 kg/m³ 829.4
Initial Boling Point ASTM D 86 °C 120.6

Page 72 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

561-Process Blending
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
561-SC-1901 HSD-VI Blending 18/09/2023 6:00 Temperature at 95% Volume ASTM D 86 °C 360 348.7
(BS VI) Station Recovery
Final Boiling Point ASTM D 86 °C 364.2
Flash Point, Abel IS 1448:P 20 °C 37 37.0
Total Sulphur ASTM D 5453 mg/kg 10 8.0
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 18/09/2023 10:00 Doctor Test ASTM D 4952 Negative
(BS VI) station
561-SC-1901 HSD-VI Blending 18/09/2023 10:00 Total Sulphur ASTM D 5453 mg/kg 10 7.5
(BS VI) Station
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 18/09/2023 14:00 Benzene Content ASTM D 3606 Vol % 0.95 0.85
(BS VI) station
Copper Strip Corrosion for 3 hrs @ ASTM D 130 1b
50°C
Density at 15°C ASTM D 4052 kg/m³ 742.8
Initial Boling Point ASTM D 86 °C 33.9
Final Boiling Point ASTM D 86 °C 195 196.2
Recovery up to 70°C (E70) ASTM D 86 Vol % 10 45 34.0
Recovery up to 100°C (E100) ASTM D 86 Vol % 40 70 54.3
Recovery up to 150°C (E150) ASTM D 86 Vol % 75 86.5
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 58 55.9
Total Sulphur ASTM D 5453 mg/kg 10 7.0
Doctor Test ASTM D 4952 Negative
561-SC-1901 HSD-VI Blending 18/09/2023 14:00 Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
(BS VI) Station 50°C
Density at 15°C ASTM D 4052 kg/m³ 829.9
Initial Boling Point ASTM D 86 °C 120.6

Page 73 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

561-Process Blending
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
561-SC-1901 HSD-VI Blending 18/09/2023 14:00 Temperature at 95% Volume ASTM D 86 °C 360 355.3
(BS VI) Station Recovery
Final Boiling Point ASTM D 86 °C 364.7
Flash Point, Abel IS 1448:P 20 °C 37 37.0
Total Sulphur ASTM D 5453 mg/kg 10 7.5
Cetane Index ASTM D 4737 52.5
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 18/09/2023 18:00 Doctor Test ASTM D 4952 Negative
(BS VI) station
561-SC-1901 HSD-VI Blending 18/09/2023 18:00 Total Sulphur ASTM D 5453 mg/kg 10 7.5
(BS VI) Station
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 18/09/2023 22:00 Benzene Content ASTM D 3606 Vol % 0.95 0.84
(BS VI) station
Copper Strip Corrosion for 3 hrs @ ASTM D 130 1b
50°C
Density at 15°C ASTM D 4052 kg/m³ 742.4
Initial Boling Point ASTM D 86 °C 34.6
Final Boiling Point ASTM D 86 °C 195 194.2
Recovery up to 70°C (E70) ASTM D 86 Vol % 10 45 36.1
Recovery up to 100°C (E100) ASTM D 86 Vol % 40 70 55.8
Recovery up to 150°C (E150) ASTM D 86 Vol % 75 86.7
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 58 56.2
Total Sulphur ASTM D 5453 mg/kg 10 6.5
Doctor Test ASTM D 4952 Negative
561-SC-1901 HSD-VI Blending 18/09/2023 22:00 Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
(BS VI) Station 50°C
Density at 15°C ASTM D 4052 kg/m³ 829.8

Page 74 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

561-Process Blending
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
561-SC-1901 HSD-VI Blending 18/09/2023 22:00 Initial Boling Point ASTM D 86 °C 121.9
(BS VI) Station
Temperature at 95% Volume ASTM D 86 °C 360 354.4
Recovery
Final Boiling Point ASTM D 86 °C 364.5
Flash Point, Abel IS 1448:P 20 °C 37 36.0
Total Sulphur ASTM D 5453 mg/kg 10 8.0
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 19/09/2023 2:00 Doctor Test ASTM D 4952 Negative
(BS VI) station
561-SC-1901 HSD-VI Blending 19/09/2023 2:00 Total Sulphur ASTM D 5453 mg/kg 10 7.5
(BS VI) Station
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 19/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 10 6.5
(BS VI) station
561-SC-1901 HSD-VI Blending 19/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 10 7.0
(BS VI) Station
# of Samples in Unit: 16
# of Analytes in Unit: 77

Page 75 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

562-Under Ground
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
562-V-03 UG Class-B Road 18/09/2023 14:00 Density at 15°C IP 432 -2000 kg/m³ 796.1 Composite
Initial Boling Point IS 1448:P 18 °C 160.1
Temperature at 5% Volume IS 1448:P 18 °C 169.5
Recovery
Temperature at 10% Volume IS 1448:P 18 °C 170.6
Recovery
Temperature at 30% Volume IS 1448:P 18 °C 176.3
Recovery
Temperature at 50% Volume IS 1448:P 18 °C 183.3
Recovery
Temperature at 70% Volume IS 1448:P 18 °C 196.0
Recovery
Temperature at 90% Volume IS 1448:P 18 °C 241.9
Recovery
Temperature at 95% Volume IS 1448:P 18 °C 295.6
Recovery
Final Boiling Point IS 1448:P 18 °C 329.1
Flash Point, Abel IS 1448:P 21 °C 44.0
Total Sulphur ISO 8754 ppm 1700.00
ASTM Colour ASTM D 1500 0.5
Flash Point, Abel IS 1448:P 21 °C 44.0 Skim Top
# of Samples in Unit: 2
# of Analytes in Unit: 14

Page 76 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

575-CPP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
575-SC-4221 Fuel Gas 18/09/2023 10:00 Hydrogen UOP 539 Vol % 5.25
Methane UOP 539 Vol % 38.006 73.87
Ethane UOP 539 Vol % 16.483 7.45
Ethylene UOP 539 Vol % 19.889 9.04
Propane UOP 539 Vol % 0.435 0.68
Propylene UOP 539 Vol % 1.664 0.26
Iso Butane UOP 539 Vol % 0.026 0.15
N Butane UOP 539 Vol % 0.1 0.46
C4 Unsaturated UOP 539 Vol % 0.18
Iso Pentane UOP 539 Vol % 0.04
n-Pentane UOP 539 Vol % 0.03
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 0.07
Oxygen UOP 539 Vol % 0.04
Nitrogen UOP 539 Vol % 2.42
Carbon Monoxide UOP 539 Vol % 0.05
Gross Calorific Value ASTM D 3588 Kcal/kg 12518.00
Net Calorific Value ASTM D 3588 Kcal/kg 11357.00
Hydrogen Sulfide Dragger Vol % 0.0006
Molecular Weight Default 18.42 21.42 18.40
575-Special 575-Special 18/09/2023 10:30 Iron Content ASTM D 1068 mg/l 0.35 EP #2 ,HWB
Sample Sample
575-SC-17UB62 CBD (Drum Water) 18/09/2023 11:20 Iron Content ASTM D 1068 ppm(w) 0.30

Page 77 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

575-CPP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
# of Samples in Unit: 3
# of Analytes in Unit: 22

Page 78 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

576-CPU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
576 SC-0103 Surface 18/09/2023 22:00 Silica ASTM D 859 ppm <0.02
Condansate
TOC ASTM D 5310 ppm 0.1
576-SC-0201 Unpolished 18/09/2023 22:00 Conductivity IS 3025:P 14 µS/cm 1.42
Condansate
Oil & Grease IS 3025:P 39 ppm 10 <0.5
Pump Discharge
Silica ASTM D 859 ppm 0.185 <0.02
TOC ASTM D 5310 ppm 0.4
TSS IS 3025:P 17 ppm 1
Turbidity IS 3025:P 10 NTU 0 3.5 <1
pH IS 3025:P 11 7.5 9.5 9.4
576-SC-0202 OIL COALASCER 18/09/2023 22:00 Oil & Grease ASTM D 3921 ppm 1 <0.5
COMMON
TOC ASTM D 5310 ppm 0.3
OUTLET
576-SC-0203 Unpolished 18/09/2023 22:00 Oil & Grease IS 3025:P 39 ppm <0.5
Condansate Tank
Common O/L
576-SC-0301 Primery ACF 18/09/2023 22:00 TOC ASTM D 5310 ppm 0.1
common O/L
576-SC-0302 Secondary ACF 18/09/2023 22:00 TOC APHA 5310 D ppm 0.1
common O/L
576-SC-0401 MB (CPU) - A O/L 18/09/2023 22:00 Conductivity IS 3025:P 14 µS/cm 0.2 1.03
Silica ASTM D 859 ppm 0.01 <0.02
pH IS 3025:P 11 6.0 7.4 9.3
576-SC-0402 MB (CPU) - B O/L 18/09/2023 22:00 Conductivity ASTM D 1125 µS/cm 0.2 0.08
Silica ASTM D 859 ppm 0.01 <0.02
pH IS 3025:P 11 6 7.4 7.1
576-SC-0403 MB (CPU) - C O/L 18/09/2023 22:00 Conductivity IS 3025:P 14 µS/cm 0.2 0.07

Page 79 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

576-CPU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
576-SC-0403 MB (CPU) - C O/L 18/09/2023 22:00 Silica ASTM D 859 ppm 0.01 <0.02
pH IS 3025:P 11 6 7.4 6.7
576-SC-0406 Polished 18/09/2023 22:00 Conductivity ASTM D 1125 µS/cm 3.5 0.54
Condensate Pump
Silica ASTM D 859 ppm 0.01 <0.02
Discharge
TOC ASTM D 5310 ppm 1 0.1
Turbidity ASTM D 6855 NTU 1
pH Vendor 7.5 9.5 8.3
Method
576-SC-CMO CPU MB Outlet 18/09/2023 22:00 Conductivity ASTM D 1125 µS/cm <5 0.06
Silica ASTM D 859 ppm 18 <0.02
pH IS 3025:P 11 7.0 9.0 6.8
576-SC-CMO-1 MB Common 18/09/2023 22:00 Conductivity IS 3025:P 14 µS/cm 0.07
Outlet
TOC ASTM D 5310 ppm 0.1
(CPU)-Before
Morpholine pH Vendor 6.5
Method
# of Samples in Unit: 12
# of Analytes in Unit: 34

Page 80 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

577-RODM
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
577-SC-0303 Ecological pond 18/09/2023 22:00 Conductivity ASTM D 1125 µS/cm 4880.0
TSS IS 3025:P 17 ppm 20 17
pH IS 3025:P 11 6.0 8.5 10.0
577-SC-0802 HRU-2 O/L 18/09/2023 22:00 Alkalinity IS 3025:P 23 ppm ND
Total Hardness IS 3025:P 21 ppm ND
577-SC-0901 Degasser outlet to 18/09/2023 22:00 Alkalinity ASTM D 1067 ND
RO-I feed tank
outlet
577-SC-1301 MB Feed Tank 18/09/2023 22:00 TDS IS 3025:P 16 ppm 15 3
Outlet
TOC ASTM D 5310 ppm 0.1
577-SC-1503 DM Water pump 18/09/2023 22:00 Conductivity IS 3025:P 14 µS/cm 0.2 0.20
discharge
Iron Content ASTM D 1068 ppm 0.01 <0.02
Silica ASTM D 859 ppm 0.01 <0.02
TOC ASTM D 5310 ppm 0.6 0.1
pH IS 3025:P 11 6.7 7.3 6.7
# of Samples in Unit: 5
# of Analytes in Unit: 13

Page 81 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

578-RWTP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
578-SC-0210 RGSF Common 18/09/2023 22:00 TSS IS 3025:P 17 mg/l 1 2
Outlet
578-SC-0402 Drinking water 18/09/2023 22:00 Iron Content ASTM D 1068 ppm(w) 0.1 <0.02
pump discharge
TSS IS 3025:P 17 mg/l 1 1
Turbidity IS 3025:P 10 NTU 1 <1
pH IS 3025:P 11 7 8 7.3
# of Samples in Unit: 2
# of Analytes in Unit: 5

Page 82 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

589 OFF SITE

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
589-SC-1701 OFFSITE FLARE 18/09/2023 2:00 Methane UOP 539 Vol % 8.92
HEADER
Ethane UOP 539 Vol % 0.67
Ethylene UOP 539 Vol % 0.47
Propane UOP 539 Vol % 0.46
Propylene UOP 539 Vol % 1.57
Iso Butane UOP 539 Vol % 0.14
N Butane UOP 539 Vol % 0.17
C4 Unsaturated UOP 539 Vol % 0.2
Iso Pentane UOP 539 Vol % 0.07
n-Pentane UOP 539 Vol % 0.04
C6+ heaviers UOP 539 Vol % 0.03
Carbon Dioxide UOP 539 Vol % 1.35
Oxygen UOP 539 Vol % 2.73
Nitrogen UOP 539 Vol % 25.22
Carbon Monoxide UOP 539 Vol % 0.12
Hydrogen UOP 539 Vol % 57.82
Hydrogen Sulfide UOP 539 Vol % 1.0000 0.0020
Total Hydrocarbon UOP 539 Vol % 12.76
Molecular Weight UOP 539 12.77
Net Calorific Value UOP 539 Kcal/kg 5347.00
Gross Calorific Value UOP 539 Kcal/kg 6083.00
589-SC-1701 OFFSITE FLARE 18/09/2023 9:00 Methane UOP 539 Vol % 7.52
HEADER
Ethane UOP 539 Vol % 0.57
Ethylene UOP 539 Vol % 0.41

Page 83 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

589 OFF SITE

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
589-SC-1701 OFFSITE FLARE 18/09/2023 9:00 Propane UOP 539 Vol % 0.54
HEADER
Propylene UOP 539 Vol % 2.31
Iso Butane UOP 539 Vol % 0.22
N Butane UOP 539 Vol % 0.19
C4 Unsaturated UOP 539 Vol % 1.4
Iso Pentane UOP 539 Vol % 0.99
n-Pentane UOP 539 Vol % 0.50
C6+ heaviers UOP 539 Vol % 0.03
Carbon Dioxide UOP 539 Vol % 1.39
Oxygen UOP 539 Vol % 2.81
Nitrogen UOP 539 Vol % 25.97
Carbon Monoxide UOP 539 Vol % 0.16
Hydrogen UOP 539 Vol % 55.03
Hydrogen Sulfide UOP 539 Vol % 1.0000 0.0060
Total Hydrocarbon UOP 539 Vol % 14.64
Molecular Weight UOP 539 14.74
Net Calorific Value UOP 539 Kcal/kg 5804.00
Gross Calorific Value UOP 539 Kcal/kg 6512.00
589-SC-1701 OFFSITE FLARE 18/09/2023 19:00 Methane UOP 539 Vol % 8.57
HEADER
Ethane UOP 539 Vol % 0.58
Ethylene UOP 539 Vol % 0.43
Propane UOP 539 Vol % 0.58
Propylene UOP 539 Vol % 2.41
Iso Butane UOP 539 Vol % 0.25

Page 84 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

589 OFF SITE

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
589-SC-1701 OFFSITE FLARE 18/09/2023 19:00 N Butane UOP 539 Vol % 0.20
HEADER
C4 Unsaturated UOP 539 Vol % 0.6
Iso Pentane UOP 539 Vol % 0.09
n-Pentane UOP 539 Vol % 0.05
C6+ heaviers UOP 539 Vol % 0.06
Carbon Dioxide UOP 539 Vol % 2.01
Oxygen UOP 539 Vol % 4.81
Nitrogen UOP 539 Vol % 30.72
Carbon Monoxide UOP 539 Vol % 0.51
Hydrogen UOP 539 Vol % 48.17
Hydrogen Sulfide UOP 539 Vol % 1.0000 0.0200
Total Hydrocarbon UOP 539 Vol % 13.78
Molecular Weight UOP 539 15.81
Net Calorific Value UOP 539 Kcal/kg 4413.00
Gross Calorific Value UOP 539 Kcal/kg 4972.00
589-SC-1701 OFFSITE FLARE 19/09/2023 0:00 Methane UOP 539 Vol % 9.07
HEADER
Ethane UOP 539 Vol % 0.64
Ethylene UOP 539 Vol % 0.46
Propane UOP 539 Vol % 0.57
Propylene UOP 539 Vol % 2.29
Iso Butane UOP 539 Vol % 0.22
N Butane UOP 539 Vol % 0.20
C4 Unsaturated UOP 539 Vol % 0.5
Iso Pentane UOP 539 Vol % 0.11

Page 85 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

589 OFF SITE

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
589-SC-1701 OFFSITE FLARE 19/09/2023 0:00 n-Pentane UOP 539 Vol % 0.04
HEADER
C6+ heaviers UOP 539 Vol % 0.03
Carbon Dioxide UOP 539 Vol % 1.42
Oxygen UOP 539 Vol % 2.00
Nitrogen UOP 539 Vol % 23.05
Carbon Monoxide UOP 539 Vol % 0.26
Hydrogen UOP 539 Vol % 59.14
Hydrogen Sulfide UOP 539 Vol % 1.0000 0.0150
Total Hydrocarbon UOP 539 Vol % 14.13
Molecular Weight UOP 539 12.64
Net Calorific Value UOP 539 Kcal/kg 6002.00
Gross Calorific Value UOP 539 Kcal/kg 6796.00
# of Samples in Unit: 4
# of Analytes in Unit: 84

Page 86 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

607-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
607-SC3-1601 Combined Hot 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 859 844.3
Feed (FSD outlet)
607-SC3-3001 Stripper bottom 18/09/2023 6:00 Doctor Test ASTM D 4952 Negative FREE
Diesel WATER
PRESENT
607-SC5-4901 Naphtha Product 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 770 718.6
Initial Boling Point IS 1448:P 18 °C 33.9
Temperature at 5% Volume IS 1448:P 18 °C 51.7
Recovery
Temperature at 10% Volume IS 1448:P 18 °C 58.4
Recovery
Temperature at 30% Volume IS 1448:P 18 °C 79.7
Recovery
Temperature at 50% Volume IS 1448:P 18 °C 100.3
Recovery
Temperature at 70% Volume IS 1448:P 18 °C 123.2
Recovery
Temperature at 90% Volume IS 1448:P 18 °C 149.5
Recovery
Temperature at 95% Volume IS 1448:P 18 °C 159.5
Recovery
Final Boiling Point IS 1448:P 18 °C 177.5
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 50 54.2
Total Sulphur ASTM D 5453 mg/kg 4 0.5
607-SC6-4101 Diesel product 18/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 820 859 828.9
Initial Boling Point IS 1448:P 18 °C 160.3
Temperature at 5% Volume IS 1448:P 18 °C 192.5
Recovery
Temperature at 10% Volume IS 1448:P 18 °C 207.3
Recovery
Page 87 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

607-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
607-SC6-4101 Diesel product 18/09/2023 6:00 Temperature at 30% Volume IS 1448:P 18 °C 241.3
Recovery
Temperature at 50% Volume IS 1448:P 18 °C 271.4
Recovery
Temperature at 70% Volume IS 1448:P 18 °C 301.4
Recovery
Temperature at 90% Volume IS 1448:P 18 °C 339.6
Recovery
Temperature at 95% Volume IS 1448:P 18 °C 360 354.9
Recovery
Final Boiling Point IS 1448:P 18 °C 367.0
Total Sulphur ASTM D 5453 mg/kg 8 5.0
607-SC4-3601 Treated Fuel Gas 18/09/2023 14:00 H2S DRAEGER Vol % 20 0.0006
TUBE
607-SC6-4101 Diesel product 18/09/2023 14:00 Total Sulphur ASTM D 5453 mg/kg 8 4.5
607-SC6-4101 Diesel product 18/09/2023 22:00 Total Sulphur ASTM D 5453 mg/kg 8 6.5
607-SC6-4101 Diesel product 19/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 8 4.5

# of Samples in Unit: 8
# of Analytes in Unit: 29

Page 88 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

912-ROG
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
912-S-21302 DGA Samples 18/09/2023 10:00 Ammonia IS 3025:P 34 mg/l 23654.000
Conductivity IS 3025:P 14 mS/cm 144.50
Iron Content APHA 3500 D ppm(w) 0.26
Oil Content Default mg/l <4
912-S-21602 DGA Samples 18/09/2023 10:00 CO2 Vendor wt.% ND
Method
H2S Default ppm(w) 164.000
Heat Stable Salt Vendor wt.% <0.01
Method
TSS IS 3025:P 17 mg/l 28.00
DGA Strength Vendor's wt.% 41.500
Method
# of Samples in Unit: 2
# of Analytes in Unit: 9

Page 89 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

917-ROG
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
917-CC-1102 Refinery Off Gas 18/09/2023 2:00 Hydrogen Sulfide UOP 539 ppm(v) <0.5
O/L
COS UOP 539 ppm(v) <0.5
Total Mercaptans ASTM D 6228 ppm vol. 4.30
Propyl Mercaptan ASTM D 6228 vol. ppm <0.5
Butyl Mercaptan ASTM D 6228 vol. ppm <0.5
Ethyl Mercaptan ASTM D 6228 vol. ppm 1.00
Methyl Mercaptan ASTM D 6228 vol. ppm 3.30
917-CC-1102 Refinery Off Gas 18/09/2023 10:00 Methane UOP 539 Vol % 36.53
O/L
Ethane UOP 539 Vol % 14.17
Ethylene UOP 539 Vol % 14.87
Propane UOP 539 Vol % 0.69
Propylene UOP 539 Vol % 0.75
Iso Butane UOP 539 Vol % 0.20
N Butane UOP 539 Vol % 1.03
C4 Unsaturated UOP 539 Vol % 0.56
Iso Pentane UOP 539 Vol % 0.10
n-Pentane UOP 539 Vol % 0.09
C5 Unsaturated UOP 539 Vol % 0.11
Carbon Dioxide UOP 539 Vol % <0.0050
Oxygen UOP 539 Vol % 0.08
Nitrogen UOP 539 Vol % 9.34
Carbon Monoxide UOP 539 Vol % 0.65
Hydrogen UOP 539 Vol % 20.78
Hydrogen Sulfide UOP 539 ppm(v) <0.5

Page 90 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

917-ROG
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
917-CC-1102 Refinery Off Gas 18/09/2023 10:00 Molecular Weight UOP 539 Default 19.42
O/L
Net Calorific Value UOP 539 Kcal/kg 10219
Gross Calorific Value UOP 539 Kcal/kg 11211
COS UOP 539 ppm(v) <0.5
Total Mercaptans ASTM D 6228 ppm vol. 2.00
Propyl Mercaptan ASTM D 6228 vol. ppm <0.5
Butyl Mercaptan ASTM D 6228 vol. ppm <0.5
Ethyl Mercaptan ASTM D 6228 vol. ppm <0.5
Methyl Mercaptan ASTM D 6228 vol. ppm <0.5
Special Sample Special Sample 18/09/2023 10:00 Oil Content Default ppm <4 PH-7.4,
917-S-11401
UCARSOL Strength Vendor's wt.% ND
Method
917-S-11201 Lean UCARSOL to 18/09/2023 17:00 CO2 Vendor wt. ppm 47 ND
Treater Method
H2S Default wt. ppm 26 34.0
UCARSOL Strength Vendor's % wt 75 70.20
Method
917-CC-1102 Refinery Off Gas 19/09/2023 0:00 Hydrogen Sulfide UOP 539 ppm(v) <0.5
O/L
COS UOP 539 ppm(v) <0.5
Total Mercaptans ASTM D 6228 ppm vol. <2
Propyl Mercaptan ASTM D 6228 vol. ppm <0.5
Butyl Mercaptan ASTM D 6228 vol. ppm <0.5
Ethyl Mercaptan ASTM D 6228 vol. ppm <0.5
Methyl Mercaptan ASTM D 6228 vol. ppm <0.5

Page 91 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

917-ROG
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
# of Samples in Unit: 5
# of Analytes in Unit: 45

Page 92 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
554-T-05D SUPERIOR 18/09/2023 1:30 Density at 15°C ASTM D 4052 kg/m3 788.3
KEROSENE
Initial Boling Point IS 1448:P 18 °C 160.2
(GRADE-A)-COQ
Temperature at 10% Volume IS 1448:P 18 °C 167.5
Recovery
Temperature at 20% Volume IS 1448:P 18 °C 168.9
Recovery
Temperature at 30% Volume IS 1448:P 18 °C 174.3
Recovery
Temperature at 50% Volume IS 1448:P 18 °C 181.3
Recovery
Temperature at 70% Volume IS 1448:P 18 °C 191.6
Recovery
Temperature at 90% Volume IS 1448:P 18 °C 212.3
Recovery
Temperature at 95% Volume IS 1448:P 18 °C 223.2
Recovery
Final Boiling Point IS 1448:P 18 °C 236.0
Residue IS 1448:P 18 Vol % 1.0
Percent Recovered below 200°C IS 1448:P 18 Vol % 80.0
Mercaptan Sulfur ASTM D 3227 mg/kg 98.00
Total Sulphur ASTM D 5453 ppm(w) 0.2
Appearance Visual Clear and
bright.Free
from
un-dissolve
d
water,foreig
n matter
and other
visible
impurities

Page 93 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
554-T-05D SUPERIOR 18/09/2023 1:30 Color -Saybolt IS 1448:P 14 +24
KEROSENE
554-T-04D MOTOR 18/09/2023 3:00 Aromatic Content IS 1448:P 23 Vol % 35 28.8
(GRADE-A)-COQ
GASOLINE
Benzene Content ASTM D 3606 Vol % 1 0.87
(BS-VI)-COQ
Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
50°C
Density at 15°C ISO 12185 kg/m3 720 775 742.0
Percent evaporated at 70°C (E 70°C) ASTM D 86 Vol % 10 45 35.8
Percent evaporated at 100°C (E ASTM D 86 Vol % 40 70 55.9
100°C)
Percent evaporated at 150°C (E ASTM D 86 Vol % 75 86.7
150°C)
Final Boiling Point ASTM D 86 °C 210 194.7
Residue ASTM D 86 Vol % 2 1.0
Lead Content (Pb) ASTM D 5059 g Pb/l 0.005 <0.005
Olefin Content IS 1448:P 23 Vol % 21 12.5
Oxidation Stability IS 1448:P 28 min 360 >360
Oxygen content ASTM D 4815 Wt% 3.7 0.13
Ether containing five or more C ASTM D 4815 Vol % 15 0.60
atoms per molecule
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 60 58.3
Total Sulphur ASTM D 5453 mg/kg 10 7.5

Page 94 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
554-T-04D MOTOR 18/09/2023 3:00 Appearance Visual Clear and
GASOLINE bright.Free
(BS-VI)-COQ from
un-dissolve
d
water,foreig
n matter
and other
visible
impurities
Engine intake system cleanliness IS 2796:Note MFA Used
5
Motor Octane Number (MON) ASTM D 2700 81 82.3
Research Octane Number (RON) ASTM D 2699 91 91.8
Vapour Lock Index (VLI) Calculation 950 833.6
Color Visual Orange
Gum Content (Solvent washed) IS 1448:P 29 g/m³ 40 12.0
513-S-710 H Poly Propylene 18/09/2023 4:00 Irg 1010 ASTM D 6247 ppm 380 520 480
I 168 ASTM D 6247 ppm 750 1050 850
DHT 4A ASTM D 6247 ppm 250 350 235
Small ( 0.20 to 0.49mm2) Default No/1520 30 28
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.10 H23I1085
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 1 Triplet
Fused Pellet Default no/5kg 1 12
Tails Default no/5kg 3 0

Page 95 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-710 H Poly Propylene 18/09/2023 4:00 Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 37
Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 4.00
Volatile Matter Licensor ppm 500 260
Method
Yellowness Index ASTM E 313 0 -3.74
562-T-08A HIGH SPEED 18/09/2023 5:25 Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
DIESEL 50°C
(BS-VI)-BFC Density at 15°C ASTM D 4052 kg/m³ 810 845 830.6
Temperature at 95% Volume IS 1448:P 18 °C 360 354.4
Recovery
Flash Point, Abel IS 1448:P 20 °C 35 37.0
Kinematic Viscosity @ 40°C IS 1448:P 25 cSt 2 4.5 2.430
Pour Point IS 1448:P 10 °C 15 -9
Total Sulphur ASTM D 5453 mg/kg 10 8.0
Appearance Visual Clear,bright,
and free
from
sediments,s
uspended
matter and
undissolved
water at
normal
ambient fuel
temperature
Cetane Index ASTM D 4737 46 52.0
513-S-710 C Poly Propylene 18/09/2023 10:00 Irg 1010 ASTM D 6247 ppm 380 520 405

Page 96 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-710 C Poly Propylene 18/09/2023 10:00 I 168 ASTM D 6247 ppm 750 1050 730
DHT 4A ASTM D 6247 ppm 250 350 215
Small ( 0.20 to 0.49mm2) Default No/1520 30 29
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.54
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 19
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 36
Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 3.76
Volatile Matter Licensor ppm 500 255
Method
Yellowness Index ASTM E 313 0 -4.21
562-T-05B SUPERIOR 18/09/2023 13:20 Flash Point, Abel IP 170 °C 35 44.5 Skim Top
KEROSENE
(GRADE-A)-BFC
562-T-05A SUPERIOR 18/09/2023 13:30 Flash Point, Abel IP 170 °C 35 45.0 Skim Top
KEROSENE
(GRADE-A)-BFC
513-S-710 G Poly Propylene 18/09/2023 15:00 Irg 1010 ASTM D 6247 ppm 380 520 400
I 168 ASTM D 6247 ppm 750 1050 710
DHT 4A ASTM D 6247 ppm 250 350 290

Page 97 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-710 G Poly Propylene 18/09/2023 15:00 Small ( 0.20 to 0.49mm2) Default No/1520 30 28
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.20
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 4
Fused Pellet Default no/5kg 1 32
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 36
Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 3.75
Volatile Matter Licensor ppm 500 260
Method
Yellowness Index ASTM E 313 0 -4.34
553-MB-01E LIQUEFIED 18/09/2023 16:00 C2 Hydrocarbon ASTM D 2163 Vol % 1.17
PETROLEUM
C3 Hydrocarbon ASTM D 2163 Vol % 27.03
GAS-COQ
C4 Hydrocarbon ASTM D 2163 Vol % 70.85
C5 Hydrocarbon ASTM D 2163 Vol % 2.5 0.95
Density at 15°C IP 432 -2000 kg/m3 570.6
Total Volatile Sulphur ASTM D 3246 ppm(w) 140 30
Vapour Pressure at 40°C IP 432 -2000 kPa 520 1050 652
Caustic test IS 4576:2018 Pass
Note 10
Copper Strip Corrosion for 1 hrs @ ASTM D 1838 1b
38°C
Page 98 of 102
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
553-MB-01E LIQUEFIED 18/09/2023 16:00 Free Water Content Visual None
PETROLEUM
Hydrogen Sulfide ASTM D 2420 Pass
GAS-COQ
Odour IS 4576:2018 Adequate
Note:12
Volatility:Evaporation Temp in°C for IS 1448:P 72 °C 2.2 0.6
95%v at760mm
513-S-710 B Poly Propylene 18/09/2023 20:00 Irg 1010 ASTM D 6247 ppm 380 520 405
I 168 ASTM D 6247 ppm 750 1050 780
DHT 4A ASTM D 6247 ppm 250 350 260
Small ( 0.20 to 0.49mm2) Default No/1520 30 29
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.31
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 2
Fused Pellet Default no/5kg 1 38
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 37
Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 3.60
Volatile Matter Licensor ppm 500 250
Method
Yellowness Index ASTM E 313 0 -4.08
554-T-05C SUPERIOR 18/09/2023 21:50
KEROSENE

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 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
(GRADE-A)-COQ Density at 15°C ASTM D 4052 kg/m3 789.2
Percent Recovered below 200°C IS 1448:P 18 Vol % 77.0
Final Boiling Point IS 1448:P 18 °C 238.4
Mercaptan Sulfur ASTM D 3227 mg/kg 101.00
Total Sulphur ASTM D 4294 ppm(w) 1648.0
Appearance Visual Clear and
bright.Free
from
un-dissolve
d
water,foreig
n matter
and other
visible
impurities
Color -Saybolt IS 1448:P 14 +24
553-MB-01D LIQUEFIED 19/09/2023 1:45 C2 Hydrocarbon ASTM D 2163 Vol % 1.10
PETROLEUM
C3 Hydrocarbon ASTM D 2163 Vol % 26.12
GAS-COQ
C4 Hydrocarbon ASTM D 2163 Vol % 71.85
C5 Hydrocarbon ASTM D 2163 Vol % 2.5 0.93
Density at 15°C IP 432 -2000 kg/m3 571.5
Total Volatile Sulphur ASTM D 3246 ppm(w) 140 25
Vapour Pressure at 40°C IP 432 -2000 kPa 520 1050 639
Caustic test IS 4576:2018 Pass
Note 10
Copper Strip Corrosion for 1 hrs @ ASTM D 1838 1b
38°C
Free Water Content Visual None

Page 100 of 102

 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
553-MB-01D LIQUEFIED 19/09/2023 1:45 Hydrogen Sulfide ASTM D 2420 Pass
PETROLEUM
Odour IS 4576:2018 Adequate
GAS-COQ
Note:12
Volatility:Evaporation Temp in°C for IS 1448:P 72 °C 2.2 0.8
95%v at760mm
513-S-710 F Poly Propylene 19/09/2023 2:00 Irg 1010 ASTM D 6247 ppm 380 520 445
I 168 ASTM D 6247 ppm 750 1050 710
DHT 4A ASTM D 6247 ppm 250 350 280
Small ( 0.20 to 0.49mm2) Default No/1520 30 28
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.26 H23I1089
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 40
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 36
Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 3.54
Volatile Matter Licensor ppm 500 260
Method
Yellowness Index ASTM E 313 0 -4.09
# of Samples in Unit: 13
# of Analytes in Unit: 163

Page 101 of 102

 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:20 hrs on 18-Sep-23 to 09:20 hrs on 19-Sep-23 Report Date: 19-Sep-23 9:21 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max

Total # of Samples: 346

Total # of Analytes: 1,716

Page 102 of 102