100

FOUR YEAR DEGREE COURSE IN

BTECH.(CHEMICALENGINEERING)
SEMESTER PATTERN CREDIT& GRADE SYSTEM
SEMESTER-V
5CH01 HEAT TRANSFER
Objective:
To introduce the concepts of heat transfer to enable the students to design
components subjected to thermal loading.
SECTION-A
UNITI: Importance of heat transfer in chemical process industries.
Modes of heat transfer, steady state conduction in one
dimension. Fourier's law. Heat transfer through plane,
cylindrical and spherical walls, compound resistance in series,
thermal insulation, critical and economic thickness. Extended
surface equipments, types, their design and operation,
introduction to unsteady state heat transfer. (7)
individual and overall
UNIT II: Heat transfer by convection, film concept, Natural and forced
coefficients and factors affecting them.
transfer.
convection. Dimnensional analysis applied to heat (7)
Dittus-Boelter equation, Limitations and application.
counter current flow, concept of
UNIT III: Heat transfer by parallel and
difference, rate of heat transfer. Heat
log mean temperature condensation in horizontal
transfer by film wise and drop wise (7)
& vertical tube.
SECTION-B

exchange equipments and their design, double pipe,

UNIT IV: Heat current, shell and tube heat exchangers,
parallel, counter heat
fouling factors, concepts of transfer units in
condensers, exchangers. (8)
exchangers, NTU concept for heat
Evaporators: Theory of boiling. Classification,
NI V: Boiling and applications ofevaporators. Single and multiple
types and field transfer through submerged coils,
effect evaporators. Heat (8)
jacketed vessels.
concept of black body, Kirchhoff's
UNIT VI: Heat transfer by radiation, gray body radiation, view factors
Black and packed and
law, Stefan's law,
non-luminous gases. Heat transfer in
Tuminous and
fluidized beds. technological forecasting in heat
and
Recent developments (8)
transfér.
 101 102

Text Books:
1) Heat Transfer by Sukhatme
UNIEV Principles
ofeelectro-candhemimoltencal technolsystem;ogjccaustic
processin igneous al proces;soda,, Electrolytic
2) Heat Trasnfer by Mc Adams Electro-thermal1Industries: (7)
chlorine.
Reference Books: UNITVI: aluminum,
Electro-chemical sources of energy andlithiun, titanium.
1) Unit Operations of Chemical Engincering by McCab storage. ()
Note: The students are expected to visit the various
2) Chemical Engineering by Coulson &Richardson, Vol.and
I Smith to have a thorough industries
3) Heat Transfer by R.C.Sachdeva understanding of thesubject.
TextBooks:
SCH02 CHEMICAL ENGINEERING PROCESS.J Austin, GI., "Shreve's Chemical I Process Industries", Fifh Edition,
1. McGraw-Hill.InternationalI Book Co, Singapore, 1984.
(Inorganic Chemical Technology)
Chemical Engineers are trained primarily to work in chemical Chemical
Dryden, C.E., "Outlines M.of.aand M. Sitig,Technology , Edited and
basic purpose is to start from one ore or other chemical rawindustries. Je 2
Revised by Gopala Rao Third edition, Affiliated
end up with a consumer product through series of material and East-West press, 1997
chemical and physicl
changes, and here it difers from other manufacturing industries which
assembly industries not are ReferenceBooks:
creative
of a number of types of chemical industries.
It will be shown in the study Editon,
Book of Industrial Chemistry", 7th
industrial process that the fundamentals Kent, J.A., Riggel's Hand
chemistry, thermodynamics, kinetics, engineering and 1.
Van Nostrant
Reinhold, 1974.
valid. economics are always Engineering Education Development
Objective: CHEMTECH 1-4, "Chemical
2. 1975-78.
After studying this subject the chemical Centre, I.I. T.,Madras
comprehensive picture of the chemical engineering student will have a
reasons and the basis for many and diverseindustry, particularly as to the ECONOMICS & MANAGEMENT
out in process. operations which are carried 5CH03 industries, marketas
primarily to work in basic concepts of
Engineersare trained about the
SECTIONA should have knowledge foreign trades, banking, etc.
UNIT-I: 1. Sugar and Starch managers. They developments in the field, managementfYom
products. Industries: Sugar, Starches and reialeu economics, latest should have basic knowledgeabout
they
2. Soap and HS a manger
UNIT-II: 1. Detergents:
Pulp and Paper Detergents, Soap and Glycerin. ()
production to marketing. understanding
student willhave about
manufacture of Industries:
and paper. Types, raw
materials, Objective: theengineering preliminary idea
2.
Cement and LimepulpIndustries: After studyingithissubject
the field of
economics and
materials, setting and Portland Cement, types, ra ofthe happenings in
processes of Portlandhardening of cement, management. SECTIONA Supply,
Demand:
and gypsum.
UNIT-II: 1. Industrial
Gases:
cement; Manufacture,manufacturws
use of lime
(8) and scope of
DemandandDemandAnalysis:
economics, demand.
of diminishing utility,
of
dioxide, hydrogen,
2. Fuel
Gases:
Manufacture and application of carbon
oxygen,andnitrogen.
UNIT-I: Nature specification,types lawof
concepts, demand
concept
analysis,Forecasting:forecasting,

Manufacture
gas, natural gas,
synthesis gas.uses of producer (8)
gas, water Consumer
of
significance surplus.
forecast,
demand
Demand
stepsin (8)
Competition,
types of
SECTION B forecasting, demandforecasting.
market-Competition.
Perfect Inflation:
UNIT-IV: 1. Techniques of
Acids: Sulfuric acid, nitric types of
Monopolistic ofinflation.(7)
2
Fertilizer Industry: acid, Meaning,
urhydre ochleammoni
oric acid.a, controlling
UNIT-II: Market: Oligopoly,effects,
Manufactphosphat
diammonium phosphate, super of
s (SSP and urea,
TSP)
Monopoly,
Causes,
measurement,

(8)
 103 1Ú4
of
UNT-I: Nature and characteristics Indian economy,
meaning, merits and demerits. Theobjectiveofaa Materials Engineer is to predict and control
Globalisation of Indian economy-meritssand
of VAT, WTO, GATT &TRIPS
exchange.
PBankinivga,izaCoFoinnGartpeig
agreement, demerits.
Objectives:
propertiesthrough an understanding of
material and
erystalline,
Imicroscopic atomic, molecular,
structures of engineering materials.
SECTION A
SECTIONB 8) Introductionto materials and their principle properties, Simple
UNITI: stresses and strains, Concept of stress, strain, shear stress,
UNIT-IV: Basic concepts and functions of
Management. Production. Management:Management,
Definition, Peersona shear strain, Hooks law, Elastic limit, stress-strain curve for
mild steel and elastomeric materials, factor of safety,
Functions and Scope, Production Planning and
significance, stages in production planning and Obnjetcrotivl,es,its
CCo Poisson's ratio, Strain energY due to axial load and impact.
Introduction to determination of mechanical properties of
Concepts of material management, inventory control. materialsASTM methods.
importance and various methods. cont(8)rol; its Basic principles intheir selection for fabrication and erection of
UNTT-V: Marketing Management: Definition of UNITIL: Testing of materials, destructive and
concept, objectives and functions of marketing. marketing, marketing chemical plant. and chemical bonds.
nondestructive tests, structure of atom material properties
Marketing Research - Meaning; Definition; objectives: crystal structures and their
infiuence on
()
Importance; Limitations; Process. Deformation and slip processes.
Advertising - meaning of advertising, Ferrous and
criticism. objectives, functions. and their alloys: Iron - carbon diagram, steels,
IUNITII: Metals special steels, stainless
(7) nonferrous alloys, mild steel, alloys, and
high
UNIT-VI: Financial Management: Introduction, brasses, aluminum alloys and titanium Metbods for
Management, Functions and Importance Objectives of Financial brasses, refractories.
material, insulation, puaching, revetting,
of low temperature
Management. Concept of capital structure and variousFinancial fabrication, rolling, bending,
central
alloys (8)
of finance. sources alloys: aluminum and its
Text Books: (7) welding. Nickel and its
SECTIONB
1
Modern Economic Theory- K.K. Corrosion attack methods, Different
2 Dewett, S.Chand and its control: biochemical, and
Principles and Practice of Management:
N.S. Bhalla Kalyani R.S. Gupta, UNITIV: Corrosion corrosion: chemical, factors afiecting
external
Publishers B.D.Sharma, types of
electrochemical: Internal and Methodsto minimize
Reference Books: chemical equipments, equipments.
1 corrosion of process
2 Principles of
Micro EconormiEconomics:-P.N. Chopra (Kalyani charts for coatings
corrosion, corrosion anticorrossive surfacecase studies
3 c
Indian Economy: Rudar DuttH.L.&Ahuja (S.Chand) Publishers).
Theory Polyaniline and corrosion prevention corosion (8)
4
K.P.M. electrochemical
Principles
& Sons) Practices of Management - Sundhram
&
from the chemical
industry. polymetric
Selection of plastic,
L.M. Prasad (Sultan synthetic: reinforced
S.
Marketing Chand natural and linings, fiber Teflonin
Management
House, Bombay). - S.A. Sherlikar
(Himalaya Publishing
UNIT V: Polymers,for equipment
materials specialpolymers
like Nylon66,
6.
Financial Management -1.M. Pandey
Delhi) application of (7)
(Vikas Publishing House, engineering. Polymer
ceramics and
glasses;
New Composites. Definitionof properties;
5CH04 processing, and and
MATERIAL SCIENCE &
Materials Science & VI: Ceramic
UNIT interaction
and
glasses:
between
structure, materials; Crystalline
cements,

Engineering is ENGI NEERIof NGmechanical, glass

ceramicand refractories,clays,()
physical, and chemical properties of the study Applicationsof silicates,
ceramics, polymers, and composites.
fengineering materials, such as metals,
noncrystalline
lass
vitreous
ceramics,borosilicate.
silica,and
 Zoning Town planning regulation of new
Legislation and enforcement industries -
Text Books:
1.
to
James F. Shacketford, Introduction 1990 Material Science, Assessiment andi Air quality,. -Environmental Impact
publishing company, New York ISBN UNTV:Samplingand/Analysis: Basic principle of sampling -Statisical
2. DZ. Jestrazebaski, Properties of Engineering Techniques - Source and ambient sarmpling - Analysis of
Toppers. Co. Ltd.
Reference Books:
Materials, Brd tà Gaseous and Particulate pollutants -Standards. (7)
1. JL. Lee and Evans, Selecting Engineering materials for TextBooks:
and process plants, Business Works 1978 D, "Air Pollution and Control Technologies", Alied
Design of machine elements, Spott M.M. Prentice Hall chemica
Anjaneyulu,
Publishers,Mumbai, 2002
2. L
3. Atext book of design, Khurmi
machine R.S. and Environmental Pollution Control Engireering, Wiley Eastern
4. Material Science & Metallurgy for Engineers, Gupta J.K, Rao,C.S. 1996
Everest Publishing House.
SFECHOS FREE ELECTIVE-I
Dr:V.D.Kodgire, 2
Ltd., NewDelhi
ReferenceBooks:
Rao H..V.N,Air Pollution Control, Tata-McGraw-Hill,
SFECHOS (1) AIR POLLUTION CONTROL Rao M.N., and
NewDelhi, 1996
Objective:
This subject covers the sources, characteristics and W.L.Heumann, Industrial Air Pollution Control Systems, McGraw-
pollution and the methods of controlling the effects of air 2
Hill, New Yark,
1997
to know about source inventory and controlsame. The student is expectet Mahajan S.P., Pollution Control in Process
Industries, Tata McGraw
mechanism. Delhi, 1991
HillPublishing Company, New Tchobanoglous C Environmental
3.
SECTIONA and
UNIT I: Sources of air pollution: Peavy S.W., Rowe D.R. New Delhi, 1985
Classification
Particulates and gaseous pollutants of air pollutants - 4.
Engineering McGraw Hill,
- Sources of air pollution "Environmental Engineering Vol. II",Khanna Publishers,
-Source inventory. 5. Garg, S.K.,
UNIT II: Effects of air (7) New Delhi
Tata
Control in Process Industries",
beings, materials,pollution: Effects of air pollution on human
vegetation, animals -global warming-ozone 6. Mahajan, S.P., "Pollution
layer depletion, Sampling and Analysis - Basic McGraw-Hill, New Delhi, 1991
Sampling - Source and ambient Principles of 5FECHO5 FREE ELECTIVE-1
pollutants -Principles. sampling - Analysis of SAFETYMANAGEMENTIN NDUSTRIES
UNIT III: Dispersion of (8) (2) RISKAND
pollutants: enhanced the impotance ot
Met e orol o gi cal Elements of atmosphere -
factors - Wind Public awareness of hazards and
risks has
today's increasingly
litigious
roses - Lapse rate
ofAtmpolospheric -stability and andmanagement in is shifting
safety assessment responsibility for saferycommercial
lutants Dispersionturbulence-Plume rise-Dispersion society. Worldwide the burden of industrial and
UNIT IV: Air
Pollution
SECTION B models-Applications. () towards those who
organizations. The
manage and work in
own,
management ofsafety and risk
integrated
needs to be
Control: Concepts of control -
design of control into the overall should be appropriate and cost-
gravita ti o nal , measures ParticulatesPrinciples ndby
-
management of the
organization. It entrepreneurial spirit of
cent
precipaitntatiocontrol rifugal
n Selection
- , filtration, scrubbing, control the innovative procedures. An
effective without dampeningbureaucraticrules and managedsoas
poBut by criteria for equipmentele-ctrostatie employees with
inflexible needsto be
potential hazards ettects. Risk and safety
UNITV: combust i on adsorpt ion, absorption. gaseous
Air Quality -Pollution control for specific organization's exposure to
majorcondensation,
in
and mitigate any calculated manner but
to reduce the chance of loss astructuredand
Management: Air quality standards i-ndustAir ries. (8)
monitoring-Preventive quality
issues need to be evaluated
ightof an overall
in
organizational strategy.
 107
108
SECTIONA
UNTT:: Hazardidentification methodologies, risk I
Thermal
radiation-determinationnof emissivity
exchanger
consequenceas es ment
-PHA, HAZOP, MCA, ETA, FTA, 3 pipeheat
Double tube heat exchanger
analysis.

an liys i ,p iN
4. andI
ShellHeatexchanger
Plate
UNTII: Hazards in work places - nature and 5.
of hazards, hazards due to improper type of work 6 transferin agitated
vessels

house-ke pinpgla,ces,
Heat
poubleeffectevaporator
due to fire in multi-floor industries and y 8
and safe methods in the above situations.
UNTT- II: Workers' exposures to hazardous
build
chemicals, of
ings, gideline,
9 evaporator
10. Openpan demonstrator
11. Heatpipebed heat transfer
physical and chemical properties of TLVs
accidents like fire explosions, ingestion and chemicals lecatheirnicgak 12 Fluidized
perform minimum EIGHT experiments
from
Nofe: The students should term. All experiments in this list shall be
in work places due to dangerous
dusts, fumes and
guidelines and safe methods in chemicals s}
inhalation, polutin the list to complete the Additional experiments relevant to the
available in the laboratory. main list.
entry into confined spaces. handling,,storaVagepous,
(8) and syllabus may be added to the
SECTIONB SCIENCE &
ENGINEERING-LAB
UNIT-IV: Hazards peculiar to industries like 5CH08 MATERIAL
petroleum, pulp and paper, tanneries,fertilizer, heavy chemical List ofExperiments: alloys. (Minimum
glass and dyes, paints,
ceramics, dairy and sugar industries, pesticidesfor Microstructure observation and study of metalsand carbon Steel, tin,
safeguarding guidelines 1. medium carbon steel, high
personnel and safeguarding five) low carbon steel, bronze.
air pollution in the above industries. against water, land and bronze, brass, phosphor polymeric materials; impact test and
UNIT- V: Safety education and training - safety
(8)
2. Study of properties of plain
fundamentals of safety tenets, measuring safetymanagement, polymeric Tests.
spray test for different samples such as
testing (salt steel.)
motivating safety performance. performance, 3. CorrOsion chrome plate steel, galvanized Rockwell hardness
UNTT VI: Legal aspects of (7) carbon steel, hardness test on metals, ie.
types of scleroscope tests.
Text Books: industrial safety, safety audit. . (7) 4. Different
Brinell
test,
hardness test, Shore
on mild steel, copper,
brass and
1. F. P. Lees, Charpy impact test
Izod and element to be
"Loss prevention in
5.
(Any one from steel,
2.
But1977.teHandl
rwortehy,-H"Indust
einermrann,ial safety1996. process industries", 2nd,
6
aluminium.
Chemical molybdenum from
analysed e.g.
and alloys
analysis ofmetals stainless steel carbon
by
Reference
1. Books: handbook", 2nd ed., McGraw-Hill,
copper from
Macrostructure
brass etc. lines
observation: (tlowsteel.)
observation in forging
lining,

ButR.S.D.P.Pe.rwort
Levinhe,, "Pr1971.otecting 3personnel at of
7.
etching sulphurprinting
Dye penetration i) Rubber
i)
macroexperiments based in,treatments.
2
3. Blake, "Industrial hazardous waste sites", Martin 8. Study Ultrasonic test, iv) Heat
8
experimentsfrom the
shall be
Techniquessafety",of safetPrenty ice Hall, 1953.
minimum
1978.Patterson, shouldperform experiments in this list
ii)
students All relevant to
Note: The complete the term. Additional experiments
List 5CH01 HEAT
of Experiments:
management", McGraw-Hill, Jlist to
available inthe laboratory.
added to the
main list.
may be
1. Heat conduction
2
Natural convection
TRANSFER- LAB the syllabus
 110
109
chart, Enthalpy-humidity charts, determination of
6CHO1 CHEMICAL humidity
(MASSENGINEERING andconcept of dehurmidification, equipments for
TRANSFER-I) humidification
operations.

OPERATION-T
humidity, (8)

UNITI: SECTION-A Crystallisation:Principles of crystalisation, equilibria,

Importance of Mass
transfer, operationsTransfer : calculation of yield, heatfractional
effects, crystal growth, properties
based Operation.
UNIT
V:C

crystallisation, caking of

gasliquiCldas-numbersifoclaitdions contar,
nucleation,
Concepts of flux, resistance,on crystals
types of crystallise's andtheir aplications.
direction of mass transfer, drriving force, of
crystals, Various
separationproces, Typessoff membrare, seçaraticn
s law Dimensionless
transfer. Diffusion, Fick'
Dependence of diffusivity on
Iand I!.
no. calculation, Determination physical equil brium Membraneseparation of liquids, Dialysis, Revese Osmosis,
gases,
pervaporisation, desalination. Recent
of developments in mass

dif usiprviotyperties, Schmida:

(8)
of transfer operation.
gas-gas, gas-liquid diffusion. in
coefficient licquid-liquik,
UNTI: Interphase mass transfer, various (7) TextBooks: Enginering: W.L. MeCabe &J.C. Samith,
and their of Operationiin Chemical
determination, resistance concept, mass
transte Unit Hil
McGraw
Concept, Mass transfer in
turbulent flow, controlling
)
Operation:RE.Treybal
Theories of Analogies of phas
transfer, Empirical equations. MassTransfer
film theory, Higbies penetration theory, mass Treas, McGrawHill
theory, ApplicationsDeriandvattraionsínerof, fvwx
ta,
ReferenceBooks:
Sherwood,RILPigford,
equation, surface renewal MassTransfer:
T.K. Richardson
Engineering:Coulson&
(7)problers.
1) Chemical
6CH02 CHEMICALENGINEERINGPROCESS-I
UNIT III: Absorptions, stagewise 2
absorption, material balance ovenl
stepwise minimum irrigation
(OrganicChemicalTechnology)
chemicalindustries.
factor calculation of numberrate,of Absorption and stripDine primarily toworkinchemicalraw
material
stages, McCabe-Thiela
graphical method, Kremsor-Brown-Sounder's
trained
Engineers are fromoneore orother ofchemical2nd
Chemical start series
Equipments of absorption, tray towers, packedequation. basic
purpose is to
consumer productthroughmanufacturingindustries
other shownin
concept of HTU, NTU, towers
Its
Continuous absorption, HETP and end up with a hereitdiffersfrom industries.Itwillbe thathe
and creative process
comparison stepwise columns, design concepts.
with physicalchanges,
assembly
industriesnot chemicalindustrialengineeringand
determination of height and
colurnn. diameter of packed absorpticn whichare
of a
typesof
numberofthermodynamics,kinetics,
the study chemistry,
(8) fundamentals havea
SECTION-B always valid. engineeringstudentwill the
economicsare particularly o
as
UNIT IV: Adsorption: chemical caried
properties of Adsorption equilibria, types of adsorption, Objective: thissubjectthechemicalindustry, operations whichrr
studying pictureofthe diverse
adsorbents, single and muiti-stage adsorption, After manyand
adsorption isotherns, principles of adsorption, Break comprehensive
thebasis
for sbsolute
curves, adsorption of liquids, basic
equations, adsorber through and
reasons SECTIONA alcobol,
adsorption equipments. Ion Exchange: design, out in process. Industries:
Iodustrial
acid
exchange, Principles of ion acidciic
rate of ion techniques
and applications, Ion exchange equilibria, Fermentation
Aceticacid
lactic
exchange. UNTTI: 1. alcohol, wine. production: polypropylene,
UNIT V: (7) echyene,
Drying and humidification: acid
Organic
Industries:Poly
cquilibrium, cross circulation Principles
SRD
of drying, phase 2 rubber,
drying, through circulation Polymerizationsyncheticfibers. synchetic
drying, drying of suspended particles, rate of drying curve, polyester Naural
rubber,
dryers for solids and pastes, dryers for solutions and slurries,
UNTTII: 1. PVC, Lndustries:
ie. various types of dryers, Rubber
wet bulb temp., dry bulb Hurmidification:andTerrns, definitions,
temperature of
2

humidity, adiabatic saturation

 Refinery: Refining of crude
Petroleum
UNITII: 1. refining.
oil, products
Petrochemicals: Significant petrochemicals
2. derivatives. and her
SECTIONB

agents, kinetics,
UNITIV: 1.
:Nitration
Nitration:
preparation
N
of nitrobenzene, mechani
nitronaphthalene.
nitronaphthalene, nitroacetanilide.
sm, indust
2. Sulphonation and Sulfation: agents, kinetics,
technical preparation of aliphatic
mechanis
sulphonation of laurylalcohol, dimethyl ether. (2 sulphonate
UNTT V: 1. Hydrogenation: Catalytic hydrogenation, kinetic:
mechanism, hydrogenation of fatty oils, synthesit
methanol.
Hydrolysis: Hydrolysis of fat, carbohydrate, star:
Manufacture of ethanol from ethylene, manufacture
phenol. ()
UNTVE 1. Halogenation: Technical preparation of halog:
compounds- allyal chloride, DDT, BHC, chlorobenzen
vinyl chloride.
2. Oxidation: Liquid and vapour phase oxidation, tectnia
oxidation of isopropyl benzene, naphthalene,
ethylbenzene, naphthalene sulfonic acid. ()
Note: The students are expected to visit the various industries tohav
athorough
Text Books:
understanding of the subject.
P.H. Groggins, "Unit Processes in Organic Synthesis", McGrawHi
Book Co.,
2 Kogakusha (1984)
JA.Kent, "Riegel'
Van Nostrand s Hand book offIndustrial Chemistry",
Reinhold Co.. New York (1974)
Reference
1. Peter
Books:
Wiseman, "An
2nd Edition,
Chemisty
2.
CHEMTECH
Introduct ion to Industrial Organic
Applied Science Publishers Ltd., (1979)
LondonDevelopm

I-4,"aChemi
Centre,LIT., Madr s 1975-cal78 Engineering Education