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This document summarizes a dissertation submitted for a Master of Science in Chemistry degree. The dissertation involves the synthesis and characterization of various pyrimidinium and quinolinium salts. Specifically, the author synthesized and analyzed 2-amino-4-chloro-6-methoxy pyrimidinium oxalate, 2-amino-4-chloro-6-methoxy pyrimidinium 4-fluorobenzoate, 2-amino-4-chloro-6-methoxy pyrimidinium N-phenylanthranilate, and 8-hydroxyquinolinium 4-methoxybenzoate. The results and discussion of these syntheses and characterizations are presented across multiple chapters.

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Rajesh Ravi
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33 views

Rajesh Front Page

This document summarizes a dissertation submitted for a Master of Science in Chemistry degree. The dissertation involves the synthesis and characterization of various pyrimidinium and quinolinium salts. Specifically, the author synthesized and analyzed 2-amino-4-chloro-6-methoxy pyrimidinium oxalate, 2-amino-4-chloro-6-methoxy pyrimidinium 4-fluorobenzoate, 2-amino-4-chloro-6-methoxy pyrimidinium N-phenylanthranilate, and 8-hydroxyquinolinium 4-methoxybenzoate. The results and discussion of these syntheses and characterizations are presented across multiple chapters.

Uploaded by

Rajesh Ravi
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© © All Rights Reserved
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SYNTHESIS AND CHARACTERIZATION OF 2-AMINO-4-

CHLORO-6-METHOXY PYRIMIDINIUM/OXINE
CARBOXYLATE SALTS

A dissertation submitted to the


BHARATHIDASAN UNIVERSITY

TIRUCHIRAPPALLI
In partial fulfillment of the requirements for the award of the degree of

MASTER OF SCIENCE IN CHEMISTRY


(2019-2021)
Submitted by

R.RAJESH
(Reg.No:P19 )

Under the guidance of


Dr. K. THANIGAIMANI M.Sc., PGDBI., Ph.D
Assistant Professor of Chemistry

PG & RESEARCH DEPARTMENT OF CHEMISTRY


Government Arts College, Tiruchirappalli- 620 022
Tamil Nadu, INDIA.
APRIL-2021
Dr.K.THNIGAIMANI, M.Sc.,PGDBI.,Ph.D.
PG & Research Department of Chemistry,
Government Arts College,
Tiruchirappalli-620 022,
Tamilnadu, India.

CERTIFICATE

This is to certify that the dissertation entitled “SYNTHESIS, AND


CHARACTERIZATION OF 2-AMINO-4-CHLORO-6-METHOXY
PYRIMIDINIUM/OXINE CARBOXYLATE was done under my guidance
and is bonafide record of project work carried out by R.RAJESH
Reg.No:P19 in partial fulfillment to quality for the degree of Master of
Science in chemistry for during the Academic period 2019-2021 and it
represents entirely an independent work of the candidate.

HEAD OF THR DEPARTMENT RESEARCH SUPERVISOR

Signature of the External Examiner

Submitted to the Viva-Voce Examination held on………………


DECLARATION

I do hereby declare that this dissertation work has been

originally carried out by me at the Department of chemistry,

Government Arts College, Trichy-22 during the academic year

2019-2021 under the guidance and Supervision of

Dr. K. THANIGAIMANI, M.Sc., PGDBI., Ph.D., Assistant Professor of

Chemistry, Government Arts college, Trichy-22 and this has been

submitted else for any other degree.

Place : Trichy-22

Date:

(R. RAJESH)

Signature of the Candidate


ACKNOWLEDGEMENT

I express my grateful thanks to

Dr.K.THANIGAIMANI, M.Sc., PGDBI., Ph.D., Assistant Professor, PG &

Research Department of Chemistry, Government Arts College, Trichirapalli-

22, for her excellent guidance, constant encouragement and valuable

suggestions rendered in bringing of this dissertation.

I thank Dr. A. SIVARAJAN, M.Sc., M.Phil., Ph.d., Assistant

Professor and Head, PG & Research Department of Chemistry, Government

Arts College, Trichirappalli-22 for his suggestions and, encouragements.

I am highly thankful to Dr. S. S. ROSE MERY, M.Com., M.Phil.,

D.L.T, M.B.A., Ph.D., Principal, Government Arts College, Trichirapalli-22

for permitting me to carry out the project in the college successful.

I am glad to thank Dr. T. ASOKAN, M.Sc., M.Phil., Ph.D., Assistant

Professor, PG & Research Department of Chemistry, Government Arts College,

Trichirapalli-22, for their fruitful suggestions and their enthusiastic

encouragement.

I thank all the teaching and non teaching staff of the Department

of Chemistry, Government Arts College-Trichy-22 for their valuable

suggestion and help.


My M.Sc friends and P.G & Department of Chemistry, Government

Arts College, Trichy, for their help snd support

First, sincerely thank my parents and my family members for

their motivation, encouragement and moral support during the entire

period of study.

Above all I thank thee my Almighty who leads me to this stage and a

powerful grace sight on me.

R. RAJESH
CONTENT
CHAPTER TOPICS PAGE
NO

1
1 INTRODUCTION

16
2 EXPERIMENTAL METHODS AND
MATERIALS

32
3 LITERATURE REVIEW

4 RESULT AND DISCUSSION

4.1. 2-AMINO 4-CHLORO-6-METHOXY


PYRIMIDINIUM-OXALATE 42

4.2. 2-AMINO 4-CHLORO-6-METHOXY


PYRIMIDINIUM-4-FLUOROBENZOATE 47

4.3. 2-AMINO 4-CHLORO-6-METHOXY


PYRIMIDINIUM-N-PHENYLANTHRANILATE 52

4.4. 8-HYDROXYQUINOLINIUM- 4-
METHOXYBENZOATE 57

63
5 CONCLUSION AND SCOPE OF FUTURE
STUDIES

65
6 REFERENCES

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