CPE 664 Design Project 2 Design Project
CPE 664 Design Project 2 Design Project
● Stream Data :
● ∆Tmin value
The minimum temperature is 10℃. To decrease
the amount of heat exchanger required to an
acceptable level with reasonable price (Rokni,
2016).
PROBLEM TABLE ANALYSIS PTA
Qhmin
Qcmin
❏ Minimum cold utilities : 9464.2 kW
❏ Pinch Temperature : 415℃
❏ Hot pinch temperature : 420℃
HEN GCC FEASIBILITY ❏ Cold pinch temperature : 410℃
STUDY OF ECONOMICS PRE AND POST
HEAT INTEGRATION
Type of Utility Before Integration After Integration
1. Percentage saving:
❖ Energy (kW): 41.72%
❖ Cost (RM): 96.37%
2. Additional of 2 unit of cold utilities
3. Total 5 units of heat exchanger
CHAPTER 8 PROCESS CONTROL AND
INSTRUMENTATION Label Meaning
_____ Capillary
HE T-101 All
R-101 H-101
CHAPTER 9 EQUIPMENT DESIGN
9.1 HEAT EXCHANGER E-108
Type of Heat
Exchanger
Inlet Temperature (°C) 130 20 ★ Log Mean Temperature Difference, ∆TLMTD is at 29.408°C
Outlet Temperature (°C) 25 40 ★ Correction factor, Ft is taken as 1
Tube Side
Outer Diameter 16 mm
Tube Pitch 20 mm
Shell Side
Load on Vessel
Total weight of heat exchanger 52.5866 kN
Flange
Support Saddle -
NOZZLE SADDLE
MOC Carbon Steel -
Nozzles
Shell nozzle diameter 200 mm
Nom
Size
Pipe
OD
Flanges Raised face
Tube nozzle diameter 125 mm
d1 D b h d4 f Baffles
Shell 200 219.1 320 20 55 258 3
Type 25% cut -
Tube 125 139.7 240 18 48 148 3
Number of baffles 16 -
Bolting Drilling Neck
No d2 k d3 h2 r
Dimension, m mm
M16 8 18 280 236 15 10
V Y C E J G t1 t2 Bolt Bolt
M16 8 18 200 155 10 8
0.48 0.15 0.55 0.24 0.19 0.095 6 5 20 25
9.2 PACKED BED REACTOR R101
Chemical Design
Specification Data
Skirt support
Skirt thickness (mm) 7.98 SS304
More
9.3 ABSORPTION COLUMN
CHEMICAL DESIGN
9.3 ABSORPTION COLUMN
9.3 ABSORPTION COLUMN
MECHANICAL DESIGN
9.4 DISTILLATION COLUMN T102
Diameter 1.53 m
Height 28.7441 m
L/D 18.8273 -
9.4 DISTILLATION COLUMN T102
Material Design:
Corrosion allowance 4 mm
CHEMICAL DESIGN
Orientation Vertical
Total height 5m
L/D 2.8829
9.5 SEPARATOR (V-102)
MECHANICAL DESIGN
Wall thickness 4 mm
Skirt thickness 9 mm
Equipment Type
Grassroot Cost
Capacity
Pressure RM 43,133,686.67
Material of Construction
MANUFACTURING COST
RM 152,358,244
PROFITABILITY ANALYSIS
Revenue = RM 190,000,000 Non-Discounted Cash Flow
Cost of Land= RM 28,749,600
Cumulative Cash Position 514.38
(millions)
FCI = RM 84,463,945
Rate of Return on 30.07%
Investment
For HAZOP
For HIRARC
E O
EMERGENCY RESPONSE PROCEDURE:
IN CASE OF CHEMICAL SPILLAGE
2D PLANT LAYOUT
Source: Tenaga
Nasional Berhad
Industrial Tariff
PFD AFTER
INTEGRATION
CHAPTER 8
PROCESS CONTROL AND
INSTRUMENTATION
HEAT EXCHANGER Cooler)
HEAT EXCHANGER Heater)
PACKED BED REACTOR R101
Stream 7 8
To maintain the Cascade control. Outlet liquid level in the Changes in Level controller will
liquid level and absorber. liquid product drive the set point
prevent overflow in flow of the and the flow
absorber. product stream controller will
of absorber. control the valve to
match the set
point.
ABSORPTION COLUMN T101
Objective Control system Manipulated variable Disturbance Control strategy
To control the flow Feedforward Flow rate of dibutyl Changes in the The flow controller
rate of solvent and control. will drive the
phthalate solvent and flow rate of
mixture of gases control valve to
into the absorber. mixture of gases. solvent and keep the flow rate
at its set point.
mixture of
gases streams.
BACK
9.3 ABSORPTION COLUMN
MOC Column Carbon steel
Design assumption:
1) Steady state
condition within
streams.
2) No phase change.
3) Non-reactive system.
Material Design
9.4 DISTILLATION COLUMN
Category Value Unit
Fair equation:
Maximum temperature 815.6 ℃ Source: A prototype knowledge based system for pressure
vessel design by Lena Gunarssson
BACK
Material and insulation
T-201 V-102
Chemical pathway Mechanical pathway
CD MD
SUMMARY
CD
SUMMARY
MD
CHEMICAL DESIGN : REFERENCE
● Svrcek, W. Y., & Monnery, W. D. (1993). Design two-phase separators within the right
limits. Chemical Engineering Progress, 89(10), 53–60.
BACK
9.6 PACKED BED WET SCRUBBER
Malaysia air quality standard
CO quality
standard
1 hr : 0.03 ppm
8 hr : 0.01 ppm
BACK
Pall Ring Packing
Advantage of Pall Ring :
● Excellent strength and stability when exposed to high temperature and high chemical
● Deliver high level of separation efficiency and operational flexibility
HE
HEAT EXCHANGER
FIXED TUBE
AEM
1) Front end header type
The A-type front header is the standard for dirty tube side fluids and the
B-type is the standard for clean tube side fluids. The tube side for E-108 is
cooling water which is categorized as dirty fluids. Thus, A-type is more
preferable. The A-type front header allows access to the tubes for cleaning
or repairing purposes without disturbing the pipework. It is easy to fix and
replace.
2) Shell type
The most common TEMA shell type is the E-shell as it is most suitable for
most industrial process cooling applications.
M-type which is fixed tubesheet exchangers are generally the most cost
effective design. The design is similar to the L-type rear header but slightly
cheaper.
HEAT EXCHANGER
Fluid Allocation
In term of corrosion and fouling, dibutyl phthalate is
not corrosive and are usually used as anti-fouling
material which is more suitable in shell-side. Cooling
water is generally kept on the tube-side because it
tends to corrode carbon steel and form scale. This
will give better control over the design fluid velocity,
and the higher allowable velocity in the tubes will
reduce corrosion and fouling. Also, the tubes will be
easier to clean. The process stream is more viscous
than cooling water fluid. A higher heat-transfer
coefficient will be obtained by allocating the more
viscous material to the shell-side, providing the flow
is turbulent.
Grassroots Cost
CAPITAL COST INVESTMENT
Working Capital
Fixed Capital Investment (FCI)
Ref
Ref:
1. S&P Global Platts, Feb 2021
2. Alibaba, 2021
3. Alibaba, 2021
Cost of Utilities
Cost of Manufacturing
Revenue
SunSirs, 2021
Taxation Rate
Project Life
The revenues made from the buildings and Forecasting demand over periods
operation of a plant are directly affected by taxes. over 20 or 30 years is challenging
In Malaysia, the taxation rate remains the same and often inaccurate, as demand
from 2015 to 2021 which is 24%. depends on many factors that
cannot be controlled by the project
company (Association of Southeast
Asian Nations, 2021)
DCFROR
DCFROR = 20.54%
CHAPTER 11
PLANT SAFETY
LIKELIHOOD OCCURRENCE
SEVERITY OF HARM
E O
RISK ASSESSMENT
E
HIRARC FORM
Overall plant
BACK L R
HIRARC FORM
L R BACK
HIRARC FORM
ABSORPTION COLUMN
T101
L R BACK
HIRARC FORM
DISTILLATION COLUMN
T102
L BACK
HIRARC FORM
SEPARATOR V102
L BACK
HIRARC FORM
L
BACK
HIRARC FORM
HEAT EXCHANGER
HEATER
L R BACK
HIRARC FORM
HEAT EXCHANGER
COOLER
L R BACK
HAZOP study for Reactor
BACK
HAZOP study for Absorber
BACK
HAZOP study for Absorber
BACK
HAZOP study for Distillation Column
BACK
HAZOP study for Distillation Column
BACK
HAZOP study for Separator
BACK
HAZOP study for Fired Heater
BACK
HAZOP study for Heat Exchanger
(Heater)
BACK
HAZOP study for Heat Exchanger
(Cooler)
BACK
BACK
ERP: In case of gas leakage ERP: In case of fire or explosion
3D PLANT LAYOUT
Tank Farm Boiler house Emergency water system
Canteen
Waste treatment system
Administration
Office
Flare
Surau
Warehouse
Assembly
Utilities
point
2D PLANT LAYOUT (DURING EMERGENCY)
DETAILS OF PLANT LAYOUT UNIT
➔ Keeping all persons ➔ Process that ➔ Storage of oil and/or ➔ Additional facility
well away from ensures the quality petrochemical equipment such as
flames and smoke is requirements are products in large chemical plant
paramount indeed met by tanks. cleaning items,
➔ To avoid debris from identifying and ➔ Segregated based paints, adhesives
collapsing correcting defects. on the service and etc.
structures. ➔ Samples of type of tank for ➔ Additional storage
➔ Location can be operation is taken economic reasons, area.
filled with all and measured. besides segregating
workers at a safe ➔ Located besides by the level of risk.
location during short control room for ➔ High hazard area.
period of time. accessibility.
DETAILS OF PLANT LAYOUT UNIT