ABDULRAHMAN AL-SUMAIT UNIVERSITY CHUKWANI ZANZIBAR

DEPARTMENT OF SCIENCE

TITLE OF EXPERIMENT: LIQUID SOLID EXPERIMENT

COURSE TITTLE: CHEMISTRY EXPERIMENT

COURSE CODE: CH113

LECTURER NAME: Mr. SALIM ABDALLAH

SUPERVISOR NAME: Mr. MUHSIN JUMA

SEMESTER: 1st YEAR 1st SEMESTER

PRACTICAL DATE: 27/11/2023GROUP MEMBERS

NAME REGISTRATION NUMBER SIGNATURE

ISMAIL MOHAMMED MABROUK 23/CG/018

MOHAMED KHAMIS SHEHA 23/BC/061

MWAMVUA AZANI JUMA 23/BC/055

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 EXPERIMENT NO 5

ABSTRACT:

The experiment was determination the concentration of NaOH and Na2CO3 in the mixture by using
double indicator method NaOH and Na2CO3 were titrated by 0.2M of HCL were prepared by Measure
4.18mls of HCL than were puted in 250mls were for prepared solution than were titrated under P.O.P the
color were Changed from pink to colorless and were got 30.7mls of HCL and were Completed the
decomposition of Na2CO3 because it were give NaHCO3 decompose partially when using M.O the color
was changed from Yellow to pale pink were got 8.1ml

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TITLE OF EXPERIMENT : VOLUMETRIC DETERMINATION THE CONCENTRATION OF
NAOH AND Na2CO3 BY USING DOUBLE INDICATOR

AIM OF EXPERIMENT: To determine the concentration give solution of NaOH and Na2CO3 by

using double indicator by titration against a standard solution of HCL

THEORY OF HYPOTHESIS:

when HCL acid reacted with Na2CO3 Under P.O.P it decompose partially to produce of NaHCO3 and
when reacted with NaOH produce salt NaCL and water at under same time when added with M .O lead to
complete reaction between NaHCO3 and HCL to produce NaCL and water according to the following
chemical reaction

Consider a mixture of NaOH(aq) and Na2CO3 (aq).

Reaction between HCl(aq) and Na2CO3 (aq) takes place in two stages:

HCl(aq) + Na2CO3 (aq) NaHCO3(aq) + H2O(l) ...................... (1)

HCl(aq) + NaHCO3(aq) NaCl(aq) + CO2(g) + H2O(l) ............. (2)

While that between HCl(aq) and NaOH(aq) completes in only one step:

HCl(aq) + NaOH(aq) NaCl(aq) + H2O(l) ............................. (3)

PRECAUTION : to wear gloves because HCL are corrosive ,also NaOH are very too hot

. To wash conical flask after every titration to avoid error

APPARATUS AND CHEMICALS: Burette, Pipette

Conical flask, funnel

HCL ,NaOH, Na2CO3

P.O.P, M.O

PROCEDURE: a) preparation of 4.18cm3 of 0.2M of HCL

3
 Given:

Mw = 36.5g/mol, density =1.18, percentage 37%

From

Mc= f×%×10÷(36.5)

=1.18×37×10÷(36.5)

=11.96 g/mol

Than

McVc = MdVd

Vc = MdVd ÷(Mc)

= 0.2×0.25÷(11.96)

= 4.18mls

b)fill the solution of HCL into burette

c) pipette 25mls of mixture of NaOH and Na2CO3 into a conical flask and were

Were added three drops of P.O.P indicator

d) titrated the mixture with standard solution of HCL solution from burette untill

pink color disappear than were recorded the volume (V1) of consumed HCL

e) added 3 drops of M .O Orange indicator to the same mixture were continue the

Titration until the colors change from yellow to pale pink. Than were find the

volume (V2) of the consumed acid in step

f) Repeated the procedure 1 to 3 until were obtain concordant than were tabulate

result

TABLE OF RESULT

Burette reading PILOT I 2 3

Final reading used 31.00 29.90 31.30 30.90

4
(P.O.P)cm³

Initial reading used 00.00 00.00 00.00 00.00

(P.O.P)cm³

Mean titre value 31.00 29.90 31.30 30.90

(P.O.P)cm³

Initial reading 31.00 29.90 31.30 30.90

(M.O)cm³

Final reading 39.00 38.60 38.90 38.90

(M.O)cm³

Mean titre value 8.00 8.70 7.60 8.00

(M.O)

OBSERVATION: When HCL titrated with Na2CO3 under P.O.P into decompose partially to

Produce NaHCO3 under the same time reacted to NaOH to produce salt

. NaCl and water the color changed from pink to colorless to complete the

Decompose of NaHCO3 into NaCl and water by using M.O indicator due the

colour change from yellow to pale pink

DISCUSSION : In this experiment the Titration was involved strong acid HCL with double

Salt Na2CO3 and NaOH as were seen in procedure above, theoretical were

were given that while during an experiment occur due P.O.P are weak indicator

than M.O

CONCLUSION: From the above experiment the neutralization reaction occur was formed

after titrated HCL and NaOH under P.O.P and between HCL titrated with

NaHCO3 under M.O the hypothesis were prove because at the end of
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 Experiment

REFERENCES

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1. South Carolina State University. & Ministry of Education and Vocational Training, Zanzibar. (2011).
Chemistry for Secondary Schools, Form 3 (Revised Ed). Oxford University Press (T) Ltd.2. Tanzania
Institute of Education. (2019). General Chemistry for Advanced Secondary Schools. TIE.3. Zumdahl, S.
S., Zumdahl, S. A., DeCoste, J.D. & Adams, G.M.(2018). Chemistry(10th ed.). Cengage Learning.