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Test Injections RM

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Riad Manamanni
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11 views

Test Injections RM

Uploaded by

Riad Manamanni
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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TEST INJECTIONS REPORT

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_SQD2 Acquired By: sqte
Project Name: SQT_E_BSM_SM_SQD_data Column serial Number:
Sample Set Method: 01a Test Injections SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Test Injections RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 1599 Result Set Id 2524
Sample Set Name: Test Injections SSM Sample Set Start Date: 12/21/2010 11:32:14 AM EST

Test Injections are performed after preparing the chromatographic system to equilibrate the system and column.
The standard deviation of the Retention Times, and the %RSD of Area and Height demonstrate the readiness of the
system to be qualified.

The standard deviation for the Sulfadimethoxine peak RT must be < or = 1.5 seconds, the %RSD for Area must be
< or = 3.0% and the %RSD for Height must be < or = 4.5%.

Sulfadimethoxine Height Results Table


Sulfadimethoxine Area Results Table
Height % RSD Height % RSD
Area % RSD Area % RSD Height % RSD
Area % RSD Specification Pass Fail
Specification Pass Fail
1 %RSD < or = 4.5 1.8 PASS
1 %RSD < or = 3.0 0.4 PASS

Sulfadimethoxine Retention Time (sec) Results Table

Retention time (sec) Retention time (sec)


Retention time (sec)
Standard Deviation Standard Deviation
Standard Deviation
Specification Pass Fail
1 SD RT < or = 1.5sec 0.6 PASS

Printed 7:36:40 PM US/Eastern 4/26/2011 Page: 1 of 3


TEST INJECTIONS REPORT

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_SQD2 Acquired By: sqte
Project Name: SQT_E_BSM_SM_SQD_data Column serial Number:
Sample Set Method: 01a Test Injections SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Test Injections RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 1599 Result Set Id 2524
Sample Set Name: Test Injections SSM Sample Set Start Date: 12/21/2010 11:32:14 AM EST

Test Inj ections Chromatograms

2.0x106

Sulfadimethoxine
1.5x106
Intensity

1.0x106

5.0x105

0.0

2.0x106

1.5x106
Sulfadimethoxine
Intensity

1.0x106

5.0x105

0.0

2.0x106
Sulfadimethoxine

1.5x106
Intensity

1.0x106

5.0x105

0.0
0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00
Minutes

Printed 7:36:40 PM US/Eastern 4/26/2011 Page: 2 of 3


TEST INJECTIONS REPORT

A C Q U I S I TI O N I N F O R M A TI O N
System Name: BSM_SM_SQD2 Acquired By: sqte
Project Name: SQT_E_BSM_SM_SQD_data Column serial Number:
Sample Set Method: 01a Test Injections SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Test Injections RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 1599 Result Set Id 2524
Sample Set Name: Test Injections SSM Sample Set Start Date: 12/21/2010 11:32:14 AM EST

Chromatographic Peak Results

Name: Sulfadimethoxine
RT RT Height Points
Injection Name Area Result Id
(min) (sec) (µV) Across Peak
1 1 Sulfadimethoxine 1.519 91.15 6556529.7 2196295.1 55 2527
2 2 Sulfadimethoxine 1.536 92.18 6601929.8 2275105.8 55 2528
3 3 Sulfadimethoxine 1.536 92.14 6569235.4 2214834.6 55 2529
Mean 91.82 6575898.30 2228745.16
Std. Dev. 0.58 23421.92 41205.67
% RSD 0.63 0.36 1.85

Printed 7:36:40 PM US/Eastern 4/26/2011 Page: 3 of 3

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