ASTM D1938-14 Standard Test Method For Tear Propagation
ASTM D1938-14 Standard Test Method For Tear Propagation
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sample shall rest on a smooth, slightly yielding surface that TABLE 1 Tear Propagation Resistance (Trouser Tear) Machine
will not injure the die blade. Care shall be taken that the cut Direction (Values Expressed in Units of Grams-Force)
edges of the specimen are parallel and perpendicular to the Material Average Sr A SRB rC RD
samples longitudinal and transverse directions. Polystyrene 5.04 1.54 3.47 4.32 9.72
Polyester 32.75 7.08 7.08 19.81 19.81
Polypropylene 70.77 20.52 38.05 57.45 106.6
7. Test Specimens HDPE No. 2 127.3 48.04 56.49 134.59 158.2
7.1 The specimens shall conform to the dimensions shown LDPE—LD 228.3 33.98 33.98 95.14 95.14
104
in Fig. 3 and shall not vary by more than 0.5 % from these LLDPE 337.1 30.95 42.74 86.66 119.7
dimensions. HDPE No. 1 482.9 49.04 106.0 137.3 296.9
A
NOTE 4—The thickness of the test specimens shall be uniform to within S r = within-laboratory standard deviation for the material stated. It is obtained by
pooling the standard deviations of the test results from each laboratory, as follows:
5 % of the thickness over the length of the unslit portion of the specimen. Sr = [(^(S1) 2 + (S2) 2 ... + (Sn) 2)/n]1/2
B
7.2 Measure the thickness of the specimen below the slit SR = between-laboratories standard deviation for the material stated. It is a
pooling of the amounts by which the average of the test results for each laboratory
(see Fig. 3) in several places and record it in millimetres to the deviate from the overall average for that material.
nearest 0.0025 mm (0.0001 in.). C
r = within-laboratory repeatability limit = 2.8 × Sr.
D
R = between-laboratories reproducibility limit = 2.8 × SR.
7.3 Cut enough specimens to provide a minimum of five
tear-propagation force determinations each in the machine
direction and in the transverse direction of the material being
tested. 10.2 For thin films and sheeting that have load-time data
characterized by Fig. 2, obtain and report the initial force to
NOTE 5—This is required because the properties of anisotropic speci- continue the propagation of the slit, the maximum force, and
mens vary with direction.
the extension at maximum force. Report both the initial load,
8. Conditioning the maximum load, and extension at maximum load.
8.1 Conditioning—Condition the test specimens at 23 6 10.3 For each series of tests, report the mean of all values
2°C (73.4 6 3.6°F) and 50 6 10 % relative humidity for not obtained to three significant figures and as the mean value of
less than 40 h prior to test in accordance with Procedure A of the particular property.
Practice D618 unless otherwise specified by agreement or the 10.4 Calculate the estimated standard deviation and report
relevant ASTM material specification. In cases of load to three significant figures and extension to two significant
disagreement, the tolerances shall be 61°C (61.8°F) and figures.
65 % relative humidity.
8.2 Test Conditions—Conduct the tests at 23 6 2°C (73.4 6 11. Report
3.6°F) and 50 6 10 % relative humidity unless otherwise 11.1 Report the following information:
specified by agreement or the relevant ASTM material speci- 11.1.1 Complete identification of the material tested, includ-
fication. In cases of disagreement, the tolerances shall be 61°C ing type, source, manufacturer’s code number, form, principal
(61.8°F) and 6 5 % relative humidity. dimensions, previous history, orientation of samples with
respect to principal directions of the material, etc.,
9. Procedure 11.1.2 Average thickness of test specimens,
9.1 Secure Tongue A (see Fig. 3) in one grip and Tongue B 11.1.3 Number of samples tested,
in the other grip of the constant-rate-of-grip separation-testing 11.1.4 Date of test, and
machine, using an initial grip separation of 50 mm (2 in.). 11.1.5 Mean of the five average tear-propagation
Align the specimen so that its major axis coincides with an determinations, usually in newtons (or pounds-force), for the
imaginary line joining the centers of the grips. materials described in 10.1; and the mean of the five initial
9.2 Using a grip-separation speed of 250 mm (10 in.)/min, tear-propagation forces, the mean of the five maximum tear-
start the instrument, and record the load versus extension. propagation forces, in newtons (or pounds-force), and the
extension to maximum force, in mm (in.) for materials de-
9.3 Continue the test until the tear has propagated through scribed in 10.2. In each case, report the standard deviation of
the entire unslit 25-mm (1-in.) portion. the data. In the cases where the specimens tear to one side, note
9.4 If the tear deviates from the center line to such an extent this together with the values obtained.
as to reach one of the edges of the specimen, note the deviation
in the report. 12. Precision and Bias
9.5 Test not less than five specimens in each of the principal 12.1 Precision:
film or sheeting directions. 12.1.1 Table 1 and Table 2 are based on a round robin4
conducted between 1986 and 1990 in accordance with Practice
10. Calculation E691 – 87, involving seven materials tested by seven labora-
10.1 For thin films and sheeting that have load-time charts tories. For each material, all the samples were prepared at one
characterized by Fig. 1, calculate the average tear propagation
force by averaging the load over a 25.4 mm (1 in.) interval, 4
Supporting data on precision are available from ASTM Headquarters. Request
disregarding the initial and final portions of the curve. RR:D20-1177.
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TABLE 2 Tear Propagation Resistance (Trouser Tear) Transverse in Practice E691 to generate data specific to their materials and
Direction (Values Expressed in Units of Grams-Force) laboratories (or between specific laboratories). The principles
Material Average Sr A SR B rC RD of 12.1.2 – 12.1.2.3 would then be valid for such data. )
Polystyrene 3.86 0.46 3.08 1.28 8.63 12.1.2 Concept of r and R in Table 1 and Table 2—If S r and
Polyester 32.47 1.74 3.68 4.86 10.31
LDPE—LD 278.6 12.21 30.29 34.18 84.40 SR have been calculated from a large enough body of data and
104 for test results that were averages from testing five specimens
Polypropylene 326.2 49.67 124.9 139.1 349.7 for each test result, then:
LLDPE 372.5 26.69 31.68 74.74 88.70
HDPE No. 2 452.6 24.68 31.28 69.10 87.59 12.1.2.1 Repeatability—Two results obtained within one
HDPE No. 1 549.7 64.10 105.4 179.5 295.0 laboratory shall be judged not equivalent if they differ by more
A
S r = within-laboratory standard deviation for the material stated. It is obtained by than the “r” value for the material. “r” is the interval repre-
pooling the standard deviations of the test results from each laboratory, as follows: senting the critical difference between the two test results for
Sr = [(^(S1) 2 + (S2) 2 ... + (Sn) 2)/n]1/2
B
SR = between-laboratories standard deviation for the material stated. It is a the same material, obtained by the same operator using the
pooling of the amounts by which the average of the test results for each laboratory same equipment on the same day in the same laboratory.
deviate from the overall average for that material.
C
r = within-laboratory repeatability limit = 2.8 × Sr.
12.1.2.2 Reproducibility—Two test results obtained by dif-
D
R = between-laboratories reproducibility limit = 2.8 × SR. ferent laboratories shall be judged not equivalent if they differ
by more than “R” value for that material. “ R” is the interval
representing the critical difference between two test results for
source, and randomized sections of film were sent to each of the same material, obtained by different operators using differ-
the laboratories which prepared the test specimens and tested ent equipment in different laboratories.
them. Each test result was the average of five determinations. 12.1.2.3 Any judgment in accordance with 12.1.2.1 or
Each laboratory obtained two test results for each material. 12.1.2.2 would have an approximate 95 % (0.95) probability of
(Warning—The explanation of r and R (12.1.2 – 12.1.2.3) are being correct.
only intended to present a meaningful way of considering the
approximate precision of this test method. The data in Table 1 12.2 Bias—There are no recognized standards to estimate
and Table 2 should not be applied to acceptance or rejection of the bias of this test method.
materials, as these data apply only to the materials tested in the
round robin and are unlikely to be rigorously representative of 13. Keywords
other lots, formulations, conditions, materials, or laboratories. 13.1 plastic film; single tear; tear; tear-propagation; thin
Users of this test method should apply the principles outlined sheeting; trouser
SUMMARY OF CHANGES
Committee D20 has identified the location of selected changes to this standard since the last issue (D1938 - 08)
that may impact the use of this standard. (December 1, 2014)
(1) Corrected a figure reference in 7.1. (3) Removed permissive language found in Section 6.
(2) Corrected a decimal error for a metric conversion in 6.2.
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