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Lab Internals

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Sudheer Babu
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5 views

Lab Internals

Internal

Uploaded by

Sudheer Babu
Copyright
© © All Rights Reserved
Available Formats
Download as PDF or read online on Scribd
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LAB INTERNAKS Determination of ‘fe (a0 present in cement experiment PART A’ Preparation eo atandoxd solution of Afsoclium Aas a ETA . A. Sanclosrd solution 4 Ebt i prepared diswolving a Known ammount ef the dligodium salt ‘eh Epta with Se ammonia and mode up with deionised water in A asoee dtandore fink ! koelght of EDTA 4 Molarity of ora = NOV URY sae . Molecular we a) EDTA salt (971224) PART B4 Estimation of (Cad im cement: 4) Standard: EDTA soluion Bure tte Conia fLosks % Ast by Coment solution + Mee oe + sed {ycerine + Beco, dietrayt. Quine « Trai cortoy © Patton and Reeders indicator End point + Wine wed +0 Clears but Cateusationss Prom the Volume, of ETA “Consumed the Portentaqe ef Cao ‘in rhe given cement Aolution ig calowrated - | TT IA recente CODe qiven Ware tnduuhiat waler- Recoral of observation ae weight OL FAS = Iegr8q &+ Volume oF FAS consumed In the back titration = 3HCe 3+ Nome 0} FAS consumed. in bank fitration = 4Se1¢¢ “He Nolerulos .wotght of FAS salt = 342q S+ Volume of waste water = 250 TO talewtote ‘top’ - “Janye £ (-W) XP x 8x lo00 vos) : WHEL V2 > Volume 6 FAS for blank titration 4g I¢c : Ny = Volume Of FAI fos Jack titration Buen: t= Novmodity , 4 FAS = weight ct EASaly OSM PN na Eqyaivolent wotgne’ of FAS 342 ok LN =o d1en = (hs si x bane Bx 07 ary 2 L(x 0:0) Gee = 63-436 myline 63-436 mal Were os ppm Ah oxygen “+ Cop Caample) 12x 8000, os COP CSampl) = Colorimnetste estimation of_copper_in given copper iujatiene Aolution - Protedure: woriting? | candards soluriom oy copper re prepared as Different 3 Joutows * rocky £) 0116) 20ce ANE ungnown Copper AUIpRate sowxion are taken 30 MOLE SLA» flasks. SCe of Ammonia olution 18 oalea 4o each Of them and mode up to ere reark. fr bank Jolwsion \F Preapred in a. eee = TEE tam Aepeiaie standard jiask by using See OF Arntoonia. ven a voove length dee ; Burorie vending (v2) = S+See «Lou 04" ac rsture solution = S0¢¢ i Fqusvaiens weld a Hl = 86S! Equine wWeghE CHstoodt S60 bi Normatity of Naow =O+F Wormatity oh HCl = Ly ; eal Naor XVp, ie 65 Total vot of oid 80 W ye Ode : paven gy OL RCL = orbs ‘ ; fol Nig acl Equot OE HCH = WU x36: 5 paeUO2X,Bb-S = jeueaey tind a tristoort = iS We WOK VOR Tal amouns o 20d, eee 6 ont gS arog SO SHENG I o4 “crstoon | = Nergcoow’ * Fapwt = 003s x §0 zl 2st gl. Do ay Vivo~ votee 12 = Colour a the COMP between aivatert Calcium Ford and evivenvome BAK Tin basic Zolution is Te tums Ted tohon tk Jorn O Complex with calc ern as EBT ts bie fn Colour and tt tur ted Tha patton and reeders indicator ts blue tolour when tt is nok complered with calcu ions Foecause endpoint otuuys wohon olution turns ue? ina coting Hot tor -PR Compler Fong been Compurtly aep taced by the tot — EDTA Comnplen Onc gre pR indiconon eds TUL Colour toe have to add Snchzo Fet> on fe tk reduce Revvic ior 10 FRrvOUs for ond a Bignt excess ts added to ensure complete edu gfe us + BAch 2 2FeCh + SnCu 44 we add Potasium Jeviayonide TL combine - stoly varth furrous jon tO form adeep but gervous fet oyonde compiex: Thus gertour ion a pot availa {oy yeootion with potartum dichon™ pnd end foint connok ve detected i ivvever & DATE: LJ ! oF o | N Re ’ fe 5 Rusk LOW: \ 3, Fewoin ‘AN. : mye 4 | Jian ‘ at, les | fe as i > Buisn rer : viscosity a He gowsion {3 inversely propotionat 40 bermperature Stqnigi idk en 4 blank tHraseR polwtion in (olomettic erinnent i i peri 4 Te ralify tee absorbance coussd cure tp the coloring Impurities praent tn he Venger ee a | emi h) os Se ‘ai “onc feo order) Thr pyoer of teil conguctviles ( a mg \j Ht) OH >CY 7 CH3000 v vob u 3x0 98 1 br ¢ The emf oh Reel in potensfomerric fitration depends o ond ichromatke 10N- ‘or cy? | cst Servic ion Trcrenting order my Osiottres cryin 4 cckatnone eerttg tone COOH (H3(00H 7 cCrehe(o0H> cHreLeoo4 D>CH3 (004 |

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