PRC 5001 Current
PRC 5001 Current
Engineering Directorate
June 2020
REVISIONS
REVISION DESCRIPTION DATE
-- Original version 5/96
A PRC reviewed and updated for accuracy. Author change. 8/5/99
TABLE OF CONTENTS
1.0 SCOPE ........................................................................................................................................... 4
2.0 APPLICABILITY.............................................................................................................................. 4
3.0 USAGE ........................................................................................................................................... 4
4.0 REFERENCES ............................................................................................................................... 5
5.0 MATERIAL REQUIREMENTS ........................................................................................................ 6
5.1 Cleanliness Levels ...................................................................................................................... 7
5.2 Non-Precision Cleanliness Levels ............................................................................................... 7
5.3 Precision Cleanliness Levels ....................................................................................................... 8
5.4 Specifying Cleanliness Level ....................................................................................................... 8
5.5 Cleaning ...................................................................................................................................... 9
5.6 Rough Cleaning........................................................................................................................... 9
5.7 Precision Cleaning .................................................................................................................... 10
5.8 Special Cleaning Processes ...................................................................................................... 10
5.9 Cleaning Compatibility ............................................................................................................... 10
5.12 Test Fluids for Precision Cleanliness Verification .................................................................... 12
5.13 Drying and Testing Gas ........................................................................................................... 12
5.14 Protecting Cleaned Surfaces ................................................................................................... 12
5.15 Handling Clean Parts............................................................................................................... 13
5.18 Identification of Cleaned Items ................................................................................................ 13
5.19 Access Controls and Storage of Cleaned Items....................................................................... 14
5.20 Certification ............................................................................................................................. 14
6.0 PROCESS REQUIREMENTS ....................................................................................................... 16
7.0 PROCESS QUALIFICATION ........................................................................................................ 15
8.0 PROCESS VERIFICATION ..........................................................................................................17
8.1 NVR......................................................................................................................................... 17
8.2 Particle Counts .........................................................................................................................17
8.3 Drying ....................................................................................................................................... 17
9.0 TRAINING AND CERTIFICATION ................................................................................................ 16
10.0 DEFINITIONS ............................................................................................................................. 17
1.0 SCOPE
2.0 APPLICABILITY
This process specification applies to cleaning of flight hardware including ground support
equipment (GSE) after fabrication (prior to assembly, after assembly, and/or prior to
delivery). It does not apply to in process cleaning during manufacturing (such as surface
preparation for bonding or coating), except the descaling of stainless-steel parts.
3.0 USAGE
All parts, components, assemblies, subsystems, systems and related equipment requiring
cleaning shall be clean to the specified cleanliness level and inspected in accordance with
this specification. This process specification shall be called out on the engineering drawing
by using a drawing note that identifies the process specification to be used and the required
level of cleanliness. Consult the Materials and Processes Branch and the NASA procuring
activity for approval of alternate specifications.
Work requests for cleaning at JSC shall be made via JF 1615 Clean Room and Laboratory
Request form or work order.
It is the responsibility of the users of this specification to review pertinent Safety Data Sheets
(SDSs) and materials specification to assure safety of the personnel, protection of the
environment and facilities in fulfilling the requirements of this document.
4.0 REFERENCES
The following applicable documents are an extension of the requirements and information
given in this specification. All documents listed assumed as the current revision unless a
specific revision listed. Refer any conflicts between the documents referred in this list to the
Materials and Processes Branch.
MPCV 70156 Cross Program Fluid Procurement and Use Control Specification
At JSC, cleanliness level requirements are defined in JPR 5322.1 Contamination Control
Requirements Manual Table 3-1 Surface Cleanliness Levels for particulate and nonvolatile
residue.
The surface cleanliness levels in JPR 5322.1, KSC-C-123 or this PRC are acceptable
alternates to the levels in IEST-STD-CC1246. (The detailed numbers of particles allowed in
each size bin vary slightly. This difference is not technically significant).
Generally Clean (GC): hardware shall be free from manufacturing residue, dirt, oil, grease
etc. The GC level should be used for hardware that is not sensitive to contamination and is
easily cleaned or recleaned. This level should be used for hardware items that do not require
cleaning before inspection. Cleaning and recleaning is required only if the item does not
pass GC inspection.
Visibly Clean (VC): hardware shall be free of all particulate and nonparticulate matter visible
to the normal unaided eye or corrected vision eye with a specified illumination using incident
lighting. Incident lighting for inspection of large acreage hardware shall be achieved by the
use of a handheld lighting source.
The contractor shall document and maintain evidence of inspection and acceptance criteria.
Table 1 outlines the levels of VC requirements, incident light levels and inspection distances
(reference GSDO-RQMT-1080, Cross-Program Contamination Control Requirements). JPR
5322.1 references these same requirements and Section 3.2 provides detailed inspection
requirements for the VC level. The VC level is standard unless otherwise specified as
sensitive (VC-S) or highly sensitive (VC-HS).
NOTES:
(1) One-foot-candle (lumens per square foot) is equivalent to 10.76 lumens per
square meter.
(2) Cleaning is required if the surface in question does not meet VC under the
specified incident light and observation distance conditions.
For all VC levels, inspect areas of suspected contamination may be inspected at closer
distances than specified above. VC level inspections are limited to exposed and accessible
surfaces. The use of inspection aids such as wipes, mirrors, borescopes, or tape lifts is
permissible for those areas of suspect condition with limited or no direct line of sight.
Allow closer inspection of piece parts when minimum inspection distance specified for the required
cleanliness level is impractical (for example, having to hold parts cleaned to level VC Standard 1.5
m [5 feet away].
Contractor shall inspect interior volumes at a distance that deviates from the defined range only
to the extent required when sufficient access to physically conduct an inspection within the
defined VC range.
The Visibly Clean, Ultraviolent level (VC+UV) inspection uses the aid of an ultraviolet light
source (black light) of 3200 to 3800 angstroms wavelength. This level requires precision
cleaning methods, but particle count is not required.
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A visual observation of the part must be performed with the unaided eye (corrective lenses are
acceptable) under UV light (3,200 to 3,800 angstroms wavelength) for the presence of
hydrocarbons., If the surface is inaccessible. The inspector shall perform a wipe test.
Any contamination detected by visual or black light inspection shall be cause for re-cleaning. If
re-cleaning fails to remove fluorescent indications, investigate to determine if the item material is
naturally fluorescent. Contractor shall inspect parts as specified in JPR 5322.1.
Cleanliness levels for hardware items shall be determined by program and system requirements
specified in the following examples:
a. Level 200 refers to size and count limits on particulate matter contamination only.
c. Level 200A refers to size and count limits on particulate matter and nonvolatile
residue (NVR) contamination limits.
d. Level 200 A is a more stringent cleaning level than 200B for both particulate matter
and NVR.
e. A component cleaned to a more stringent level than required for a system level
application may be used in a system application. (i.e., a Level 200A part may be
used in a Level 300 or 300A system)
f. The GC and VC cleanliness levels do not use particle counting or NVR methods.
However, the VC-Sensitive (VC-S) cleanliness level is considered to be more
stringent that IEST-STD-CC1246 Level 500, which is sometimes called out for
visual cleanliness by other organizations.
5.5 CLEANING
Poor handling and exposure to contamination can easily compromise the state of
cleanliness. The intent of this section is to specify those general requirements applicable
to cleaning processes. There are two categories for cleaning: precleaning (rough) and
precision cleaning. Cleaning contractor shall control all cleaning processes with
documented procedures approved by the NASA JSC Materials and Processes Branch. At
JSC, procedures are detailed process instructions (DPI) or standing operation procedures
(SOPs). The cleaning methods selected and used depend on the material selection for the
fabricating parts. Since the characteristics of the assemblies or components vary, this
section does not describe all cleaning methods and processes. At JSC, details of which
cleaning solutions and solvents to use for which materials are in DPI-5001-04 Hardware
Cleaning and DP1-5001-06 Cleanliness Verification Using Deionized Water and Total
Carbon Analyzer and DPI-5001-07 Final Cleaning and Cleanliness Verification of Precision
Cleaned Aerospace Hardware.
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Assembled items that do not lend themselves to this type of treatment must be treated
prior to assembly. Surface treated areas degraded during subsequent fabrication and
assembly shall be reprocessed as required to restore the original protective finish.
All steps in pre-cleaning procedures must progress in an uninterrupted workflow through the final
rinse and drying operation. If the workflow is unavoidably interrupted, a recycling operation shall
be specified in the pre-cleaning procedure. Pre-cleaning procedures include, as a minimum,
protection of the item by interim packaging or other approved means to prevent recontamination
through all subsequent operations.
Hardware that requires a level of product cleanliness greater than the level detected by
visual means and cleanliness verification by particle analysis and/or nonvolatile residue
analysis shall be precision cleaned. Parts/items shall be inspected to the visibly clean (VC)
level prior to precision cleaning.
Special attention to cleaning convoluted flex hoses is required. All convoluted flex hose
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components shall be cleaned and dried in a vertical orientation. For cleanliness verification,
the fluid sample must be collected while the flexhose is in the vertical position.
b. Non-explosive.
c. Noncorrosive under normal use.
d. Nonflammable.
e. Environmentally sound.
f. Compatible with the system, product materials and hardware.
NOTE:
(i) The cleaning contractor must verify complete solvent removal after final cleaning.
(ii) This does not limit potential cleaning fluids only to nonflammable fluids
(iii) Combustible cleaning agents must be used with care to clean systems or products that
may combust the cleaning agent during cleaning; or even at a later time such as when
the system or product is packaged, stored, used, etc.
Compatibility issues that must be evaluated before selecting a cleaning process are:
a. Corrosion
b. Embrittlement
c. Leaching
d. Residue
e. Crazing (non-metallics)
f. Reversion (non-metallics)
g. Hydrolysis (non-metallics)
For all cleaning fluids, establish, document, and implement requirements and procedures
that control fluid composition, purity, cleanliness, and use. Cleaning fluids selected for use in
pre-cleaning solutions shall be controlled by analysis, solution replacement, or adjustment to
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maintain cleaning effectiveness and compatibility with the specific material type.
The cleaning contractor must maintain records indicating the scheduled analysis, analysis
results, and any solution replacement or adjustment activities.
For passivation and pickling baths at JSC, control tank chemistry per PRC-5002 Process
Specification for Passivation and Pickling of Metallic Materials.
All fluids, equipment, and facilities used for cleaning to the VC or VC + UV cleanliness levels
shall be subject to the same minimum requirements specified for pre-cleaning procedures.
Cleaning with an approved, compatible solvent (e.g., solvent wipe) is mandatory for VC and
VC + UV items, unless other methods required by the hardware in question. GC items do
not require cleaning before inspection; cleaning is required only if the item does not pass GC
inspection. Use a GC cleaning process compatible with the hardware materials.
Test fluids shall be selected by the user and approved by the NASA procuring activity.
At JSC, HFE-7100 and high purity deionized water are approved test fluids and used for
precision cleaning. Analyze final flush and verification fluids for precision cleanliness for NVR
prior to use to determine compliance with the stipulated specification requirements.
Nonvolatile residue for HFE-7100 shall not be greater than 10 milligrams per one liter (mg/L)
as determined by SSP 30573.
Isopropanol (IPA) must meet the requirements of TT-I-735A filtered to 10 microns or better
prior to use.
Aqueous based fluids must utilize reagent grade water. The reagent water must meet the
requirements of ASTM D1193, Type II except that silica content is not required. Milli-Q water
is a permissible substitute for reagent water. If water is the verification fluid, it must meet the
requirements of Grade A water in JSC-SPEC-C-20D
Cleaning contractor shall use facilities for precision cleaning, assembly, processing and
functional testing of the hardware that provide airborne contamination levels compatible
with the hardware cleanliness requirements per JPR 5322.1 Contamination Control
Manual or the engineering drawing. Clean rooms and other environmentally controlled
areas (ECAs) shall be controlled by approved documented procedures.
Package all visibly cleaned and precision-cleaned items immediately after cleaning and
drying in accordance to packaging methods per JPR 5322.1 Contamination Control
Manual or approved documented procedures using materials that are compatible with the
item to be protected.
Refer to JSC 29253 “SR&QA Recommendation for Clean Room Gloves” for gloves for wet
and dry handling of hardware. Clean room gloves shall be worn when handling VC
cleaned and precision cleaned parts. Gloves are not required for handling generally clean
parts. Any hardware not precision cleaned shall not be brought into the vicinity of
precision cleaned hardware without protecting the precision cleaned hardware.
5.16 FILTERS
Ground support test equipment that interfaces with precision cleaned flight fluid systems
must incorporate filters and located as close to the interface as possible where flow could
occur into the flight hardware. This may also include outlet lines if it is determined that
some operations such as servicing and describing fluids could permit flow in a reverse
direction.
5.17 INSPECTIONS
Only trained and/or certified personnel must perform disassembly, cleaning and inspection
operations on cleaned parts. Accomplish non-UV visual inspection under a white light of
sufficient intensity to illuminate the surface being inspected.
Inspect stored precision-cleaned items periodically, at least once every two (2) years for
the integrity of the outer bag and, on a sample basis, for corrosion or other degradation of
the packaged item. To inspect, remove the outer bag and visually inspect the item through
the inner wrap. Any discoloration, visible contamination, etc., shall be cause for rejection
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and re- cleaning of the lot sampled. If the part passes inspection, apply a new outer bag
and reseal in the normal manner.
Cleaning contractor shall use documented procedures for packaging clean items. The
GC level does not require a cleanliness certification decal, since protective packaging
for contamination control is not required. Liquid oxygen (LOX) and gaseous oxygen
(GOX) parts, components, subsystems, and systems shall be protected by an inner
bag of LOX/GOX-compatible film, as specified in JPR 5322.1.
Identify the bagged item with a decal containing identification, inspection, and certification of
cleanliness information. Decals procured to meet the requirements of this section are not
intended for direct application to parts or equipment; therefore, the decals need not be
compatible with fuels or oxidizers. Apply decals to the outside of the inner bag and over the
ends of tape-sealed closures. Decals shall include:
b. Date of Cleaning
e. Acceptance stamps
f. Cleanliness Level
NOTE: Do not use preservative materials on items, which have been precision-cleaned.
Package dissimilar metals together.
Establish adequate controls and procedures to limit access to storage areas for precision-
cleaned items to personnel specifically trained in the handling of precision-cleaned items.
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Remove clean and precision-clean, packaged items from the clean room and place in an
appropriate container or storage area to protect the plastic bags and contents.
Store all cleaned and precision-cleaned items in an enclosed, controlled area where
temperature and humidity maintained within limits compatible with the item and its
packaging material. Filter the air supply through an industrial-grade filter. Maintain the
enclosed area in a manner consistent with good housekeeping practices. Establish and
document periodic cleaning schedules.
5.20 CERTIFICATION
The cleaning contractor shall adhere to the applicable contamination control requirements
of
this specification and JPR 5322.1 Contamination Control Manual. The contractor shall
perform periodic certifications to establish and implement the requirements for clean rooms,
clean work areas or other environmentally controlled areas. The certification process shall
use established and documented procedures.
At JSC, the Safety and Mission Assurance Directorate has the approval authority for the
certification.
Perform all work to written procedures. The work instructions shall contain sufficient detail to
ensure that the manufacturing process produces consistent, repeatable products that comply
with this specification.
For work performed at JSC facilities, these work procedures consist of Detailed Process
Instructions (DPI’s).
For contracted work, the contractor shall be responsible for preparing and maintaining, and
certifying written work procedures that meet the requirements of this specification.
For the introduction of new materials, cleaning solutions, cleaning solvents or the
development of new cleaning processes not documented by existing procedures, the
Materials and Processes Branch must be consulted to approve materials, cleaning
processes and address compatibility concerns. Materials or sample parts that duplicate for
use in the new process must be tested to demonstrate compatibility and to qualify the
process.
a. Proposed cleanliness levels including analysis and rationale for the selected
cleanliness level.
b. Descriptions of items to be cleaned including identification of materials including
trade names, specifications, chemical and physical properties and compatibility
information.
c. Cleaning fluids information to include as applicable, trade names, specifications,
safety data sheet, chemical and physical properties, and compatibility information.
d. Processing equipment and cleaning procedures to be used (e.g. ultrasonic
equipment, precision cleaning).
e. Quality assurance provisions. This must include inspection(s) and in-process
control procedures to prevent contamination, latent corrosion, or other degradation
of surfaces and opened systems.
f. Controlled environment levels maintained for cleaning and handling.
g. Preservation methods and materials.
h. Verification method.
Consult the Materials and Processes Branch and the NASA procuring activity for approval
alternate verification procedures.
Following precision cleaning, each item shall be rinsed with an appropriate amount of unused
precision-cleaning solvent usually (100 mL) for each square foot of critical surface. Determine
non-volatile residue (NVR) in accordance with ASTM D2109-01. If high purity water is the
final rinse solution for verification, hydrocarbon content shall be determined using total
organic carbon (TOC) analyzing techniques per ASTM G144-01.
8.3 DRYING
Flammable solvent used for cleaning, flushing, or testing the residual concentration of
flammable solvent shall be verified as within acceptable limits. Positive verification requires
purging with an inert gas and a 24-hour lockup” of the component or assembly at a
minimum temperature of 15 °C. Analysis of lockup gas samples to shall be verified that the
solvent concentration does not exceed 18 ppm when measured as methane or 10 ppm
when measured using an instrument calibrated to the specific solvent utilized and capable
of detecting 1 ppm.
The cleaning contractor must provide training for all personnel performing contamination
control and ECA operations per JPR 5322.1 and all operations that encompass their
particular job responsibilities. The training certification course shall establish requirements
for personnel working with precision-cleaned hardware. The cleaning contractor shall retrain
and recertify all personnel at a specified time interval. Training records and certifications
must be kept with traceable documentation.
Personnel requiring entry into the ECA on a visit or on a temporary basis must be trained
basic ECA and contamination control disciplines. The ECA supervisor controls access to the
ECA for visitors or temporary workers for overpopulation prevention or ECA compromise.
10.0 DEFINITIONS
Visibly Clean + Ultraviolet (VC + UV) Visibly clean (as defined above) and without
fluorescent matter detectable with a UV light (black
light) of 3,200 to 3,800 angstroms wavelength