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14 views

Continue of Research

Uploaded by

Ahmed Mansour
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© © All Rights Reserved
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Comparison between flame atomic absorption spectroscopy and graphite

furnace or electrothermal atomic absorption spectroscopy .

Flame atomic Graphite furnace


absorption or
spectroscopy electrothermal
AAS
Advantages 1-Inexpensive 1-All sample used
2-Easy to use 2-Longer time of
3-High precision sample over light
source
3-lower limit of
detection
Disadvantages 1-No sample 1-slow
efficiency 2-not as precision
2-small amount of as flame
sample needed in 3-expensive
light
3- need large
quantity of sample

PAGE 15
Atomization :
Process of convertion of analyte from liquid to vapour in atom scale
Need high temperature
Flame atomic absorption spectroscopy :
Steps :
I. Nebulization : solution sample before against it to flame must convert it to
droplets (spray)
II. Desolvation : separation of analyte from solution (solvent) to be easy to separate
and continue process
III. Vaporization : convertion of analyte to gas phase and as it is in molecule
IV. Dissociation : break up gas phases molecule into atoms
V. Ionization : break up gas phases into atom but in charged shape
*Both IV and V are types of Atomization
VI. Excitation : continue process with light or heat

PAGE 16
Refrences :
• "TAS-990 Atomic Absorption Spectrophotometer-纳米材料工程研究
中心". ercn.henu.edu.cn. Retrieved 2022-10-12.
• "Robert Bunsen and Gustav Kirchhoff". Science History Institute.
Retrieved 20 March 2018.
• McCarthy, G.J. "Walsh, Alan - Biographical entry". Encyclopedia of
Australian Science. Retrieved 22 May 2012.
• Koirtyohann, S. R. (1991). "A History of Atomic Absorption
Spectrometry". Analytical Chemistry. 63 (21): 1024A–1031A.
doi:10.1021/ac00021a716. ISSN 0003-2700.
• L'vov, Boris (1990). "Recent advances in absolute analysis by graphite
furnace atomic absorption spectrometry". Spectrochimica Acta Part B:
Atomic Spectroscopy. 45 (7): 633–655. Bibcode:1990AcSpe..45..633L.
doi:10.1016/0584-8547(90)80046-L.
• "Analytical Methods for Graphite Tube Atomizers" (PDF). agilent.com.
Agilent Technologies. Archived (PDF) from the original on 2022-10-09.
• "Atomic Spectroscopy - GF-AAS". sites.chem.utoronto.ca. Retrieved
2021-03-08.
• Harvey, David (2016-05-25). "Atomic Absorption Spectroscopy".
chem.libretexts.org. Archived from the original on 2017-10-06.
Retrieved 2017-10-06.
• "Sample Atomization – Atomic Absorption Spectroscopy Learning
Module". blogs.maryville.edu. Retrieved 2017-11-02.
• Walsh, Alan; Becker-Ross, Helmut; Florek, Stefan; Heitmann, Uwe (19
January 2006). High-Resolution Continuum Source AAS. Weinheim:
Wiley-VCH Verlag GmbH & Co. KGaA. p. 2. ISBN 9783527307364.
• Rakshit, Amitava. "Basics of Laboratory Safety: Common laboratory
rules and regulations". The International Association for Ecology.
Intecol. Archived from the original on 27 September 2016. Retrieved
26 September 2016.

PAGE 17

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