Operating Instructions

Stamolys CA71SI
Silicate Analyser

BA364C/07/en/06.04
51512332
Valid of:
Software version 5.4
 Brief overview

AUTO MESSEN

3 30
38

163

15
M CE E K

110
Ø 27
15 9 Photometer +17V Photometer -17V Photometer 0V fx
Analog Out Kanal 1
Channel 1
Kanal 2
Schirm/ MP5 MP6 Channel 2
0/4-20mA
250 BK 65 COM
F4 M 0.2 A M 0.2 A Screen 28 22 16

ALARM 2
F5

ALARM 2
330

OPTION
Schirm
GN 64 0V BK 58 40 NC
160 Schirm Schirm
Screen
keine Probe
27 21 15
80 75 V4 70 Screen BN 63 -17 V YE 57 39 I2 + NO
Screen No sample
15 140 OR 79 74 V3 69
n.b.
WH 62 +17 V WH 56 Reserve 38 I2 - COM
26 20 14

SCHRITTMOTOR
n.c. 25 19 13

STÖRUNG
STEP MOTOR

ALARM 1
100

ALARM 1
Mess 2

ERROR
n.b. n.b.
BK 78 73 V2 68 YE 61 fx 55 37 31 NC
n.c. Meas 2 n.c.
60
24 18 12
n.b. n.b.

LEAK S.
+24V

LECKF.
RD 77 72 V 1 BU 67 60 54 36 I1 + 30 NO
n.c. n.c. 23 17 11
71 0 V BN 66 Status GN 53
A
YE 76 GY 59 0V 35 I1 - 29 0V RELAIS / Relay:
max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC

120
D
Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!!

243

Ø 26
Terminals voltage to ground even when the unit is switched off !!!

200
F2 NETZ
AC Motor MAINS
7 L2

Ø 21
T 0.1A

165
M E K

125

AC MOTOR
N 3 L

47
6
RS 232
L1 Elektronik F1 N
5 2

555
524
Electronics

580
648
4 PE T 0.5A 1 PE

78
119
326

Ø 21
Ø 26
ENDRESS+HAUSER R
STAMOLYS CA 71
360 207
436

B C

1 2 3

12 4

M E K RS 232

11 5

155 131 134

3
2
P 1
161 160 120 200
R S
10 6
P

A
130 154

123 131 144 140 120

9 8 7
P

E
130 120

A 121
143
B
141

170/171
142

S R1 R2 R3

P 121 122 B
P

135 135

F
C07-CA71XXx-00-08-00-xx-100.eps

Page 9 Analyser overview: most important parts

Page 10 Dimensions, installation conditions

Page 13 Installation and installation examples

Page 16 Terminal assignment, signals, switching contacts

Page 24 Operation: parameter entry and configuration

Page 30 Calibration
Page 48 Operating matrix
Page 32 Commissioning

Page 34 Maintenance schedule

Page 35 Replacing spare and wear parts
Page 40 Accessories

Page 41 Trouble-shooting instructions

Page 43 Spare parts

Page 46 Technical data

Endress+Hauser
Stamolys CA71SI

Table of contents
1 Safety instructions . . . . . . . . . . . . . . . . 4 8 Accessories . . . . . . . . . . . . . . . . . . . . . 40
1.1 Designated use . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 8.1 Collecting vessel . . . . . . . . . . . . . . . . . . . . . . . . . . 40
1.2 Installation, commissioning and operation . . . . . . . . 4 8.2 Reagents, cleaner, standard solution . . . . . . . . . . . . 40
1.3 Operational safety . . . . . . . . . . . . . . . . . . . . . . . . . . 5 8.3 Hose cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
1.4 Return . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 8.4 Additional accessories . . . . . . . . . . . . . . . . . . . . . . 40
1.5 Notes on safety icons and symbols . . . . . . . . . . . . . . 5
9 Trouble-shooting . . . . . . . . . . . . . . . . . 41
2 Identification . . . . . . . . . . . . . . . . . . . . 6 9.1 Trouble-shooting instructions . . . . . . . . . . . . . . . . . 41
2.1 Device designation . . . . . . . . . . . . . . . . . . . . . . . . . 6 9.2 System error messages . . . . . . . . . . . . . . . . . . . . . . 41
2.2 Scope of delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 9.3 Process errors without messages . . . . . . . . . . . . . . 42
2.3 Certificates and approvals . . . . . . . . . . . . . . . . . . . . 8 9.4 Spare parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
9.5 Return . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
3 Installation . . . . . . . . . . . . . . . . . . . . . . 9 9.6 Disposal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

3.1 Analyser overview . . . . . . . . . . . . . . . . . . . . . . . . . . 9

3.2 Incoming acceptance, transport, storage . . . . . . . . . 10
10 Technical data . . . . . . . . . . . . . . . . . . . 46
3.3 Installation conditions . . . . . . . . . . . . . . . . . . . . . . 10 10.1 Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
3.4 Installation instructions . . . . . . . . . . . . . . . . . . . . . 13 10.2 Output . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
3.5 Installation examples . . . . . . . . . . . . . . . . . . . . . . . 14 10.3 Power supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
3.6 Post-installation check . . . . . . . . . . . . . . . . . . . . . . 15 10.4 Performance characteristics . . . . . . . . . . . . . . . . . . 46
10.5 Environment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
4 Wiring . . . . . . . . . . . . . . . . . . . . . . . . 16 10.6 Process . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
10.7 Mechanical construction . . . . . . . . . . . . . . . . . . . . 47
4.1 Electrical connection . . . . . . . . . . . . . . . . . . . . . . . 16
4.2 Signal connection . . . . . . . . . . . . . . . . . . . . . . . . . 18
4.3 Switching contacts . . . . . . . . . . . . . . . . . . . . . . . . 19
11 Appendix . . . . . . . . . . . . . . . . . . . . . . . 48
4.4 Serial interface . . . . . . . . . . . . . . . . . . . . . . . . . . . 20 11.1 Operating matrix . . . . . . . . . . . . . . . . . . . . . . . . . . 48
4.5 Post-connection check . . . . . . . . . . . . . . . . . . . . . . 21 11.2 Ordering forms . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
11.3 Analyser settings . . . . . . . . . . . . . . . . . . . . . . . . . . 54
5 Operation . . . . . . . . . . . . . . . . . . . . . . 22 11.4 Maintenance schedule . . . . . . . . . . . . . . . . . . . . . . 56

5.1 Operation and commissioning . . . . . . . . . . . . . . . . 22

5.2 Display and operating elements . . . . . . . . . . . . . . . 22
Index . . . . . . . . . . . . . . . . . . . . . . . . . . 57
5.3 Local operation . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
5.4 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

6 Commissioning. . . . . . . . . . . . . . . . . . 32
6.1 Function check . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
6.2 Switch-on . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

7 Maintenance. . . . . . . . . . . . . . . . . . . . 34
7.1 Maintenance schedule . . . . . . . . . . . . . . . . . . . . . . 34
7.2 Replacing reagents . . . . . . . . . . . . . . . . . . . . . . . . . 35
7.3 Replacing pump hoses . . . . . . . . . . . . . . . . . . . . . . 35
7.4 Checking the sample flow rate . . . . . . . . . . . . . . . . 37
7.5 Replacing valve hoses . . . . . . . . . . . . . . . . . . . . . . 37
7.6 Replacing the static mixer . . . . . . . . . . . . . . . . . . . 38
7.7 Replacing the photometer optical cell . . . . . . . . . . . 38
7.8 Cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
7.9 Placing out of service . . . . . . . . . . . . . . . . . . . . . . . 39

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Safety instructions Stamolys CA71SI

1 Safety instructions

1.1 Designated use

With 18% silicon is the second most frequent element of the earth crust. It occurs chemically
bonded as silicate or silicon dioxide in a variety of minerals. From these minerals silicate or silicic
acid is washed out in low quantities to waters.
There are no standard limits for drinking water since silicate is not known to be harmful to health.
But in boiler feed water and boiler water, there may be only low silicate concentrations. Under
thermal charge or under high pressure insoluble silicon dioxide is formed. It solidifies in boilers, heat
exchangers and turbine blades and thus reduces the heat exchanger’s efficiency or causes
overheating.
The standard limit for boiler feed water is 0.02 ppm silicic acid (SiO2). For injection and boiler water
the standard limits are pressure dependent. For example, at an operational pressure of 68 bar (986
psi), the concentration of silicic acid in boiler water must not exceed 10 ppb.
The analyser is a compact photometric analysis system.
It is designed for the almost continuous monitoring of the silicate content in ultrapure water and
boiler feed water.
In particular, the analyser is intended for:
• steam and condensate analysis
• reversed osmosis
• demineralisers.
Any other use than the one described here compromises the safety of persons and the entire
measuring system and is, therefore, not permitted.
The manufacturer is not liable for damage caused by improper or non-designated use.

1.2 Installation, commissioning and operation

Please note the following items:
• Installation, electrical connection, commissioning, operation and maintenance of the measuring
system must only be carried out by trained technical personnel.
The technical personnel must be authorised for the specified activities by the system operator.
• Technical personnel must have read and understood these Operating Instructions and must
adhere to them.
• Before commissioning the entire measuring point, check all the connections for
correctness. Ensure that electrical cables and hose connections are not damaged.
• Do not operate damaged products and secure them against unintentional
commissioning. Mark the damaged product as being defective.
• Measuring point faults may only be rectified by authorised and specially trained
personnel.
• If faults can not be rectified, the products must be taken out of service and secured against
unintentional commissioning.
• Repairs not described in these Operating Instructions may only be carried out at the
manufacturer’s or by the service organisation.

4 Endress+Hauser
Stamolys CA71SI Safety instructions

1.3 Operational safety

The analyser has been designed and tested according to the state of the art and left the factory in
perfect functioning order.
Relevant regulations and European standards have been met.
As the user, you are responsible for complying with the following safety conditions:
• Installation instructions
• Local prevailing standards and regulations.

1.4 Return
If the analyser has to be repaired, please return it cleaned to the sales centre responsible.
Please use the original packaging, if possible.

Please enclose the completed "Declaration of contamination" (copy the second last page of these
Operating Instructions) with the packaging and the transportation documents.
No repair without completed "Declaration of contamination"!

1.5 Notes on safety icons and symbols

Warning!

# This symbol alerts you to hazards. They can cause serious damage to the instrument or to persons
if ignored.

Caution!

" This symbol alerts you to possible faults which could arise from incorrect operation. They could
cause damage to the instrument if ignored.

! Note!
This symbol indicates important items of information.

Endress+Hauser 5
Identification Stamolys CA71SI

2 Identification

2.1 Device designation

2.1.1 Nameplate
Check the order code on the nameplate (at the analyser) with the product structure (see below) and
your order.

Stamolys CA71
order code / Best.Nr.: CA71SI-A10A2A1
serial no. / Ser.-Nr: 3B90003C3AN1

measuring range / Messbereich: 1-200 µg/l SiO4-Si

output 1 / Ausgang 1: 0/4-20mA, RS232C

output 2 / Ausgang 2: -
mains / Netz: 230VAC,50Hz,50VA

prot. class / Schutzart: IP 43

ambient temp. / Umgebungstemp.: +5°C .... +40°C

C07-CA71SIx-18-08-00-xx-001.EPS

Fig. 1: Example of a nameplate

2.1.2 Product structure

Measuring range
A Measuring range 1.0 ... 200 µg/l Si
B Measuring range 50 ... 5000 µg/l Si
Y Special version acc. to customer’s specification

Sample transfer
1 Sample transfer from one measuring point (one-channel version)
2 Sample transfer from two measuring points (two-channel version)

Power supply
0 Power supply 230 V AC / 50 Hz
1 Power supply 115 V AC / 60 Hz

Collecting vessel for up to 3 analysers

A Without collecting vessel
B With collecting vessel without level measurement
D With two collecting vessels without level measurement (two-channel version)

Housing version
1 Without housing
2 With GFK housing
3 With stainless steel 1.4301 (AISI 304) housing

Communication
A 0/4 ... 20 mA, RS 232

Additional equipment
1 Quality certificate
2 Quality certificate + set of inactive reagents
3 Quality certificate + three sets of inactive reagents

CA71SI - complete order code

6 Endress+Hauser
Stamolys CA71SI Identification

2.2 Scope of delivery

2.2.1 Version SI-A

The scope of delivery comprises:
• an analyser with mains plug
• a cleaning injector
• a tin of silicone spray
• a Norprene hose, length 2.5 m (8.2 ft), ID 1.6 mm (0.06")
• a Grifflex hose, length 2.0 m (6.56 ft), ID 19 mm (0.75")
• a C-flex hose, length 2.5 m (8.2 ft), ID 3.2 mm (0.12")
• two hose fittings of each size:
– 1.6 mm x 1.6 mm (0.06" x 0.06")
– 1.6 mm x 3.2 mm (0.06" x 0.12")
• two T-hose fittings of each size:
– 1.6 mm x 1.6 mm x 1.6 mm (0.06" x 0.06" x 0.06")
– 3.2 mm x 3.2 mm x 3.2 mm (0.12" x 0.12" x 0.12")
• an interference suppressor for the current output
• a screwed socket for the outlet pipe
• 4 edge covers
• a quality certificate
• Operating Instructions (English).

! Note!
Please, order reagents separately with analyser version CA71 XX-XXXXXX1.
With all other versions, inactive reagents are included in the scope of delivery. You have to mix the
reagents before using them. Please, read the mixing instructions attached to the reagents.

2.2.2 Version SI-B

The scope of delivery comprises:
• an analyser with mains plug
• a cleaning injector
• a tin of silicone spray
• a Norprene hose, length 2.5 m (8.2 ft), ID 1.6 mm (0.06")
• a C-flex hose, length 2.5 m (8.2 ft), ID 6.4 mm (0.25")
• a C-flex hose, length 2.5 m (8.2 ft), ID 3.2 mm (0.12")
• two hose fittings of each size:
– 1.6 mm x 1.6 mm (0.06" x 0.06")
– 1.6 mm x 3.2 mm (0.06" x 0.12")
– 6.4 mm x 3.2 mm (0.25" x 0.12")
• two T-hose fittings of each size:
– 1.6 mm x 1.6 mm x 1.6 mm (0.06" x 0.06" x 0.06")
– 3.2 mm x 3.2 mm x 3.2 mm (0.12" x 0.12" x 0.12")
• an interference suppressor for the current output
• 4 edge covers
• a quality certificate
• Operating Instructions (English).

! Note!
Please, order reagents separately with analyser version CA71 XX-XXXXXX1.
With all other versions, inactive reagents are included in the scope of delivery. You have to mix the
reagents before using them. Please, read the mixing instructions attached to the reagents.

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Identification Stamolys CA71SI

2.3 Certificates and approvals

2.3.1 4 approval
Declaration of conformity
The product meets the legal requirements of the harmonised European standards.
The manufacturer confirms compliance with the standards by affixing the 4 symbol.

2.3.2 Manufacturer certificate

Quality certificate
With the certificate the manufacturer confirms compliance with all technical regulations and the
successful testing individually for your product.

8 Endress+Hauser
Stamolys CA71SI Installation

3 Installation

3.1 Analyser overview

1 2 3

12 4

M E K RS 232

11 5

10 6

9 8 7
C07-CA71XXx-03-08-00-xx-001.eps

Fig. 2: Analyser (housing version, without hoses)

1 Reagents pump (P2), inlet from canister 7 Dosage loop (with CA71SI only)
2 Display 8 Valve V2
3 Serial interface RS 232 9 Sample resp. reagents mix outlet (left or right, acc.
4 Photometer optical cell to version)
5 Static mixer (acc. to version) 10 Valve V1
6 Valve V4 (version with sample outlet rightside 11 Channel switch: above channel 1, below channel 2
only) 12 Sample pump P1, inlet see below

Inlet to the sample pump:

• Valve V1
– hose in front: sample inlet
– hose at the back: inlet from valve V2 (cleaner or standard solution)
• Valve V2
– hose in front: inlet from canister with standard solution
– hose at the back: inlet from canister with cleaner (if used, depending on version)

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Installation Stamolys CA71SI

3.2 Incoming acceptance, transport, storage

• Make sure the packaging is undamaged!
Inform the supplier about damage to the packaging.
Keep the damaged packaging until the matter has been settled.
• Make sure the contents are undamaged!
Inform the supplier about damage to the delivery contents.
Keep the damaged products until the matter has been settled.
• Check that the scope of delivery is complete and agrees with your order and the
shipping documents.
• The packaging material used to store or to transport the product must provide shock protection
and humidity protection. The original packaging offers the best protection. Also, keep to the
approved ambient conditions (see "Technical data").
• If you have any questions, please contact your supplier or your sales centre responsible.

3.3 Installation conditions

3.3.1 Design, dimensions

SS version, SI-A and SI-B

3/0.12 Detail A 30/1.18

38/1.5

15/0.59
163/6.42
110/4.33
Ø 27/1.06

15/0.59 9/0.35

250/9.84
330/12.99
160/6.30

15/0.59 140/5.51
100/3.94
60/2.36

A
120/4.72

Ø 26 / 1.02
243/9.57

200/7.87
165/6.50

Ø 21/0.83
125/4.92

47/1.85

580/22.83
648/25.51
555/21.85
524/20.63

78/3.07
119/4.69

Ø 21/0.83

326/12.83

Ø 26/1.02

360/14.17 207/8.15

436/17.17 mm / inch
C07-CA71xxx-06-08-00-en-001.eps

Fig. 3: CA71 dimensions, stainless steel version

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Stamolys CA71SI Installation

GFK version, SI-A

38/1.5

250/9.84
160/6.30

110/
4.33
140/5.51

Ø 27/1.06
100/3.94
330/12.99
60/2.36

Ø 26/1.02
7-11/

120/
4.72
0.28 - 0.43
(M 6)

243/9.57

Ø 21/0.83
165/6.50
200/7.87

125/4.92

47/1.85
555/21.85

Ø 21/

648/25.51
0.83
78/3.07
119/4.69
Ø 26/1.02
326/12.83

Ø 16/0.63

360/14.17
436/17.17 Ø 27/1.06
465/18.31 120/4.72
500/19.69
mm / inch
C07-CA71xxx-06-08-00-en-002.eps

Fig. 4: CA71 dimensions, GFK version

GFK version, SI-B

163 / 6.42

250/9.84
120 / 4.72

160/6.30
Ø 26/1.02
Ø 16/0.63

140/5.51
100/3.94
330 / 12.99
60/2.36
Ø 26/1.02

7-11/
120/
4.72

0.28 - 0.43
(M 6)
243/9.57

Ø 21/0.83
165/6.50

200/7.87
125/4.92

47/1.85
555/21.85

Ø 21/

648/25.51
0.83
78/3.07
119/4.69

Ø 26/1.02
326/12.83

Ø 16/0.63

360/14.17
436/17.17 Ø 27/1.06
465/18.31 120/4.72
500/19.69
mm / inch
C07-CA71xxx-06-08-00-en-020.eps

Fig. 5: GFK version

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Installation Stamolys CA71SI

Open version, SI-A and SI-B

381/15
351/13.82
19/0.75 197/7.76

192/7.56
Ø6/0.24

RS 232

540/21.26

562/22.13

175/6.89
325/12.80
9/0.35 8/0.31 mm/inch
C07-CA71xxx-06-08-00-en-003.eps

Fig. 6: Open version (without housing)

3.3.2 Connecting the sample line

1 5

2 6

3 7

C07-CA71xxx-11-08-00-xx-001.eps C07-CA71xxx-06-08-02-en-003.eps

Fig. 7: Collecting vessel at analyser (optional) Fig. 8: Collecting vessel dimensions

1 Ventilation * variable, freely adjustable dimensions
2 Sample inlet from sampling 6 Sampling for analyser
3 Collecting vessel 7 Analyser outlet
4 Electrical connections 8 Sample overflow
5 Analyser sample inlet

12 Endress+Hauser
Stamolys CA71SI Installation

One-channel version

Collecting vessel (at analyser, without level measurement)

Connection hose ID 3.2 mm (0.13")

Customer collecting vessel

Connection hose ID 1.6 mm (0.06")
Max. distance from collecting vessel to analyser 1 m (3.28 ft)
Max. height difference from collecting vessel to analyser 0.5 m (1.64 ft)

Two-channel version
• Depending on the ordered version, one or two collecting vessels (without level measurement) are
included in the scope of delivery.
• Only one collecting vessel can be mounted at the housing. The second is to be placed nearby the
analyser.

3.4 Installation instructions

To install the analyser at the intended location, proceed as follows:
1. Place the analyser in position and secure it to a wall using M6 screws.
For the installation dimensions, please see previous chapter.
2. Use a spirit level to check that the cabinet is hanging level. This is the only way to ensure that
any air bubbles that occur can escape from the optical cell.
3. Place the edge covers on the analyser edges (with GFK housing only).
4. Lay the drain pipe for the reaction products. Where possible, use fixed pipes (PVC or PE,
internal diameter ¾ " with 3% incline).
5. Insert the valve hoses according to Fig. 9. For the transportation, the hoses were removed from
the valves. This prevents the hoses from sticking together or being pressed against the same
position for a long period of time.

1 2 3

V3 V1 V2 V4

7 6 5 4
C07-CA71xxx-00-08-00-xx-005.eps

Fig. 9: Valves and valve hoses

V1-4 Valves 1, 2 and 4
V3 Two channel switch (optional)
1 Sample
2 To the pump
3 Y-piece, connecting hose to valve 1, back
4 Outlet hose
5 Hose valve 2 front, standard
6 Hose valve 2 back, cleaning agent
7 Hose valve 1 front, sample

6. Secure the hose cassettes in the pump brackets:

Sample pump on the left, reagent pump on the right. Here, the flow direction of sample and
reagent must be anticlockwise.
7. Connect the sample supply.

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Installation Stamolys CA71SI

! Note!
The sample can be obtained as follows:
– Directly or after a reversible flow filter or a cross current filter by means of a small pump
(rating approx. 300 ml/min), suitable for clear media, e.g. in the discharge channel of a
sewage treatment plant
– From a sedimentation tank or after microfiltration; suitable for media containing flocculants,
e.g. in an activated sludge basin
– Sample conditioning using ultrafiltration for heavily soiled media,
e.g. from the primary settling tank

For questions regarding sample conditioning and its automation, please contact your Service
or your Sales Centre responsible.
8. Connect the tubes from canisters containing reagents, standard and cleaning agents to the
following nozzles:

Canister Hose designation (mark)

Sample P
Reagent 1 SI1
Reagent 2 SI2
Reagent 3 SI3
Standard solution S
Cleaner R

! Note!
• The pressure of the hose cassette is set at the factory such that the sample and reagent are fed in
without bubbles.
• Only change the pressure if the factory setting does not meet your requirements. The setting is
changed by turning the adjustment screw using a 2.5 mm Allen key.
• The minimum flow rate in the sample line must be 14 ml/min.

3.5 Installation examples

3.5.1 CAT430 or customer-specific ultra filtration and two CA71

analysers

• Permeate can contain air bubbles (CAT430) 5

or is free of bubbles (customer-supplied
ultrafiltration)
• Distance between the analysers as short as CA 71 CA 71
possible: sampling line between T-piece and
the second analyser (Fig. 10, item 2) shorter
than 1.5 m
• Cross-section of sampling line ID 3.2 - 4 mm
• Only one sample receiver required
! Note! 1 2 3 4
C07-CA71xxx-11-08-00-xx-007.eps
Ensure that there is always sufficient sample Fig. 10: Installation example
available for both analysers. Observe this when
1 Sample from CAT430
selecting maintenance intervals for CAT430 and
2 Sampling line
when setting the buffer volume on the collecting 3 Sample receiver overflow
vessel. 4 T-piece
5 Collecting vessel

14 Endress+Hauser
Stamolys CA71SI Installation

3.5.2 CAT411, CAT430 and two CA71 analysers (two-channel

version)

• Permeate not free of air bubbles

• Distance between the analysers as short as 1 6
possible: sampling line between T-piece and
2
the second analyser (Fig. 11, item 5) shorter CA 71
than 1.5 m 3
• Cross-section of sampling line ID 3.2 - 4 mm CA 71
4
• One sample receiver each (without level
measurement) for CAT411 or CAT430 5

! Note!
Ensure that there is always sufficient sample
C07-CA71xxx-11-08-00-xx-006.eps
available for both analysers. Observe this when Fig. 11: Installation example
selecting maintenance intervals for CAT411 and
1 Sample from CAT430
CAT430.
2 Sample from CAT411
3 Collecting vessel
4 Collecting vessel overflow
5 Sampling lines
6 T-pieces

3.6 Post-installation check

• After installation, check that all connections are fitted tightly and are leakage resistant.
• Ensure that the hoses cannot be removed without effort.
• Check all hoses for damage.

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Wiring Stamolys CA71SI

4 Wiring

4.1 Electrical connection

# Warning!
• The electrical connection must only be carried out by authorised technical personnel.
• Technical personnel must have read and understood the instructions in this manual and must
adhere to them.
• Ensure that there is no voltage at the power cable before beginning the connection work.

" Caution!
Before swinging out the analyser frame, remove the hoses from the outlet pipe. Otherwise there is
danger of overflow. After swinging in the frame, reconnect the hoses.

! Note!
To reach the terminal strip, you must swing out the analyser frame.
1. Loosen the two lower Allen screws SW 6 by 3 to 4 turns (Fig. 12, pos. 1).
2. Unscrew the two upper Allen screws until the analyser frame swings out. Thus you can reach
the terminal strip (pos. 2).

M E K RS 232

1 2

C07-CA71xxx-04-08-00-xx-002.eps

Fig. 12: Swing out of the analyser frame

1 Allen screws SW 6
2 Terminal strip

4.1.1 Quick wiring guide

0V fx Kanal 1 Kanal 2
Photometer +17V Photometer -17V Photometer Analog Out Channel 1
Schirm/ MP5 MP6 Channel 2
BK 65 0/4-20mA COM
F4 M 0.2 A M 0.2 A Screen 28 22 16
ALARM 2

F5
ALARM 2

OPTION

Schirm
GN 64 0V BK 58 40 NC
Screen 27 21 15
Schirm Schirm keine Probe
80 75 V4 70 Screen BN 63 -17 V YE 57 39 I2 + NO
Screen No sample 26 20 14
n.b.
OR 79 74 V3 69 WH 62 +17 V WH 56 Reserve 38 I2 - COM
SCHRITTMOTOR

n.c. 25 19 13
STÖRUNG
STEP MOTOR

ALARM 1
ALARM 1

Mess 2
ERROR

n.b. n.b.
BK 78 73 V2 68 YE 61 fx 55 37 31 NC
n.c. Meas 2 n.c. 24 18 12
n.b. n.b.
LEAK S.

+24V
LECKF.

RD 77 72 V 1 BU 67 60 54 36 I1 + 30 NO
n.c. n.c. 23 17 11
YE 76 71 0 V BN 66 GY 59 Status GN 53 0V 35 I1 - 29 0V RELAIS / Relay:
max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC

Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!!

Terminals voltage to ground even when the unit is switched off !!!

F2 NETZ
AC Motor MAINS
7 L2 T 0.1A
AC MOTOR

6 N 3 L

L1 Elektronik F1 N
5 2
Electronics
4 PE T 0.5A 1 PE

C07-CA71xxxx-04-08-00-a2-001.eps

Fig. 13: Connection sticker

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Stamolys CA71SI Wiring

! Note!
The device does not have a mains switch. Therefore, it is advantageous to have a fused socket near
to the device.

4.1.2 Terminal assignment

Function Designation Terminal one channel Terminal

two channels

L 3 3

Mains N 2 2

PE 1 1

COM 25 25

Alarm value 1, channel 1 NC 24 24

NO 23 23

COM 28 28

Alarm value 2, channel 1 NC 27 27

NO 26 26

COM – 13

Alarm value 1, channel 2 NC – 12

NO – 11

COM – 16

Alarm value 2, channel 2 NC – 15

NO – 14

COM 19 19

Fault NC 18 18

NO 17 17

COM 22 22

Reserve (unassigned terminals) NC 21 21

NO 20 20

+ 36 36
Analog output 1
– 35 35
0/4 ... 20 mA
Screen PE1 PE1

+ – 39
Analog output 2
– – 38
0/4 ... 20 mA
Screen – PE1

Sample conditioning Input 57 57

remote control 0V 53 53

Input – 55
Channel switch-over
0V – 53

1) Brass screw with bolt top right in the connection compartment (marked with *)

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Wiring Stamolys CA71SI

! Note!
• Alarm values 1 and 2 do not need to be connected if the PLC sets its own alarm values at the
analog output.
• When using a sample conditioning system:
Connect terminals 57 and 53 on the analyser to the corresponding terminals on the sample
conditioning system. For the allocation of these terminals, please see the sample conditioning
system operating instructions.
• If there is a 24 V voltage at terminal 57, the analyser will not begin measurement (sample not
ready). To start measurement, the voltage must stay at 0 V for at least 5 seconds.

4.2 Signal connection

4.2.1 Screening of the analog outputs

The interference suppressor attenuates electromagnetic effects on control, power and signal lines.
After the connection of the data transfer cables clip the interference suppressor (in scope of delivery)
on the cable cores (not on the outer insulation of the cable!). Place the cable screen out of the
interference suppressor and connect it to PE (brass screw with bolt, top right in the connection
compartment) (→ Fig. 14).

C07-CA71xxx-03-08-00-xx-001.eps

Fig. 14: Interference protection of the signal cable

1 Cable screen (to PE )
2 Signal cable
3 Interference suppressor
4 Cable cores of the signal cable

! Note!
With the two-channel version, place the cable cores of all cables (data cables to analog output 1 and
to analog output 2) through the interference suppressor.

4.2.2 One-channel version

Connection Designation Function

Leak Liquid has collected in the drip pan

Signal inputs No sample No sample available, measurement is not started, display
flashes

AV 1 Alarm value 1 exceeded or undershot

Signal outputs AV 2 Alarm value 2 exceeded or undershot

Fault Retrieves error message using operation menu

l-1 channel 1 0 or 4 mA = measuring range start

Analog output
20 mA = measuring range end

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Stamolys CA71SI Wiring

4.2.3 Two-channel version

Connection Designation Function

Leak Liquid has collected in the drip pan

Signal inputs No sample No sample available, measurement is not started,
display flashes

AV 1-1 Alarm value 1, channel 1 exceeded or undershot

AV 2-1 Alarm value 2, channel 1 exceeded or undershot

AV 1-2 Alarm value 1, channel 2 exceeded or undershot

Signal outputs AV 2-2 Alarm value 2, channel 2 exceeded or undershot

Fault Retrieves error message using operation menu

Channel ½ or measurement Displays active channel

end1 Displays "Measurement finished" (5 s)

l-1 channel 1 0 or 4 mA = measuring range start

20 mA = measuring range end
Analog output
l-2 channel 2 0 or 4 mA = measuring range start
20 mA = measuring range end

Meas. 2 0 V = channel 1
Channel selection
24 V = channel 2

1) Alternative selection

4.3 Switching contacts

One-channel version

Connection Terminal connection for Terminal connection for Terminal connection for
condition fulfilled condition not fulfilled power off

AV 1 A: 25 - 23 A: 25 - 24 25 - 24
R: 25 - 24 R: 25 - 23

AV 2 A: 28 - 26 A: 28 - 27 28 - 27
R: 28 - 27 R: 28 - 26

Fault A: 19 - 17 A: 19 - 18 19 - 18
R: 19 - 18 R: 19 - 17

Unassigned 22 - 20 22 - 21 22 - 21
16 - 14 16 - 15 16 - 15
13 - 11 13 - 12 13 - 12

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Wiring Stamolys CA71SI

Two-channel version

Connection Terminal connection for Terminal connection for Terminal connection for
condition fulfilled condition not fulfilled power off

AV 1 - 1 A: 25 - 23 A: 25 - 24 25 - 24
R: 25 - 24 R: 25 - 23

AV 1 - 2 A: 13 - 11 A: 13 - 12 13 - 12
R: 13 - 12 R: 13 - 11

AV 2 - 1 A: 28 - 26 A: 28 - 27 28 - 27
R: 28 - 27 R: 28 - 26

AV 2 - 2 A: 16 - 14 A: 16 - 15 16 - 15
R: 16 - 15 R: 16 - 14

Fault A: 19 - 17 A: 19 - 18 19 - 18
R: 19 - 18 R: 19 - 17

Channel ½ A: 22 - 20 A: 22 - 21 22 - 21
measurement end R: 22 - 21 R: 22 - 20

A = NO current configured
R = NC current configured

! Note!
Condition fulfilled means:
• AV 1: concentration > Alarm value 1
• AV 2: concentration > Alarm value 2
• Fault: error occurred
Contacts AV 1, AV 2 and fault are only affected during automatic operation.

4.4 Serial interface

RS 232 of CA 71 COM 1/2 at PC

SUB-D, nine-pin Function Function SUB-D, nine-pin

3 TxD RxD 2

2 RxD TxD 3

8 CTS RTS 7

CTS 8

5 GND GND 5

Software protocol: 9600, N, 8, 1

Output format: ASCII

The results (measured value+unit of measure+CR) are output in the "Data memory Measured
values" menu.
The calibration results (measured value+unit of measure+CR) are output in the "Data
memory-Calibration factors" menu.

! Note!
• A null modem cable is required (not a crossed one).
• The analyser does not have to be configured for the interface.
The following commands can be sent from the PC, in order to read out data:
• "D" = Data memory-Measured values
• "C" = Data memory-Calibration factors
• "S" = Setup (parameter entry, configuration...)
• "F" = Frequency (current)

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Stamolys CA71SI Wiring

4.5 Post-connection check

Carry out the following checks after electrical connection:

Device status and specifications Note

Is the analyser or cable externally undamaged? Visual inspection

Electrical connection Note

Does the supply voltage correspond to the data on the nameplate? 230 V AC / 50 Hz 115 V AC / 60 Hz

Are current outputs screened and connected?

Are the mounted cables relieved of tension?

Cable type properly disconnected? Guide power supply and signal lines
separate over the entire travel distance.
Separate cable channels are ideal.

Cable routing without scuffing or cross-overs?

Are power supply and signal lines connected correctly according to wiring
diagram?

Are all screw terminals tightened?

Are all cable entries mounted, tightened and leak-resistant?

Interference suppressor at the analogue output?

Current output simulation See procedure below

Current output simulation:

1. Hold both arrow keys down (see "Display and operating elements" chapter) and connect the
analyser to the mains or switch the mains switch on (if available). Wait until the display "0 mA"
appears.
2. Check on your PLC, PCS or you data logger whether the current value is the same.
3. Press the F key. Browse to the next current values (4, 12, 20 mA, depending on the setting).
4. Check that the respective current values are also on your PLC, PCS or your data logger.
5. If the values are not there, check the terminal assignment for analogue output
1 or 2.

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Operation Stamolys CA71SI

5 Operation

5.1 Operation and commissioning

The following chapters provide you with information on the analyser's operating elements and
explain how to make settings.
In chapter “Commissioning” you will find the procedure for initial start-up and for daily analyser
operation.

5.2 Display and operating elements

1 2

M CE E K RS 232

4 3
C07-CA71xxx-19-08-00-xx-005.eps

Fig. 15: CA71 display and operating elements

1 LED (measured value)
2 LC display (measured value and status)
3 Serial interface RS 232
4 Operating keys and control LEDs

5.3 Local operation

The operating keys and the integrated indicator LEDs have the following functions:

Key Key function Indicator LED function

H – “Auto measuring” option

– back to the main menu from all sub-menus
Alarm value 1 exceeded

K – backwards in the sub-menu

(horizontal, see Appendix,)
Alarm value 2 exceeded

V – backwards in the main menu (vertical)

– Increase value
Measuring range exceeded

W – forwards in the main menu (vertical)

– Reduce value
Measuring range undershot

F – Select option
– Adopt value, forwards in the sub-menu (horizontal)
Retrieve error message

J – Selection in the sub-menu unassigned

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Stamolys CA71SI Operation

5.3.1 Main menu

Access the main menu by holding down the Hkey until “AUTO MEASURING” is displayed.
For the main menu options and information about them, please see the following table.

Selection Display Info

AUTO MEASURING Calibration, measurement, flushing time-controlled

AUTO MEASURING
actions

PARAMETER ENTRY Default settings for measuring ranges, alarm values,

PARAMETER ENTRY
calibration, flushing

Basic settings such as parameters, measuring units,

CONFIGURATION CONFIGURATION arrangement of analog outputs and alarm values (NO,
NC), date, time, offset values

LANGUAGE LANGUAGE Selecting menu language

ERROR DISPLAY ERROR DISPLAY Displaying error messages

SERVICE SERVICE Manually switching valves and pumps

DATA MEMORY 1 DATA MEMORY 1 Last 1024 measured values channel 1

DATA MEMORY 2 DATA MEMORY 2 Last 1024 measured values channel 2

(Two-channel version only)

5.3.2 AUTO MEASURING

The actions "calibration", "measuring" and "flushing" are triggered by time-control.
The settings for these actions are made in the "PARAMETER ENTRY" menu.
The respective action is displayed in the LC display. The most recently registered concentration
value is displayed until the end of the next measurement.
Otherwise, "wait" is displayed when
• the time of the first measurement has not yet been reached or
• the measuring interval has not yet expired.

! Note!
"Measuring" flashes when the analyser is ready for the next measurement but has not yet received
the enable signal from the sample collector or the sample conditioning unit.

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Operation Stamolys CA71SI

5.3.3 CONFIGURATION

! Note!
Some settings that can be made in this menu affect the defaults in the PARAMETER ENTRY menu.
In view of this, complete the CONFIGURATION menu first during initial start-up.

! Note!
In the following table and in the tables in the next chapter, example images can be found for each
option under "Display". In addition to the numerical values, the parameter is also displayed in some
options. This is not shown in the images. Moreover, individual numerical values in the images can
differ from the actual settings.
The actual factory settings can in any case be found in column 2 "Range of adjustment / Factory
settings" in bold.

Option Range of adjustment Display Info

(default settings in bold)

Input 03.
Code number 03 Code-Nr. If an incorrect code is entered the program exits the
0
sub-menu.

This setting displays the parameter that is being measured

Depending on specification: (e.g. SI-A). This is defined by the product specification
Photometer SI-A Photometer and set in this option at the factory. Do not change the
SI-B value. Otherwise, you will receive an "Incorrect
photometer" error message.

If "yes" is selected, all settings are reset to default.

You have to set date and time to the current before (scroll
Default settings yes / no default setup to the third last fuction in this menu).
y: + n: E
With the reset, the date for the 1st calibration and for the
1st flushing are set to the next day.

µg/l Unit of measure

Measuring unit
ppb mg/l

The calibration factor is the ratio of the measured

concentration of the calibration standard to the
pre-defined concentration of the standard (see
"PARAMETER ENTRY", calibration solution). The
deviation results from factors such as reagent ageing,
ageing of constructive components, etc.
The calibration factor compensates for these effects.
CA71 checks the registered calibration factor logically. If
0.20 ... 5.00 Calibr. factor
Calibration factor the factor lies outside of the error tolerance, the
1.00 1.00
calibration is automatically repeated. If the repeat also lies
outside, an error message appears and the analyser
continues to work with the most recently registered,
logically correct factor.
The last 10 calibration factors are filed in the memory
with the date and time and can be retrieved by pressing
the J key.
The calibration factor ca be changed manually.

Concentration c-Offset The offset specifies the zero shift of the calibration
0.00 ... 50.0 mg/l
offset + 0.00 mg/l function. (Change the sign with the J key.)

If the sample is to be diluted between taking the sample

Dilution 0.10 ... 1.00 Dilution and the analyser, the dilution factor has to be entered
1.00
here (factor times measured value).

Dosing time for sample or standard (20 ... 120 s). During
20 ... 300 s this time, the entire system is flushed with sample or
Delay to sample 120 s (SI-A) Delay to sample standard, so when the reagent is added there is definitely
80 s
160 s (SI-B) only fresh sample in the mixer. If there is sufficient
sample available, select the highest possible value.

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Stamolys CA71SI Operation

Option Range of adjustment Display Info

(default settings in bold)

Selection for the scope of channel 1 measuring range. If

Analog output 1 the concentration measuring range is 0 ... x mg/l, this
Analog output 1
4-20 mA corresponds to 0 mg/l either 4 mA or 0 mA. The end of
the measuring range is the same in both cases at 20 mA.

Two-channel version only! Selecting scope of channel

0 ... 20 mA / 4 ... 20 mA 2 measuring range.
The scopes of the measuring range are independent of
Analog output 2 Analog output 2 each other for channel 1 and channel 2 and are
4-20 mA
determined by the start of measuring range (channel 1 /
channel 2) or end of measuring range (channel 1 /
channel 2) setting in the PARAMETER ENTRY menu.

Alarm val. 1-1 Setting for whether contact for alarm value 1, channel 1
Alarm value AV 1-1
norm. closed works as NO current or NC current contact.

Alarm val. 2-1 Setting for whether contact for alarm value 2, channel 1
Alarm value AV 2-1
norm. closed works as NO current or NC current contact.
NO current
NC current Two-channel version only!
Alarm value AV 1-2
! Note!
Changes will only be activated after a
Alarm val. 1-2
norm. closed
Setting for whether contact for alarm value 1, channel 2
works as NO current or NC current contact.
Reset (Power off/on)!
Two-channel version only!
Alarm value AV 2-2 Alarm val. 2-2 Setting for whether contact for alarm value 2, channel 2
norm. closed
works as NO current or NC current contact.

Error contact Setting for whether error contact works as

Error contact
norm. closed NO current or NC current contact

act. Date/Time Setting the system clock.

Current date/time 01.01.96 00:00... 31.12.95 23:59
25.01.02 15:45 Format DD.MM.YY hh:mm.

Frequency offset1
Calibrate offset yes / no Calibrate offs Pressing the J key starts a blind value measurement for
yes: K no: E
compensating the reagent's inherent colour.

– 5000 ... +5000 f-Offset [Hz]

Frequency offset Manually changing the frequency offset.1
0 0

1) Do not change the default setting. The frequency offset has to be 0 Hz. A determination is not necessary.

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Operation Stamolys CA71SI

5.3.4 PARAMETER ENTRY

Option Range of adjustment Display Info

(default settings in bold)

Measuring range Range start 1 The specified concentration is allocated a value of 0 or 4

Start 1 0.00 mg/l mA at analog output 1.
SI-A: 1 ... 200 µg/l / 0 µg/l
SI-B: 100 ... 5000 µg/l / 0 µg/l Two-channel version only!
Measuring range Range start 2 The specified concentration is allocated a value of 0 or 4
Start 2 0.00 mg/l
mA at analog output 2.

Measuring range Range end 1 The specified concentration is allocated a value of 20 mA

End 1 2.50 mg/l at analog output 1.
SI-A: 1 ... 200 µg/l / 200 µg/l
SI-B: 100 ... 5000 µg/l / 5000 µg/l Two-channel version only!
Measuring range Range end 2 The specified concentration is allocated a value of 20 mA
End 2 2.50 mg/l
at analog output 2.

Alarm value SI-A: 1 ... 200 µg/l / 100 µg/l Alarm val. 1-1 Concentration threshold value limit relay 1, channel 1
AV 1 - 1 SI-B: 100 ... 5000 µg/l / 2500 µg/l 2.50 mg/l (differential hysteresis 2% of alarm value).

Alarm value SI-A: 1 ... 200 µg/l / 200 µg/l Alarm val. 2-1 Concentration threshold value limit relay 2, channel 1
AV 2 - 1 SI-B: 100 ... 5000 µg/l / 5000 µg/l 1.25 mg/l (differential hysteresis 2% of alarm value).

Two-channel version only!

Alarm value SI-A: 1 ... 200 µg/l / 100 µg/l Alarm val. 1-2 Concentration threshold value limit relay 1, channel 2
AV 1 - 2 SI-B: 100 ... 5000 µg/l / 2500 µg/l 1.25 mg/l
(differential hysteresis 2% of alarm value).

Two-channel version only!

Alarm value SI-A: 1 ... 200 µg/l / 200 µg/l Alarm val. 2-2 Concentration threshold value limit relay 2, channel 2
AV 2 - 2 SI-B: 100 ... 5000 µg/l / 5000 µg/l 2.50 mg/l
(differential hysteresis 2% of alarm value).

Date format DD.MM.YY, time hh.mm. After each change

Time 1. Measurement the instrument does not wait for the measuring interval. If
01.01.96 00:00... 31.12.95 23:59
1st measurement 10.02.02 08:00 the measurement is to start immediately, set the time in
the past.

Time between two measurements.

6 ... 120 min Meas. interval
Measuring interval If the setting is 2 minutes, the measurements take place
10 10 min
without any pauses.

Two-channel version only!

Frequency of measurement 0 ... 9 n* Channel 1: Number of measurements at channel 1 before switching
Channel 1 11 9
to channel 2.

Two-channel version only!

Frequency of measurement 0 ... 9 n* Channel 2: Number of measurements at channel 2 before switching
Channel 2 11 1
to channel 1.

Time of 1st calibration (DD.MM.YY, time hh.mm). After

each change the instrument does not wait for the
calibration interval. If the calibration is to start
immediately, set the time in the past.
Analysers are delivered pre-calibrated.
Date of the 1. Calibration – Start 1st calibration 2 hours after the initial start-up at
01.01.96 00:00... 31.12.95 23:59
1st Calibration 01.01.02 08:00 the earliest (warm-up phase)
– Set the time to 8:00 to reproduce impacts on
calibration in the curve.
– If you have started a calibration manually, you should
re-define the time of the 1st calibration because the
interval is dependent on the last calibration.

Time between two calibrations.

0 ... 720 h Calib.interval
Calibration interval The "0 h" setting stops calibration.
48 h 48 h
Recommended: calibration interval of 48 ... 72 h.

Concentration of the calibration standard.

SI-A: 1 ... 200 µg/l / 500 µg/l Calib. solution
Calibration solution Select a standard, whose concentration is in the upper
SI-B: 100 ... 5000 µg/l / 500 µg/l 1.00 mg/l
third of the measuring range.

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Stamolys CA71SI Operation

Option Range of adjustment Display Info

(default settings in bold)

Time of 1st flushing (DD.MM.YY, time hh.mm). After

each change the instrument does not wait for the
calibration interval. If the flushing is to start immediately,
set the time in the past.
Date of the 1. Flushing
01.01.96 00:00... 31.12.95 23:59 – Set the time to 4:00 to reproduce impacts on flushing
1st flushing 01.01.02 08:10
in the curve.
– If you have started flushing manually, you should
re-define the time of the 1st flushing because the
interval is dependent on the last flushing.

0 ... 720 h
Flush. interval Time between two flushings.
Flushing interval 0 h (SI-A)
48 h The "0 h" setting stops cleaning.
48 h (SI-B)

0 ... 60 s Dwell time of flushing solution in the

Flushing hold on 0 s (SI-A) Flushing hold on pump-mixer-photometer line.
60 s
60 s (SI-B) Recommended: 30 ... 60 s.

1) All channels set to 0 means, the channel selection is provided by an external device. All channels set to 1 means, alterning beginning with channel 1.

! Note!
• Always synchronise calibration and flushing time.
• Carry out flushing with standard cleaning solution approx. 3-4 hours before the next calibration.
• Flushing with special cleaning solution (e.g. hydrochloric acid) has a lasting effect on calibration.
Therefore, carry out this cleaning 3-4 hours after calibration.

5.3.5 LANGUAGE
The following languages are available:
• Deutsch
• English
• Français
• Suomi
• Polski
• Italiano.

5.3.6 ERROR DISPLAY

! Note!
• This menu is a "Read-Only-Menu".
• You can find the individual error messages, their meaning and solutions to problems in chapter
"Trouble-shooting instructions".
• If there is at least one error message, the signal output is set to "fault".
• Causes of faults are requested for every measurement. If an error which occurred previously no
longer exists, it is automatically cancelled. If this should not happen automatically, error messages
can be deleted by quickly switching the analyser off and back on again.

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Operation Stamolys CA71SI

5.3.7 SERVICE
Navigate through the main menu with the W key to the "SERVICE" option and press the F key
to enter the menu.

Option Display Info

"Virtual switching board"

Various valve and pump combinations can be selected.
The setting options are:
– Valve 1:
P (sample) or S (standard)
– Valve 2:
S (standard) or C (cleaning agent)
– Valve 3 (Two-channel version only):
1 (channel 1) or 2 (channel 2)
– Valve 4 (for optical cell outlet, improves cleaning and
avoids memory effects):
s (stop) or g (go)
– Pump 1 and pump 2:
s (stop) or g (go)
– Mixture
The reagent and sample pumps can be switched on
Pumps and valves V1 2 3 4 P1 2 G together, so that they run in the same ratio as for filling
P S 1 s s s s the sample-reagent mixture in measuring mode.
s (stop) and g (go)

! Note!
P1 and P2 are inactiv, when G is at go. If P1 or P2 is at
go, G is not available.
The following valve combinations are possible:
(applies to one-channel and two-channel version,
whereby where the latter is concerned selection is made
by positioning valve 3 between channel 1 and 2)
– V1: P, V2: S
Passage for the sample. This combination is
automatically reset on leaving the service menu.
– V1: S, V2: S
Passage for standard solution
– V1: S, V2: R
Passage for cleaning agent

Signal frequency 0 Hz Signal frequency of the photometer

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Stamolys CA71SI Operation

5.3.8 DATA STORAGE-Measured values

! Note!
Two menus, "DATA MEMORY 1" and "DATA MEMORY 2", are only for the two-channel
version. In the one-channel version there is only one menu "DATA MEMORY".

Selection Display Info

The data memory contains the last 1024 concentration

measured values with date and time. If there are no
Measured values 53. 1 ppb values available, "Empty set" appears.
02.02.99 22:47
Browse through the data sets by pressing the
V and W keys.
You can output all data sets (in ASCII-format) via the
serial interface. For this, the receiving end (PC) must be
Serial output Serial output configured like this: 9600, N, 8, 1.
yes: K no: E
To send data, the receiving end (PC) must send the ASCII
character 81 ("Shift", "D").

Clear data Clear data This deletes all data sets.

y: + n: E

5.3.9 DATA STORAGE-Calibration data

! Note!
To enter this menu select the CONFIGURATION menu, browse to the "Calibration factor" option
and press the J key.

Selection Display Info

This data memory contains the last 100 calibration factors

with date and time. If there are no values available,
Calibration factor Calibr. factor "Empty set" appears.
1.00
Browse through the data sets by pressing the
V and W keys.
You can output all data sets (in ASCII-format) via the
serial interface. For this, the receiving end (PC) must be
Serial output
no display configured like this: 9600, N, 8, 1.
only available via PC!
To send data, the receiving end (PC) must send the ASCII
character 81 ("Shift", "C").

Clear data Clear data This deletes all data sets.

y: + n: E

Endress+Hauser 29
Operation Stamolys CA71SI

5.4 Calibration

5.4.1 Standard calibration data

The signal strength is processed device-internally as a frequency.
The following table provides an overview of the standard calibration data.

! Note!
Compare these values to your own data.
After changes in the CONFIGURATION menu and in case of software updates, you can check and,
if necessary, change the calibration data in the sub-menu.

Measuring range Concentration [mg/l] Frequency [Hz]

Silicate, lower measuring range 1 ... 200 µg/l 0.000 0

SI-A 0.020 68
0.040 142
0.060 217
0.080 289
0.100 369
0.120 443
0.140 515
0.160 591
0.200 742

Silicate, upper measuring range 0.00 ... 5.00 mg/l 0.00 0

SI-B 0.10 107
0.50 211
1.00 311
1.50 396
2.00 515
2.50 555
3.00 636
4.00 671
5.00 858

5.4.2 Interferences

Interferring substance Interference

Colour eliminated by calibration

Iron interferences from 1 mg/l

Phosphate interferences from 50 mg/l

Sulfide interferences at high concentrations

Turbidity eliminated by calibration

Extreme pH values pH must be lower than 7

30 Endress+Hauser
Stamolys CA71SI Operation

5.4.3 Calibration example

Proceed as follows if you want to activate an immediate calibration (e.g. after you have replaced the
reagents).
Ensure that you have changed the reagents, filled the hoses again (no air bubbles) and the analyser
is in measuring mode.
1. Hold H down until AUTO MEASURING appears.
2. Use W to move through the PARAMETER ENTRY menu and press F.
3. Use F to go to the "1st calibration" option.
4. Select the option with F
5. Now use the W or V and F keys to set a time which lies in the past.
6. Press F to accept the value and then press H twice to return to the main menu
7. Press F again. This takes you back to measuring mode.
The calibration is now carried out automatically.

" Caution!
After the calibration has finished, the analyser automatically goes into measuring mode. You now
have to set the time of the 1st calibration back into the future in order to align the calibration and
rinsing times to each other. The rinse must be performed 3-4 hours before the next calibration.
Proceed as described above to change the setting for the time of the 1st calibration. After changing
to measuring mode, the analyser automatically begins measuring, rinsing and calibrating at the
defined times.

Endress+Hauser 31
Commissioning Stamolys CA71SI

6 Commissioning

6.1 Function check

# Warning!
• Check that all connections have been made correctly. Check, in particular, that all hose
connections are secure, so that no leaks occur.
• Ensure that the mains voltage corresponds to the voltage specified on the nameplate.

6.2 Switch-on

6.2.1 Dry commissioning

! Note!
• If possible, let the analyser warm up in standby mode before commissioning ("Auto measuring"
display). The time can be defined via the "1st measurement" option in the PARAMETER ENTRY
menu.
• At the start of measurement with a cold analyser, the first measuring results will be errored. The
reaction is temperature-dependent and if the temperature is too low the pre-defined reaction time
is insufficient for a complete reaction. For this reason, never carry out calibration with a cold
analyser. Wait at least two hours before carrying out calibration.
When the analyser has been configured and calibrated, the measuring cycle starts automatically.
Entering parameters is no longer necessary.
To perform initial start-up or to readjust the device parameters, proceed as follows:
1. Plug-in the plug into a socket.
2. Press the H key until AUTO MEASURING is displayed.
3. Select the CONFIGURATION menu and program the individual options up to and including
the "Current date/time". With H you can return to the main menu.
4. Now complete the PARAMETER ENTRY and SERVICE menus.
With H you can return to the main menu.
5. Select CONFIGURATION again and use F to go to the "Calibrate offset" option.
6. Connect a vessel containing distilled water to the "Sample" connection and start the frequency
offset (J key). The registered value is displayed and saved.
7. Then reconnect the sampling line.
With H you can return to the main menu.
The analyser starts the "Calibration", "Measurement", and "Flushing" procedures automatically
(triggered by control signal or integrated timer) in accordance with the device parameters that you
have set (1st calibration, 1st measurement, 1st flushing times and the respective intervals control
the temporal procedure).

32 Endress+Hauser
Stamolys CA71SI Commissioning

The following summary shows procedures carried out in the device and the programmed intervals:
Function Duration [s] Range of adjustment

Measurement Flushing (sample) 3 x 15

Delay to sample 20 ... 300 CONFIGURATION / "Delay to sample"
Stabilisation 4
1st measurement
Flushing (reag. line) 2
Fill mixture 15 ... 18 SERVICE / "Pumps and valves"
Reaction s. Techn. data
2nd measurement
Flushing (sample) 30

Calibration Flushing (standard) 3 x 15

Delay to standard 20 ... 300 CONFIGURATION / "Delay to sample"
Stabilisation 4
1st measurement
Flushing (reag. line) 2
Fill mixture 15 ... 18 SERVICE / "Pumps and valves"
Reaction s. Techn. data
2nd measurement
Flushing (sample) 30

Flushing Pump cleaning solution Flush hold on: 2 PARAMETER ENTRY / "Flush hold on"
Allow to react 5
Pump cleaning solution Flush hold on: 2

6.2.2 Wet commissioning

This is different to the dry commissioning in that, for wet commissioning the reagent lines are filled
before the automatic measurement, calibration and flushing cycle is started.
Proceed as follows:
1. Plug-in the plug into a socket.
2. Press the H key until AUTO MEASURING is displayed.
3. Select the SERVICE menu.
4. Switch the P2 reagent pump "on" (with F select P2 and with V set to"g") and leave it running
until you can tell that there are reagents at the T-connector. After this, switch P2 "off" (s) again
with W.
5. Now switch the valves to passage for standard (select V1: S, V2: S; with F or K switch to
"S" with V) and then switch the P1 sample pump "on". Leave the pump running until you can
tell that there is standard at the T-connector. Switch P1 back "off".
6. Now switch the valves to passage for cleaning agent (select V1: S, V2: R; with F or K switch
to "R" or "S" with V ) and then switch the P1 sample pump "on". Leave the pump running
until you can tell that there is cleaning agent at the T-connector. Switch P1 back "off".
7. Now switch the valves to passage for sample (select V1: P, V2: S; with F or K switch to "P"
or "S" with V ) and then switch the P1 sample pump "on". Leave the pump running until you
can tell that there is sample at the T-connector. Switch P1 back "off".

! Note!
For the two-channel version, valve V3 must be set additionally for switch-over between channel 1
and channel 2.
8. Now proceed as with dry commissioning (from step 2).

Endress+Hauser 33
Maintenance Stamolys CA71SI

7 Maintenance
" Caution!
You must not carry out any procedures not listed in the following chapters, yourself.
This work must only be carried out by the service.

7.1 Maintenance schedule

All maintenance duties that have to be carried out during normal operation of the analyser are
explained below.
If you are using a sample conditioning unit, e.g. CAT430, coordinate the maintenance work
required for it with that of the analyser. For this, read the maintenance chapter in the respective
operating instructions.

Period of time Duty Note

weekly – Check and note calibration factor (for service CONFIGURATION

purposes)
– Move valve hoses into their position and
spray with silicone (extends the service life).

monthly – Flush sample line hose system with – see chapter "Replacing reagents"
pressurized water (disposable syringe), check – Remove the cassette of the
and replace sample pump.
reagents if necessary – Connect the one-way syringe instead of the
– Flush the sample tubing system with 12.5% sample inlet.
bleaching lye (sodium hypochloride) and – SERVICE:
reflush thoroughly with water V1: S, P1: g, P2: s, V2: S

# Warning!
Corrosive. Wear protective gloves and
Add solution to sampling connection

goggles. Beware of reagent splashing.

– Spray pump hoses with silicone spray
– Check sample collector for fouling and clean
it if necessary
– Rotate pump hoses

every 3 months – Cleaning the drain lines:

Flush all hoses with 10% ammonia solution
and then with sample for at least 30 minutes

every 6 months – Replace pump hoses – see chapter "Replacing pump hoses"
– Replace valve hoses

! Note!
Whenever working on the reagent hoses, the hoses must be disconnected from the canisters, in
order to prevent contamination of the reagents.

34 Endress+Hauser
Stamolys CA71SI Maintenance

7.2 Replacing reagents

# Warning!
• There is a danger of crushing limbs at doors, inserts and pump heads.
• Refer to the warning instructions in the safety data sheets when handling reagents. Wear
protective clothing, gloves and goggles.
• Make sure the workplace is well ventilated when you work with chlorine bleach. If you feel
unwell, consult a physician immediately.
• If reagents come into contact with the skin or eyes, carefully rinse with copious amounts of water
and consult a physician immediately.
• Never add water to reagents. Reagents containing acids may splash and heat may build up.
If you store the reagents correctly (in the dark, not over 20 °C) they will be stable for minimum
12 weeks from the date of manufacture (batch number). When this period of time has expired, the
reagents must be replaced. Shelf life can be prolonged by keeping the reagents in a dark, cool storage
place. The reagents absolutely must be replaced when:
• the reagents have been contaminated by sample (see "Trouble-shooting instructions")
• the reagents are too old
• the reagents have been spoilt by incorrect storage conditions or environmental influences.
Reagents check
a. Check the standard solution concentration in the laboratory. Adapt the values (PARAMETER
ENTRY, "Calibration solution") or replace the standard solution.
b. Mix 10 ml standard solution (c=500 µg/l or higher) and 5 ml of reagent SI-1 in a vessel.
c. After 5 minutes, add 5 ml of reagents SI 2 and SI 3.
The mixture must be free of particles.
You must replace the reagents, if there is no visible colouration (blue) after 2 minutes or if the
mixture is not free of particles.
Replacing the reagents
1. Carefully remove the hoses from the canisters and wipe them with a dry (paper) cloth. Wear
protective gloves when doing this.
2. Switch on the reagent pump for about 5 seconds.
3. Flush the reagent hose with plenty of distilled water (see SERVICE).
4. Replace the reagent canister and feed the hoses into the new canister.
5. Fill the reagent hose with the new reagents (SERVICE). Switch all pumps to "g". If there are
no more air bubbles to be seen in the hoses, switch the pumps to "s".
6. Then carry out a calibration (see chapter "Calibration").

7.3 Replacing pump hoses

# Warning!
When removing hoses from the hose nozzles, beware of reagent splashing. For this reason, wear
protective gloves and goggles.
The peristaltic pumps used for the analyser convey the medium in a combination of vacuum and
displacement pump. The pump rate is dependent on the elasticity of the pump hoses. Elasticity
decreases as mechanical stress increases and the pump rate drops. Wear depends on mechanical
stress (measuring interval, pump starting pressure). Up to a certain degree, the wear-effect can be
compensated by calibration. If the elasticity is too low, the pump rate is no longer reproducible
which leads to incorrect measurements. This is why it is necessary to replace the hoses.

Endress+Hauser 35
Maintenance Stamolys CA71SI

Removing the old hoses:

1. Flush the old hoses with water first and then empty them (see SERVICE).
2. Remove the hoses from the connecting nipples on the pump(s) (Fig. 16, pos. 5).
3. Remove the reagent hoses from the reagent canisters, in order to prevent contamination of the
reagents.
4. Loosen the hose cassette(s) (1 to 3 per pump):
– Press to the lower holder (pos. 3).
– Now you can remove the cassette with the hose.
– Remove the hose from the cassette and dispose it.
– Clean the cassette and the wheel head (pos. 1) with of water.

1 Wheel head
1 2 2 Upper holder of the cassette
3 Lower holder of the cassette
4 Guidance at the pump hose
5 Nipple with guidance

5 3

C07-CA71xxx-00-08-00-xx-998.eps

Fig. 16:

Installation of the new hoses:

1. Insert the new hose in the cassette.
2. Pull down the hose at each end and then press the guidance at the hose (pos. 4) into the
guidance of the nipple (pos. 3) at the cassette. Ensure correct fit.
3. Spray the new pump hoses, the hose cassettes and the wheel heads with silicon spray.
4. Reconnect the reagent hoses to the canisters.
5. Refill the hoses with sample, standard or cleaning agent (SERVICE menu).
6. Carry out a frequency offset1 and a calibration (PARAMETER ENTRY menu).

" Caution!
Ensure that you connect the new pump hoses to the correct connections at theT-connector.
For the order numbers of the pump hoses see chapter "Trouble-shooting"/"Spare parts".

1) not necessary with CA71SI

36 Endress+Hauser
Stamolys CA71SI Maintenance

7.4 Checking the sample flow rate

The sample flow rate has to be 14 ± 0.5 ml/min.

1 2
C07-CA71XXx-03-08-00-xx-002.eps C07-CA71XXx-00-08-00-xx-997.eps

Fig. 17: Sample hose at pump outlet Fig. 18: Sample pump
1 Sample hose from pump outlet 3 Adjusting screw for the application force
2 T-piece

Check the sample flow rate after replacing the pump hoses:
1. Remove the sample hose from the T-piece (Fig. 17, pos. 2) and put it into a measuring cylinder.
2. Switch on the sample pump (SERVICE menu).
3. Measure the sample volume in a defined time interval.
4. If the determined flow rate is not 14 ± 0.5 ml/min, you must adjust the application force by
the adjusting screw (Fig. 18, pos. 3, Allen screw) at the hose cassette.
5. Measure resp. adjust until the flow rate is correct.

7.5 Replacing valve hoses

To replace the hoses, proceed as follows:
1. Rinse the old hoses first with water and then with air to empty them (see SERVICE).
2. Remove the hoses from the valves:
a. You can disconnect the front hoses directly because the valves are open when
de-energised.
b. To remove the back hoses, press the black button on the valve and disconnect the hoses.
3. Install the new pump hoses in the reverse sequence of operations.
Ensure that the hoses are connected correctly (→ Fig. 19).
4. After installation, refill the hoses with sample, standard or cleaning agent (SERVICE).
5. Carry out a calibration (PARAMETER ENTRY).

Endress+Hauser 37
Maintenance Stamolys CA71SI

1 2 3

V3 V1 V2 V4

7 6 5 4
C07-CA71xxx-00-08-00-xx-005.eps

Fig. 19: Valves and valve hoses

V1-4 Valves 1, 2 and 4
V3 Two channel switch (optional)
1 Sample
2 To the pump
3 Y-piece, connecting hose to valve 1, behind it
4 Outlet hose
5 Hose valve 2, front, standard
6 Hose valve 2 back, cleaning agent
7 Hose valve 1 front, sample

7.6 Replacing the static mixer

To replace the mixer, proceed as follows:
1. Rinse first with water and then with air (see SERVICE).
2. Unscrew the four screws on the photometer housing and remove it.
3. Disconnect the mixer from the photometer and from the T-piece below the photometer
housing.
4. Remove the old mixer and insert the new one.
5. Connect the new mixer to the photometer and the T-piece again.
6. Attach the photometer housing and screw it down.
7. After installation, refill the hoses with sample, standard or cleaning agent (SERVICE).
8. Carry out a calibration (PARAMETER ENTRY).

7.7 Replacing the optical cell of the photometer

" Caution!
Handling with electronic componentries
Electronic componentries are sensitive to ESD. Discharge yourself, e.g. at an earth conductor, before
handling electronic componentries.
To replace the optical cell, proceed as follows:
1. Rinse first with water and then with air (see SERVICE).
2. Unscrew the four screws on the photometer housing and remove it.
3. Unscrew the four screws on the side of the photometer, where there is no ribbon cable.
4. Separate the photometer's electronics from each other.
5. Take out the cell and remove the hoses.
6. Insert the new cell.

" Caution!
Do not under any circumstances touch the optical window of the cell with your fingers!
Otherwise, traces of grease remain on the optical surfaces. This can lead to corrupted measured
values.

38 Endress+Hauser
Stamolys CA71SI Maintenance

7. Connect the cell to the hoses such that the sample is fed in from below.
8. Secure the hoses with the supplied cable connectors to stop them from slipping off the cell.
9. Reassemble the photometer and tighten the screws.
10. Attach the photometer housing and screw it down.
11. After installation, refill the hoses with sample, standard or cleaning agent (SERVICE).
12. Carry out a calibration (PARAMETER ENTRY).

7.8 Cleaning
" Caution!
When cleaning, ensure that you do not damage the nameplate on the analyser. Do not use any
solvent-based cleaning agents.
To clean the analyser housing, proceed as follows:
• Stainless steel housing (stainless steel SS 1.4301 (AISI 304)):
with a lint-free cloth and Glittol RG 10.51
• GFR housing:
with a damp cloth or with tenside-based (alkaline) cleaning agent.

7.9 Placing out of service

You must place the analyser out of service before shipping or before longer operation breaks (more
than 5 days).

" Caution!
Before placing the instrument out of service, thoroughly rinse all of the lines of the measuring system
with clean water.
To place the analyser out of service, proceed as follows:
1. Remove the reagent and standard hoses from the canisters and immerse them in a tank
containing clean water.
2. Switch valve 1 to "Standard" and switch pumps 1 and 2 on for one minute (SERVICE menu).
3. Remove hoses from the water and allow the pumps to run until the hoses are completely dry.
4. If you are using a continuous sample supply,
disconnect sampling line.
5. Flush sampling hoses with clean water and then with compressed air, in order to completely
empty the hoses.
6. Remove the valve hoses from the valves.
7. Remove the load from the pump hoses by removing the hose cassette from the bracket below.

Endress+Hauser 39
Accessories Stamolys CA71SI

8 Accessories

8.1 Collecting vessel

• for sampling from pressurised systems
• results in an unpressurised continuous sample stream
❑Collecting vessel without level measurement; order no. 51512088

8.2 Reagents, cleaner, standard solution

❑Reagent set active, 1 l SI1+SI2+SI3 each; order no. CAY643-V10AAE
❑Reagent set, inactive, 1 l SI1+SI2+SI3 each; order no. CAY643-V10AAH
❑Cleaning agent, 1 l; order no. CAY641-V10AAE
❑Standard solution 0.1 mg/l SiO2- Si; order no. CAY642-V10C01AAE
❑Standard solution 0.5 mg/l SiO2- Si; order no. CAY642-V10C05AAE
❑Standard solution 1.0 mg/l SiO2- Si; order no. CAY642-V10C10AAE

! Note!
Please, note the disposal instructions in the safety data sheets of the reagents!

8.3 Hose cleaner

❑Cleaning agent, alkaline, 100 ml; order no. CAY746-V01AAE
❑Cleaning agent, acidic, 100 ml; order no. CAY747-V01AAE

8.4 Additional accessories

❑Maintenance kit CAV 740 (SI-A):
– 1 set pump hoses violet/white
– 1 set pump hoses black/black
– 1 Grifflex hose, 2 m (6.56 ft), ID 19 mm (0.75")
– 1 set hose connectors per hose set
order no. CAV 740-4C
❑Maintenance kit CAV 740 (SI-B):
– 1 set pump hoses violet/white
– 1 set pump hoses black/black
– 1 set hose connectors per hose set
order no. CAV 740-4A
❑Interference suppressor for control, power and signal lines
order no. 51512800
❑Silicon spray
order no. 51504155
❑Valve set, 2 pieces, for two-channel version
order no. 51512234
❑Upgrade kit for upgrading from one-channel to two-channel version
order no. 51512640
❑Six channel change-over as TSP
❑Sample cooling and / or sample pressure reduction as TSP

40 Endress+Hauser
Stamolys CA71SI Trouble-shooting

9 Trouble-shooting

9.1 Trouble-shooting instructions

Although the analyser is not very prone to faults due to its simple assembly, problems can, of course,
not be completely ruled out.
Possible errors, their causes and their possible remedies are listed below.

9.2 System error messages

Error message Possible cause Tests and / or corrective measures

If a calibration fails, you can enter a new calibration factor manually (CONFIGURATION menu,
"Calibration factor"). Cancel the error message by switching the analyser off and on briefly.
If the error occurs frequently, you will have to search for the cause.

Air bubbles in system Start calibration manually (PARAMETER ENTRY, "1st calibration", change the date accordingly,
start measurement) or enter a new calibration factor.

Incorrect concentration of standard Check the concentration in the laboratory. Adjust the standard accordingly (PARAMETER ENTRY,
Calibration failed "Calibration solution") or replace the standard.

Reagents contaminated or aged Simple check: Add about 10 to 100 ml of standard solution with about 1 ml of reagent in a beaker.
If it does not change colour after max. 10 min, replace the reagents.

Standard dosing defective Check the valves for contamination, obstructions (visual inspection). Replace valve hoses if
neccessary.

Wrong photometer Check the setting in the CONFIGURATION menu.

Optical cell dirty Not enough light intensity sent to – Flush with 12.5% bleaching lye
receiver, e.g. due to sedimented – When using a CAT430:
particles Check the filter.

Wrong photometer Wrong photometer Check the setting in the CONFIGURATION menu, "Photometer".

No sample Establish sample transfer.

No sample
Level measurement defective Check level measurement on sample collector.

Leak at canisters or hoses Replace defective components and clean and dry the CA 70 or those components affected by the
Spillage error
leak.

Photometer defective Inform Service

No measuring signal Electrical connection Check all electrical connections and the tight fit of the fuses.

Fuse defective Replace fuse F4 or F5 (medium time-lag 0.2 A)

Endress+Hauser 41
Trouble-shooting Stamolys CA71SI

9.3 Process errors without messages

Error Possible cause Tests and / or corrective measures

Reagents contaminated or Simple check: Add about 10-100 ml of standard solution with about 1 ml of reagent in a vessel. If it does
aged not change colour after max. 10 min, replace the reagents .
Measured values always
the same No sample, no reagents Make sure sample and reagents are supplied, check level monitor and clean if necessary

System blocked Flush with 12.5% bleaching lye (monthly maintenance)

Incorrect concentration of Check the concentration in the laboratory. Adjust the standard accordingly
standard ("PARAMETER ENTRY", "Calibration solution") or replace the standard.

Reagents contaminated or Simple check: Add about 10-100 ml of standard solution with about 1 ml of reagent in a vessel. If it does
aged not change colour after max. 10 min, replace the reagents.

Reagent blank value too After replacing the reagents, carry out an offset calibration and then a calibration (CONFIGURATION,
high "Offset calibration")

Wrong dimension Check the setting in the CONFIGURATION menu, "Measuring unit".

Wrong optical cell Check the setting in the CONFIGURATION menu, "Photometer"

Sample suction time too Increase the suction time (CONFIGURATION, "Delay to sample")
short
Measured values Matrix effects Detect interfering substances (see Technical Information, "Measuring principle"),
inaccurate (substances that interfere possibly use sample conditioning
with the photometric
methods)

Standard is dosed to the Check the valves and valve settings. Replace valve hoses if necessary.
sample

Filter life too long Take counter sample at analyser inlet and check the concentration in the laboratory. If the analyser
measured values have no deviations, clean ultrafiltration modules or backflush filters more frequently.

System block or Flush with 12.5% bleaching lye (monthly maintenance)

contaminated

Dosing Replace pump hoses.

Optical cell dirty Flush with 12.5% bleaching lye first and then with 5% hydrochloric acid

Counter sample in the Sample ageing Shorten time between sampling and analysis.
laboratory delivers
deviating measured
values

Wrong size of analog Check the setting (CONFIGURATION, "Analog output 1" " 2").
output
Measured value transfer
Incorrect measuring Adjust measuring range (PARAMETER ENTRY, "Measuring range")
errored
range

Background noise Check line for interference from strong sources of induction.

Analyser will not No power Check the electrical connection and ensure power supply.
switch on Fuse Replace fuse F1 (time-lag 0.5 A)

Analyser is running but Initialisation failed Switch the analyser off and after approx. 30 seconds back on.
display reading is garbled
or off

Leak See "Spillage error" error message

Leak sensor bypassed Interrupt contact between two leak sensors (pins 67-66)
Pumps fail to run
Fuse Check all fuses and replace if necessary.

Pump defective Service

Measurement does not Leak on photometer Service

start

Time of 1st measurement The date must be between 01.01.1996 and the current date.
"Measurement" display not reached
flashes
Interval not expired Change parameters.

42 Endress+Hauser
Stamolys CA71SI Trouble-shooting

Error Possible cause Tests and / or corrective measures

Time of 1st calibration The date must be between 01.01.1996 and the current date.
not reached

Calibration does not start Interval not expired or 0 Change parameters.

h

Leak on photometer Service

Time of 1st flushing not The date must be between 01.01.1996 and the current date.
Flushing does not start reached

Interval not expired or 0h Change parameters.

Leak on Device or discharge Remove blockage.

Photometer blocked Service

Water hardness Lime deposits can by flushing with 5% hydrochloric acid .

Blockage, deposits in If necessary, dose EDTA in sample stream to prevent sedimentation (do not use EDTA with CA71HA!).
device Not enough sample Shorten cleaning intervals of sample conditioning..
conditioning

9.4 Spare parts

9.4.1 SI-A version

155 131 134 185 161 160 161 160 144 200

V3 V1 V2 V4 184 184

130 A 154
V4
V1 V2
H

183 B 141 130

121 170/171 R S R2 R3
R1

121
B
135 135 123 182

120
C
C07-CA71XXx-00-08-xx-111.eps

Fig. 20: Overview parts

A Sample input two-channel version R1 Reagent 1 canister

B Standards and reagent canisters R2 Reagent 2 canister
C Collecting vessel R3 Reagent 3 canister
P Sample S Standard solution canister
R Cleaner canister H Holder for dosage loop

Fig. 20 shows the components of the analyser. Please, take the spare parts order numbers from the
following sections.

Endress+Hauser 43
Trouble-shooting Stamolys CA71SI

Item Spare part Order number

120 Hose made of Norprene, 1.6 mm 51504116

121 Hose made of C-Flex, 3.2 mm (permeate inlet and overflow with sample collector) 51504114
122 Hose made of C-Flex, 6.4 mm 51504115
123 Hose made of C-Flex, 1.5 mm 51512535
130 Hose adapter, 1.6 mm x 1.6 mm (10 pieces) 51506495
131 Hose adapter T, 1.6 mm x 1.6 mm x 1.6 mm (10 pieces) 51506490
134 Hose adapter Y, 1.6 mm x 1.6 mm x 1.6 mm (10 pieces) 51512096
135 Connection nipples for sampler (10 pieces) 51512099
136 Hose adapter T, 3.2 mm x 3.2 mm x 3.2 mm (10 pieces) 51516166
141 Collecting tank 51512102
154 Valve, complete 51512100
155 Valve set for two-channel version 51512235
160 Wheel head with holder for hose pump 51512085
161 Hose casette for pump 51512086
170 Collecting vessel with level measurement 51512089
171 Collecting vessel without level measurement 51512088
161 Hose casette for pump 51512086
170 Collecting vessel with level measurement 51512089
171 Collecting vessel without level measurement 51512088
185 Outlet valve 51515580

9.4.2 SI-B version

155 131 134 161 160 161 160 144 200

V3 V1 V2

130 A 154

V1 V2
H

143 B 141 130

121 170/171 R S R2 R3
R1

121
B
135 135 142 123

122 120
C
C07-CA71XXx-00-08-xx-102.eps

Fig. 21: Overview parts

A Sample input two-channel version R1 Reagent 1 canister
B Standards and reagent canisters R2 Reagent 2 canister
C Collecting vessel R3 Reagent 3 canister
P Sample S Standard solution canister
R Cleaner canister H Holder for dosage loop

44 Endress+Hauser
Stamolys CA71SI Trouble-shooting

Fig. 21 shows the components of the analyser. Please, take the spare parts order numbers from the
following sections.

Item Spare part Order number

120 Hose made of Norprene, 1.6 mm 51504116

121 Hose made of C-Flex, 3.2 mm (permeate inlet and overflow with sample collector) 51504114
122 Hose made of C-Flex, 6.4 mm 51504115
123 Hose made of C-Flex, 1.5 mm 51512535
130 Hose adapter, 1.6 mm x 1.6 mm (10 pieces) 51506495
131 Hose adapter T, 1.6 mm x 1.6 mm x 1.6 mm (10 pieces) 51506490
134 Hose adapter Y, 1.6 mm x 1.6 mm x 1.6 mm (10 pieces) 51512096
135 Connection nipples for sampler (10 pieces) 51512099
136 Hose adapter T, 3.2 mm x 3.2 mm x 3.2 mm (10 pieces) 51516166
140 Mixer set, complete (2 pieces) 51512101
141 Collecting tank 51512102
142 Outlet pipe with hose nibble (2 pieces) 51512104
143 Leak sensor for collecting tank 51512103
154 Valve, complete 51512100
155 Valve set for two-channel version 51512235
160 Wheel head with holder for hose pump 51512085
161 Hose casette for pump 51512086
170 Collecting vessel with level measurement 51512089
171 Collecting vessel without level measurement 51512088

9.4.3 Analyser specific spare parts

Item Spare part Order number

Maintenance kit CAV 740 (SI-A): CAV740-4C

– 1 set pump hoses violet/white
– 1 set pump hoses black/black
– 1 Grifflex hose, 2 m (6.56 ft), ID 19 mm (0.75")
130-133 – per 1 set hose connectors

Maintenance kit CAV 740 (SI-B): CAV740-4A

– 1 set pump hoses violet/white
– 1 set pump hoses black/black
– per 1 set hose connectors

H Holder for dosage loop 51508960

144 Photometer optical cell

– SI-A 51513566
– SI-B 51505776

200 Photometer Silicate

– SI-A 51512078
– SI-B 51512079

9.5 Return
If the device requires repair, please send it cleaned to the sales centre responsible. Please use the
original packaging, if possible.
Please enclose the completed "Declaration of contamination" (copy the second last page of these
Operating Instructions) with the packaging and the transportation documents.
No repair without completed "Declaration of contamination"!

9.6 Disposal
The device contains electronic components and must therefore be disposed of in accordance with
regulations on the disposal of electronic waste. Please observe local regulations.

Endress+Hauser 45
Technical data Stamolys CA71SI

10 Technical data

10.1 Input

Measured variable SiO2 [µg/l / mg/l]

Measuring range 1 ... 200 µg/l (SI-A)

0.05 ... 5.00 mg/l (SI-B)

Wave length 810 nm

Reference wave length 565 nm (SI-B only)

10.2 Output

Output signal 0/4 ... 20 mA

Signal on alarm Contacts: 2 limit contacts (per channel), 1 system alarm contact
optional: end of measurement (with two channel version display of channel
no. available)

Load max. 500 Ω

Serial interface RS 232 C

Load capacity 230 V / 115 V AC max. 2 A, 30 V DC max. 1 A

10.3 Power supply

Supply voltage 115 V AC / 230 V AC ±10%, 50/60 Hz

Power consumption approx. 50 VA

Current consumption approx. 0.2 A at 230 V

approx. 0.5 A at 115 V

Fuses 1 x time-lag 0.5 A for electronics

2 x medium time-lag 0.2 A for photometer
1 x time-lag 0.1 A for motors

10.4 Performance characteristics

Time between two measurements tmes = reaction time + sampling + waiting time + rinse again time + 2x
filling time + reagent refusal time (min. waiting time = 0 min)

Maximum measured error 2 % of measuring range end

Measuring interval tmes to 120 min

Reaction time SI-A: 90 s

SI-B: 120 s

Sample requirement 20 ml (0.0053 US.gal.) per measurement

Reagent requirement SI-A: 3 x 0.288 ml

0.86 l (0.227 US.gal) per reagent per month with 15 minute measuring
interval
SI-A: 3 x 0.288 ml
0.52 l (0.137 US.gal) per reagent per month with 15 minute measuring
interval

Calibration interval 0 to 72 h

Rinse interval (SI-B only) 0 to 72 h

Sampling selectable from 20 to 300 s (standard = 160 s for SI-A, 120 s for SI-B)

46 Endress+Hauser
Stamolys CA71SI Technical data

Rinse again time SI-A 60 s

Rinse again time SI-B 30 s

Filling time SI-A 24 s

Filling time SI-B 15 s

Maintenance interval 6 months (typical)

Servicing requirement 15 minutes per week (typical)

10.5 Environment

Ambient temperature 5 ... 40 °C (41... 104 °F), avoid strong fluctuations

Humidity below the condensation limit, installation in usual, clean rooms

outdoor installation only possible with protective devices (customer
supplied)

Ingress protection IP 43

10.6 Process

Sample flow rate min. 5 ml (0.0013 US.gal.) per min

Consistance of the sample low solid content (< 50 ppm)

Sample inlet pressureless

10.7 Mechanical construction

Design, dimensions see chapter "Installation"

GFK housing approx. 28 kg (61.7 lb)

Weight
Stainless steel housing approx. 33 kg (72.8 lb)

Housing Stainless steel 1.4301 (AISI 304) or GFK

Front windows Plexiglass®

Materials Endless hose C-Flex®, Norprene®

Pump hose Tygon®, Viton®

Valves Tygon®

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Appendix Stamolys CA71SI

11 Appendix

11.1 Operating matrix

One-channel version

AUTO
MEASURING F Calibration Measuring Flushing Waiting

PARAMETER
ENTRY F Measuring
range start
Measuring
range end
Alarm value
1
Alarm value
2
1st
Measurem.
Measuring
interval
1st
Calibration
Calibration
interval

CONFI-
GURATION F Code
number
Photometer
Default
settings
Measuring
unit
Calibration
factor
Concentrat.
offset
Dilution
Delay to
sample

LANGUAGE
F Deutsch English Français Suomi Polski Italiano

ERROR
DISPLAY F Error
messages

SERVICE
F Pumps
and valves
Frequency

DATA
MEMORY F Measured
values
Output Clear data

48 Endress+Hauser
Stamolys CA71SI Appendix

Standard 1st Flushing Flushing

solution Flushing interval time

Analog Alarm value Alarm value Error act. Date/ Calibrate Frequency
output 1 2 contact time offset offset

Endress+Hauser 49
Appendix Stamolys CA71SI

Two-channel version

AUTO
MEASURING F Calibration Measuring Flushing Waiting

PARAMETER
ENTRY F Measuring
range start1
Measuring
range start2
Measuring
range end 1
Measuring
range end 2
Alarm value
1-1
Alarm value
2-1
Alarm value
1-2
Alarm value
2-2

CONFI-
GURATION F Code
number
Photometer
Default
settings
Measuring
unit
Calibration
factor
Concentr.
offset
Dilution
Delay to
sample

LANGUAGE
F Deutsch English Français Suomi Polski Italiano

ERROR
DISPLAY F Error
messages

SERVICE
F Pumps
and valves
Frequency

DATA
MEMORY 1 F Measured
values
Output Clear data

DATA
MEMORY 2 F Measured
values
Output Clear data

50 Endress+Hauser
Stamolys CA71SI Appendix

1st Measuring n* n* 1 st Calibration Calibration 1st Flushing Flushing

Measurem. interval Channel 1 Channel 2 Calibration interval solution Flushing interval time

Analog Analog Alarm value Alarm value Alarm value Alarm value Error act. Date/ Calibrate Frequency
output 1 output 2 1-1 2-1 1-2 2-2 contact time offset offset

Endress+Hauser 51
Appendix Stamolys CA71SI

11.2 Ordering forms

to Fax no:

Telefax for chemicals ordering

to (adress of your sales centre) from (invoice adress)

Company:
Concern:
Street:
Zip code / Town:
Telefax / Telephone:

Adress for delivery (if not the above adress)

Company / Name:
Street / Zip code / Town:

Chemicals for CA71 Silicate

Quantity Order no. Description

CAY640-V10AAE Reagent set active, 1 l SI1+SI2+SI3 each

CAY640-V10AAH Reagent set, inactive, 1 l SI1+SI2+SI3 each

CAY641-V10AAE Cleaning agent, 1 l

CAY642-V10C01AAE Standard solution 0.1 mg/l SiO2- Si

CAY642-V10C05AAE Standard solution 0.5 mg/l SiO2- Si

CAY642-V10C10AAE Standard solution 1.0 mg/l SiO2- Si

Chemicals for Ultra filtration

Quantity Order no. Description

CAY746-V01AAE Alkaline cleaning agent P3-Ultrasil 130, 100 ml

CAY746-V10AAE Alkaline cleaning agent P3-Ultrasil 130, 1 l

CAY746-V50AAE Alkaline cleaning agent P3-Ultrasil 130, 5 l

CAY747-V01AAE Acidic cleaning agent P3-Ultrasil 130, 100 ml

CAY747-V10AAE Acidic cleaning agent P3-Ultrasil 130, 1 l

CAY747-V50AAE Acidic cleaning agent P3-Ultrasil 130, 5 l

Place Date Signature

Delivery one week after orders received. Delivery is unpaid.

52 Endress+Hauser
Stamolys CA71SI Appendix

to Fax no:

Telefax for wear parts ordering

to (adress of your sales centre) from (invoice adress)

Company:
Concern:
Street:
Zip code / Town:
Telefax / Telephone:

Adress for delivery (if not the above adress)

Company / Name:
Street / Zip code / Town:

Quantity Order no. Description

CAV740-4A Maintenance kit CA 7X

• 1 Set pump hoses violet/white (12 pieces)
• 1 Set pump hoses black/black (12 pieces)
• 1 Set of each hose adapter pos. 130-134 (10 pieces each)

Spare parts for maintenance and service

Quantity Position Pieces/pack. Description Order no.

110 12 Tygon pump hose yellow/blue 51506434

111 12 Tygon pump hose black/black 51506437
120 15 m Norpren hose ID 1.6 mm 51504116
121 7.5 m C-Flex hose ID 3.2 mm 51504114
122 7.5 m C-Flex hose ID 6.4 mm 51504115
123 1m C-Flex hose ID 1.5 mm 51512535
130 10 Hose adapter 1.6 mm x 1.6 mm 51506495
131 10 Hose adapter T 1.6 mm x 1.6 mm x 1.6 mm 51506490
132 10 Hose adapter 3.2 mm x 3.2 mm 51506491
10 Hose adapter T 6.4 mm x 6.4 mm x 6.4 mm 51506493
10 Hose adapter 6.4 mm x 6.4 mm 51506494
133 10 Hose adapter 3.2 mm x 6.4 mm 51506492
134 10 Y Hose adapter 1.6 mm x 1.6 mm x 1.6 mm 51512096
135 10 Connection nipples for sampler (10 pieces) 51512099
155 1 Valve set for two-channel version 51512235
160 1 Wheel head with holder for hose pump 51512085
161 1 Hose casette for pump 51512086
170 1 Collecting vessel with level measurement 51512089
171 1 Collecting vessel without level measurement 51512088
1:
200 1 Photometer Type
1 Silicon spray 51504155
1 Cleaning syringe 51503943

1) Please, take the photometer type and the order no. from chapter "Trouble-shooting/Spare parts" and write it down here!

Place Date Signature

Delivery one week after orders received. Delivery is unpaid.

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Appendix Stamolys CA71SI

11.3 Analyser settings

Place:
Type:
Serial no. analyser:
Serial no. Photometer:
Software version:
Date:

Photometer Type:

Measuring unit:

Calibration factor:

c-offset: ❑ mg/l ❑ µg/l

Dilution:

Delay to sample: s

Analog output: ❑ 0-20 mA ❑ 4-20 mA

AV 1: ❑ normally closed ❑ normally open

AV 2: ❑ normally closed ❑ normally open

Fault signal: ❑ normally closed ❑ normally open

Frequency offset: Hz

Ground line: (demineralised water without reagent) Hz

Measuring range start: ❑ mg/l ❑ µg/l

Measuring range end: ❑ mg/l ❑ µg/l

AV 1: ❑ mg/l ❑ µg/l

AV 2: ❑ mg/l ❑ µg/l

1st measuring:

Measuring interval: min

1st calibration:

Calibration interval: h

Calibration solution: ❑ mg/l ❑ µg/l

1st rinsing:

Rinse interval: h

Rinse time: s

54 Endress+Hauser
Stamolys CA71SI Appendix

Submenu

Error mask:

MB >:

MBE:

Rinse again:

Filling time:

Reaction time:

U/min:

K floating mean:

N: Points

C1: mg/l / µg/l F 1: Hz

C2: mg/l / µg/l F 2: Hz

C3: mg/l / µg/l F 3: Hz

C4: mg/l / µg/l F 4: Hz

C5: mg/l / µg/l F 5: Hz

C6: mg/l / µg/l F 6: Hz

C7: mg/l / µg/l F 7: Hz

C8: mg/l / µg/l F 8: Hz

C9: mg/l / µg/l F 9: Hz

C10: mg/l / µg/l F 10: Hz

Date: Service technician:

Endress+Hauser 55
Appendix Stamolys CA71SI

11.4 Maintenance schedule

Form

Maintenance schedule for Analyser Nr. ...................

weekly
⇒ Check and note calibration factor
⇒ visible control (Soiling or blinding, pump tubings, reagent, sample inlet etc.)
done KW 1 KW 2 KW 3 KW 4 KW 5 KW 6 KW 7 KW 8 KW 9 KW 10 KW 11 KW 12
date
done KW 13 KW 14 KW 15 KW 16 KW 17 KW 18 KW 19 KW 20 KW 21 KW 22 KW 23 KW 24
date
done KW 25 KW 26 KW 27 KW 28 KW 29 KW 30 KW 31 KW 32 KW 33 KW 34 KW 35 KW 36
date
done KW 37 KW 38 KW 39 KW 40 KW 41 KW 42 KW 43 KW 44 KW 45 KW 46 KW 47 KW 48
date
done KW 49 KW 50 KW 51 KW 52 KW 53
date

2-weekly
⇒ Check concentration of the calibration factor in the laboratory
May be Concentration in the menue parameter entry chanching or new standard produce.
⇒ Flush sample tubing system with pressurised water (disposable syringe). Remove hose holder unit from the
pump.
Done KW 1 KW 3 KW 5 KW 7 KW 9 KW 11 KW 13 KW 15 KW 17 KW 19 KW 21 KW 23
Date
Done KW 25 KW 27 KW 29 KW 31 KW 33 KW 35 KW 37 KW 39 KW 41 KW 43 KW 45 KW 47
Date
Done KW 49 KW 51 KW 53
Date

monthly or if it‘s needed

⇒ replace raegents
⇒ flush the sample tuing system with 12.5% bleaching lye (sodium hypochloride) and reflush thoroughly with
water (Menue Service V1: P, P1: e, P2: a, V2: S, (two channel version also V3))
⇒ check sample collector for fouling and clean it if necassary
⇒ spray pump hoses with silicone spray
done Jan Feb Mär Apr Mai Jun Jul Aug Sep Okt Nov Dez
date

all 3 month / all 6 month

⇒ turn on the pump tubings in the hose holder unit (monthly) , change (all 6 month)
Attention: Whenever working on the reagent hoses, the hoses must be disconnected from the canisters
and the T-connectors near the reagent pump, in order to prevent contamination of the reagents.
⇒ cleaning drain lines
done Jan Feb Mär Apr Mai Jun Jul Aug Sep Okt Nov Dez
date

C07-CA71XXx-16-08-00-en-006.pdf

56 Endress+Hauser
Stamolys CA71SI

Index
A I
Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 Icons . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Hose cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 Incoming acceptance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Maintenance kit. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Reagents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4, 9–10, 13
Standard solutions . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 Examples . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
Analyser overview. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 Interference suppressor . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
AUTO MEASURING . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23 Interferences . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

C K
Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30 Klemmenleiste erreichen . . . . . . . . . . . . . . . . . . . . . . . . . . 16
Certificates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Checking L
Connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21 LANGUAGE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Function . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 M
Cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 Main menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
Collecting vessel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 Schedule . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
Commissioning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4, 32 Maintenance kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
Dry . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 Mechanical construction . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Wet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33 Menu
CONFIGURATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24 Auto Measuring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Connection Configuration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Electrical . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 Data storage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
Sample line . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 Error display. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Serial interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20 Language . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Signals. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18 Main menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Contacts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 Parameter entry . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
Service. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
D Mixer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
DATA STORAGE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
Declaration of conformity . . . . . . . . . . . . . . . . . . . . . . . . . . 8 N
Designated use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Nameplate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
Disposal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
O
Operating matrix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
E Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4, 22
Electrical connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 Operational safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Environment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 Ordering information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
ERROR DISPLAY. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27 Output . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Error messages . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Errors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
Process errors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
P
System errors. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41 PARAMETER ENTRY . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
Performance characteristics . . . . . . . . . . . . . . . . . . . . . . . . 46
F Photometer optical cell . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
Flow rate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37 Placing out of service . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
Power supply. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
H Process . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Hose cleaner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 Product structure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Pump hoses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Pumps. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

Q
Quality certificate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

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 Stamolys CA71SI

R
Reagents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35, 40
Replacing
Mixer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
Photometer optical cell. . . . . . . . . . . . . . . . . . . . . . . . . 38
Pump hoses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Reagents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Valve hoses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
Return. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5, 45

S
Safety icons . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Sample flow . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
Sample line . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Scope of delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Screening . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
Serial interface. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
SERVICE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
Signal connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
Spare parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
Standard solution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
Storage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Switching contacts. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Switch-on . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
Symbols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

T
Technical data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46–47
Terminal assignment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Transport . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

U
Use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

V
Valve hoses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
Valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

W
Wiring
Connection sticker . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

58 Endress+Hauser
Declaration of contamination
Dear customer,
Because of legal determinations and for the safety of our employees and operating equipment, we need this "Declaration of
contamination" with your signature before your order can be handled. Please, include the completely filled in declaration with the
device and the shipping documents in any case. Add also safety sheets and / or specific handling instructions if necessary.

Type of device / sensor: Serial no.:

Medium / concentration: Temperature: Pressure:
Cleaned with: Conductivity: Viscosity:

Warning hints for medium used (mark the appropriate hints)

SAFE

radioactive explosive caustic poisonous harmful to biologically inflammable safe

health hazardous

Reason for return

Company data
Company: Contact person:

Department:
Address: Phone:
Fax / e-mail:
Your order no.:

I hereby certify that the returned equipment has been cleaned and decontaminated acc. to good industrial practices and is in
compliance with all regulations. This equipment poses no health or safety risks due to contamination.

(Place, date) (Company stamp and legally binding signature)

More information about services and repairs:

www.services.endress.com
 www.endress.com/worldwide

BA364C/07/en/06.04
Printed in Germany / FM+SGML 6.0 / DT
51512332