Disti Guide
Disti Guide
www.erbsloeh.com
A good distillate conveys the flavour and aroma of the processed base product to your
customers in a concentrated form. Outstanding quality depends on the raw material’s
properties and faultless processing. We trust to nature and farming for the quality of the fruit
from tree, bush and field. Where processing and raw material yield are concerned, our
range and customised advice are there to help.
ERBSLÖH’s DistiGuide offers you a compilation of all our products. You can also discover
how our products should be used to achieve optimum results. These pages contain what
you need to know, be it for mash, fermentation, distillation or maturation.
Would you like to contact ERBSLÖH’s test laboratory with a specific product query? We, our
expertise and experience are also available to you at any time. Simply contact us.
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Enzymes are already present in low concentrations in many raw materials. These proteins,
also known as biocatalysts, accelerate biochemical processes. Every enzyme has a sub-
strate-specific action, though, and usually influences just one specific reaction.
Often the enzyme’s function can be inferred are too low, on the other hand, slow down bio-
from its name: a pectinase, for example, is a pec- chemical reactions or bring them to a complete
tin-cleaving enzyme. In this case, the enzyme stop.
and substrate often fit together like jigsaw puzzle
pieces. This is how natural reactions are acceler- It is therefore important to know and adhere to the
ated. As a rule the process does not consume the correct pH and temperature ranges at which the
enzyme. enzymes are correspondingly effective.
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Pectins are the sup- distillate. Due to different pectin contents and dif-
porting substance in ferent side chains, the need for pectolytic enzymes
fruit and are therefore varies depending on the fruit and degree of ripe-
present in virtually all types ness. Fruit softening during ripening also indicates
of fruit. Apricots, plums and the action of enzymes naturally contained in the
blackcurrants have the highest fruit. In the case of fruit placed in cold storage for
absolute pectin content. Where a long time, the fruit’s own enzyme activity is no
sugar content is concerned, fruits such longer sufficient to even begin to ensure adequate
as blackberries and raspberries have a liquefaction of the mash. Low viscosity mashes
higher pectin content than apples and pears. facilitate efficient processing and offer numerous
This can cause increased methanol content in the other advantages.
Your benefits
Less
Better Faster Lower Optimum
expansion Improved
additive fermentation blanket heat
space pumpability
distribution onset formation transfer
required
14,0
11,5
Pectin content in %
8,9
7,9
6,4
5,6
5,4
5,1
3,8 3,7
2,9 2,9
2,4
1,6
1,1
1,0 0,9
0,6 0,5 0,7
0,3 0,4
Pectin content of selected varieties of fruit based on fresh tissue, dry mass and proportion of sugar
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Methanol
Strategic avoidance with pectinlyase
Different fruits have greatly varying degrees of Polygalacturonases cleave the main pectin strand
methylation, with another major variation in terms and ensure visible mash liquefaction. Enzyme
of the total quantity of pectin. The potential for doses and contact times can be controlled in
a problematic methanol content in the distillate order to limit methanol release. Rapid fermenta-
therefore has to be assessed individually for every tion also minimises the phytoenzyme’s influence.
fruit processed. EU Regulation 2019/787 specifies Furthermore, there are very hard-fleshed fruit, such
maximum distillate contents at 1000 g/hL pure as quince and service tree. For these the mash has
alcohol for fruit distillates, 1350 g/hL pure alcohol to be liquefied so that there is sufficient mobility, in
for hard-fleshed fruits and those with a very high other words optimum access for the yeast to the
pectin content and 1500 g/hL pure alcohol for fruit fruit sugar, and to ensure expulsion of the resulting
pomace brandy. carbonic acid from fermentation. This occurs most
efficiently using macerating enzymes such as
Pectinlyase Endo-polygalacturonase Pectin methyltransferase Distizym® FM-TOP.
200
180
The use of pectin lyase represents a different
160
140
approach to pure pectin degradation. Like poly-
Relative activity in %
The methanol reserve is released when the fruit During the fermentation period of at least one
becomes overripe or when it ripens further during week, the mash’s viscosity is sufficiently lowered to
storage and continues during fermentation and ensure rapid alcohol formation and to avoid stub-
interim storage of the fermented mash. The pectin born deposits in the still. The low volume of meth-
esterases added during mashing use this nat- anol released can then be removed by distillation,
ural process. These enzymes run smoothly along as in the classic process.
the pectin chain and release the methanol.
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Control With use of enzymes Control Trenolin ® BouquetPLUS Distizym ® FM-Top
6000 600
5000 500
4000 400
in μg/L-*/10
in μg/L
3000 300
2000 200
1000 100
0 0
α-Pinene β-Myrcene Limonene Linalool α-Terpineol trans β-Myrcene α-Terpineol Limonene Linalool
Nerolidol
Typical aroma components in Italian bitter oranges Typical aroma components in Italian juniper berries
Each fruit and botanical has its own distinctive They also release aromas from the phenol group,
aroma potential. These are the typical vola- such as eugenol from berries (raspberries) and
tile compounds released when cutting open or stone fruits (plums), which contribute to a more
squeezing fruit. complex aroma. The enzyme therefore acceler-
ates the natural ripening process, without having
There is, however, always a pool of non-volatile to accept the usual loss of quality due to overripe
compounds present, which are available as poten- fruit.
tial aromatics. These substances are glycosidically
bonded with a residual sugar, making them too This effect is not limited to just the fruits’ aromatic
heavy to be volatile, in other words, effective for compounds; roots and spices, in other words
aroma. botanicals for producing gin, bitters and herb-
based spirits, can benefit from its use too.
These compounds are disposed of, unused, with
the spent wash. Strongly macerating enzymes,
such as Distizym® FM-TOP, make access to the
compounds easier, however, so that glycosidically
acting enzymes such as Trenolin® BouquetPLUS can
cleave the bonded aromatics from the residual
sugars.
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A Benefit from the new process for producing spirits and infusions.
S If you want to obtain the maximum aroma from Used in this way the enzyme develops its full acti-
H your raw materials, then use our enzymatic extrac- vating effect on raw materials such as juniper ber-
tion process. ries and orange or lemon peel.
First carry out enzymatic maceration at a max- After 18 to 36 hours the now volatile aromas are
imum alcohol content of 15% ABV with Trenolin® dissolved in your infusion as a result of subsequent
BouquetPLUS and/or Distizym® FM-TOP. At this point fortification. You can continue the rest of pro-
you should adjust the pH value to pH 4-5 with cessing as normal.
StabiMash.
Distizym ® FM-Top
max.
15% ABV
pH 4 – 5 18 – 36 h 40 – 70% ABV
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Our distillery enzymes at a glance A
S
H
Dosage
Function Application
(mL/t)
500
Starchy raw materials such as (Starch)
Breaks starches and dextrins
Enerzym HT grain (including malt), pota-
down into fermentable sugars 50 – 150
toes and apples
(Juice)
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Yeast
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T
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O
in the
N
istillery
d
Small effort, big impact
Choosing the right yeast is a key decision in the produc-
tion process because in addition to producing ethanol, it can
do a whole lot more for you.
Yeast can also unlock unused aromatic potential. As a rule, pure yeasts for malolactic fermentation
Individual fermentation management and choice are selected from wine yeasts and habituated
of yeast strain are important artisanal methods of to higher alcohol contents through targeted
achieving expressive distillates. adaptation.
A basic supply of Vitamon® Combi for the yeast All ERBSLÖH yeasts ferment to at least 12% ABV in
flora is generally recommended for guaranteed appropriate fermentation conditions.
complete fermentation.
If the supply of nutrients is good, high-performing
Vitamon Combi
® yeasts such as Spiriferm Arom can generate 15%
ABV and more.
Nitrogen and thiamine that can be used by yeast
For products like whisky, which are made from
Under problematic conditions vitamin and min- malt, yeasts that can handle maltose well are
eral-rich nutrient complex VitaFerm® Ultra can be important. In this case Oenoferm® C2 provides
used.
VitaFerm® Ultra
Yeast addition VitaDrive®
For low fermentation onset temperature or
diluted batch
42 °C
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E
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complete fermentation, even for high gravity saccharomyces bayanus type are particularly tol- N
worts, whilst simultaneously forming exciting, fruity erant of adverse conditions. T
aromas. A
Some yeasts have higher glycosidic enzyme T
Different yeast strains vary with regard not only to activity and are therefore able to split off bonded I
formation of fermentation by-products, such as aromatics, such as terpenes. These are also known O
higher alcohols and esters, but also in fermentation as bouquet yeasts which, in addition to these N
behaviour and tolerance of unfavourable external properties, are also characterized by increased
conditions. These include low temperatures or a formation of aromatic active substances, such as
poor nutrient supply. Fermentation yeasts of the higher alcohols and esters.
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E Four steps for a safe fermentation process
R
M
E Rehydration Monitoring
N Thoroughly stir the yeast into lukewarm water Monitor fermentation progress daily, reduce
T (37-42 °C). Prevent clumps forming. Alterna- cooling if fermentation slows.
A tively, use a water-mash mix.
T The fermentation tank must only be cooled
I during the first fermentation phase (2-3 days).
O Yeast activator
Thereafter, the speed of fermentation self-reg-
N Addition of VitaDrive® direct to the rehydration ulates at a moderate level and continued
batch. Use the same dosage as for the yeast. cooling would be counterproductive. When
providing external cooling by exposing the
tanks to a stream of water, attention must be
Nutrient paid to thorough mixing, as temperatures inside
Thoroughly stir the yeast into the fermentation can far exceed 20 °C.
substrate. Use Vitamon® Combi yeast nutrient
(25–40 g/100kg) at the start of fermentation. Incorporate additional doses of Vitamon®
Combi if necessary.
Coated or black surfaces in the still can be seen Acetaldehyde and total SO2 content after fermentation
with Oenoferm ® Icone, compared to conventional yeasts
after distillation of mashes and wines with a high
sulphur content.
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Chemical cleaning of the still must then be carried In the wine industry Oenoferm® Icone and Oeno- E
out so that reactive copper is once again avail- ferm® wild & pure have already exhibited these R
able, in order to produce a high-quality distillate characteristics for years. They are now increasingly M
from the next batch. finding their way into the distillery. E
N
As this is scarcely achievable from an economic Oenoferm® Icone is an alcohol-tolerant, strongly T
viewpoint, subsequent batches will exhibit much fermenting yeast that ferments reliably even at A
higher sulphur contents from the same raw mate- heavier must weights. T
rials and suffer in sensory terms due to the absence I
of a reactive copper surface. Oenoferm® wild & pure is a mixture of Torulaspora
O
delbrueckii and Saccharomyces cerevisiae, which
N
If the intention is to distil products with low sulphur has the exciting property of spontaneous fer-
contents, it is recommended that a yeast that mentation, whilst simultaneously offering reliable
demonstrably forms less sulphuric acid be used fermentation.
during fermentation.
Light fermenting yeasts of the genus Metschnikowia are an asset for fruit distillation. These
yeasts are already used under certain conditions in wine production and to improve soft
fruit’s shelf life.
Oenoferm® MProtect offers innovative protection Oenoferm® MProtect is fertile and biologically fully
against undesirable microbiological activity. It effective, without forming the typical off-flavours
exploits the fruits’ natural aroma activation to the and signs of spoiling, such as lactic or acetic acid.
maximum under reliable storage conditions. The yeast attracts large quantities of iron ions from
its environment and in this way suppresses growth
Early use of Oenoferm® MProtect effectively sup- of wild flora like yeasts and bacteria.
presses proliferation of acetic acid bacteria, mould
spores and apiculatus yeasts. At the same time Oenoferm® MProtect exhibits
aroma-enzymatic activity. As a result this further
In principle it can be used on the whole fruit in a enhances the aromatic potential of many types of
storage container or during mashing without simul- fruit. The yeast’s own proteases facilitate the onset
taneous onset of fermentation. Controlling temper- of fermentation for the subsequent cultivated
atures at 5-15 °C is recommended to assist this. yeast. The main yeasts can now bring fermentation
to a successful conclusion unimpeded.
w
result of our continuous development. Consequently a small quan-
e
tity is sufficient for successful bioprotection. Just 2–7 g/hL of this
N
improved yeast strain are sufficient to protect the harvest effec-
tively against micro-organisms during transport and standing times.
Even faster colonisation with Metschnikowia pulcherrima is possible due
to a particularly high reproduction rate. Harmful organisms don’t stand a
chance!
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E Our distillery yeasts at a glance
R
M 0,5 kg
Spiriferm
E
Universal fermentation of distilling mashes
N
T Product and effect
A • Rapid fermentation onset
T • Low SO2 and H2S formation
I • Universally suitable for every fruit
O Recommended fermentation temperature 16 – 22 °C
N Alcohol tolerance 14% ABV
Dosage
25 – 30 g/hL
0,5 kg
Spiriferm Classic
Rapid fermentation of distilling mashes and musts
Product and effect
• Rapid fermentation onset
• Low SO2 and H2S formation
• Suitable for pome fruit, cherries, grain and molasses
Recommended fermentation temperature 18 – 25 °C
Alcohol tolerance 12% ABV
Dosage
20 – 30 g/hL (for fruit)
40 – 60 g/hL (for grain)
0,5 kg
Spiriferm Arom
Optimum aroma development for distilling mashes
Product and effect
• For production of intensely aromatic distillates
• Low SO2 and H2S formation
• For yellow stone fruit, grapes and pomace
Recommended fermentation temperature 18 – 25 °C
Alcohol tolerance 15% ABV
Dosage
20 – 30 g/hL
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0,5 | 10 kg
Oenoferm C2 ® E
Fermentation of whisky mashes and worts R
M
Product and effect
E
• Reliable onset and fermentation, even under adverse conditions
N
• Moderate nutrient requirement
T
• Subtle formation of fermentation aromas
• High alcohol yield
A
T
Recommended fermentation temperature 14 – 38 °C
Alcohol tolerance 16% ABV I
O
Dosage
N
20 – 40 g/hL (for fruit)
40 – 80 g/hL (for whisky and rum)
0,5 kg | 10 kg
Oenoferm® Champ
Bayanus yeast for grape and pomace distillates, and rum molasses
Product and effect
• Originally selected as a sparkling wine yeast in the province of Champagne
• Rapid, uniform fermentation speed
• Formation of delicate fruity to nutty, yeasty aromas
Recommended fermentation temperature 14 – 26 °C
Alcohol tolerance 16% ABV
Dosage
20 – 40 g/hL (for fruit)
40 – 60 g/hL (for rum)
0,1 kg | 0,5 kg | 10 kg
Oenoferm® Freddo
Bayanus yeast for diverse cold fermentations of fruit and grain
Product and effect
• Complete final fermentation from 10 °C
• Emphasises an expressive fruit aroma
• Very strongly fermenting, low foam
• Marked killer properties counteracting corrupting yeasts and bacteria
Recommended fermentation temperature 13 – 17 °C (possible from 10 °C)
Alcohol tolerance 15% ABV
Dosage
20 – 40 g/hL (for fruit)
40 – 60 g/hL (for grain)
0,5 kg
Oenoferm® Icone
Cerevisiae yeast for fruit mashes and molasses
Product and effect
• Strongly fermenting yeast, even under difficult conditions
• Fruity-floral fermentation aroma
• Avoids sulphurous notes in subtle distillates
• Particularly alcohol tolerant
Recommended fermentation temperature 18 – 33 °C
Alcohol tolerance 16,5% ABV
Dosage
20 – 40 g/hL
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0,5 kg
E Oenoferm® MProtect
R Metschnikowia pulcherrima yeast for bioprotection
M
Product and effect
E
• Suppresses wild yeasts and mould during the harvest
N
• Bioprotection of raw materials and fermentation batch
T
• Aromatic enzyme activity for developing the intrinsic fruit bouquet
A
Recommended fermentation temperature 5 – 15 °C
T
Alcohol tolerance 6% ABV
I
O Dosage
N 2 – 7 g/hL
0,5 kg
Oenoferm® wild & pure
Blend of Saccharomyces cerevisiae and wild yeast Torulaspora delbrueckii for whisky, grain
and fruit brandy and rum molasses
Product and effect
• Exotic aroma profile with a guaranteed fermentation result
• Creation of a unique product style
• Low SO2 formation
Recommended fermentation temperature 16 – 33 °C
Alcohol tolerance 14% ABV
Dosage
20 – 40 g/hL (for fruit)
40 – 80 g/hL (for whisky and rum)
0,5 | 10 kg
Oenoferm® X-treme
Hybrid yeast for fruit brandies and molasses
Product and effect
• Extremely fast fermentation ability at low temperatures
• Spicy-fruity fermentation aroma
• Can also be used without rehydration
Direct
Recommended fermentation temperature 10 – 17 °C YEAST
Alcohol tolerance 17% ABV oc
u l a ti o
In
Dosage n
20 – 40 g/hL
0,5 kg
BrewMasters FruitAle
For grain brandies that emphasise fruit and esters
Product and effect
• Very rapid fermentation speed
• High-quality fermentation
• Increased production of fruity aromas at temperatures > 22 °C
• Also suitable for co-fermentation, with wine yeasts, for example
Recommended fermentation temperature 16 – 28 °C
Alcohol tolerance 10% ABV
Dosage
50 – 100 g/hL
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equipment I
L
L
A
Sulphite separation using Kupzit T
I
Copper is an ancient, yet current tool in the distillery. Despite the availability of steel and O
glass, modern distillation equipment still tends towards copper. N
In order to fully exploit the fermented fruit’s aro- Kupzit® provides the distiller with a copper citrate
matic potential, modern distillation equipment has treatment agent which binds sulphurous com-
rectifiying columns, dephlegmators and catalysts. pounds at the mash stage and makes it possible to
These are all made from copper to favour a good exploit all of the distillate’s potential aroma.
aroma. In addition to the obvious effect, copper
also offers technical advantages.
Kupzit®
Copper primarily binds sulphur compounds that
Copper citrate preparation to treat off-flavours
have a negative sensory impact on the fermenta-
tion bouquet. This is mainly H2S, formed to a varying
extent as a by-product of every yeast. 20-50 g/100 kg Kupzit® is added to the mash just
before distillation and is evenly distributed with the
mixer running during the distillation process.
e.AntiFoam
H2S and other substances that impair the sensory
Silicon defoamer for the distillery
properties are bound at the liquid phase and the
distillation equipment copper is available as a
If H2S contents are very low, the smell of rotten reaction partner for longer. At the same time this
eggs, or the “off” impression is masked by the fer- reduces the need for frequent chemical cleaning
mentation bouquet. If contents are higher, it is pos- with acid in order to restore the still’s surface. This
sible to detect this off odour in the mash or wine cuts down the general need for cleaning agents,
itself. protects your still’s material and increases lon-
gevity. Overall, the use of Kupzit® saves effort, time
As copper bonds with these problematic negative and money.
sulphur compounds, it is still the material of choice
for producing aromatic distillates.
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Sustainable
G
E
I
alternatives
N
G
to barrels
e.Staves and e.Bois®
Your distillate is given the finishing touch by refining the product with
lengthy barrel maturation. The product gains visually and sensorially as a
result. In this way you achieve a better quality that is worthwhile.
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e.Staves
e.Bois®
DISCLAIMER:
The application recommendations given herein describe the intended use of the product as a processing aid or additive, as part
of good manufacturing practice. The end product’s food safety can only be achieved if used exclusively in this way. Please note:
Our recommendations are based on our current knowledge and experience. They must be seen as general information about our
products only. We cannot accept any liability for use on a case-by-case basis due to the imponderabilities of treating natural prod-
ucts and potential prior treatments. The user must always check for himself compliance with the laws and safety regulations which
apply to use of our products. All data is therefore provided without any warranty. All information is subject to change without prior
notice. Our General Terms and Conditions of Business also apply (downloadable from www.erbsloeh.com).
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ERBSLÖH Geisenheim GmbH · Erbslöhstraße 1 · 65366 Geisenheim · [email protected]