TO WHOM IT MAY CONCERN Certificate of Sampling and Analysis
We have examined the sample(s) of
and report the following to be the result:
Date : 28 May 2024
Our ref. : 2405023RUS Ye
Material : COAL IN BULK
Ex : m/v “MANNA”
Lot : AVERAGE
Weight : 53’900.000 mt
Port : Kavkaz, Russia
Sampling date : 29 April - 22 May 2024
We, the undersigned Incolab Services R.S.C., confirm to have attended the loading and
sampling the material of coal, which was loaded on board of the vessel “MANNA” on 29 - 23
May 2024 at the IPL Kavkaz port.
SAMPLING
Sampling of coal was carried out during all loading in accordance with ISO Standards.
ANALYSIS
TOTAL MOISTURE : 11.0 % ISO 589
INHERENT MOISTURE : 3.0 %
ASH IN DRY : 11.5 % ISO 1171
ASH IN AIR DRY : 11.2 %
ASH AS RECEIVED : 10.2 %
VOLATILE MATTER IN DRY : 35.1 % ISO 562
VOLATILE MATTER IN AIR DRY : 34.0 %
VOLATILE MATTER AS RECEIVED : 31.2 %
GROSS AND NET CALORIFIC VALUE ISO 1928
GROSS CALORIFIC VALUE IN DRY : 7013 kcal/kg
GROSS CALORIFIC VALUE IN AIR DRY : 6803 kcal/kg
GROSS CALORIFIC VALUE AS RECEIVED : 6243 kcal/kg
NET CALORIFIC VALUE IN DRY : 6778 kcal/kg
NET CALORIFIC VALUE IN AUR DRY : 6558 kcal/kg
NET CALORIFIC VALUE AS RECEIVED : 5974 kcal/kg
SULPHUR IN DRY : 0.47 % ISO 19579
SULPHUR IN AIR DRY : 0.46 %
SULPHUR AS RECEIVED : 0.42 %
H.G.I. at 1.0 % residual moisture : 55 ISO 5074
Our ref.: 2405023RUS Ye
Page 2
ASH FUSION TEMPERATURE IN REDUCING ATMOSPHERE ISO 540
INITIAL DEFORMATION : 1250 0C
SPHERE : 1290 0C
HEMISPHERE : 1330 0C
FLUID : 1360 0C
ASH FUSION TEMPERATURE IN OXIDIZING ATMOSPHERE ISO 540
INITIAL DEFORMATION : 1330 0C
SPHERE : 1360 0C
HEMISPHERE : 1390 0C
FLUID : 1420 0C
ASH MINERAL ANALYSIS ASTM D 6349
SILICON DIOXIDE (SiO2) : 57.64 %
ALUMINIUM OXIDE (Al2O3) : 22.74 %
IRON OXIDE (Fe2O3) : 5.62 %
CALCIUM OXIDE (CaO) : 4.85 %
MAGNESIUM OXIDE (MgO) : 2.19 %
SODIUM OXIDE (Na2O) : 0.62 %
POTASSIUM OXIDE (K20) : 1.64 %
MANGANESE DIOXIDE (MnO2) : 0.04 %
TITANIUM DIOXIDE (TiO2) : 0.87 %
PHOSPHORUS PENTOXIDE (P2O5) : 0.82 %
SULPHUR TRIOXIDE (SO3) : 2.37 %
BARIUM OXIDE (BaO) : 0.14 %
STRONTIUM OXIDE (SrO) : 0.16 %
OTHERS : 0.28 %
SIZING TEST ISO 1953
+ 50 mm : 2.0 %
- 50 mm : 98.0 %
100.0 %
The sizing test was performed using round openings sieves.
For and on behalf of,
Incolab Services R.S.C.
